Automatic sampling device for peroxide production inspection

By designing an automatic sampling device, using the cooperation of multiple sampling cylinders and piston blocks, synchronous collection and storage of multi-layer peroxide samples is achieved, and the problems of low sampling efficiency and sample mixing in the prior art are solved, and the problem of low sampling efficiency and sample mixing is realized. Efficient and accurate sample collection and storage.

CN222505908UActive Publication Date: 2025-02-18ANHUI CHANGHE CHEM CO LTD

Patent Information

Application Number
CN202420954726.8
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-05-06
Publication Date
2025-02-18
Estimated Expiration
2034-05-06

AI Technical Summary

Technical Problem

The existing automatic samplers cannot complete the acquisition operation synchronously when collecting multi-layer samples, resulting in inefficient sampling of multi-layer peroxide samples. Moreover, samples at different levels may be mixed during multiple sampling, affecting the accuracy of the inspection results.

Method used

An automatic sampling device is designed to achieve synchronous extraction and collection of peroxide samples at different levels by installing multiple sampling cylinders at different locations on the mounting column and using the cooperation of the piston block and the movable rod. At the same time, the motor drives the screw to rotate, automatically block the communication pipe to avoid sample leakage, and the sample cylinder is disassembled and sample storage is realized through the cooperation of the fixed card block and screw.

Benefits of technology

The sampling efficiency of multi-layer peroxide samples is improved, the inaccurate inspection results caused by sample mixing is avoided, and the safe storage and efficient inspection of samples are achieved.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the technical field of peroxide sampling, in particular to an automatic sampling device for peroxide production inspection, which comprises a mounting column, a plurality of sampling barrels are mounted on the outer side wall of the mounting column along the length direction of the mounting column, the bottom of one side of each sampling barrel is fixedly communicated with a communicating pipe, and a piston block is slidably connected in each sampling barrel. A movable rod slidably connected with the sampling barrel is fixedly connected to the top of one side of the piston block, a movable groove is formed in the outer wall of one side of the mounting column, and a movable column matched with the movable rod to drive the piston block to move is slidably connected into the movable groove; according to the peroxide sampling device disclosed by the utility model, the plurality of sampling barrels at different positions are detachably mounted on the mounting column, so that peroxides at different layers can be extracted and collected at the same time, and compared with a mode that only single-layer samples can be collected each time in the prior art, the peroxide sampling device disclosed by the utility model can effectively improve the sampling efficiency of multiple layers of peroxide samples.
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Description

Technical Field

[0001] The utility model relates to the technical field of peroxide sampling, in particular to an automatic sampling device used for peroxide production inspection. Background Art

[0002] When the production of peroxide using a reactor is about to be completed, the produced peroxide needs to be inspected, so an automatic sampling device is needed to sample the produced peroxide.

[0003] For example, in the prior art, there is an automatic sampler for organic peroxide production with a publication number of CN219757798U. Although the automatic sampler can avoid the problem that the traditional sampler cannot sample at different levels in the reactor, which requires personnel to enter the dangerous area for sampling, each time sampling is performed, only a single layer of samples can be sampled and collected. When sampling multiple layers of samples, the sampling operation cannot be completed synchronously, and it is difficult to further improve the sampling efficiency of multi-layer peroxide samples.

[0004] In view of the above technical defects, a solution is now proposed. Utility Model Content

[0005] The purpose of the utility model is to provide an automatic sampling device for peroxide production inspection to solve the above-mentioned technical defects. The utility model can extract and collect peroxides at different levels at the same time by detachably installing multiple sampling barrels at different positions on a mounting column. Compared with the method of collecting only a single layer of samples at a time in the prior art, the sampling efficiency of multi-layer peroxide samples can be effectively improved; and the sampling barrel can be directly used to store samples, avoiding the problem of inaccurate inspection results caused by mixing samples of different levels when multiple samplings are performed.

[0006] This is achieved through the following technical solutions:

[0007] An automatic sampling device for peroxide production inspection comprises a mounting column, a plurality of sampling barrels are mounted on the outer wall of the mounting column along the length direction thereof, a connecting tube is fixedly connected to the bottom of one side of the sampling barrel, a piston block is slidably connected to the inside of the sampling barrel, and a movable rod slidably connected to the sampling barrel is fixedly connected to the top of one side of the piston block;

[0008] A movable groove is provided on the outer wall of one side of the mounting column, and a movable column is slidably connected in the movable groove and cooperates with the movable rod to drive the piston block to move. The top of the movable groove is rotatably connected to a screw rod threadedly connected to the movable column, and the top bolt of the mounting column is installed with a motor for driving the screw rod to rotate.

[0009] Preferably, a sliding slot is provided inside the mounting column and passes through the bottom thereof, and a plurality of fixing holes are provided on an inner wall on one side of the sliding slot at equal distances along its length direction, and a fixing block is fixedly connected to the sampling tube and is slidably connected to the sliding slot, and a fixing pin matching the fixing hole is provided on the fixing block.

[0010] Preferably, a groove is provided on the side of the fixed block away from the movable rod, and a movable plate fixed to the fixed pin is slidably connected in the groove, a screw rod 1 threadedly connected to the movable plate is rotatably connected in the groove, and a clearance groove connected to the sliding groove is provided on the outer wall of the mounting column, and the free end of the screw rod 1 extends to the outside of the mounting column through the clearance groove and is fixedly connected to a torsion wheel 1.

[0011] Preferably, the top end of the movable rod passes through the outside of the sampling tube and is rotatably connected to screw rod 2, a plurality of fixing holes 2 that are compatible with screw rod 2 are equidistantly provided on the outer wall of one side of the movable column along its length direction, a fixing hole 3 that is compatible with screw rod 2 is provided on the top of one side of the fixed block close to the movable rod, and one end of the screw rod 2 is fixedly connected to torsion wheel 2.

[0012] Preferably, a sealing ball is rotatably connected to the inside of the connecting tube via a rotating shaft, and a connecting hole is penetrated through the sealing ball. One end of the rotating shaft penetrates to the outside of the connecting tube and is fixedly connected to a gear.

[0013] Preferably, an L-shaped rod is fixedly connected to the movable rod, and a toothed plate matched with the gear is fixedly connected to the bottom of one side of the L-shaped rod.

[0014] The beneficial effects of the utility model are as follows:

[0015] (1) When the utility model is in use, by arranging a plurality of sampling tubes at different positions on the mounting column and cooperating with the movement of the internal piston block, the peroxides at different layers can be extracted and collected at the same time. Compared with the method in the prior art that can only collect a single layer of samples at a time, the sampling efficiency of multi-layer peroxide samples can be effectively improved; and by cooperating with the fixing pins on the fixed card block and the fixing holes at different heights, the positions of the plurality of sampling tubes can be adjusted, so that it is convenient to sample the peroxide samples at different layers according to the actual inspection requirements, thereby further improving the scope of use of the device;

[0016] (2) The utility model drives the screw to rotate by a motor, and the screw drives the movable column to move upward. The movable column drives the piston block to move to sample the peroxide with the help of screw 2 and the movable rod. At the same time, the movable rod drives the L-shaped rod to move synchronously until the sampling is about to be completed. The toothed plate on the L-shaped rod engages with the gear, forcing the sealing ball in the connecting pipe to rotate, thereby realizing automatic sealing of the connecting pipe, thereby avoiding the problem of leakage of the sample; and the sampling tube is disassembled by separating the fixed block from the mounting column and the movable rod from the movable column, and the engagement of screw 2 with the fixed hole 3 is used to achieve the effect of directly using the sampling tube to store the sample, thereby avoiding the problem of inaccurate test results caused by mixing samples at different levels when multiple sampling is performed. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] The utility model is further described below in conjunction with the accompanying drawings;

[0018] Figure 1 It is a structural schematic diagram of the utility model;

[0019] Figure 2 It is a structural schematic diagram of the installation column of the utility model;

[0020] Figure 3 It is a schematic diagram of the internal structure of the sampling tube of the utility model;

[0021] Figure 4 It is a structural schematic diagram of the sampling tube after sampling of the utility model;

[0022] Figure 5 It is a structural schematic diagram of the fixed card block of the utility model;

[0023] Figure 6 It is a structural schematic diagram of the connecting pipe of the utility model.

[0024] Legend:

[0025] 1. Mounting column; 11. Movable slot; 12. Moving column; 13. Screw rod; 14. Motor; 15. Sliding slot; 16. Fixing hole 1; 17. Giving way slot; 18. Fixing hole 2;

[0026] 2. Sampling cylinder; 21. Connecting tube; 22. Piston block; 23. Movable rod; 24. Fixed block; 25. Fixed pin; 26. Groove; 27. Movable plate; 28. Screw rod 1; 29. ​​Twist wheel 1; 210. Screw rod 2; 211. Fixed hole 3; 212. Twist wheel 2; 213. Sealing ball; 214. Connecting hole; 215. Gear; 216. L-shaped rod; 217. Tooth plate. DETAILED DESCRIPTION

[0027] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0028] The problem that only a single layer of samples can be sampled and collected at a time in the prior art and multi-layer sample collection cannot be completed synchronously can be solved by the following solution;

[0029] See also Figure 1 - Figure 6 As shown, an automatic sampling device for peroxide production inspection includes a mounting column 1, and a plurality of sampling barrels 2 are mounted on the outer wall of the mounting column 1 along its length direction. When sampling, the mounting column 1 is vertically placed in a peroxide solution, and a plurality of sampling barrels 2 at different positions are arranged on the outer side thereof, so that peroxides at different layers can be extracted and collected at the same time. Compared with the method in the prior art that only a single layer of samples can be collected each time, the sampling efficiency of multi-layer peroxide samples can be effectively improved;

[0030] A connecting tube 21 is fixedly connected to the bottom of one side of the sampling tube 2 for extracting and discharging the peroxide sample. A piston block 22 is slidably connected to the inside of the sampling tube 2. A movable rod 23 slidably connected to the sampling tube 2 is fixedly connected to the top of one side of the piston block 2. The piston block 22 is driven to move upward in the sampling tube 2 by the movable rod 23 and cooperates with the connecting tube 21 to collect and sample the sample. The piston block 22 is driven to move downward in the sampling tube 2 by the movable rod 23 and cooperates with the connecting tube 21 to remove the sample.

[0031] A movable groove 11 is provided on the outer wall of one side of the mounting column 1, and a movable column 12 is slidably connected in the movable groove 11 to cooperate with a movable rod 23 to drive the piston block 22 to move. Limiting grooves are provided on the inner walls on both sides of the movable groove 11, and limiting blocks adapted to the corresponding limiting grooves are fixedly connected on the outer side wall of the movable column 12, thereby ensuring the stable sliding installation of the movable column 12 in the movable groove 11. A screw rod 13 threadedly connected to the movable column 12 is rotatably connected to the top of the movable groove 11, and a motor 14 for driving the screw rod 13 to rotate is installed on the top bolt of the mounting column 1. The screw rod 13 is driven to rotate by the motor 14, and the screw rod 13 drives the movable column 12 to rise in the movable groove 11. The movable column 12 cooperates with the corresponding movable rod 23 to drive multiple piston blocks 22 to move synchronously, thereby realizing the synchronous collection of multi-layer peroxide samples, thereby improving the collection efficiency.

[0032] A sliding card slot 15 is provided inside the mounting column 1 and runs through the bottom thereof, and a plurality of fixing holes 16 are provided on the inner wall of one side of the sliding card slot 15 at equal intervals along the length direction thereof, and a fixing card block 24 is fixedly connected to the sampling tube 2 and is slidably connected to the sliding card slot 15. The sliding card slot 15 runs through the bottom of the mounting column 1, so that the sampling tube 2 and the mounting column 1 can be disassembled and separated, so that the sampling tube 2 can be directly used to store the peroxide sample, so that the problem of inaccurate test results caused by the mixing of samples at different levels when multiple samplings are performed can be avoided, and the number of sampling tubes 2 can be controlled according to the samples at the required number of levels, so that the remaining sampling tubes 2 can be contaminated with samples at unnecessary levels, so that the sampling tubes 2 cannot be directly used;

[0033] A fixing pin 25 matched with the fixing hole 16 is provided on the fixing block 24. The fixing pin 25 on the fixing block 24 cooperates with the fixing holes 16 at different heights to achieve adjustment of the positions of multiple sampling tubes 2, thereby facilitating sampling of peroxide samples at different heights according to actual inspection needs, thereby further improving the scope of use of the device.

[0034] A groove 26 is provided on the fixed block 24 on one side away from the movable rod 23, and a movable plate 27 fixedly connected to the fixed pin 25 is slidably connected in the groove 26, and a screw 28 threadedly connected to the movable plate 27 is rotatably connected in the groove 26. When the position adjustment of the sampling tube 2 is completed, the movable plate 27 is driven to slide in the groove 26 by rotating the screw 28, so that the fixed pin 25 on the movable plate 27 is inserted into the fixed hole 16 at the corresponding position, that is, the position of the sampling tube 2 is fixed, and a yield groove 17 connected to the sliding groove 15 is provided on the outer side wall of the mounting column 1, which is used to extend the free end of the screw 28 to the outside of the mounting column 1, thereby facilitating the rotation of the screw 28. The free end of the screw 28 extends to the outside of the mounting column 1 through the yield groove 17 and is fixedly connected to a torsion wheel 29.

[0035] The top of the movable rod 23 penetrates the outside of the sampling tube 2 and is rotatably connected with a screw rod 210. A plurality of fixing holes 18 that are compatible with the screw rod 210 are equidistantly provided on the outer wall of one side of the movable column 12 along its length direction. Through the cooperation between the screw rod 210 and the fixing hole 18, the connection between the movable column 12 and the movable rod 23 can be completed when the sampling tube 2 is in different positions, thereby not affecting the sampling of the peroxide sample. A fixing hole 3 211 that is compatible with the screw rod 210 is provided on the top of one side of the fixed block 24 close to the movable rod 23. When the sampling tube 2 is removed from the mounting column 1, when the peroxide sample is stored in the sampling tube 2, the movement of the piston block 22 in the sampling tube 2 can be limited by the insertion of the screw rod 210 and the fixing hole 3 211, thereby ensuring that the sample discharge problem will not occur due to misoperation of the movable rod 23 during the transportation of the sampling tube 2. One end of the screw rod 210 is fixedly connected with a torsion wheel 212.

[0036] The interior of the connecting tube 21 is rotatably connected to a sealing ball 213 via a rotating shaft, and a connecting hole 214 is penetrated by the sealing ball 213. One end of the rotating shaft penetrates to the outside of the connecting tube 21 and is fixedly connected to a gear 215. When sampling is completed, the sealing ball 213 is driven to rotate in the connecting tube 21 by rotating the gear 215 to achieve sealing of the connecting hole 214, which can further avoid the problem of leakage of the peroxide sample.

[0037] An L-shaped rod 216 is fixedly connected to the movable rod 23, and a toothed plate 217 matched with the gear 215 is fixedly connected to the bottom of one side of the L-shaped rod 216. When the movable rod 23 drives the piston block 22 to move to sample the peroxide, the movable rod 23 drives the L-shaped rod 216 to move synchronously. When the sampling is about to be completed, the toothed plate 217 on the L-shaped rod 216 engages with the gear 215, forcing the sealing ball 213 in the connecting pipe 21 to rotate, thereby realizing automatic sealing of the connecting pipe 21.

[0038] The working process and principle of the utility model are as follows:

[0039] During use, the utility model places the mounting column 1 vertically in the peroxide solution, drives the screw rod 13 to rotate through the motor 14, drives the moving column 12 to move upward in the movable groove 11, and the moving column 12 cooperates with the corresponding screw rod 210 and the movable rod 23 to drive the multiple piston blocks 22 to move upward synchronously in the sampling tube 2, and extracts the peroxide samples at different levels synchronously through the connecting tube 21;

[0040] The movable rod 23 drives the piston block 22 to move to sample the peroxide, and the movable rod 23 drives the L-shaped rod 216 to move synchronously. When the sampling is about to be completed, the toothed plate 217 on the L-shaped rod 216 meshes with the gear 215, and the rising toothed plate 217 drives the gear 215 to rotate. The gear 215 drives the sealing ball 213 to rotate in the connecting pipe 21, and the connecting hole 214 is blocked, and the connecting pipe 21 is automatically blocked.

[0041] After sampling, the second twist wheel 212 is rotated to drive the second screw rod 210 to separate from the second fixing hole 18, and the twist wheel 1 29 is rotated to drive the screw rod 28 to rotate. The rotation of the screw rod 28 drives the movable plate 27 to slide in the groove 26, so that the fixing pin 25 on the movable plate 27 is separated from the fixing hole 16 at the corresponding position, so that the sampling tube 2 can be removed from the mounting column 1. After removal, the second twist wheel 212 is rotated to drive the second screw rod 210 to be plugged into the fixing hole 3 211, so as to prevent the sampling tube 2 from being discharged due to misoperation of the movable rod 23 during transportation, and by means of the plugging of the fixing pin 25 on the movable plate 27 with the fixing hole 16 at different positions, and the plugging of the second screw rod 210 with the fixing hole 18 at the corresponding position, the peroxide samples of different heights can be sampled according to the actual inspection needs.

[0042] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes within the technical scope disclosed by the present invention according to the technical scheme and the utility model concept of the present invention, which should be covered by the protection scope of the present invention.

Claims

1. An automatic sampling device for peroxide production inspection, comprising a mounting column (1), characterized in that: A plurality of sampling cylinders (2) are mounted on the outer wall of the mounting column (1) along its length direction, and a connecting tube (21) is fixedly connected to the bottom of one side of the sampling cylinder (2), a piston block (22) is slidably connected to the inside of the sampling cylinder (2), and a movable rod (23) slidably connected to the sampling cylinder (2) is fixedly connected to the top of one side of the piston block (22); A movable groove (11) is provided on an outer wall of one side of the mounting column (1), a movable column (12) is slidably connected in the movable groove (11) and cooperates with a movable rod (23) to drive the piston block (22) to move, a screw rod (13) threadedly connected to the movable column (12) is rotatably connected at the top of the movable groove (11), and a motor (14) for driving the screw rod (13) to rotate is installed on the top bolt of the mounting column (1).

2. An automatic sampling device for peroxide production inspection according to claim 1, characterized in that: The mounting column (1) is provided with a sliding slot (15) penetrating the bottom thereof, and a plurality of fixing holes (16) are provided on an inner wall of one side of the sliding slot (15) at equal intervals along its length direction. The sampling tube (2) is fixedly connected with a fixing block (24) slidably connected with the sliding slot (15), and the fixing block (24) is provided with a fixing pin (25) matched with the fixing hole (16).

3. An automatic sampling device for peroxide production inspection according to claim 2, characterized in that: A groove (26) is provided on the side of the fixed block (24) away from the movable rod (23), and a movable plate (27) fixedly connected to the fixed pin (25) is slidably connected in the groove (26), and a screw rod (28) threadedly connected to the movable plate (27) is rotatably connected in the groove (26). A clearance groove (17) connected to the sliding groove (15) is provided on the outer wall of the mounting column (1), and the free end of the screw rod (28) extends to the outer side of the mounting column (1) through the clearance groove (17) and is fixedly connected to a torsion wheel (29).

4. An automatic sampling device for peroxide production inspection according to claim 3, characterized in that: The top end of the movable rod (23) penetrates the outside of the sampling tube (2) and is rotatably connected to the second screw rod (210); a plurality of second fixing holes (18) that are compatible with the second screw rod (210) are equidistantly provided on the outer wall of one side of the movable column (12) along its length direction; a third fixing hole (211) that is compatible with the second screw rod (210) is provided on the top of one side of the fixed block (24) close to the movable rod (23); one end of the second screw rod (210) is fixedly connected to the second torsion wheel (212).

5. An automatic sampling device for peroxide production inspection according to claim 1, characterized in that: The interior of the connecting tube (21) is rotatably connected to a sealing ball (213) via a rotating shaft, and a connecting hole (214) is formed through the sealing ball (213). One end of the rotating shaft passes through the outside of the connecting tube (21) and is fixedly connected to a gear (215).

6. An automatic sampling device for peroxide production inspection according to claim 5, characterized in that: An L-shaped rod (216) is fixedly connected to the movable rod (23), and a toothed plate (217) adapted to the gear (215) is fixedly connected to a bottom of one side of the L-shaped rod (216).

Citation Information

Patent Citations

  • Automatic sampler in organic peroxide production

    CN219757798U

Cited By

  • Sampling and collecting device for preparing di-tert-butyl peroxide

    CN224136974U