VOCs adsorbent all-silicon Beta molecular sieve synthesis processing device

By introducing a stirring and pushing mechanism into a horizontal reactor, the problem of uneven material mixing was solved, enabling efficient and uniform synthesis of all-silica Beta molecular sieves and improving product quality and production efficiency.

CN223615903UActive Publication Date: 2025-12-02JIANGSU TIANNUO NEW MATERIAL TECH
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Patent Information

Application Number
CN202423177926.6
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-12-23
Publication Date
2025-12-02
Estimated Expiration
2034-12-23

AI Technical Summary

Technical Problem

In the existing horizontal reactor process for VOCs adsorbent synthesis, uneven mixing of materials during flow leads to problems such as uneven reaction and inconsistent product quality.

Method used

A synthesis and processing device for VOCs adsorbent all-silica Beta molecular sieves was designed. It adopts a stirring mechanism and a pushing mechanism driven by a drive motor. Through the coordinated movement of the stirring rod and the spiral blade, the material is continuously stirred and pushed, avoiding material stratification and ensuring uniform mixing.

Benefits of technology

It improves the uniformity of material mixing, ensures the uniformity of the product and the synthesis effect, avoids mixing dead zones and stratification, and improves production efficiency.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a VOCs (Volatile Organic Compounds) adsorbent all-silicon Beta molecular sieve synthesis processing device in the technical field of zeolite molecular sieve synthesis equipment, which comprises a synthesis tank body arranged on a mounting frame, a driving motor I is mounted above the synthesis tank body, and a hopper I and a hopper II are respectively arranged on two sides of the driving motor I; feeders are respectively arranged at the lower parts of the hopper I and the hopper II; the feeders are connected with material pipes to convey raw materials into the synthesis tank body; the output shaft end of the driving motor I extends into the synthesis tank body and is in transmission connection with a bevel gear connecting structure, the bevel gear connecting structure is connected with a stirring mechanism and a pushing mechanism towards two sides respectively, and the stirring mechanism and the pushing mechanism are oppositely arranged in the synthesis tank body along the inner wall of the synthesis tank body; one end, close to the discharge port of the synthesis tank body, of the pushing mechanism is connected with a discharge push rod, and a discharge valve is arranged on the discharge port of the synthesis tank body. The device can promote the raw materials to be fully mixed, avoid uneven mixing and ensure the synthesis effect.
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Description

Technical Field

[0001] This utility model relates to the technical field of zeolite molecular sieve synthesis equipment, and in particular to a mixing device for the synthesis and processing of zeolite molecular sieves. Background Technology

[0002] VOCs adsorbent all-silica Beta molecular sieves have advantages such as high silica-to-alumina ratio, large specific surface area, and good hydrophobicity. During synthesis, thorough mixing of the raw materials is required. Crystallization synthesis of molecular sieves requires a crystallization reactor, which is available in vertical and horizontal types. Vertical reactors typically operate in batches, adding materials to the reactor for each production run, reacting, and then discharging the product. This is suitable for experimental research, multi-variety small-batch production, and scenarios requiring precise control of reaction conditions. Its disadvantage is low production capacity. Horizontal reactors generally operate continuously, suitable for large-scale production. Materials continuously enter the reactor from one end, gradually moving to the other end under stirring while reacting, and finally continuously discharging the product from the outlet, achieving a highly efficient and stable production process. The horizontal design of the reactor allows for smooth material flow within the reactor, reducing material stagnation and dead zones, and minimizing localized overheating or overcooling. However, its disadvantage is that the internal structure may cause variations in material flow velocity, affecting reaction uniformity and leading to inconsistent product quality. Utility Model Content

[0003] The purpose of this invention is to overcome the defects in the prior art and provide a synthesis and processing device for VOCs adsorbent all-silica Beta molecular sieves, which promotes full mixing of raw materials, avoids uneven mixing, and ensures the synthesis effect.

[0004] The purpose of this utility model is achieved as follows: A synthesis and processing device for VOCs adsorbent all-silica Beta molecular sieve includes a synthesis tank mounted on a mounting frame. A drive motor is mounted on the mounting frame above the synthesis tank. A hopper and a feeder are respectively provided on both sides of the drive motor. The lower part of the hoppers is provided with feeders. The feeders are connected to a material pipe to transport raw materials into the synthesis tank. The output shaft of the drive motor extends into the synthesis tank and is connected to a bevel gear connection structure for transmission. A stirring mechanism and a pushing mechanism are respectively connected to both sides of the bevel gear connection structure. The stirring mechanism and the pushing mechanism are arranged opposite each other in the synthesis tank along the inner wall of the synthesis tank. A discharge push rod is connected to the end of the pushing mechanism near the outlet of the synthesis tank. A discharge valve is provided on the outlet of the synthesis tank.

[0005] In operation, raw materials are added into the synthesis tank through hopper one and hopper two. The stirring mechanism and the pushing mechanism inside the synthesis tank are driven by the drive motor one. The stirring mechanism continuously stirs and mixes the raw materials in the synthesis tank, and the pushing mechanism continuously pushes and conveys the raw materials in the synthesis tank from bottom to top, so as to promote continuous stirring and mixing of the raw materials inside the synthesis tank, avoid uneven mixing of materials in layers, and improve the uniformity of the product.

[0006] Compared with the prior art, the beneficial effects of this utility model are as follows:

[0007] First, in this device, the material at the bottom of the synthesis tank is continuously pushed upward by the pushing mechanism, which mixes it thoroughly with the material at the top, promotes uniform mixing of the material inside the synthesis tank, avoids material stratification, and ensures the quality of product synthesis.

[0008] Secondly, the stirring mechanism of this device is equipped with several elastic stirring rods, which continuously stir and mix the materials inside the synthesis tank. The elastic stirring rods can also break up the materials and promote uniform mixing.

[0009] Third, the synthesis tank of this device is movably connected to the mounting frame through a plane bearing. The drive motor drives the synthesis tank to rotate within a certain limit along the horizontal direction of the plane bearing. This works in conjunction with the internal pushing and stirring mechanisms to avoid dead zones in the mixing inside the synthesis tank, ensuring uniform mixing and improving product quality.

[0010] Furthermore, the stirring mechanism includes a stirring rod that is driven to one side of the bevel gear connection structure, and the stirring rod is provided with a stirring bar.

[0011] Furthermore, the stirring rod is made of an elastic material, and multiple stirring rods are spaced apart along the surface of the stirring rod.

[0012] Furthermore, the pushing mechanism includes a pushing rod that is driven to the other side of the bevel gear connection structure, and the pushing rod is provided with helical blades.

[0013] Furthermore, the bevel gear connection structure includes a bevel gear one that is driven and connected to the output shaft of a drive motor. Bevel gear two and bevel gear three are perpendicularly meshed on both sides of bevel gear one. One side of bevel gear two is connected to bevel gear four via a transmission rod. Bevel gear four is meshed with bevel gear five. Bevel gear five is driven and connected to the stirring rod of the stirring mechanism. One side of bevel gear three is connected to bevel gear six via a transmission rod. Bevel gear six is ​​meshed with bevel gear seven. Bevel gear seven is driven and connected to the pushing rod of the pushing mechanism.

[0014] Furthermore, the synthesis tank is an inverted cone shape that is wider at the top and narrower at the bottom. The upper and lower parts of the synthesis tank are movably connected to the mounting frame via planar bearings fixedly mounted on support rod one. The mounting frame is also provided with support rod two, and drive motor two is fixedly mounted on support rod two. The output shaft end of drive motor two is connected to a gear, which meshes with a gear ring set along the outer periphery of the synthesis tank. Drive motor two drives the gear to rotate, causing the synthesis tank to rotate to a certain extent in the horizontal direction of the planar bearing.

[0015] Furthermore, the discharge valve is a disc valve. Attached Figure Description

[0016] Figure 1 This is a schematic diagram of the internal structure of the molecular sieve synthesis and processing device of this utility model.

[0017] Figure 2 This is a schematic diagram of the bevel gear connection structure of this utility model.

[0018] In the diagram above, 1 is drive motor one, 2 is hopper one, 3 is bevel gear connection structure, 31 is bevel gear one, 32 is bevel gear two, 33 is bevel gear three, 34 is bevel gear four, 35 is bevel gear five, 36 is bevel gear six, 37 is bevel gear seven, 4 is plane bearing, 5 is stirring rod, 6 is gear, 7 is support rod two, 8 is drive motor two, 9 is feeder, 10 is synthesis tank body, 11 is spiral blade, 12 is gear ring, 13 is mounting bracket, 14 is support rod one, 15 is discharge push rod, 16 is discharge valve, and 17 is hopper two. Detailed Implementation

[0019] like Figure 1 , 2 The apparatus shown is a synthesis and processing device for a VOCs adsorbent, all-silica Beta molecular sieve. It includes a synthesis tank 10 mounted on a mounting frame 13. A drive motor 1 is mounted on the mounting frame 13 above the synthesis tank 10. A hopper 2 and a hopper 2 17 are respectively provided on both sides of the drive motor 1. The lower part of the hopper 2 and the hopper 2 17 are respectively provided with a feeder 9. The feeder 9 is connected to a material pipe to convey raw materials into the synthesis tank 10. The output shaft of the drive motor 1 extends into the synthesis tank 10 and is connected to a bevel gear connection structure 3. A stirring mechanism and a pushing mechanism are respectively connected to both sides of the bevel gear connection structure 3. The stirring mechanism and the pushing mechanism are arranged opposite each other in the synthesis tank 10 along the inner wall of the synthesis tank 10. A discharge push rod 15 is connected to the end of the pushing mechanism near the discharge port of the synthesis tank 10. A discharge valve 16 is provided on the discharge port of the synthesis tank 10. The discharge valve 16 is a disc valve.

[0020] The stirring mechanism includes a stirring rod that is driven to one side of the bevel gear connection structure 3. The stirring rod is provided with stirring bars 5, which are made of elastic material and are provided with multiple stirring bars 5 at intervals along the surface of the stirring rod.

[0021] The pushing mechanism includes a pushing rod that is driven to the other side of the bevel gear connection structure 3, and the pushing rod is provided with a spiral blade 11.

[0022] The bevel gear connection structure 3 includes a bevel gear 31 that is driven and connected to the output shaft of the drive motor 1. Bevel gear 31 has bevel gear 32 and bevel gear 33 meshing perpendicularly on both sides. One side of bevel gear 32 is connected to bevel gear 34 via a transmission rod. Bevel gear 34 is meshed with bevel gear 35. Bevel gear 35 is driven and connected to the stirring rod of the stirring mechanism. One side of bevel gear 33 is connected to bevel gear 36 via a transmission rod. Bevel gear 36 is meshed with bevel gear 37. Bevel gear 37 is driven and connected to the pushing rod of the pushing mechanism.

[0023] The synthesis tank 10 is an inverted cone shape that is wider at the top and narrower at the bottom. The upper and lower parts of the synthesis tank 10 are movably connected to the mounting frame 13 through a plane bearing 4 fixedly mounted on the support rod 14. The mounting frame 13 is also provided with a support rod 7. A drive motor 8 is fixedly mounted on the support rod 7. A gear 6 is driven to the output shaft end of the drive motor 8. The gear 6 meshes with a gear ring 12 arranged along the outer circumference of the synthesis tank 10. The drive motor 8 drives the gear to rotate, causing the synthesis tank 10 to rotate to a certain extent in the horizontal direction of the plane bearing 4.

[0024] In operation, raw materials enter hopper 12 and hopper 217. Feeders 9 are connected to the bottom of hoppers 12 and hopper 217 respectively, and feeders 9 are connected to material pipes below them, continuously conveying the raw materials into the synthesis tank 10. During synthesis, drive motor 1 operates, driving the bevel gear connection structure 3 inside the synthesis tank 10 to operate the stirring mechanism and the pushing mechanism. The stirring rod 5 on the stirring mechanism continuously stirs the materials under the continuous rotation of the stirring rod. The spiral blades 11 on the pushing mechanism continuously convey the materials in the synthesis tank 10 from the bottom to the top, promoting thorough and uniform mixing. The elastic stirring rod 5 can disperse the materials during the stirring process, promoting uniform mixing. To further improve the uniformity of the mixture inside the synthesis tank 10... The synthesis tank 10 of this device is an inverted cone shape, wider at the top and narrower at the bottom, and is movably mounted on a plane bearing 4. The plane bearing 4 is fixedly mounted on the support rod 14 of the mounting frame 13. A gear ring 12 is provided along the outer circumference of the middle of the synthesis tank 10. When the drive motor 8 is activated, it drives the gear 6 meshing with the gear ring 12 to rotate, causing the synthesis tank 10 to rotate a certain distance in the horizontal direction of the plane bearing 4. This, in conjunction with the pushing mechanism and the stirring mechanism, promotes thorough mixing of materials and avoids dead zones in the synthesis tank 10. The pushing mechanism is connected to a discharge push rod 15 at the bottom outlet of the synthesis tank 10. When the discharge valve 16 is opened, the discharge push rod 15 rotates together with the upper push rod, conveying the mixed materials at the bottom upwards, thereby preventing material accumulation and blockage at the outlet and avoiding arching at the outlet. The zeolite molecular sieve synthesis and processing device of this invention can effectively improve the mixing uniformity of the synthesis raw materials, avoid the phenomenon of stratification, improve the uniformity of the product, and ensure the synthesis effect.

[0025] This utility model is not limited to the above embodiments. Based on the technical solutions disclosed in this utility model, those skilled in the art can make some substitutions and modifications to some of the technical features without creative labor, and these substitutions and modifications are all within the protection scope of this utility model.

Claims

1. A synthesis and processing apparatus for a VOCs adsorbent, all-silica Beta molecular sieve, comprising a synthesis tank mounted on a mounting frame, characterized in that: A drive motor is mounted on the mounting bracket above the synthesis tank. A hopper and a feeder are respectively located on either side of the drive motor. Feeders are located at the lower parts of the hoppers, and these feeders are connected to a material pipe to deliver raw materials into the synthesis tank. The output shaft of the drive motor extends into the synthesis tank and is connected to a bevel gear connection structure. A stirring mechanism and a pushing mechanism are respectively connected to both sides of the bevel gear connection structure. The stirring mechanism and the pushing mechanism are arranged opposite each other along the inner wall of the synthesis tank. A discharge push rod is connected to the end of the pushing mechanism near the outlet of the synthesis tank. A discharge valve is located at the outlet of the synthesis tank.

2. The apparatus for synthesizing and processing VOCs adsorbent all-silica Beta molecular sieves according to claim 1, characterized in that: The stirring mechanism includes a stirring rod that is driven to one side of the bevel gear connection structure, and the stirring rod is provided with a stirring bar.

3. The apparatus for synthesizing and processing VOCs adsorbent all-silica Beta molecular sieves according to claim 2, characterized in that: The stirring rod is made of an elastic material, and multiple stirring rods are spaced apart along the surface of the stirring rod.

4. The apparatus for synthesizing and processing VOCs adsorbent all-silica Beta molecular sieves according to claim 2, characterized in that: The pushing mechanism includes a pushing rod that is driven to the other side of the bevel gear connection structure, and the pushing rod is provided with helical blades.

5. The apparatus for synthesizing and processing VOCs adsorbent all-silica Beta molecular sieves according to claim 4, characterized in that: The bevel gear connection structure includes a first bevel gear that is driven and connected to the output shaft of a drive motor. The first bevel gear has a second bevel gear and a third bevel gear that are perpendicularly meshed on both sides. The second bevel gear is connected to a fourth bevel gear on one side via a transmission rod. The fourth bevel gear is meshed with a fifth bevel gear, which is driven and connected to the stirring rod of the stirring mechanism. The third bevel gear is connected to a sixth bevel gear on one side via a transmission rod. The sixth bevel gear is meshed with a seventh bevel gear, which is driven and connected to the pushing rod of the pushing mechanism.

6. The apparatus for synthesizing and processing VOCs adsorbent all-silica Beta molecular sieves according to claim 1, characterized in that: The synthesis tank is an inverted cone shape, wider at the top and narrower at the bottom. The upper and lower parts of the synthesis tank are movably connected to the mounting frame via planar bearings fixedly mounted on support rod one. The mounting frame is also provided with support rod two, and drive motor two is fixedly mounted on support rod two. The output shaft end of drive motor two is connected to a gear, which meshes with a gear ring set along the outer periphery of the synthesis tank. Drive motor two drives the gear to rotate, causing the synthesis tank to rotate to a certain extent in the horizontal direction of the planar bearing.

7. The apparatus for synthesizing and processing VOCs adsorbent all-silica Beta molecular sieves according to claim 1, characterized in that: The discharge valve is a disc valve.