Rectification device of reaction kettle
By installing rotating internal spheres and feeding brackets in the reactor, the problem that the existing reactor needs to wait for the reaction liquid to heat up is solved, and the effect of rapidly generating target steam is achieved and the production efficiency is improved.
Patent Information
- Application Number
- CN202421384446.4
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-06-17
- Publication Date
- 2025-03-25
- Estimated Expiration
- 2034-06-17
AI Technical Summary
When performing distillation operations in existing reactors, they need to wait for the reaction liquid to heat up to the boiling point before a large amount of target steam can be generated, resulting in low production efficiency.
A distillation device for a reactor is designed. By installing an internal sphere and rotating it, the heating area of the reaction liquid is increased, and the heating area is quickly increased and evaporated under the action of the heating plate. At the same time, the feeding bracket and the cold water bracket are used to improve the steam generation efficiency.
It is possible to quickly generate a large amount of target steam after adding the reaction liquid, without waiting for the reaction liquid to heat up to the boiling point, which improves the production efficiency of the device and enhances the practicality of the device.
Smart Images
Figure CN222657790U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the field of reactors, in particular to a rectification device for a reactor. Background Art
[0002] A reactor is a container for physical or chemical reactions. It is widely used in industrial production. The materials of reactors are generally carbon-manganese steel, stainless steel, zirconium, nickel-based alloys and other composite materials. Reactors can also be used for reactive distillation. It uses the different boiling points of components in a mixed liquid or liquid-solid system to evaporate the low-boiling-point component and then condense it to separate the entire component. It is a unit operation process that combines evaporation and condensation. Compared with other separation methods, such as extraction, filtration and crystallization, it has the advantage of not requiring the use of other solvents other than the system components, thereby ensuring that no new impurities are introduced. At present, reactors on the market usually have some heating sources at the bottom of the reaction liquid, and then a stirring rod is set inside the reaction liquid to distill the reaction liquid. In this method, since the reaction liquids are gathered together, it is necessary to wait for the reaction liquid to heat up to the boiling point before a large amount of target steam can be generated. The time waiting for the reaction liquid to heat up is relatively long, which affects the production efficiency of the reactor. Utility Model Content
[0003] The utility model aims to provide a rectification device for a reaction kettle.
[0004] In order to achieve the above purpose, the utility model provides the following technical solutions:
[0005] The utility model provides a rectification device for a reactor, comprising a reactor body:
[0006] A flip connection bracket is installed on both sides of the reactor body through bearings, an extension tube is arranged on the outside of the flip connection bracket, the extension tube is welded to the flip connection bracket, an internal sphere is arranged on the side of the extension tube away from the flip connection bracket, the internal sphere and the flip connection bracket are arranged as an integral structure, a middle adjustment bracket is arranged inside the flip connection bracket, the middle adjustment bracket is rotatably connected to the flip connection bracket, a material-diverting bracket is installed on the upper end of the middle adjustment bracket, and the material-diverting bracket is fixedly connected to the middle adjustment bracket;
[0007] A steam exhaust rotating sleeve is arranged on the outside of the extension tube, the steam exhaust rotating sleeve is rotatably connected to the extension tube, a steam exhaust pipe is installed on the upper end of the steam exhaust rotating sleeve, the steam exhaust pipe is welded to the steam exhaust rotating sleeve, a heating bracket is installed on the outside of the internal sphere, the heating bracket is welded to the internal sphere, and a heating plate is installed on the inner side of the heating bracket.
[0008] Furthermore, a junction condenser is installed at the upper end of the steam exhaust pipe, and the junction condenser is welded to the steam exhaust pipe. A cold water bracket is installed at the upper end of the outside of the reactor body, and the cold water bracket is welded to the reactor body.
[0009] Furthermore, a water inlet pipe is installed at the rear end of the upper end surface of the cold water bracket, and the water inlet pipe is welded to the cold water bracket. A drainage pipe is installed at the front end of the lower end surface of the cold water bracket, and the drainage pipe is welded to the cold water bracket.
[0010] Furthermore, a collecting box is installed at the lower end of the cold water support, the collecting box is welded to the reactor body, and a collecting pipe is installed at the lower end of the collecting box.
[0011] Furthermore, a flip motor is installed on one side of the reactor body, the flip motor is fixedly connected to the reactor body, and the flip motor is connected to the flip connection bracket through a coupling.
[0012] Furthermore, an adjusting motor is installed on the other side of the reactor body, the adjusting motor is fixedly connected to the reactor body, and the adjusting motor is connected to the middle adjusting bracket through a coupling.
[0013] Furthermore, a support bracket is installed at the lower end of the reactor body, the support bracket is welded to the reactor body, and the heating bracket slides on the upper end of the support bracket.
[0014] Furthermore, an inner feed door is installed on one side of the inner sphere, and the inner feed door is connected to the inner sphere by screws. An outer feed door is installed on one side of the reactor body, and the outer feed door is connected to the reactor body by screws.
[0015] In the above technical solution, the distillation device of a reactor provided by the utility model has the following beneficial effects:
[0016] 1. Install the internal sphere to make it rotate, so that the reaction liquid inside the internal sphere can be evenly distributed inside the internal sphere, increasing the heating area of the reaction liquid. When the internal sphere rotates, the amount of reaction liquid remaining on the inner wall of the internal sphere is small, so that it can be quickly heated up under the action of the heating plate and evaporated in a short time. After the reaction liquid is added, the device can immediately generate a large amount of target steam without waiting for the reaction liquid to be fully heated to the boiling point, thereby improving the production efficiency of the device;
[0017] 2. Installing the material shifting bracket can make it possible to shift the reaction liquid inside the internal sphere under the action of the regulating motor, so that the reaction liquid is heated more evenly. Installing the cold water bracket can water-cool the intersection condenser tube, so that the target steam inside the intersection condenser tube is cooled and liquefied into liquid, thereby enhancing the practicality of the device. BRIEF DESCRIPTION OF THE DRAWINGS
[0018] In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings required for use in the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments recorded in the present utility model. For ordinary technicians in this field, other drawings can also be obtained based on these drawings.
[0019] Figure 1 It is a three-dimensional internal diagram of a distillation device of a reactor;
[0020] Figure 2 A three-dimensional top view of a distillation device of a reactor;
[0021] Figure 3 It is a three-dimensional image of a distillation device of a reactor when viewed from above;
[0022] Figure 4 A diagram showing the connection relationship between an extension tube and a flip connection bracket in a distillation device of a reactor;
[0023] Figure 5 The invention is an exploded view of the connection between an extension pipe, an inverted connecting bracket and a steam exhaust rotating sleeve in a distillation device of a reactor.
[0024] In the figure: reactor body 1, flip motor 2, flip connecting bracket 3, steam exhaust rotating sleeve 4, middle adjustment bracket 5, adjustment motor 6, material discharging bracket 7, internal sphere 8, heating bracket 9, heating plate 10, cold water bracket 11, steam exhaust pipe 12, intersection condenser 13, collecting box 14, supporting bracket 15, water inlet pipe 16, drainage pipe 17, collecting pipe 18, extension pipe 19, feed inner door 20, feed outer door 21. DETAILED DESCRIPTION
[0025] In order to enable those skilled in the art to better understand the technical solution of the present invention, the present invention will be further described in detail below in conjunction with the accompanying drawings.
[0026] Reference Figure 1-5 The utility model provides an embodiment: a distillation device for a reactor, comprising a reactor body 1:
[0027] The flip connection bracket 3 is installed on both sides of the reactor body 1 through bearings. An extension tube 19 is arranged outside the flip connection bracket 3. The extension tube 19 is welded to the flip connection bracket 3. An internal sphere 8 is arranged on the side of the extension tube 19 away from the flip connection bracket 3. The internal sphere 8 is installed to rotate, so that the reaction liquid inside the internal sphere 8 can be evenly distributed inside the internal sphere 8, increasing the heating area of the reaction liquid. When the internal sphere 8 rotates, the amount of reaction liquid remaining on the inner wall of the internal sphere 8 is small, so that it is quickly heated under the action of the heating plate 10 and evaporated in a short time. The device can generate a large amount of target steam immediately after adding the reaction liquid, without waiting for the reaction liquid to be completely heated to the boiling point, thereby improving the production efficiency of the device. The internal sphere 8 and the flip connection bracket 3 are set as an integrally formed structure, and a middle adjustment bracket 5 is arranged inside the flip connection bracket 3. The middle adjustment bracket 5 is rotatably connected to the flip connection bracket 3, and a material-digging bracket 7 is installed on the upper end of the middle adjustment bracket 5. The installation of the material-digging bracket 7 can make it possible to dig the reaction liquid inside the internal sphere 8 under the action of the adjustment motor 6, so that the reaction liquid is heated more evenly, and the material-digging bracket 7 is fixedly connected to the middle adjustment bracket 5;
[0028] The steam exhaust rotating sleeve 4 is arranged on the outside of the extension tube 19. The steam exhaust rotating sleeve 4 is rotatably connected to the extension tube 19. The installation of the steam exhaust rotating sleeve 4 can facilitate the target steam exhaust device, ensure the functional integrity of the device, and facilitate the collection of target steam. The upper end of the steam exhaust rotating sleeve 4 is installed with a steam exhaust pipe 12, and the steam exhaust pipe 12 is welded to the steam exhaust rotating sleeve 4. A heating bracket 9 is installed on the outside of the internal sphere 8, and the heating bracket 9 is welded to the internal sphere 8. A heating plate 10 is installed on the inner side of the heating bracket 9.
[0029] Reference Figure 1 , Figure 2 , Figure 3 , Figure 4 and Figure 5A converging condenser pipe 13 is installed at the upper end of the steam exhaust pipe 12, and the converging condenser pipe 13 is welded to the steam exhaust pipe 12. A cold water bracket 11 is installed at the upper end of the outside of the reactor body 1. The installation of the cold water bracket 11 can water-cool the converging condenser pipe 13, so that the target steam inside the converging condenser pipe 13 is cooled and liquefied into liquid, thereby enhancing the practicality of the device. The cold water bracket 11 is welded to the reactor body 1, and a water inlet pipe 16 is installed at the rear end of the upper end surface of the cold water bracket 11, and the water inlet pipe 16 is welded to the cold water bracket 11. A drainage pipe 17 is installed at the front end of the lower end surface of the cold water bracket 11, and the drainage pipe 17 is welded to the cold water bracket 11. A collecting box 14 is installed at the lower end of the cold water bracket 11, and the collecting box 14 is welded to the reactor body 1. A collecting pipe 18 is installed at the lower end of the collecting box 14, and the reactor body 1 A flip motor 2 is installed on one side, and the flip motor 2 is fixedly connected to the reactor body 1, and the flip motor 2 is connected to the flip connecting bracket 3 through a coupling, and an adjusting motor 6 is installed on the other side of the reactor body 1, and the adjusting motor 6 is fixedly connected to the reactor body 1, and the adjusting motor 6 is connected to the middle adjusting bracket 5 through a coupling, and a supporting bracket 15 is installed at the lower end of the reactor body 1, and the supporting bracket 15 is welded to the reactor body 1, and the heating bracket 9 slides on the upper end of the supporting bracket 15, and a feed inner door 20 is installed on one side of the internal sphere 8, which can play a supporting role to prevent the internal sphere 8 from shaking and ensure the stability of the device during operation. The feed inner door 20 is connected to the internal sphere 8 by screws, and a feed outer door 21 is installed on one side of the reactor body 1, and the feed outer door 21 is connected to the reactor body 1 by screws.
[0030] The specific use process of the utility model is as follows: the staff opens the inner feeding door 20 and the outer feeding door 21, and adds the reaction liquid into the inner sphere 8, so that the height of the reaction liquid in the inner sphere 8 is not higher than the extension tube 19, and then closes the inner feeding door 20 and the outer feeding door 21, and connects the water inlet pipe 16 to the outlet pipe of the external chiller of the device, and connects the drainage pipe 17 to the water inlet pipe of the external chiller of the device, and then the heating plate 10 heats the inside of the inner sphere 8, and at the same time, the flip motor 2 drives the inner sphere 8 to rotate by flipping the connecting bracket 3 and the extension tube 19, so that the reaction liquid in the inner sphere 8 is evenly distributed inside the inner sphere 8, increasing the heating area of the reaction liquid, and when the inner sphere 8 rotates, the amount of reaction liquid remaining on the inner wall of the inner sphere 8 is small, The temperature is quickly raised under the action of the heating plate 10, and the internal part evaporates in a short time, so that the device can immediately generate a large amount of target steam after the reaction liquid is added, without waiting for the reaction liquid to be completely heated to the boiling point, thereby improving the production efficiency of the device. Then the target steam enters the steam exhaust rotating sleeve 4 through the gap between the flip connection bracket 3 and the heating bracket 9, and then the target steam enters the middle adjustment bracket 5 through the hole at the upper end of the steam exhaust rotating sleeve 4, and then the target steam enters the intersection condensation tube 13. At this time, the target steam is cooled and liquefied in the intersection condensation tube 13, and then the liquefied product enters the collection box 14. The device is equipped with a material shifting bracket 7, which can make it shift the reaction liquid inside the internal sphere 8 under the action of the adjusting motor 6, so that the reaction liquid is heated more evenly.
[0031] Reactor body 1 flip motor 2 flip connection bracket 3 steam exhaust rotating sleeve 4 middle adjustment bracket 5 adjustment motor 6 material discharging bracket 7 internal sphere 8 heating bracket 9 heating plate 10 cold water bracket 11 steam exhaust pipe 12 intersection condensation pipe 13 collection box 14 support bracket 15 water inlet pipe 16 drainage pipe 17 collection pipe 18 extension pipe 19 feed inner door 20 feed outer door 21.
[0032] The above only describes some exemplary embodiments of the present invention by way of illustration. It is undoubted that those skilled in the art can modify the described embodiments in various ways without departing from the spirit and scope of the present invention. Therefore, the above drawings and descriptions are illustrative in nature and should not be construed as limiting the scope of protection of the claims of the present invention.
Claims
1. A rectification device for a reactor, comprising a reactor body (1), characterized in that: A flip connection bracket (3) is installed on both sides of the reactor body (1) via bearings; an extension tube (19) is arranged outside the flip connection bracket (3); the extension tube (19) is welded to the flip connection bracket (3); an internal sphere (8) is arranged on the side of the extension tube (19) away from the flip connection bracket (3); the internal sphere (8) and the flip connection bracket (3) are arranged as an integral structure; a middle adjustment bracket (5) is arranged inside the flip connection bracket (3); the middle adjustment bracket (5) is rotatably connected to the flip connection bracket (3); a material shifting bracket (7) is installed at the upper end of the middle adjustment bracket (5); the material shifting bracket (7) is fixedly connected to the middle adjustment bracket (5); A steam exhaust rotary sleeve (4) is arranged outside the extension tube (19), the steam exhaust rotary sleeve (4) is rotatably connected to the extension tube (19), a steam exhaust pipe (12) is installed at the upper end of the steam exhaust rotary sleeve (4), the steam exhaust pipe (12) is welded to the steam exhaust rotary sleeve (4), a heating bracket (9) is installed outside the internal sphere (8), the heating bracket (9) is welded to the internal sphere (8), and a heating plate (10) is installed inside the heating bracket (9).
2. A rectification device for a reactor according to claim 1, characterized in that: A converging condenser (13) is installed at the upper end of the steam exhaust pipe (12), and the converging condenser (13) is welded to the steam exhaust pipe (12). A cold water bracket (11) is installed at the upper end of the outside of the reactor body (1), and the cold water bracket (11) is welded to the reactor body (1).
3. A rectification device for a reactor according to claim 2, characterized in that: A water inlet pipe (16) is installed at the rear end of the upper end surface of the cold water support (11), and the water inlet pipe (16) is welded to the cold water support (11). A drainage pipe (17) is installed at the front end of the lower end surface of the cold water support (11), and the drainage pipe (17) is welded to the cold water support (11).
4. The rectification device of a reactor according to claim 2, characterized in that: A collecting box (14) is installed at the lower end of the cold water support (11), the collecting box (14) is welded to the reactor body (1), and a collecting pipe (18) is installed at the lower end of the collecting box (14).
5. The rectification device of a reactor according to claim 1, characterized in that: A flip motor (2) is installed on one side of the reactor body (1); the flip motor (2) is fixedly connected to the reactor body (1); and the flip motor (2) is connected to a flip connection bracket (3) via a coupling.
6. The rectification device of a reactor according to claim 1, characterized in that: An adjusting motor (6) is installed on the other side of the reactor body (1); the adjusting motor (6) is fixedly connected to the reactor body (1); and the adjusting motor (6) is connected to the middle adjusting bracket (5) via a coupling.
7. The rectification device of a reactor according to claim 1, characterized in that: A support bracket (15) is installed at the lower end of the reactor body (1), the support bracket (15) is welded to the reactor body (1), and the heating bracket (9) slides on the upper end of the support bracket (15).
8. The rectification device of a reactor according to claim 1, characterized in that: An inner feed door (20) is installed on one side of the inner sphere (8), and the inner feed door (20) is connected to the inner sphere (8) by screws. An outer feed door (21) is installed on one side of the reactor body (1), and the outer feed door (21) is connected to the reactor body (1) by screws.
Citation Information
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