Salting-out treatment device for trimethyl borate
By installing a transparent acrylic plate salting-out chamber and a filter screen in the salting-out treatment device, the problems of low purity and inconvenient observation of trimethyl borate were solved, enabling the production of high-purity trimethyl borate and timely reaction adjustment.
Patent Information
- Application Number
- CN202423065519.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-12-12
- Publication Date
- 2025-11-25
- Estimated Expiration
- 2034-12-12
AI Technical Summary
Existing salting-out equipment for trimethyl borate cannot effectively filter and remove impurities, resulting in low purity. Furthermore, the salting-out state cannot be visually observed, affecting the timeliness of the reaction process.
A salting-out chamber made of transparent acrylic sheet was designed. The upper left end has a feed inlet and a filter screen. Combined with a stirring motor and stirring shaft, it can filter and remove impurities from raw material particles and liquid, and observe the salting-out state through the transparent material.
This improved the purity of trimethyl borate and allowed for timely observation of the salting-out process, facilitating timely adjustments to the reaction and enhancing the treatment effect.
Smart Images
Figure CN223587150U_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The utility model relates to the related equipment technical field of salting out treatment device, concretely relates to a kind of salting out treatment device of borate trimethyl ester. BACKGROUND
[0002] Salting out is a common physical separation method, which separates substances in mixed solution by using the influence of salt on aqueous solution. The principle of salting out is mainly to use the influence of salt on the ionic strength and solubility of aqueous solution, so as to realize the separation of substances in solution. When salting out trimethyl borate, a salting out treatment device will be used.
[0003] The existing salting out treatment device of trimethyl borate cannot filter and remove impurities from raw material particles and liquid for preparing trimethyl borate during use, resulting in low purity of trimethyl borate obtained after salting out. Secondly, it is not conducive to observation and timely response to make treatment reaction because the salting state of the salting out chamber cannot be directly observed during the salting out process. Therefore, there is an urgent need for a salting out treatment device of trimethyl borate to solve the above technical problems. UTILITY MODEL CONTENT
[0004] The utility model aims to provide a kind of salting out treatment device of borate trimethyl ester, to solve the problems of the existing salting out treatment device of trimethyl borate in the above background art, which cannot filter and remove impurities from raw material particles and liquid for preparing trimethyl borate during use, resulting in low purity of trimethyl borate obtained after salting out, and cannot directly observe the salting state of the salting out chamber during the salting out process, which is not conducive to observation and timely response to make treatment reaction.
[0005] To achieve the above purpose, the utility model adopts the technical scheme: a kind of salting out treatment device of borate trimethyl ester, including device box, the bottom of the device box both sides are supported foot, the top of the device box is installed with stirring motor in the middle, the inside of the device box is provided with salting out chamber, the inside of the salting out chamber is provided with stirring shaft in the middle, the output shaft of the stirring motor is connected with coupling by passing through the top of device box, the top of the stirring shaft is connected with the lower end of coupling by passing through the top of salting out chamber, the bottom of the salting out chamber is provided with discharge port, the left upper end of the salting out chamber is provided with inlet, the inside of the inlet is provided with filter screen, the front end of the device box both sides are connected with box door by hinge, the discharge port is installed with valve, the bottom of the salting out chamber both sides are connected with the inside bottom of device box by stand column, the right upper end of the salting out chamber is provided with sampling port.
[0006] As a preferred technical scheme of the utility model, the salting out chamber is made of transparent acrylic plate material.
[0007] As a preferred technical scheme of the utility model, the filter screen is arranged obliquely and is left high and right low.
[0008] As a preferred technical scheme of the utility model, the number of the hinges is four, and the four hinges are arranged oppositely in pairs about the device box.
[0009] As a preferred technical scheme of the utility model, the number of the supporting feet is four.
[0010] As a preferred technical scheme of the utility model, the discharge port and the feeding port are respectively spaced from the bottom and the top of the device box.
[0011] Due to the use of the above technical scheme, the application has the beneficial effects compared with the prior art, which are as follows:
[0012] The salt precipitation treatment device of trimethyl borate of the application filters the raw material particles and liquid for preparing trimethyl borate through the filter screen arranged at the upper left end of the salt precipitation chamber, so that the purity of trimethyl borate obtained after salt precipitation treatment is improved; the salt precipitation chamber is made of transparent acrylic plate material, so that the salt precipitation state of the salt precipitation chamber can be directly observed during the salt precipitation process, which is beneficial to observation and facilitates timely treatment reaction. BRIEF DESCRIPTION OF DRAWINGS
[0013] In order to more clearly illustrate the specific embodiments of the utility model or the technical scheme in the prior art, the drawings needed in the specific embodiments or the prior art description will be briefly introduced as follows. Obviously, the drawings in the following description are some embodiments of the utility model, and those skilled in the art can also obtain other drawings according to these drawings without creative labor.
[0014] Figure 1 It is the overall structure schematic view of the utility model;
[0015] Figure 2 It is the overall structure sectional view schematic view of the utility model;
[0016] Figure 3 It is the overall structure sectional view schematic view of the utility model; Figure 2 The enlarged structure schematic view of A in the utility model.
[0017] In the drawing: 1, device box; 2, supporting foot; 3, salt precipitation chamber; 4, hinge; 5, discharge port; 6, valve; 7, stand column; 8, stirring motor; 9, coupling; 10, stirring shaft; 11, sampling port; 12, feeding port; 13, filter screen; 14, box door. DETAILED DESCRIPTION
[0018] In order to make the person skilled in the art better understand the scheme of the present application, the technical scheme in the embodiments of the present application will be clearly and completely described below in conjunction with the drawings in the embodiments of the present application. Obviously, the described embodiments are only a part of the embodiments of the present application, not all the embodiments. Based on the embodiments in the present application, all other embodiments obtained by the person skilled in the art without creative labor should belong to the scope of protection of the present application.
[0019] It should be noted that the terms "first", "second" and the like in the specification and claims of the present application and the above-described drawings are used to distinguish similar objects, and do not necessarily have to describe a specific order or sequence. It should be understood that the data thus used can be interchanged under appropriate circumstances, so that the embodiments of the present application described herein. In addition, the terms "include" and "have" and any variations thereof are intended to cover non-exclusive inclusion, for example, a process, method, system, product or device including a series of steps or units does not have to be limited to those steps or units clearly listed, but can include other steps or units not clearly listed or inherent to these processes, methods, products or devices.
[0020] In the present application, the terms "upper", "lower", "left", "right", "front", "back", "top", "bottom", "inner", "outer", "middle", "vertical", "horizontal", "lateral", "longitudinal" and the like indicate the orientation or positional relationship based on the orientation or positional relationship shown in the drawings. These terms are mainly used to better describe the present application and its embodiments, and are not intended to limit the indicated devices, elements or components to have a specific orientation, or to be constructed and operated in a specific orientation.
[0021] In addition, in addition to being used to indicate the orientation or positional relationship, the above-mentioned part of the terms can also be used to indicate other meanings, for example, the term "upper" can also be used to indicate a certain dependent relationship or connection relationship in some cases. For the person skilled in the art, the specific meaning of these terms in the present application can be understood according to the specific circumstances.
[0022] In addition, the terms "mount", "set", "provided with", "connected", "connected", "sleeved" should be broadly understood. For example, it can be fixedly connected, detachably connected, or integrally constructed; it can be mechanically connected, or electrically connected; it can be directly connected, or indirectly connected through an intermediate medium, or internal communication between two devices, elements or components. For the person skilled in the art, the specific meaning of the above-mentioned terms in the present application can be understood according to the specific circumstances.
[0023] It should be noted that the embodiments in the present application and the features in the embodiments can be combined with each other in the case of no conflict. The present application will be described in detail below with reference to the drawings and in combination with the embodiments.
[0024] Embodiment one
[0025] Appendix Figures 1-3 The utility model discloses a salt processing device of trimethyl borate, including the device box 1, the both sides of the bottom of device box 1 all support feet 2, the top middle part of device box 1 is installed with stirring motor 8, the inside of device box 1 is provided with salt room 3, the inside middle part of salt room 3 is provided with stirring shaft 10, the output shaft of stirring motor 8 passes through the top of device box 1 and is connected with the coupling 9, the top of stirring shaft 10 passes through the top of salt room 3 and is connected with the lower end of coupling 9, the bottom of salt room 3 is set up and is discharged 5, the left upper end of salt room 3 is set up and is entered 12, the inside of entered 12 is provided with filter screen 13, the both sides of the front end of device box 1 all are connected with the box door 14 through the hinge 4, the valve 6 is installed on the discharge outlet 5, the both sides of the bottom of salt room 3 all are connected with the inside bottom of device box 1 through stand 7, the right upper end of salt room 3 is set up and is taken 11.
[0026] Among them, the salt room 3 is made of transparent acrylic plate material, so that the salt state of the salt room 3 can be observed intuitively during the salt process, which is beneficial to observation and facilitates timely response.
[0027] Among them, the filter screen 13 is inclined and left high right low, the filter screen 13 is set in the left upper end of the salt room 3, and the filter screen 13 is set in the inside of the inlet 12, the filter screen 13 is set to filter and remove impurities of the raw material particles and liquid for preparing trimethyl borate, and the purity of trimethyl borate obtained after salt treatment is improved.
[0028] Among them, the number of hinges 4 is four, and the four hinges 4 are arranged opposite to each other about the device box 1.
[0029] Among them, the number of support feet 2 is four.
[0030] Among them, the discharge outlet 5 and the inlet 12 are respectively spaced from the bottom and the top of the device box 1.
[0031] The working principle and use process of the utility model are as follows: firstly, the constant-boiling substance composed of trimethyl borate and methanol and calcium chloride are poured into the salting-out chamber 3 from the feeding port 12, the filter screen 13 is arranged in the feeding port 12, the filter screen 13 is arranged to filter and remove impurities from the raw material particles and liquid for preparing trimethyl borate, the purity of trimethyl borate obtained after salting-out treatment is improved, after filtration, the trimethyl borate enters the salting-out chamber 3, at this time, the stirring motor 8 drives the stirring shaft 10 on the coupling 9, the constant-boiling substance composed of trimethyl borate and methanol and calcium chloride in the salting-out chamber 3 are mixed and stirred through the stirring shaft 10, then, after standing for a certain time, the trimethyl borate layer can be obtained from the upper layer liquid taken out from the sampling port 11, the remaining part is discharged from the discharging port 5 by opening the valve 6, the salting-out chamber 3 is made of transparent acrylic plate material, so that the salting-out state of the salting-out chamber can be directly observed during the salting-out process, which is beneficial to observation and facilitates timely treatment reaction, the contents not described in detail in the description belong to the prior art known to the person skilled in the art.
[0032] Finally, it should be noted that the above is only the preferred embodiment of the utility model, and is not used to limit the utility model, although the utility model is described in detail with reference to the foregoing embodiments, for the person skilled in the art, the technical scheme recorded in the foregoing embodiments can be modified, or some technical features can be replaced, any modification, equivalent replacement, improvement, etc. within the spirit and principles of the utility model should be included in the protection scope of the utility model.
Claims
1. A salting-out treatment apparatus for trimethyl borate, comprising an apparatus housing, characterized in that: The device housing has support feet on both sides of its bottom. A stirring motor is installed in the middle of the top of the housing. A salting-out chamber is located inside the housing, and a stirring shaft is located in the middle of the salting-out chamber. The output shaft of the stirring motor passes through the top of the housing and is connected to a coupling. The top of the stirring shaft passes through the top of the salting-out chamber and is connected to the lower end of the coupling. A discharge port is located at the bottom of the salting-out chamber, and a feed port is located at the upper left end of the chamber. A filter screen is installed inside the feed port. Doors are connected to both sides of the front of the housing via hinges. A valve is installed on the discharge port. The bottom sides of the salting-out chamber are connected to the bottom of the housing via columns. A sampling port is located at the upper right end of the salting-out chamber.
2. The salting-out treatment apparatus for trimethyl borate according to claim 1, characterized in that: The salting-out chamber is made of transparent acrylic sheet material.
3. The salting-out treatment apparatus for trimethyl borate according to claim 1, characterized in that: The filter screen is tilted and is oriented with the left side higher than the right.
4. The salting-out treatment apparatus for trimethyl borate according to claim 1, characterized in that: The number of hinges is set to four, and the four hinges are arranged in pairs facing each other about the device housing.
5. The salting-out treatment apparatus for trimethyl borate according to claim 1, characterized in that: The number of support feet is set to four.
6. The salting-out treatment apparatus for trimethyl borate according to claim 1, characterized in that: The discharge port and the inlet port are respectively spaced from the bottom and top of the device housing.