Auxiliary device for preparing porphyrin metal organic framework material

Abstract

The utility model provides an auxiliary device for preparing porphyrin metal organic framework materials. The auxiliary device comprises a body, a limiting frame is arranged in the body, a plurality of reset grooves are formed in the limiting frame, reset blocks are connected in the reset grooves in a sliding mode, and one end of each reset block is fixedly connected with a reset rope. According to the preparation auxiliary device of the porphyrin metal organic framework material, the multiple inner containers placed in the body are separately stored through the limiting frames, so that collision and damage between the inner containers are prevented, the limiting frames and the body are limited through the cooperation of the limiting seats and the limiting blocks, and the stability of the inner containers is improved. The limiting frame can be conveniently mounted and dismounted, meanwhile, the reset grooves are matched with the reset blocks, the reset ropes and the reset springs, the two reset handles can extend, move and be combined towards the middle, and therefore the limiting frame can be conveniently taken out from the interior of the body through the two reset handles.

Description

Technical Field

[0001] This utility model relates to the field of porphyrin-based metals, and more particularly to an auxiliary device for the preparation of porphyrin-based metal-organic framework materials. Background Technology

[0002] Porphyrins are a class of large cyclic compounds formed by four pyrrole subunits linked by a methylene bridge. They generally have a cavity at the center that can coordinate with metal ions. This special structure gives them a strong ability to complex metal ions.

[0003] Now, a certain amount of tetracarboxyphenylporphyrin and ferric chloride are added to the inner liner of the reactor, and then an anhydrous ethanol solution of hydrochloric acid and dimethylbenzamine are added as solvents. At this time, the inner liner of the reactor containing the solvent is placed in an ultrasonic cleaner and shaken for 20 minutes to mix evenly.

[0004] However, nowadays, the inner liner is placed directly in the ultrasonic cleaner, which causes collisions between the inner liners when multiple reactor inner liners are mixed at the same time, making the inner liners prone to damage.

[0005] Therefore, it is necessary to provide an auxiliary device for the preparation of porphyrin-based metal-organic framework materials to solve the above-mentioned technical problems. Utility Model Content

[0006] This invention provides an auxiliary device for the preparation of porphyrin-based metal-organic framework materials, which solves the problem that collisions occur between inner tanks when the inner tank is directly placed in an ultrasonic cleaner.

[0007] To solve the above-mentioned technical problems, this utility model provides an auxiliary device for the preparation of porphyrin-based metal-organic framework materials, comprising:

[0008] ontology;

[0009] A limiting frame is provided inside the main body. The limiting frame has multiple reset slots inside, and a reset block is slidably connected inside each of the multiple reset slots. A reset rope is fixedly connected to one end of each of the multiple reset blocks. A reset spring is provided at one end of each of the multiple reset blocks and inside the multiple reset slots. Two reset handles are provided at one end of each of the multiple reset ropes.

[0010] Multiple storage slots, all of which are disposed inside the limiting frame;

[0011] Two limiting seats are provided on the top of the main body, and a limiting block is slidably connected inside each of the two limiting seats.

[0012] Preferably, one end of each of the plurality of reset ropes is fixedly connected to the bottom of both ends of the two reset handles.

[0013] Preferably, the bottom of one end of each of the two limiting blocks is fixedly connected to both ends of the top of the limiting frame.

[0014] Preferably, each of the two limiting blocks has two fixing holes inside, and each of the fixing holes is slidably connected with a fixing pin.

[0015] Preferably, each of the two limiting seats has two fixing slots inside, and each of the two fixing slots is provided with a fixing spring.

[0016] Preferably, extension sleeves are fixedly installed at both ends of the main body, and extension rods are slidably connected inside the two extension sleeves.

[0017] Preferably, both of the extension sleeves are provided with positioning elements inside, each positioning element including a positioning hole, and a positioning pin is threaded into the positioning hole.

[0018] Compared with related technologies, the auxiliary device for preparing porphyrin-based metal-organic framework materials provided by this utility model has the following beneficial effects:

[0019] This invention provides an auxiliary device for the preparation of porphyrin-based metal-organic framework materials. A limiting frame separates multiple inner liner units placed inside the main body, preventing collisions and damage between the inner liner units. A limiting seat, in conjunction with a limiting block, limits the distance between the limiting frame and the main body, facilitating the installation and removal of the limiting frame. Simultaneously, a reset groove, in conjunction with a reset block, reset rope, and reset spring, allows two reset handles to extend and merge towards the center, facilitating the removal of the limiting frame from the main body using the two reset handles. Attached Figure Description

[0020] Figure 1 A schematic diagram of the structure of a first embodiment of an auxiliary device for preparing porphyrin-based metal-organic framework materials provided by this utility model;

[0021] Figure 2 for Figure 1 A cross-sectional structural schematic diagram of the main body shown;

[0022] Figure 3 for Figure 2 The enlarged schematic diagram of part A shown below;

[0023] Figure 4 for Figure 2 The enlarged schematic diagram of section B is shown below;

[0024] Figure 5A schematic diagram of the structure of a second embodiment of an auxiliary device for preparing porphyrin-based metal-organic framework materials provided by this utility model;

[0025] Figure 6 for Figure 5 The enlarged schematic diagram of section C is shown.

[0026] The following are the labels in the diagram: 1. Main body, 2. Limiting frame, 21. Reset groove, 22. Reset block, 23. Reset rope, 24. Reset spring, 25. Reset handle, 3. Storage groove, 4. Limiting seat, 5. Limiting block, 6. Fixing hole, 7. Fixing pin, 8. Fixing groove, 9. Fixing spring, 10. Extension sleeve, 11. Extension rod, 12. Positioning component. Detailed Implementation

[0027] The present invention will be further described below with reference to the accompanying drawings and embodiments.

[0028] First Embodiment

[0029] Please refer to the following: Figure 1 , Figure 2 , Figure 3 and Figure 4 ,in, Figure 1 A schematic diagram of the structure of a first embodiment of an auxiliary device for preparing porphyrin-based metal-organic framework materials provided by this utility model; Figure 2 for Figure 1 A cross-sectional structural schematic diagram of the main body shown; Figure 3 for Figure 2 The enlarged schematic diagram of part A shown below;

[0030] Figure 4 for Figure 2 The enlarged schematic diagram of part B is shown. An auxiliary device for the preparation of porphyrin-based metal-organic framework materials includes:

[0031] Ontology 1;

[0032] The limiting frame 2 is disposed inside the body 1. The limiting frame 2 has multiple reset slots 21 inside. Each of the multiple reset slots 21 is slidably connected to a reset block 22. One end of each of the multiple reset blocks 22 is fixedly connected to a reset rope 23. One end of each of the multiple reset blocks 22 and located inside the multiple reset slots 21 is provided with a reset spring 24. One end of each of the multiple reset ropes 23 is provided with two reset handles 25.

[0033] Multiple storage slots 3 are provided inside the limiting frame 2;

[0034] Two limiting seats 4 are provided on the top of the main body 1, and a limiting block 5 is slidably connected inside each of the two limiting seats 4.

[0035] One end of each of the multiple reset ropes 23 is fixedly connected to the top of the multiple reset blocks 22 and the two ends of the bottom of the two reset handles 25, respectively, so as to drive the reset ropes 23 connected to the reset blocks 22 to move upward inside the reset groove 21 when the reset handles 25 are pulled.

[0036] Multiple storage slots 3 are located inside the limiting frame 2 for storing and limiting the contents of the reactor.

[0037] The limiting seat 4 is a U-shaped seat, which is used to limit the limiting block 5 after the limiting block 5 is inserted into the inside of the limiting seat 4, thereby limiting the limiting clamp 2.

[0038] One end of each of the reset ropes 23 is fixedly connected to the bottom of both ends of the two reset handles 25.

[0039] The bottom of one end of each of the two limiting blocks 5 is fixedly connected to the two ends of the top of the limiting frame 2.

[0040] Each of the two limiting blocks 5 has two fixing holes 6 inside, and fixing pins 7 are slidably connected inside the multiple fixing holes 6.

[0041] One end of the fixing pin 7 is semi-circular, and the interior of each of the two limiting blocks 5 has two semi-circular fixing holes 6 that are adapted to the fixing pin 7.

[0042] Each of the two limiting seats 4 has two fixing grooves 8 inside, and each of the two fixing grooves 8 is provided with a fixing spring 9.

[0043] Multiple fixing pins 7 are slidably connected to the inside of fixing grooves 8, and fixing springs 9 are provided at one end of each fixing pin 7 and inside each fixing groove 8.

[0044] When the two limiting blocks 5 enter the interior of the two limiting seats 4, they compress the multiple fixing pins 7 and move them to one side within the multiple fixing grooves 8, while simultaneously compressing the multiple fixing springs 9. When the two limiting blocks 5 enter the appropriate positions within the two limiting seats 4, the multiple fixing springs 9 push the multiple fixing pins 7 to move and reset to one side within the multiple fixing grooves 8, thereby allowing one end of each fixing pin 7 to enter the appropriate position within the multiple fixing holes 6, thus limiting the limiting blocks 5.

[0045] The limiting block 5 moves to one side and is removed, causing the multiple fixing pins 7 to move to one side and separate from the temporal part of the multiple fixing holes 6.

[0046] The working principle of the auxiliary device for preparing porphyrin-based metal-organic framework materials provided by this utility model is as follows:

[0047] In use, after placing the limiting frame 2 inside the main body 1, the two limiting blocks 5 enter the two limiting seats 4 respectively, and then the inner liner is placed inside the limiting frame 2.

[0048] When the limit frame 2 is removed, by moving the two reset handles 25 upward, multiple reset ropes 23 connected to multiple reset blocks 22 move upward inside multiple reset slots 21, while squeezing multiple reset springs 24. When the two reset handles 25 are combined, pulling the reset handles 25 upward causes the limit frame 2 to move upward inside the body 1 and separate, and then the limit frame 2 can be removed.

[0049] After the two reset handles 25 are released, multiple reset springs 24 push multiple reset blocks 22 to move to one side inside the two reset slots 21 to reset, thereby driving multiple reset ropes 23 connected to the two reset handles 25 to reset.

[0050] Compared with related technologies, the auxiliary device for preparing porphyrin-based metal-organic framework materials provided by this utility model has the following beneficial effects:

[0051] This utility model provides an auxiliary device for the preparation of porphyrin-based metal-organic framework materials. The device uses a limiting frame 2 to separate multiple inner liner placed inside the main body 1, thereby preventing collisions and damage between the inner liners. The limiting seat 4, in conjunction with the limiting block 5, limits the distance between the limiting frame 2 and the main body 1, facilitating the installation and removal of the limiting frame 2. At the same time, the reset groove 21, in conjunction with the reset block 22, the reset rope 23, and the reset spring 24, allows the two reset handles 25 to extend and merge towards the middle, thereby facilitating the removal of the limiting frame 2 from the inside of the main body 1 through the two reset handles 25.

[0052] Second Embodiment

[0053] Please refer to the following: Figure 5 and Figure 6 Based on the auxiliary device for preparing porphyrin-based metal-organic framework materials provided in the first embodiment of this application, the second embodiment of this application proposes another auxiliary device for preparing porphyrin-based metal-organic framework materials. The second embodiment is merely a preferred embodiment of the first embodiment, and the implementation of the second embodiment will not affect the separate implementation of the first embodiment.

[0054] Specifically, the difference in the preparation auxiliary device for porphyrin-based metal-organic framework materials provided in the second embodiment of this application is that, in the preparation auxiliary device for porphyrin-based metal-organic framework materials, both ends of the main body 1 are fixedly installed with extension sleeves 10, and extension rods 11 are slidably connected inside the two extension sleeves 10.

[0055] One end of each of the two extension rods 11 is fixedly connected to one side of each of the two limiting seats 4, so that when the extension rods 11 move up or down, they can drive the limiting seats 4 to move up or down.

[0056] Both of the extension sleeves 10 are provided with positioning elements 12 inside, each positioning element 12 including a positioning hole, and a positioning pin is threaded into the positioning hole.

[0057] The positioning pin is a bolt. The extension sleeve 10 has a positioning hole that matches the positioning pin. When the positioning pin rotates to one side, the extension sleeve 10 moves to one side inside the positioning hole. When one end of the positioning pin contacts the surface of the extension rod 11, it limits the extension rod 11. When one end of the positioning pin separates from the surface of the extension rod 11, the extension rod 11 can move inside the extension sleeve 10.

[0058] The working principle of the auxiliary device for preparing porphyrin-based metal-organic framework materials provided by this utility model is as follows:

[0059] In use, after releasing the two positioning pieces 12, the two limit seats 4 are moved upward to drive the two extension rods 11 to move upward to the appropriate position inside the two extension sleeves 10 respectively, and then the two positioning pieces 12 are reset.

[0060] Compared with related technologies, the auxiliary device for preparing porphyrin-based metal-organic framework materials provided by this utility model has the following beneficial effects:

[0061] This invention provides an auxiliary device for the preparation of porphyrin-based metal-organic framework materials. By using an extension sleeve 10 in conjunction with an extension rod 11 and a positioning member 12, the limiting frame 2 can be raised to a suitable position and then limited, thereby filtering out water stains adhering to the inner surface.

[0062] The above description is merely an embodiment of this utility model and does not limit the patent scope of this utility model. Any equivalent structural or procedural transformations made based on the content of this utility model specification and drawings, or direct or indirect applications in other related technical fields, are similarly included within the patent protection scope of this utility model.

Claims

1. An auxiliary device for the preparation of porphyrin-based metal-organic framework materials, characterized in that, include: ontology; A limiting frame is provided inside the main body. The limiting frame has multiple reset slots inside, and a reset block is slidably connected inside each of the multiple reset slots. A reset rope is fixedly connected to one end of each of the multiple reset blocks. A reset spring is provided at one end of each of the multiple reset blocks and inside the multiple reset slots. Two reset handles are provided at one end of each of the multiple reset ropes. Multiple storage slots, all of which are disposed inside the limiting frame; Two limiting seats are provided on the top of the main body, and a limiting block is slidably connected inside each of the two limiting seats.

2. The auxiliary device for preparing porphyrin-based metal-organic framework materials according to claim 1, characterized in that, One end of each of the reset ropes is fixedly connected to the bottom of both ends of the two reset handles.

3. The auxiliary device for preparing porphyrin-based metal-organic framework materials according to claim 1, characterized in that, The bottom of one end of each of the two limiting blocks is fixedly connected to the two ends of the top of the limiting frame.

4. The auxiliary device for preparing porphyrin-based metal-organic framework materials according to claim 3, characterized in that, Each of the two limiting blocks has two fixing holes inside, and each of the fixing holes is slidably connected with a fixing pin.

5. The auxiliary device for preparing porphyrin-based metal-organic framework materials according to claim 1, characterized in that, Each of the two limiting seats has two fixing slots inside, and each of the two fixing slots is equipped with a fixing spring.

6. The auxiliary device for preparing porphyrin-based metal-organic framework materials according to claim 1, characterized in that, Both ends of the main body are fixedly installed with extension sleeves, and extension rods are slidably connected inside the two extension sleeves.

7. The auxiliary device for preparing porphyrin-based metal-organic framework materials according to claim 6, characterized in that, Both of the extension sleeves are provided with positioning elements inside, each positioning element including a positioning hole, and a positioning pin is threaded into the positioning hole.

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