Multifunctional extracting tank
By designing a multi-functional extraction tank, using welding vertical rods, solenoid valves, magnetic couplers and other components, the low reaction efficiency problem caused by insufficient mixing structure in the existing extraction tank is solved, and efficient mixing and reaction during the perovskite extraction process is achieved.
Patent Information
- Application Number
- CN202420655131.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-04-01
- Publication Date
- 2025-03-18
- Estimated Expiration
- 2034-04-01
AI Technical Summary
The existing extraction tanks lack effective mixing structures during perovskite extraction, resulting in low reaction efficiency.
A multifunctional extraction tank is designed, including a welding vertical rod, a solenoid valve, a magnetic coupler, a motor, a disc seat, a heating coil, agitating blade and agitating rod between tank A and tank B, and efficient mixing and reaction are achieved through these components.
Through a magnetic coupler and a motor-driven stirring device, the mixing efficiency of ammonium titanate and calcium hydroxide is improved, and the efficient generation of perovskite crystals is achieved under heating coils and high-pressure conditions, thereby improving the reaction efficiency.
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Figure CN222624533U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of extraction tanks, in particular to a multifunctional extraction tank. Background Art
[0002] Perovskite is a metal oxide ceramic material with excellent optical, electrical, magnetic and mechanical properties. Perovskite is widely used in electronic devices, solar cells, optical devices and other fields. When using an extraction tank to extract perovskite, one of the methods is the hydrothermal method, which is a method of preparing perovskite using a high-temperature and high-pressure aqueous solution. In this process, ammonium titanate and calcium hydroxide are mixed and added to water, and reacted under high temperature and high pressure conditions for a certain period of time to form perovskite crystals. However, when using an extraction tank to extract perovskite, there is generally no good mixing structure inside the extraction tank, and the mixed extraction is performed separately, while the reaction efficiency of extraction using natural reactions is low. For this reason, we propose a multifunctional extraction tank. Utility Model Content
[0003] In view of the problems in the prior art, the utility model provides a multifunctional extraction tank.
[0004] The technical solution adopted by the utility model to solve the technical problem is a multifunctional extraction tank, comprising a tank body A and a tank body B, a vertical rod for auxiliary support is welded between the tank body A and the tank body B, and there are multiple groups of vertical rods, a solenoid valve is installed at the connection between the tank body A and the tank body B, the top surface of the tank body A and the outer peripheral surface of the tank body B are both equipped with magnetic couplers, and the inner peripheral surfaces of the tank body A and the tank body B are both equipped with disc seats that are transmission-connected to the magnetic couplers, and the ends of the two groups of disc seats away from the magnetic couplers are respectively equipped with stirring blades and stirring rods, the power input end of the magnetic coupler is equipped with a motor, and the inner peripheral surface of the tank body B is equipped with a heating coil;
[0005] A ring sleeve for protection is welded between the tank body A and the tank body B, and ears for connection are welded on the outer periphery of the ring sleeve, and there are multiple groups of ears.
[0006] By adopting the above technical solution, when extracting perovskite, it is convenient to add ammonium titanate and calcium hydroxide raw materials into the inner side of tank body A, and make the motor operate. The operation of the motor is convenient to drive the stirring rod on the surface of the inner disc seat of tank body A to rotate under the operation of the magnetic coupler, so that the stirring rod can stir the materials inside tank body A, which is convenient for improving the mixing efficiency. At the same time, after the mixing is completed, it directly enters the inner side of tank body B. At the same time, the stirring blade inside tank body B rotates and conveniently stirs the water and the mixed solution of ammonium titanate and calcium hydroxide, and reacts under the heating of the heating coil and the high pressure provided by the external equipment, which is convenient for the reaction to generate perovskite crystals, and the efficiency of mixing and reacting is higher;
[0007] When using the extraction tank to extract perovskite, since tank body A and tank body B are connected by a vertical rod, tank body A and tank body B can form a whole, which is convenient for mixing ammonium titanate and calcium hydroxide raw materials and then directly discharging them into tank body B for reaction, thereby reducing the time consumed by separate operations between the two. At the same time, the ring sleeve between the two is convenient for protecting tank body A and tank body B, so that tank body A and tank body B can operate more stably and safely, and the perovskite can be extracted stably. At the same time, with multiple sets of ear seats, it is convenient to install the extraction tank in a suitable position, so that the extraction tank can operate stably.
[0008] Specifically, a branch pipe is installed on the top surface of the ring sleeve, and a valve is installed inside the branch pipe.
[0009] By adopting the above technical solution, the branch pipe can cooperate with the vacuum pump to extract the air between the ring sleeve and the tank body A and the tank body B, so that a vacuum state is formed inside the ring sleeve, so that the internal structure of the tank body A and the tank body B can operate more stably. At the same time, the valve can conveniently control the opening and closing of the branch pipe, so as to facilitate the blocking of the branch pipe.
[0010] Specifically, the top surface of the tank body A is equipped with conduits that can be used for adding materials, and there are multiple groups of conduits.
[0011] By adopting the above technical solution, the multiple groups of conduits on the top of the tank body A facilitate adding raw materials for preparing perovskite to the inside of the tank body A, and can also be interconnected with corresponding detection equipment to facilitate detection during mixing.
[0012] Specifically, the top surface of the ring sleeve is equipped with vertical pipes connected to the tank body B, and there are multiple groups of vertical pipes.
[0013] By adopting the above technical solution, the vertical pipes on the outer periphery of the ring sleeve can be easily connected to the corresponding detection equipment, so as to detect the reaction status of the material inside the tank body B, add the water source for the reaction, and extract the perovskite.
[0014] Specifically, the outer peripheral surface of the tank body B is equipped with a heat-insulating cotton layer located inside the ring sleeve, and the outer peripheral surface of the heat-insulating cotton layer is equipped with a heat-insulating pad located inside the ring sleeve.
[0015] By adopting the above technical solution, the thermal insulation cotton layer and the thermal insulation pad located on the inner side of the ring sleeve on the outer periphery of the tank body B can cooperate with each other to reduce the heat loss inside the tank body B and facilitate heat preservation, so that the mixed liquid inside the tank body B can react more stably.
[0016] Compared with the prior art, the utility model has the following beneficial effects:
[0017] 1. The technical solution of the present application, through the design of tank body A, tank body B, magnetic coupling, motor, disc seat, heating coil, stirring blade and stirring rod, can conveniently add ammonium titanate and calcium hydroxide raw materials to the inner side of tank body A when extracting perovskite, and make the motor operate. The operation of the motor is convenient to drive the stirring rod on the surface of the disc seat inside the tank body A to rotate under the operation of the magnetic coupling, so that the stirring rod can stir the material inside the tank body A, which is convenient to improve the mixing efficiency. At the same time, after the mixing is completed, it directly enters the inner side of the tank body B. At the same time, the stirring blade inside the tank body B rotates and conveniently stirs the water and the mixed solution of ammonium titanate and calcium hydroxide, and reacts under the heating of the heating coil and the high pressure provided by the external equipment, which is convenient for the reaction to generate perovskite crystals, and the efficiency of mixing and reacting is higher.
[0018] 2. The technical solution of the present application adopts the design of vertical rods, solenoid valves and ring sleeves. When the extraction tank is used to extract perovskite, since tank body A and tank body B are connected by the vertical rod, tank body A and tank body B can form a whole, which is convenient for mixing ammonium titanate and calcium hydroxide raw materials and directly discharging them into tank body B for reaction, thereby reducing the time consumed by separate operations between the two. At the same time, the ring sleeve between the two facilitates the protection of tank body A and tank body B, so that tank body A and tank body B can operate more stably and safely, and the perovskite can be extracted stably. At the same time, with multiple sets of ear seats, it is convenient to install the extraction tank in a suitable position, so that the extraction tank can operate stably. BRIEF DESCRIPTION OF THE DRAWINGS
[0019] The utility model is further described below in conjunction with the accompanying drawings and embodiments.
[0020] Figure 1 It is an axonometric drawing of the utility model;
[0021] Figure 2 This is a schematic diagram of the connection structure between tank body A and tank body B of the utility model;
[0022] Figure 3 It is a cross-sectional schematic diagram of the connection structure between tank body A and tank body B of the utility model;
[0023] In the figure: 1. tank body A; 2. tank body B; 3. vertical rod; 4. solenoid valve; 5. magnetic coupler; 6. motor; 7. plate seat; 8. stirring rod; 9. stirring blade; 10. heating coil; 11. ring sleeve; 12. ear seat; 13. vertical pipe; 14. thermal insulation cotton layer; 15. thermal insulation pad; 16. branch pipe; 17. valve; 18. conduit. DETAILED DESCRIPTION
[0024] In order to make the technical means, creative features, objectives and effects achieved by the present invention easy to understand, the present invention is further described below in conjunction with specific implementation methods.
[0025] See also Figure 1-3 The utility model embodiment provides a technical solution: a multifunctional extraction tank, including a tank body A1 and a tank body B2, a vertical rod 3 for auxiliary support is welded between the tank body A1 and the tank body B2, and there are multiple groups of vertical rods 3, a solenoid valve 4 is installed at the connection between the tank body A1 and the tank body B2, the top surface of the tank body A1 and the outer peripheral surface of the tank body B2 are both equipped with magnetic couplers 5, and the inner peripheral surfaces of the tank body A1 and the tank body B2 are both equipped with disc seats 7 that are transmission-connected to the magnetic couplers 5, and the two groups of disc seats 7 are respectively equipped with stirring blades 9 and stirring rods 8 at one end away from the magnetic coupler 5, a motor 6 is installed at the power input end of the magnetic coupler 5, and a heating coil 10 is installed on the inner peripheral surface of the tank body B2; a ring sleeve 11 for protection is welded between the tank body A1 and the tank body B2, and an ear seat 12 for connection is welded on the outer periphery of the ring sleeve 11, and there are multiple groups of ear seats 12.
[0026] When in use, when extracting perovskite, it is convenient to add ammonium titanate and calcium hydroxide raw materials into the inner side of the tank body A1, and operate the motor 6. The operation of the motor 6 is convenient to drive the stirring rod 8 on the surface of the inner disc seat 7 of the tank body A1 to rotate under the operation of the magnetic coupler 5, so that the stirring rod 8 can stir the materials inside the tank body A1, which is convenient for improving the mixing efficiency. At the same time, after the mixing is completed, it directly enters the inner side of the tank body B2. At the same time, the stirring blade 9 inside the tank body B2 rotates and conveniently stirs the water and the ammonium titanate and calcium hydroxide mixed solution, and reacts under the heating of the heating coil 10 and the high pressure provided by the external equipment, which is convenient for the reaction to generate perovskite crystals, and the efficiency of mixing and reacting is higher;
[0027] When the extraction tank is used to extract the perovskite, since the tank body A1 and the tank body B2 are connected by the vertical rod 3, the tank body A1 and the tank body B2 can form a whole, which is convenient for the ammonium titanate and calcium hydroxide raw materials to be directly discharged into the tank body B2 for reaction after mixing, so as to reduce the time consumed by the separate operation between the two. At the same time, the ring sleeve 11 between the two is convenient for protecting the tank body A1 and the tank body B2, so that the tank body A1 and the tank body B2 can operate more stably and safely, and the perovskite can be extracted stably. At the same time, with multiple sets of ear seats 12, it is convenient to install the extraction tank in a suitable position, so that the extraction tank can operate stably.
[0028] like Figure 1 As shown, a branch pipe 16 is mounted on the top surface of the ring sleeve 11 , and a valve 17 is mounted inside the branch pipe 16 .
[0029] When in use, the branch pipe 16 can cooperate with the vacuum pump to extract the air between the ring sleeve 11 and the tank bodies A1 and B2, so that a vacuum state is formed inside the ring sleeve 11, so that the internal structures of the tank bodies A1 and B2 can operate more stably. At the same time, the valve 17 facilitates the control of the opening and closing of the branch pipe 16, so as to facilitate the blocking of the branch pipe 16.
[0030] like Figure 1 , Figure 2 and Figure 3 As shown, the top surface of the tank body A1 is equipped with conduits 18 for adding materials, and the conduits 18 are provided in multiple groups.
[0031] When in use, the multiple groups of conduits 18 on the top of the tank body A1 facilitate adding raw materials for preparing perovskite to the inside of the tank body A1, and can also be interconnected with corresponding detection equipment to facilitate detection during mixing.
[0032] like Figure 1 and Figure 3 As shown, the top surface of the ring sleeve 11 is equipped with vertical pipes 13 connected to the tank body B2, and there are multiple groups of vertical pipes 13.
[0033] When in use, the vertical pipe 13 on the outer periphery of the ring sleeve 11 is conveniently connected to the corresponding detection equipment, so as to detect the reaction status of the material inside the tank body B2, add the water source for the reaction, and extract the perovskite.
[0034] like Figure 3 As shown, the outer peripheral surface of the tank body B2 is equipped with a heat-insulating cotton layer 14 located inside the ring sleeve 11, and the outer peripheral surface of the heat-insulating cotton layer 14 is equipped with a heat-insulating pad 15 located inside the ring sleeve 11.
[0035] When in use, the heat-insulating cotton layer 14 and the heat-insulating pad 15 located on the inner side of the ring sleeve 11 and the outer periphery of the tank body B2 can cooperate with each other to reduce the heat loss inside the tank body B2 and facilitate heat preservation, so that the mixed liquid inside the tank body B2 can react more stably.
[0036] The working principle and use process of the utility model are as follows: when using, first install the corresponding structural components in a suitable position, and when extracting perovskite, it is convenient to add ammonium titanate and calcium hydroxide raw materials into the inner side of the tank body A1, and make the motor 6 operate. The operation of the motor 6 is convenient to drive the stirring rod 8 on the surface of the inner disk seat 7 of the tank body A1 to rotate under the operation of the magnetic coupler 5, so that the stirring rod 8 can stir the materials inside the tank body A1, which is convenient for improving the mixing efficiency. At the same time, after the mixing is completed, it directly enters the inner side of the tank body B2, and at the same time, the stirring blade 9 inside the tank body B2 rotates and conveniently stirs the water and the mixed solution of ammonium titanate and calcium hydroxide, and reacts under the heating of the heating coil 10 and the high pressure provided by the external equipment, which is convenient for the reaction production. The perovskite crystals are formed, and the efficiency of mixing and reacting is higher. At the same time, when the extraction tank is used to extract the perovskite, since the tank body A1 and the tank body B2 are connected by the vertical rod 3, the tank body A1 and the tank body B2 can form a whole, which is convenient for mixing the ammonium titanate and the calcium hydroxide raw materials and directly discharging them into the tank body B2 for reaction, which is convenient for reducing the time consumed by separate operations between the two. At the same time, the ring sleeve 11 between the two is convenient for protecting the tank body A1 and the tank body B2, so that the tank body A1 and the tank body B2 can operate more stably and safely, and the perovskite can be extracted stably. At the same time, with multiple groups of ear seats 12, it is convenient to install the extraction tank in a suitable position, so that the extraction tank can operate stably.
[0037] The above shows and describes the basic principles, main features and advantages of the utility model. Those skilled in the art should understand that the utility model is not limited by the above embodiments. The above embodiments and descriptions in the specification are only to illustrate the principles of the utility model. Without departing from the spirit and scope of the utility model, the utility model may have various changes and improvements, which fall within the scope of the protection required by the utility model. The scope of protection required by the utility model is defined by the attached claims and their equivalents.
Claims
1. A multifunctional extraction tank, characterized in that: The invention comprises a tank body A (1) and a tank body B (2), wherein a vertical rod (3) for auxiliary support is welded between the tank body A (1) and the tank body B (2), and the vertical rod (3) is provided in multiple groups. A solenoid valve (4) is provided at the connection point between the tank body A (1) and the tank body B (2), a magnetic coupler (5) is provided at the top surface of the tank body A (1) and the outer peripheral surface of the tank body B (2), and a disc seat (7) which is transmission-connected to the magnetic coupler (5) is provided at the inner peripheral surface of the tank body A (1) and the tank body B (2), and a stirring blade (9) and a stirring rod (8) are provided at the ends of the two groups of the disc seats (7) away from the magnetic coupler (5), respectively. A motor (6) is provided at the power input end of the magnetic coupler (5), and a heating coil (10) is provided at the inner peripheral surface of the tank body B (2); A ring sleeve (11) for protection is welded between the tank body A (1) and the tank body B (2), and an ear seat (12) for connection is welded on the outer periphery of the ring sleeve (11), and there are multiple groups of ear seats (12).
2. A multifunctional extraction tank according to claim 1, characterized in that: The top surface of the ring sleeve (11) is equipped with a branch pipe (16), and the inner side of the branch pipe (16) is equipped with a valve (17).
3. A multifunctional extraction tank according to claim 1, characterized in that: The top surface of the tank body A (1) is equipped with a conduit (18) for adding materials, and there are multiple groups of conduits (18).
4. A multifunctional extraction tank according to claim 1, characterized in that: The top surface of the ring sleeve (11) is equipped with a vertical pipe (13) connected to the tank body B (2), and there are multiple groups of vertical pipes (13).
5. The multifunctional extraction tank according to claim 1, characterized in that: The outer peripheral surface of the tank body B (2) is equipped with a heat-insulating cotton layer (14) located inside the ring sleeve (11), and the outer peripheral surface of the heat-insulating cotton layer (14) is equipped with a heat-insulating pad (15) located inside the ring sleeve (11).