Liquid component detector based on precision analysis

Abstract

The utility model provides a liquid component detector based on precision analysis, which relates to the technical field of detection equipment and comprises a detector, a sampling tube connected to the top end of the detector, a sample box arranged on the side surface of the detector, a placing tray movably connected in the sample box, and a rotating rod fixed at the bottom of the placing tray, a stand column is arranged on the side face of the detector, a movable support is connected into a cavity of the stand column, the movable support is fixed to the surface of the sample box, a sealing cover is arranged on one side of the sample box, and a rotating disc is connected to one side of the sealing cover; a sample on the sample disc can be lifted to a position where a detector can extract by adopting a mode that the sample box and the placing disc in the sample box are lifted, and meanwhile, the sample box can be lifted to control the position of the sampling tube in the sample tube according to conditions, so that supernate obtained after liquid dilution and mixing can be effectively extracted, and the detection efficiency is improved; and meanwhile, automation is realized.

Description

Technical Field

[0001] The utility model relates to the technical field of detection equipment, in particular to a liquid component detector based on precision analysis. Background Art

[0002] According to the patent publication number CN212586312U, a high performance liquid chromatography tandem mass spectrometer relates to the technical field of mass spectrometers, which includes an instrument body, a test bottle and a box body fixed to the upper side of the instrument body, the box body has a storage cavity, the test bottle is embedded in the storage cavity, the bottom of the storage cavity is provided with a plurality of suction cups, the opening of the suction cup is arranged toward a side away from the instrument body, and the test bottle is adsorbed and connected to the suction cup. The utility model has the effect that when the test bottle is hit, it is not easy to move or tilt, and the contamination of the instrument body by the solution in the test bottle is reduced.

[0003] The above-mentioned liquid mass spectrometer is introduced, which is mainly used to analyze and detect the components in liquids. Usually, when testing liquids, the testers are required to manually dilute and mix the samples. The sample pretreatment operation is more troublesome and cannot be automated. If no pretreatment is performed, the sample will be too concentrated to exceed the detection range or cause instrument failure. Utility Model Content

[0004] The purpose of the utility model is to solve the technical problem in the prior art that the detection personnel need to pre-process the sample manually, which reduces the detection efficiency, and propose a liquid component detector based on precise analysis.

[0005] In order to achieve the above-mentioned purpose, the utility model adopts the following technical scheme: a liquid component detector based on precision analysis, including a detector, a sampling tube is connected to the top of the detector, a sample box is provided on the side of the detector, a placement plate is movably connected in the sample box, a rotating rod is fixed at the bottom of the placement plate, and the rotating rod is rotatably connected to the interface at the bottom of the sample box, a column is provided on the side of the detector, a movable bracket is connected in the cavity of the column, and the movable bracket is fixed to the surface of the sample box, a sealing cover is provided on one side of the sample box, and a turntable is connected to one side of the sealing cover.

[0006] Preferably, a screw rod is provided in the cavity of the column, and the movable end of the movable bracket is sleeved on the surface of the screw rod, and the movable end of the movable bracket is threadedly connected to the surface of the screw rod.

[0007] Preferably, a driving assembly is provided at the bottom of the sample box, and a circular array of placement grooves is provided on the top surface of the placement plate.

[0008] Preferably, one end of the sealing cover is connected to a support column, and the connecting end at the bottom of the support column is bolted to the column and the side of the detector respectively.

[0009] Preferably, one end of the sealing cover is axially connected to a connection point at the top end of the support column, and drive shells are respectively provided on both sides of the support column.

[0010] Preferably, a hose is connected to the top surface interface of the sealing cover, and the sealing cover is movably connected to the turntable.

[0011] Beneficial Effects

[0012] In the utility model, the sample box is lifted together with the placement tray inside, and the sample on the sample tray can be lifted to a position where the detector can extract it. After the personnel put the required samples in the specified positions of the placement tray in turn, a specific reagent is added to dilute the liquid, and the placement tray can be rotated together with the sample to complete the mixing in combination with the self-rotation of the placement tray, and finally it is lifted to the specified position to extract the sample into the detector through the sampling tube to wait for detection. At the same time, since the sample box can be lifted and lowered, the position of the sampling tube in the sample tube can be controlled according to the situation, and the supernatant after the liquid dilution and mixing can be effectively extracted, so as to prevent the mixed precipitate from being extracted into the instrument and causing inaccurate detection. In addition, combined with the rotation of the placement tray, multiple groups of samples can be extracted simultaneously in turn, thereby improving the efficiency of detection and realizing automation.

[0013] In the utility model, the sealing cover is rotatable along the top part of the supporting column, the sealing cover can be rotated to the top of the sample box and aligned with the sample box, and the height of the sample box is adjusted so that the sample tube in the placement tray abuts against the turntable at the sealing cover, and it is ensured that the inlet of the sample tube corresponds to the position of the through hole of the turntable. At this time, the sample tube can be rotated and mixed in coordination with the rotation of the sample tray, and the opening of the sample tube can be sealed by the sealing cover to prevent a large amount of liquid from flowing out during mixing. At the same time, as the sample tray rotates, the liquid for dilution and mixing can be extracted from the hose to the corresponding sample. After completion, the sealing cover can be returned to its original position, so that the sample box can be normally raised to the extraction position, and the operation is simple and convenient. BRIEF DESCRIPTION OF THE DRAWINGS

[0014] Figure 1 It is an axonometric drawing of the utility model;

[0015] Figure 2 It is a three-dimensional diagram of the utility model;

[0016] Figure 3 It is a rear view of the utility model;

[0017] Figure 4 It is a front view of the utility model;

[0018] Figure 5 It is a side view of the utility model.

[0019] Legend:

[0020] 1. Detector; 2. Sampling tube; 3. Column; 4. Screw; 5. Mobile bracket; 6. Sample box; 7. Placement plate; 8. Support column; 9. Sealing cover; 10. Turntable; 11. Hose; 12. Drive housing; 13. Turn rod; 14. Drive assembly. DETAILED DESCRIPTION

[0021] In order to make the technical means, creative features, objectives and effects of the present invention easy to understand, the present invention is further described below in conjunction with specific embodiments and drawings, but the following embodiments are only preferred embodiments of the present invention, not all. Based on the embodiments in the implementation mode, other embodiments obtained by those skilled in the art without creative work are all within the protection scope of the present invention.

[0022] The specific embodiments of the present utility model are described below in conjunction with the accompanying drawings. Specific embodiment:

[0024] Embodiment 1:

[0025] Reference Figure 1-5 The liquid component detector based on precision analysis includes a detector 1. The detector 1 is a liquid mass spectrometer, which can detect organic matter, inorganic matter, medicine and other components in the liquid. A sampling tube 2 is connected to the top of the detector 1. A sample box 6 is provided on the side of the detector 1. A placement tray 7 is movably connected to the sample box 6. The sample box 6 is the outer shell of the placement tray 7. The liquid sample to be tested is placed in the placement position of the placement tray 7. After waiting for dilution and mixing, it can be extracted by the sampling tube 2 of the detector 1 and wait for the detection to be completed. Due to the different concentrations of different liquids, for example, the liquid samples of oral liquids are relatively concentrated. If they are directly put into the detector 1 for detection, they may exceed the detection range or cause instrument failure. Therefore, it is necessary to dilute the sample to an appropriate concentration range for detection. The detector 1 includes a power system, a sampling system, a separation system, a detection system and a data processing system. The detector of the detection system can convert the signals of each component in the sample into electrical signals and finally perform data analysis to obtain the results.

[0026] A column 3 is provided on the side of the detector 1, and a movable bracket 5 is connected to the cavity of the column 3, and the movable bracket 5 is fixed to the surface of the sample box 6. A screw 4 is provided in the cavity of the column 3, and the movable end of the movable bracket 5 is sleeved on the surface of the screw 4, and the movable end of the movable bracket 5 is threadedly connected to the surface of the screw 4. The sample box 6 is connected to the screw 4 in the column 3 by the movable bracket 5 and is threadedly connected to it. After adding components such as a motor to the screw 4, it can be rotated. When the screw 4 rotates, the movable bracket 5 can move linearly along the surface of the screw 4, and the shape of the cavity in the column 3 is used to limit the movable bracket 5 so that it can only be lifted and lowered linearly.

[0027] A rotating rod 13 is fixed to the bottom of the placement tray 7, and the rotating rod 13 is rotatably connected to the interface at the bottom of the sample box 6. A driving component 14 is provided at the bottom of the sample box 6. A placement groove is arranged in a circular array on the top surface of the placement tray 7. The placement tray 7 is connected to the interface at the bottom of the sample box through the rotating rod 13, and the two are rotatably connected. A driving component 14 is added to the rotating rod 13 to make the rotating rod 13 rotate together with the placement tray 7 in the sample box 6. Further explanation: the driving component 14 is composed of a motor, a bevel gear and other components. The bevel gear on the surface of the rotating rod 13 is meshed with the bevel gear at the rotating end of the motor. When the motor is working, the rotating rod 13 can be rotated by the bevel gear transmission to complete the rotation of the placement tray 7. The rotation of the placement tray 7 can mix the sample added with a specific liquid to complete the dilution and the precipitation of the precipitate.

[0028] The sample box 6 can be raised and lowered together with the placement plate 7. After the dilution and mixing are completed, the sample can be raised to the specified sampling height for extraction. Since the sample will produce sediment after dilution and mixing, the free rise can accurately control the supernatant of the sample to be extracted, thereby improving the accuracy of the detection and analysis and making the detection result more precise. The mixed sample rises to the extraction height, and one group of samples is aligned with the sampling tube 2. After waiting for the sample here to be extracted, it is lowered a certain distance so that the placement plate 7 can rotate normally. After rotating a fixed angle, the next group of samples is aligned with the sampling tube 2 and then raised to extract the next group of samples. The operation is carried out in sequence and the detection result of the detector 1 can be waited.

[0029] Embodiment 2:

[0030] Reference Figure 1-5 A sealing cover 9 is provided on one side of the sample box 6, a turntable 10 is connected to one side of the sealing cover 9, a hose 11 is connected to the top interface of the sealing cover 9, and the sealing cover 9 is movably connected to the turntable 10. When adding diluent, the sample box 6 is lowered to the lowest end in advance, and the sealing cover 9 is rotated 90°. At this time, the position of the placement plate 7 is adjusted to align the sample with the through hole on the turntable 10, so that the sample tube rises and contacts the turntable 10, and a water pump and other components are added to send the required added liquid into the hose 11, and the liquid in the group is sent to the sample tube through the hose 11 The placing plate 7 is rotated in sequence to pass the sample tubes through the hose 11 of the sealing tube in sequence, and the liquid addition can be completed. It is necessary to explain that the turntable 10 can rotate in the interface of the sealing cover 9, and the two do not affect each other. At the same time, the interface of the hose 11 of the sealing cover 9 runs through the sealing cover 9, ensuring that when the turntable 10 rotates, the two interfaces will overlap. At the same time, because the top of the sample tube is against the turntable 10, the turntable 10 can be rotated together when the placing plate 7 is rotated. When mixing is required, it only needs to be rotated. When the sample is rotated and mixed, the sealing cover 9 can be used to prevent the sample from flowing out

[0031] One end of the sealing cover 9 is connected to the support column 8, and the connecting end at the bottom of the support column 8 is bolted to the column 3 and the side of the detector 1 respectively. One end of the sealing cover 9 is axially connected to the connection at the top of the support column 8. Drive shells 12 are respectively provided on both sides of the support column 8. Further explanation: one end of the sealing cover 9 is axially connected to the connecting end at the top of the support column 8, and drive shells 12 are added on both sides of the support column 8. The interior of the drive shell 12 includes components such as a motor and a gear set, which are used to drive the connecting shaft at the top of the support column 8 to make the sealing cover 9 complete the rotation, thereby ensuring that the sealing cover 9 returns to its original position after dilution and mixing without affecting the lifting and lowering of the sample box 6.

[0032] In the present utility model, unless otherwise clearly specified and limited, a first feature being "above" or "below" a second feature may include that the first and second features are in direct contact, or may include that the first and second features are not in direct contact but are in contact through another feature between them. Moreover, a first feature being "above", "above" and "above" a second feature includes that the first feature is directly above and obliquely above the second feature, or simply indicates that the first feature is higher in level than the second feature. A first feature being "below", "below" and "below" a second feature includes that the first feature is directly below and obliquely below the second feature, or simply indicates that the first feature is lower in level than the second feature.

[0033] The above shows and describes the basic principle, main features and advantages of the utility model. Those skilled in the art should understand that the utility model is not limited by the above embodiments. The above embodiments and descriptions are only preferred examples of the utility model and are not used to limit the utility model. Without departing from the spirit and scope of the utility model, the utility model may have various changes and improvements, which fall within the scope of the utility model to be protected. The scope of protection of the utility model is defined by the attached claims and their equivalents.

Claims

1. A liquid component detector based on precision analysis, comprising a detector (1), characterized in that: The top of the detector (1) is connected to a sampling tube (2), a sample box (6) is provided on the side of the detector (1), a placement plate (7) is movably connected inside the sample box (6), a rotating rod (13) is fixed at the bottom of the placement plate (7), and the rotating rod (13) is rotatably connected to the interface at the bottom of the sample box (6), a column (3) is provided on the side of the detector (1), a movable bracket (5) is connected in the cavity of the column (3), and the movable bracket (5) is fixed to the surface of the sample box (6), a sealing cover (9) is provided on one side of the sample box (6), and a rotating disk (10) is connected to one side of the sealing cover (9).

2. The liquid component detector based on precision analysis according to claim 1, characterized in that: A screw rod (4) is arranged in the cavity of the upright column (3), and the movable end of the movable bracket (5) is sleeved on the surface of the screw rod (4), and the movable end of the movable bracket (5) is threadedly connected to the surface of the screw rod (4).

3. The liquid component detector based on precision analysis according to claim 1, characterized in that: The bottom of the sample box (6) is provided with a driving assembly (14), and the top surface of the placement plate (7) has placement grooves in a circumferential array.

4. The liquid component detector based on precision analysis according to claim 1, characterized in that: One end of the sealing cover (9) is connected to a support column (8), and the connection end at the bottom of the support column (8) is bolted to the column (3) and the side of the detector (1) respectively.

5. The liquid component detector based on precision analysis according to claim 4, characterized in that: One end of the sealing cover (9) is axially connected to a connection point at the top end of the support column (8), and drive shells (12) are respectively provided on two sides of the support column (8).

6. The liquid component detector based on precision analysis according to claim 1, characterized in that: A hose (11) is connected to the top surface interface of the sealing cover (9), and the sealing cover (9) is movably connected to the rotating disk (10).

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