EDTA-2Na (Ethylene Diamine Tetraacetic Acid-2Na) wet-process automatic feeding device in decabromodiphenyl ethane production process

The automated EDTA-2Na wet feeding system addresses the inefficiencies of manual addition by providing precise and consistent EDTA-2Na delivery, improving reaction efficiency and product quality.

CN223096732UActive Publication Date: 2025-07-15SHANDONG HAIWANG CHEM
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Patent Information

Application Number
CN202422100167.7
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-08-28
Publication Date
2025-07-15
Estimated Expiration
2034-08-28

AI Technical Summary

Technical Problem

The traditional manual feeding method is labor-intensive and has irregular operation in the production of decabromodiphenylethane, resulting in inaccurate feeding and affecting product quality and consistency.

Method used

An EDTA-2Na wet automatic feeding device is designed, including a chassis, universal wheel, vertical plate, slideway, electric telescopic rod, feeding box, electronic flowmeter and other components to realize the accurate automatic delivery of EDTA-2Na aqueous solution, and ensure the uniformity of dissolution through stirring and heating.

Benefits of technology

Improve feeding efficiency and safety, ensure product quality and consistency, and the mobility and flexibility of the device make it suitable for different reaction equipment.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the technical field of decabromodiphenyl ethane production, in particular to an EDTA-2Na wet-process automatic feeding device in a decabromodiphenyl ethane production process, which comprises a bottom frame, a vertical plate is fixedly mounted at the top of the bottom frame, a slide way is arranged on one side of the vertical plate, and a threaded rod is rotatably mounted in the slide way. According to the EDTA-2Na wet-process automatic feeding device in the decabromodiphenyl ethane production process, through cooperative use of the bottom frame, universal wheels, a vertical plate, a slide way, an electric telescopic rod, a mounting plate, a first motor, a feeding pipe, a feeding box body, a feeding pipe, a threaded rod, an electric valve, an electronic flow meter and an adjusting block, an EDTA-2Na aqueous solution in the feeding box body is added into reaction equipment through the feeding pipe; in the process that a water solution passes through the interior of the feeding pipe, the electronic flowmeter can monitor the flow of the water solution in real time, and when the adding amount is reached, the electronic flowmeter can send a signal to the master controller to control the electric valve to be closed, so that accurate feeding is achieved.
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Description

Technical Field

[0001] The utility model relates to the technical field of decabromodiphenylethane production, in particular to a wet automatic feeding device for EDTA-2Na in the production process of decabromodiphenylethane. Background Technique

[0002] In the production process of decabromodiphenylethane, EDTA-2Na (disodium ethylenediaminetetraacetate) serves as an important complexing agent and plays a crucial role. EDTA-2Na can effectively form stable complexes with metal ions, thereby preventing the interference of metal ions on the reaction. This complexing agent needs to be added accurately and timely according to the changes in reaction conditions during the production process to ensure the smooth progress of the reaction and the high purity of the final product.

[0003] Traditional manual feeding methods have many problems in industrial production. First of all, this method usually requires operators to perform manual operations at the production site. Not only is the labor intensity high, but the operation process often requires long-term physical labor, which is prone to fatigue. Fatigued operators may have problems such as inattentiveness or non-standard operations, increasing the risk of inaccurate feeding. Secondly, due to factors such as personnel experience, operating environment, and the accuracy of weighing tools, it is difficult to ensure that the amount of materials added each time is exactly the same. This inconsistency will not only lead to incomplete reactions or increased side reactions, but also affect the quality and consistency of the product.

[0004] Therefore, it is necessary to provide a wet automatic feeding device for EDTA-2Na in the production process of decabromodiphenylethane to solve the above technical problems. Content of the Utility Model

[0005] The purpose of the utility model is to provide a wet automatic feeding device for EDTA-2Na in the production process of decabromodiphenylethane to solve the problems raised in the above background technique.

[0006] To achieve the above purpose, the utility model provides the following technical solutions:

[0007] A wet automatic feeding device for EDTA-2Na in the production process of decabromodiphenylethane, which includes:

[0008] A chassis, on the top of which a vertical plate is fixedly installed. On one side of the vertical plate, a slideway is opened. Inside the slideway, a threaded rod is rotatably installed. On the top of the vertical plate, a first motor is fixedly installed, and the driving end of the first motor penetrates through the top of the vertical plate and extends into the inside of the slideway to be fixedly connected to the top end of the threaded rod. A regulating block is threadedly connected to the outer wall of the threaded rod, and the regulating block is slidably connected to the slideway;

[0009] One side of the adjusting block is fixedly installed with a mounting plate. One side of the mounting plate is fixedly installed with an electric telescopic rod. The driving end of the electric telescopic rod is fixedly installed with a feeding box body. Both sides of the top of the feeding box body are fixedly inserted and installed with feed pipes. The bottom of the feeding box body is fixedly inserted and installed with a feeding pipe. An electric valve and an electronic flowmeter are respectively arranged on the feeding pipe. Universal wheels are symmetrically fixedly installed on both sides of the bottom of the chassis.

[0010] Preferably, a stirring shaft is rotatably installed inside the feeding box body. A second motor is fixedly installed on the top of the feeding box body. The driving end of the second motor penetrates through the top of the feeding box body and extends into the inside of the feeding box body to be fixedly connected with the top end of the stirring shaft. A plurality of stirring rollers are fixedly installed on the outer wall of the stirring shaft. Heating plates are fixedly installed on both sides of the inner wall of the feeding box body. A temperature sensor is fixedly installed on the inner wall of the feeding box body.

[0011] Preferably, an operation window is opened on the front of the feeding box body. A sealing plate adapted to the operation window is hinged on the front of the feeding box body. A lock is arranged between the sealing plate and the front of the feeding box body. A sealing gasket is adhered to the inner wall of the operation window.

[0012] Preferably, a plurality of automatic telescopic rods are fixedly installed on one side of the mounting plate. The telescopic ends of the automatic telescopic rods are fixedly connected with one side of the feeding box body close to the mounting plate.

[0013] Preferably, symmetrically distributed limiting grooves are opened on the inner wall of the slideway. Limiting blocks are fixedly installed on the front and back of the adjusting block. The limiting blocks are slidably connected with the limiting grooves.

[0014] Preferably, a support block is fixedly installed between the lower part of one side of the vertical plate and the top of the chassis. A counterweight block is arranged on the top of the chassis on the other side of the vertical plate.

[0015] Compared with the prior art, the beneficial effects of the utility model are:

[0016] 1. The utility model realizes the automatic feeding of the EDTA-2Na aqueous solution in the feeding box body to the reaction equipment through the cooperation of the chassis, universal wheels, vertical plates, sliding rails, electric telescopic rods, mounting plates, first motors, feeding pipes, feeding box bodies, feeding pipes, threaded rods, electric valves, electronic flow meters and adjusting blocks. During the process of the aqueous solution passing through the feeding pipe, the electronic flow meter will monitor the flow rate of the aqueous solution in real time. When the added amount is reached, the electronic flow meter will send a signal to the main controller to control the electric valve to close, achieving accurate feeding. During the entire feeding process, it is automatically completed by this device, avoiding the non-standard operation of manual feeding, improving the feeding efficiency and safety, ensuring the quality and consistency of the product, and through the mobility of the device, as well as the vertical and horizontal movement of the feeding box body, enabling the device to be better matched with different reaction equipment, improving the flexibility of the device.

[0017] 2. The utility model realizes the stirring, heating and temperature monitoring of the materials added to the inside of the feeding box body through the cooperation of the second motor, stirring shaft, stirring roller, heating plate and temperature sensor, ensuring the complete dissolution of EDTA-2Na and water, as well as the uniformity of EDTA-2Na during the feeding process, preventing caking, and further improving the quality and consistency of the product.

[0018] 3. Through the cooperation of the limiting block and the limiting groove, during the sliding process of the adjusting block on the sliding rail, it will drive the limiting block to have a sliding contact with the limiting groove, playing a role of limiting and supporting the adjusting block, ensuring that the adjusting block has sufficient strength to support the structures installed on its side, and improving the stability and reliability of the device during use. Brief Description of the Drawings

[0019] Figure 1 is the structural schematic diagram of the utility model;

[0020] Figure 2 is the front sectional structural schematic diagram of the utility model;

[0021] Figure 3 is the connection structural schematic diagram of the adjusting block and the limiting block in the utility model;

[0022] Figure 4 is of the utility model Figure 2 The enlarged structural schematic diagram at position A.

[0023] In the figure: 1, chassis; 2, universal wheel; 3, counterweight; 4, support block; 5, vertical plate; 6, slideway; 7, electric telescopic rod; 8, mounting plate; 9, automatic telescopic rod; 10, first motor; 11, feed pipe; 12, second motor; 13, feeding box body; 14, operation window; 15, sealing plate; 16, feeding pipe; 17, threaded rod; 18, stirring shaft; 19, stirring roller; 20, temperature sensor; 21, heating plate; 22, electric valve; 23, electronic flowmeter; 24, limit groove; 25, limit block; 26, adjusting block. Specific embodiments

[0024] In order to make the technical means, creative features, achieved purposes and functions of the present utility model easy to understand, the present utility model will be further described below in conjunction with specific embodiments.

[0025] In the description of the present utility model, it should be noted that the orientation or positional relationship indicated by the terms "upper", "lower", "inner", "outer", "front end", "rear end", "both ends", "one end", "the other end", etc. is based on the orientation or positional relationship shown in the drawings, and is only for the convenience of describing the present utility model and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of the present utility model. In addition, the terms "first" and "second" are only used for descriptive purposes and cannot be construed as indicating or implying relative importance.

[0026] In the description of the present utility model, it should be noted that unless otherwise clearly specified and limited, the terms "installation", "provided with", "connection", etc. should be understood in a broad sense. For example, "connection" can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be directly connected or indirectly connected through an intermediate medium, and it can be the communication inside two elements. For those of ordinary skill in the art, the specific meanings of the above terms in the present utility model can be understood according to specific situations.

[0027] Next, the technical solutions in the embodiments of the present utility model will be clearly and completely described in conjunction with the drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all the embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without making creative efforts belong to the protection scope of the present utility model.

[0028] Please refer to Figures 1-4 , the embodiment provided by the present utility model:

[0029] An EDTA-2Na wet automatic feeding device in the production process of decabromodiphenylethane, which includes:

[0030] The chassis 1 has a vertical plate 5 fixedly installed on the top thereof. A slideway 6 is provided on one side of the vertical plate 5. A threaded rod 17 is rotatably installed inside the slideway 6. A first motor 10 is fixedly installed on the top of the vertical plate 5, and the driving end of the first motor 10 penetrates through the top of the vertical plate 5 and extends into the slideway 6 to be fixedly connected to the top end of the threaded rod 17. A regulating block 26 is threadedly connected to the outer wall of the threaded rod 17, and the regulating block 26 is slidably connected to the slideway 6;

[0031] One side of the regulating block 26 is fixedly installed with a mounting plate 8. One side of the mounting plate 8 is fixedly installed with an electric telescopic rod 7. The driving end of the electric telescopic rod 7 is fixedly installed with a feeding box body 13. Both sides of the top of the feeding box body 13 are fixedly inserted and installed with feeding pipes 11. The bottom of the feeding box body 13 is fixedly inserted and installed with a feeding pipe 16. An electric valve 22 and an electronic flowmeter 23 are respectively arranged on the feeding pipe 16. Symmetrically distributed universal wheels 2 are fixedly installed on both sides of the bottom of the chassis 1.

[0032] A stirring shaft 18 is rotatably installed inside the feeding box body 13. A second motor 12 is fixedly installed on the top of the feeding box body 13, and the driving end of the second motor 12 penetrates through the top of the feeding box body 13 and extends into the feeding box body 13 to be fixedly connected to the top end of the stirring shaft 18. A plurality of stirring rollers 19 are fixedly installed on the outer wall of the stirring shaft 18. Heating plates 21 are fixedly installed on both sides of the inner wall of the feeding box body 13. A temperature sensor 20 is fixedly installed on the inner wall of the feeding box body 13.

[0033] In one embodiment, an operation window 14 is provided on the front of the feeding box body 13. A sealing plate 15 adapted to the operation window 14 is hinged on the front of the feeding box body 13. A lock catch is arranged between the sealing plate 15 and the front of the feeding box body 13. A sealing gasket is adhered to the inner wall of the operation window 14, which is convenient for the staff to open the sealing plate 15 after the device is used and carry out the cleaning and maintenance work on the inside of the feeding box body 13 through the operation window 14.

[0034] In one preferred embodiment, a plurality of automatic telescopic rods 9 are fixedly installed on one side of the mounting plate 8, and the telescopic ends of the automatic telescopic rods 9 are fixedly connected to one side of the feeding box body 13 close to the mounting plate 8. The automatic telescopic rods 9 play a role in supporting and limiting the feeding box body 13, avoiding the weight of the feeding box body 13 acting completely on the electric telescopic rod 7, reducing the burden on the electric telescopic rod 7, thereby prolonging the service life of the electric telescopic rod 7 and reducing the risk of failure caused by overloading.

[0035] In one embodiment, symmetrically distributed limiting grooves 24 are provided on the inner wall of the slideway 6. Limiting blocks 25 are fixedly installed on the front and back of the regulating block 26, and the limiting blocks 25 are slidably connected to the limiting grooves 24.

[0036] In one of the preferred embodiments, a support block 4 is fixedly installed between the lower part of one side of the vertical plate 5 and the top of the chassis 1. A counterweight block 3 is arranged on the top of the chassis 1 on the other side of the vertical plate 5. The arrangement of the support block 4 improves the connection strength between the vertical plate 5 and the chassis 1, enabling it to support the device more stably. The arrangement of the counterweight block 3 maintains the overall balance of the device and avoids the phenomenon of tipping over.

[0037] The working principle of the present utility model is as follows: all the electrical components mentioned in the text are electrically connected to the main controller and the power supply. The main controller can be a conventional known device such as a computer for control, and the existing publicly disclosed electrical connection technologies are not elaborated in the text. The parts not involved in this device are the same as the prior art or can be implemented using the prior art. When in use, first control the first motor 10 to start working. The driving end of the first motor 10 drives the threaded rod 17 to rotate. Through the threaded transmission between the threaded rod 17 and the adjusting block 26, and the sliding relationship between the adjusting block 26 and the slideway 6, the adjusting block 26 moves vertically stably. The movement of the adjusting block 26 drives the mounting plate 8 to move. The movement of the mounting plate 8 drives the electric telescopic rod 7 to move. The movement of the electric telescopic rod 7 drives the feeding box body 13 to move. Therefore, through the drive of the first motor 10, the vertical movement of the feeding box body 13 can be realized. The feeding box body 13 is moved downward to a position where the staff can easily reach. Then, a certain proportion of EDTA-2Na and water are added into the feeding box body 13 through the feeding pipe 11 to form an aqueous solution of EDTA-2Na. Then, control the feeding box body 13 to move up to the specified height, and through the rolling contact of the universal wheels 2 with the ground, move the device to the side of the decabromodiphenylethane production reaction equipment. At the same time, control the electric telescopic rod 7 to start working. The driving end of the electric telescopic rod 7 drives the feeding box body 13 to move horizontally, so that the feeding pipe 16 at the bottom of the feeding box body 13 moves above the feeding end of the reaction equipment. Then, control the vertical movement of the feeding box body 13 to insert the bottom end of the feeding pipe 16 into the inside of the feeding end. Subsequently, control the electric valve 22 and the electronic flowmeter 23 to start working. After the electric valve 22 is opened, the EDTA-2Na aqueous solution inside the feeding box body 13 is added into the reaction equipment through the feeding pipe 16. During the process of the aqueous solution passing through the inside of the feeding pipe 16, the electronic flowmeter 23 will monitor the flow rate of the aqueous solution in real time. When the added amount is reached, the electronic flowmeter 23 will send a signal to the main controller to control the electric valve 22 to close, achieving precise feeding. Throughout the feeding process, it is all automatically completed by this device, avoiding the non-standard operation of manual feeding, improving the feeding efficiency and safety, ensuring the quality and consistency of the product, and through the mobility of the device, as well as the vertical and horizontal movement of the feeding box body 13, enabling the device to be better matched with different reaction equipment, improving the flexibility of the device.

[0038] After adding EDTA-2Na and water into the feeding box body 13 in a certain proportion, the second motor 12 can be controlled to start working. The driving end of the second motor 12 drives the stirring shaft 18 to rotate. The rotation of the stirring shaft 18 drives the stirring roller 19 to rotate. The rotation of the stirring roller 19 stirs the materials inside the feeding box body 13. At the same time, the heating plate 21 is controlled to start working. The heating plate 21 heats the materials inside the feeding box body 13. Cooperating with the temperature sensor 20, the temperature of the solution inside the feeding box body 13 can be monitored in real time, realizing the stirring, heating and temperature monitoring of the materials added into the feeding box body 13, ensuring the complete dissolution of EDTA-2Na and water, and the uniformity of EDTA-2Na during the feeding process, preventing caking, and further improving the quality and consistency of the product.

[0039] The above shows and describes the basic principle, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited by the above embodiments. The above embodiments and the descriptions in the specification are only preferred examples of the present invention and are not used to limit the present invention. Without departing from the spirit and scope of the present invention, the present invention will have various changes and improvements, and these changes and improvements all fall within the scope of the present invention claimed. The scope of protection claimed by the present invention is defined by the appended claims and their equivalents.

Claims

1. An EDTA-2Na wet automatic feeding device in the production process of decabromodiphenylethane, characterized in that, It includes: A chassis (1), on the top of the chassis (1), a vertical plate (5) is fixedly installed. On one side of the vertical plate (5), a slideway (6) is provided. Inside the slideway (6), a threaded rod (17) is rotatably installed. On the top of the vertical plate (5), a first motor (10) is fixedly installed, and the driving end of the first motor (10) penetrates through the top of the vertical plate (5) and extends into the inside of the slideway (6) and is fixedly connected to the top end of the threaded rod (17). A regulating block (26) is threadedly connected to the outer wall of the threaded rod (17), and the regulating block (26) is slidably connected to the slideway (6); On one side of the regulating block (26), a mounting plate (8) is fixedly installed. On one side of the mounting plate (8), an electric telescopic rod (7) is fixedly installed. The driving end of the electric telescopic rod (7) is fixedly installed with a feeding box body (13). On both sides of the top of the feeding box body (13), feeding pipes (11) are fixedly inserted. At the bottom of the feeding box body (13), a feeding pipe (16) is fixedly inserted. An electric valve (22) and an electronic flowmeter (23) are respectively arranged on the feeding pipe (16). On both sides of the bottom of the chassis (1), symmetrically distributed universal wheels (2) are fixedly installed.

2. The EDTA-2Na wet automatic feeding device in the production process of decabromodiphenylethane according to claim 1, characterized in that: Inside the feeding box body (13), a stirring shaft (18) is rotatably installed. On the top of the feeding box body (13), a second motor (12) is fixedly installed, and the driving end of the second motor (12) penetrates through the top of the feeding box body (13) and extends into the inside of the feeding box body (13) and is fixedly connected to the top end of the stirring shaft (18). A number of stirring rollers (19) are fixedly installed on the outer wall of the stirring shaft (18). On both sides of the inner wall of the feeding box body (13), heating plates (21) are fixedly installed. A temperature sensor (20) is fixedly installed on the inner wall of the feeding box body (13).

3. The EDTA-2Na wet automatic feeding device in the production process of decabromodiphenylethane according to claim 1, wherein: On the front of the feeding box body (13), an operation window (14) is provided. On the front of the feeding box body (13), a sealing plate (15) adapted to the operation window (14) is hinged. A lock is arranged between the sealing plate (15) and the front of the feeding box body (13). A sealing gasket is adhered to the inner wall of the operation window (14).

4. The EDTA-2Na wet automatic feeding device in the production process of decabromodiphenylethane according to claim 1, characterized in that: On one side of the mounting plate (8), a number of automatic telescopic rods (9) are fixedly installed, and the telescopic ends of the automatic telescopic rods (9) are fixedly connected to one side of the feeding box body (13) close to the mounting plate (8).

5. The EDTA-2Na wet automatic feeding device in the production process of decabromodiphenylethane according to claim 1, characterized in that: On the inner wall of the slideway (6), symmetrically distributed limiting grooves (24) are provided. On the front and back of the regulating block (26), limiting blocks (25) are fixedly installed, and the limiting blocks (25) are slidably connected to the limiting grooves (24).

6. The EDTA-2Na wet automatic feeding device in the production process of decabromodiphenylethane according to claim 1, characterized in that: Between the lower part of one side of the vertical plate (5) and the top of the chassis (1), a support block (4) is fixedly installed. On the top of the chassis (1), on the other side of the vertical plate (5), a counterweight block (3) is arranged.