Organic silicon hydrolysis reaction tower

Abstract

The utility model discloses an organic silicon hydrolysis reaction tower, and belongs to the technical field of hydrolysis reaction towers, the organic silicon hydrolysis reaction tower comprises a hydrolysis reaction tower main body, a first-stage filter plate, a second-stage filter plate and a third-stage filter plate are sequentially and fixedly mounted in the hydrolysis reaction tower main body from top to bottom; the interior of the hydrolysis reaction tower main body is sequentially divided into a first-stage decomposition tank, a second-stage decomposition tank, a third-stage decomposition tank and a hydrolysis tank from top to bottom through a first-stage filter plate, a second-stage filter plate and a third-stage filter plate; the organic silicon raw materials in the first-stage decomposition tank and the second-stage decomposition tank are decomposed through the decomposition knife, and the organic silicon raw materials decomposed twice are ground and refined through the grinding roller, so that the organic silicon raw materials with different particle sizes can be decomposed and ground into organic silicon raw materials with uniform standard particle sizes; and then the raw materials are put into the hydrolysis tank for hydrolytic condensation reaction, so that the problems that the raw materials are wasted due to different particle sizes of the raw materials, the production quality is influenced, and the production benefit is reduced are avoided.

Description

Technical Field

[0001] The present application relates to the technical field of hydrolysis reaction towers, and in particular to an organosilicon hydrolysis reaction tower. Background Art

[0002] Silicone is an organic material that is widely used in various industries in life. Silicone has strong wetting properties and can significantly improve the adhesion of pesticides on the surface of plant leaves. Therefore, it has a wide range of usage needs. To obtain practical silicone, it needs to be hydrolyzed from silicone monomers. The existing silicone hydrolysis technology is to configure water and silicone monomers in proportion, pour them into a reaction container, and separate the silicone again after the hydrolysis is completed.

[0003] The particle sizes of organosilicon raw materials are different, and during the hydrolysis and mixing reaction process, organosilicon raw material particles of different particle sizes often exhibit different movement behaviors. The existing preparation equipment cannot properly react to raw materials of different particle sizes when producing organosilicon, which will consume a lot of production costs and reduce the production efficiency of organosilicon. Therefore, improvements are now made to the organosilicon hydrolysis reaction tower. Utility Model Content

[0004] In view of the shortcomings of the prior art, the present application provides an organosilicon hydrolysis reaction tower, which overcomes the shortcomings of the prior art and aims to solve the problem that the existing preparation equipment is unable to properly react with raw materials of different particle sizes when producing organosilicon, thereby consuming a large amount of production costs and reducing the production efficiency of organosilicon.

[0005] To achieve the above-mentioned purpose, the present application provides the following technical scheme: an organosilicon hydrolysis reaction tower, comprising a hydrolysis reaction tower body, wherein a primary filter plate, a secondary filter plate and a tertiary filter plate are fixedly installed in sequence from top to bottom inside the hydrolysis reaction tower body, and the interior of the hydrolysis reaction tower body is divided into a primary decomposition tank, a secondary decomposition tank, a tertiary decomposition tank and a hydrolysis tank in sequence from top to bottom through the primary filter plate, the secondary filter plate and the tertiary filter plate, a rotating rod is arranged inside the hydrolysis reaction tower body, a driving motor for driving the rotating rod to rotate is fixedly installed at a center position of the upper surface of the hydrolysis reaction tower body, a plurality of decomposition knives are fixedly installed on the outer surface of the rotating rod located inside the primary decomposition tank and the secondary decomposition tank, a fixed rod is fixedly installed on one side of the outer surface of the rotating rod located inside the tertiary decomposition tank, and a rolling roller is rotatably installed on the outer surface of the fixed rod.

[0006] By adopting the above technical scheme, the driving motor drives the rotating rod to rotate, thereby driving the decomposition knife to rotate synchronously, and the organic silicon raw materials located in the primary decomposition tank and the secondary decomposition tank are decomposed in turn, and the organic silicon raw materials that have been decomposed twice are subjected to the final step of rolling and refining by the provided rolling roller, that is, the organic silicon raw materials of different particle sizes can be decomposed and rolled into organic silicon raw materials of uniform particle size standards, and then put into the hydrolysis tank for hydrolysis and condensation reaction, thereby avoiding the waste of raw materials due to different particle sizes of raw materials, affecting production quality, and causing the problem of reduced production efficiency.

[0007] As a preferred technical solution of the present application, a circular hole is opened through the center of the upper surface of the primary filter plate and the secondary filter plate, and a rotating shaft is rotatably installed inside the two circular holes, and the two rotating shafts are fixedly sleeved on the outer surface of the rotating rod, the upper end of the rotating rod is fixedly connected to the output end of the driving motor, and the lower end of the rotating rod is located above the tertiary filter plate.

[0008] By adopting the above technical solution and setting a rotating shaft, the rotating rod can be rotated inside the primary filter plate and the secondary filter plate.

[0009] As a preferred technical solution of the present application, the upper surfaces of the primary filter plate, the secondary filter plate and the tertiary filter plate are each provided with a plurality of filter holes, and the apertures of the filter holes on the primary filter plate, the secondary filter plate and the tertiary filter plate decrease successively from top to bottom.

[0010] By adopting the above technical solution, the organosilicon raw materials are filtered and separated layer by layer by setting filter holes with decreasing apertures from top to bottom. Only the organosilicon raw materials that meet the aperture of the current filter plate can enter the next layer, ensuring that the organosilicon raw materials that finally enter the hydrolysis tank are of uniform particle size.

[0011] As a preferred technical solution of the present application, a scraper is fixedly mounted on the outer surface of the rotating rod on one side of the fixed rod, and the bottom of the scraper fits with the top of the three-stage filter plate.

[0012] By adopting the above technical solution, the organic silicon raw material adhered to the three-stage filter plate due to the rolling of the rolling roller is scraped by the scraper.

[0013] As a preferred technical solution of the present application, a plurality of rolling bumps are fixedly connected to the outer surface of the rolling roller, and the plurality of rolling bumps are evenly distributed in a circular array on the outer surface of the rolling roller.

[0014] By adopting the above technical solution, the rolling force of the rolling roller is further improved.

[0015] As a preferred technical solution of the present application, a feed inlet is fixedly installed on the upper surface of the hydrolysis reaction tower body on one side of the driving motor, a discharge port is fixedly installed on the lower end of the hydrolysis reaction tower body, and a solenoid valve is fixedly installed inside the discharge port.

[0016] By adopting the above technical solution, raw materials are added into the interior of the hydrolysis reaction tower body through the feed inlet, and the hydrolyzed product is discharged from the hydrolysis reaction tower body through the discharge port.

[0017] As a preferred technical solution of the present application, a nozzle is fixedly installed on the inner top wall of the hydrolysis reaction tower body on one side of the rotating rod, the upper end of the nozzle is fixedly connected to a threaded pipe, and the upper end of the threaded pipe is threadedly connected to a water pipe.

[0018] By adopting the above technical solution, the nozzle is connected to the external water source through the threaded pipe and the water pipe. After the hydrolysis reaction is completed, water is sprayed into the interior of the hydrolysis reaction tower body through the nozzle to clean it.

[0019] Compared with the prior art, the beneficial effects of the utility model are:

[0020] In the utility model, a driving motor is provided to drive the rotating rod to rotate, thereby driving the decomposition knife to rotate synchronously, and the organic silicon raw materials located inside the primary decomposition tank and the secondary decomposition tank are decomposed in turn, and the organic silicon raw materials that have been decomposed twice are subjected to the final step of rolling and refining by the provided rolling roller, that is, organic silicon raw materials of different particle sizes can be decomposed and rolled into organic silicon raw materials of uniform particle size standards, and then put into the hydrolysis tank for hydrolysis and condensation reaction, thereby avoiding the waste of raw materials due to different particle sizes of raw materials, affecting production quality, and causing the problem of reduced production efficiency.

[0021] With reference to the following description and drawings, specific embodiments of the present invention are disclosed in detail, indicating the manner in which the principles of the present invention can be adopted. It should be understood that the embodiments of the present invention are not limited in scope thereby. BRIEF DESCRIPTION OF THE DRAWINGS

[0022] The accompanying drawings are used to provide a further understanding of the present invention and constitute a part of the specification. Together with the embodiments of the present invention, they are used to explain the present invention and do not constitute a limitation of the present invention. In the accompanying drawings:

[0023] Figure 1 This is a schematic diagram of the overall structure of this application;

[0024] Figure 2 This is a front cross-sectional structural schematic diagram of the present application;

[0025] Figure 3 It is a schematic diagram of the local structure of this application;

[0026] Figure 4 This is a schematic diagram of the connection of the rotating rod of the present application.

[0027] In the figure: 1. hydrolysis reaction tower body; 2. primary filter plate; 3. secondary filter plate; 4. tertiary filter plate; 5. primary decomposition tank; 6. secondary decomposition tank; 7. tertiary decomposition tank; 8. hydrolysis tank; 9. rotating rod; 10. driving motor; 11. decomposition knife; 12. fixing rod; 13. rolling roller; 14. rolling bump; 15. scraper; 16. filter hole; 17. rotating shaft; 18. feed port; 19. discharge port; 20. solenoid valve; 21. nozzle; 22. threaded pipe; 23. water pipe. DETAILED DESCRIPTION

[0028] In order to make the technical means, creative features, objectives and effects achieved by the present invention easy to understand, the present invention is further described below in conjunction with specific implementation methods.

[0029] like Figure 1 - Figure 4 As shown, the organosilicon hydrolysis reaction tower provided in this embodiment includes a hydrolysis reaction tower body 1, wherein a primary filter plate 2, a secondary filter plate 3 and a tertiary filter plate 4 are fixedly installed in the interior of the hydrolysis reaction tower body 1 in sequence from top to bottom, and the interior of the hydrolysis reaction tower body 1 is divided into a primary decomposition tank 5, a secondary decomposition tank 6, a tertiary decomposition tank 7 and a hydrolysis tank 8 in sequence from top to bottom by the primary filter plate 2, the secondary filter plate 3 and the tertiary filter plate 4, and a rotating rod 9 is arranged in the interior of the hydrolysis reaction tower body 1, and a driving motor 10 for driving the rotating rod 9 to rotate is fixedly installed in the center position of the upper surface of the hydrolysis reaction tower body 1, and a plurality of decomposition knives 11 are fixedly installed on the outer surface of the rotating rod 9 in the primary decomposition tank 5 and the secondary decomposition tank 6, and the outer surface of the rotating rod 9 A fixed rod 12 is fixedly installed inside the tertiary decomposition tank 7 on one side, and a rolling roller 13 is rotatably installed on the outer surface of the fixed rod 12. When in use, the driving motor 10 drives the rotating rod 9 to rotate, thereby driving the decomposition knife 11 to rotate synchronously, and the organic silicon raw materials located inside the primary decomposition tank 5 and the secondary decomposition tank 6 are decomposed in turn. The organic silicon raw materials that have been decomposed twice are rolled and refined in the final step by the arranged rolling roller 13, that is, the organic silicon raw materials of different particle sizes can be decomposed and rolled into organic silicon raw materials of uniform particle size standards, and then put into the hydrolysis tank 8 for hydrolysis and condensation reaction, thereby avoiding the waste of raw materials due to different particle sizes of raw materials, affecting production quality, and causing the problem of reduced production efficiency.

[0030] In this embodiment, if Figure 2 and 3As shown, a circular hole is opened through the center of the upper surface of the primary filter plate 2 and the secondary filter plate 3, and a rotating shaft 17 is rotatably installed inside the two circular holes, and the two rotating shafts 17 are fixedly sleeved on the outer surface of the rotating rod 9. The upper end of the rotating rod 9 is fixedly connected to the output end of the driving motor 10, and the lower end of the rotating rod 9 is located above the tertiary filter plate 4. When in use, the rotating shaft 17 is set to facilitate the rotating rod 9 to rotate inside the primary filter plate 2 and the secondary filter plate 3.

[0031] In this embodiment, if Figure 3 As shown, the upper surfaces of the primary filter plate 2, the secondary filter plate 3 and the tertiary filter plate 4 are all provided with a plurality of filter holes 16, and the apertures of the filter holes 16 on the primary filter plate 2, the secondary filter plate 3 and the tertiary filter plate 4 decrease from top to bottom. When in use, the organic silicon raw materials are filtered and separated layer by layer by setting the filter holes 16 with apertures decreasing from top to bottom. Only the organic silicon raw materials meeting the aperture of the current filter plate can enter the next layer, ensuring that the organic silicon raw materials finally entering the hydrolysis tank 8 are of uniform particle size.

[0032] In this embodiment, if Figure 4 As shown, a scraper 15 is fixedly installed on the outer surface of the rotating rod 9 on one side of the fixed rod 12, and the bottom of the scraper 15 is in contact with the top of the tertiary filter plate 4. When in use, the scraper 15 is used to scrape the organic silicon raw material adhered to the tertiary filter plate 4 due to the rolling of the rolling roller 13.

[0033] In this embodiment, if Figure 4 As shown, a plurality of rolling bumps 14 are fixedly connected to the outer surface of the rolling roller 13 , and the plurality of rolling bumps 14 are evenly distributed in a circumferential array on the outer surface of the rolling roller 13 , which further improve the rolling strength of the rolling roller 13 when in use.

[0034] In this embodiment, if Figure 2 As shown, a feed port 18 is fixedly installed on the upper surface of the hydrolysis reaction tower body 1 on one side of the driving motor 10, a discharge port 19 is fixedly installed on the lower end of the hydrolysis reaction tower body 1, and a solenoid valve 20 is fixedly installed inside the discharge port 19. When in use, raw materials are added to the inside of the hydrolysis reaction tower body 1 through the feed port 18, and the hydrolyzed product is discharged from the hydrolysis reaction tower body 1 through the discharge port 19.

[0035] In this embodiment, if Figure 2As shown, the inner top wall of the hydrolysis reaction tower body 1 is located on one side of the rotating rod 9 and a nozzle 21 is fixedly installed thereon. A threaded pipe 22 is fixedly connected to the upper end of the nozzle 21, and a water pipe 23 is threadedly connected to the upper end of the threaded pipe 22. When in use, the nozzle 21 is connected to an external water source through the threaded pipe 22 and the water pipe 23. After the hydrolysis reaction is completed, water is sprayed into the interior of the hydrolysis reaction tower body 1 through the nozzle 21 to clean it.

[0036] The working principle of the utility model is as follows: when the organosilicon hydrolysis reaction tower of the present application is used, the driving motor 10 is provided to drive the rotating rod 9 to rotate, thereby driving the decomposition knife 11 to rotate synchronously, and the organosilicon raw materials located inside the primary decomposition tank 5 and the secondary decomposition tank 6 are decomposed in turn, and the organosilicon raw materials that have been decomposed twice are subjected to the final step of rolling and refining by the provided rolling roller 13, that is, the organosilicon raw materials of different particle sizes can be decomposed and rolled into organosilicon raw materials of uniform particle size standards, and then put into the hydrolysis tank 8 for hydrolysis and condensation reaction, thereby avoiding the waste of raw materials due to different particle sizes of raw materials, affecting production quality, and causing the problem of reduced production efficiency. After the hydrolysis reaction is completed, water is sprayed into the interior of the hydrolysis reaction tower body 1 through the nozzle 21 to clean it.

[0037] The present invention is described above in conjunction with specific implementation methods, but those skilled in the art should be aware that these descriptions are exemplary and are not limitations on the scope of protection of the present invention. Those skilled in the art can make various variations and modifications to the present invention based on the spirit and principles of the present invention, and these variations and modifications are also within the scope of the present invention.

Claims

1. An organosilicon hydrolysis reaction tower, comprising a hydrolysis reaction tower body (1), characterized in that: The hydrolysis reaction tower body (1) is provided with a primary filter plate (2), a secondary filter plate (3) and a tertiary filter plate (4) fixedly installed in sequence from top to bottom. The hydrolysis reaction tower body (1) is divided into a primary decomposition tank (5), a secondary decomposition tank (6), a tertiary decomposition tank (7) and a hydrolysis tank (8) in sequence from top to bottom by the primary filter plate (2), the secondary filter plate (3) and the tertiary filter plate (4). A rotating rod (9) is arranged in the hydrolysis reaction tower body (1). A driving motor (10) for driving the rotating rod (9) to rotate is fixedly installed at a central position on the upper surface of the hydrolysis reaction tower body (1). A plurality of decomposition knives (11) are fixedly installed on the outer surface of the rotating rod (9) located inside the primary decomposition tank (5) and the secondary decomposition tank (6). A fixed rod (12) is fixedly installed on one side of the outer surface of the rotating rod (9) located inside the tertiary decomposition tank (7). A rolling roller (13) is rotatably installed on the outer surface of the fixed rod (12).

2. The organosilicon hydrolysis reaction tower according to claim 1, characterized in that: A circular hole is provided at the center of the upper surface of the primary filter plate (2) and the secondary filter plate (3), and a rotating shaft (17) is rotatably mounted inside the two circular holes. The two rotating shafts (17) are fixedly sleeved on the outer surface of a rotating rod (9), and the upper end of the rotating rod (9) is fixedly connected to the output end of a driving motor (10). The lower end of the rotating rod (9) is located above the tertiary filter plate (4).

3. The organosilicon hydrolysis reaction tower according to claim 1, characterized in that: The upper surfaces of the primary filter plate (2), the secondary filter plate (3) and the tertiary filter plate (4) are each provided with a plurality of filter holes (16), and the apertures of the filter holes (16) on the primary filter plate (2), the secondary filter plate (3) and the tertiary filter plate (4) decrease in sequence from top to bottom.

4. The organosilicon hydrolysis reaction tower according to claim 1, characterized in that: A scraper (15) is fixedly mounted on the outer surface of the rotating rod (9) at one side of the fixed rod (12), and the bottom of the scraper (15) is in contact with the top of the three-stage filter plate (4).

5. The organosilicon hydrolysis reaction tower according to claim 1, characterized in that: A plurality of rolling convex blocks (14) are fixedly connected to the outer surface of the rolling roller (13), and the plurality of rolling convex blocks (14) are evenly distributed in a circumferential array on the outer surface of the rolling roller (13).

6. The organosilicon hydrolysis reaction tower according to claim 1, characterized in that: A feed port (18) is fixedly installed on the upper surface of the hydrolysis reaction tower body (1) at one side of the driving motor (10), a discharge port (19) is fixedly installed at the lower end of the hydrolysis reaction tower body (1), and a solenoid valve (20) is fixedly installed inside the discharge port (19).

7. The organosilicon hydrolysis reaction tower according to claim 1, characterized in that: A nozzle (21) is fixedly mounted on the inner top wall of the hydrolysis reaction tower body (1) at one side of the rotating rod (9), a threaded pipe (22) is fixedly connected to the upper end of the nozzle (21), and a water pipe (23) is threadedly connected to the upper end of the threaded pipe (22).

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