Amantadine amination process reaction device

Abstract

The utility model discloses an amantadine amination process reaction device, which belongs to the technical field of reaction equipment, and comprises a reaction kettle for amantadine amination reaction, the top end of a base is fixedly connected with a mounting frame, and the inner side of the mounting frame is rotatably connected with two driving shafts connected with the reaction kettle; the side surface of the mounting frame is provided with a fixed end of a stepping motor, the driving end of the stepping motor and the periphery of the driving shaft are both provided with gears, the two gears are in meshed connection, the side surface of the reaction kettle is provided with a heating assembly, and the side surface of the mounting frame is provided with a fixed end of a second hydraulic rod; and the driving end of the second hydraulic rod penetrates through the mounting frame and is fixedly connected with a limiting plate, the side face of the limiting plate is provided with the fixed end of a servo motor, and the driving end of the servo motor is fixedly connected with an L-shaped linkage plate. According to the amantadine amination process reaction device, the reaction kettle can be automatically cleaned, so that the cleaning operation of the device is more time-saving and labor-saving.

Description

Technical Field

[0001] This utility model belongs to the field of reaction equipment technology, and in particular to a reaction device for the amination process of adamantaneamine. Background Technology

[0002] Adamantane is a cyclic tetrahedral hydrocarbon containing 10 carbon atoms and 16 hydrogen atoms. Its basic structure is chair-shaped cyclohexane, and its carbon skeleton structure is equivalent to a cell in a diamond lattice network, hence the name adamantane. Adamantane is a highly symmetrical and very stable compound, and its derivatives can be used as pharmaceuticals. Existing adamantane amination requires the use of a reaction vessel during the reaction process. In order to increase the practicality of the device, a mixing component is installed to accelerate the adamantane amination reaction process and greatly improve the processing efficiency of the device. Although the processing efficiency of the device is increased to a certain extent, the subsequent cleaning of the reaction vessel requires manual assistance, making the cleaning of the device more time-saving and labor-saving.

[0003] A search revealed Chinese patent document (authorization announcement number CN219217490U), which discloses a reaction apparatus for the amination process of adamantaneamine. The technical solution is as follows: an amination reactor jacket is provided on the outer wall of the amination reactor; a feeding port is located at the top of the amination reactor; the upper end of the amination reactor is connected to a distillation buffer tank via a discharge pipeline and a tail gas buffer tank via a tail gas pipeline; the inlet end of the amination reactor jacket is connected to a low-pressure steam tank via a pipeline, and the outlet end of the amination reactor jacket is connected to a steam condensate tank via a pipeline. The beneficial effect is that by opening the low-pressure steam tank, the amination reactor is slowly heated, and the solid brominated adamantane and solid urea are uniformly mixed and added into the amination reactor. The temperature is controlled to initiate the amination reaction, and the steam is stopped and the reactor is allowed to cool naturally after the reaction is complete. While this patent increases the processing efficiency of the apparatus to some extent, the subsequent cleaning of the reactor requires manual assistance, making the cleaning of the apparatus relatively time-saving and labor-saving. Utility Model Content

[0004] The purpose of this invention is to provide a reaction apparatus for the amination process of adamantaneamine to solve the problems mentioned in the background art.

[0005] To achieve the above objectives, this utility model provides the following technical solution: a reaction apparatus for adamantane amination process, comprising a reactor for adamantane amination reaction, an L-shaped base at the bottom of the reactor, an adjustment component and an auxiliary component mounted on the side of the base, a mounting frame fixedly connected to the top of the base, two drive shafts rotatably connected to the reactor on the inner side of the mounting frame, a fixed end of a stepper motor mounted on the side of the mounting frame, gears mounted on the drive end of the stepper motor and the outer periphery of the drive shafts, the two gears meshing with each other, a heating component mounted on the side of the reactor, a fixed end of a second hydraulic rod mounted on the side of the mounting frame, a limit plate fixedly connected to the drive end of the second hydraulic rod through the mounting frame, a fixed end of a servo motor mounted on the side of the limit plate, an L-shaped linkage plate fixedly connected to the drive end of the servo motor, and a cleaning brush adhered to the side of the linkage plate.

[0006] Preferably, the adjustment assembly includes two mounting boxes embedded in the top of the base, an electric push rod mounted on the top of the mounting box, and a guide rod fixedly connected to the inside of the mounting box.

[0007] Preferably, a movable block is slidably connected to the outer periphery of the guide rod, and a movable rod is hinged to the top of the movable block via a hinge. One end of the movable rod is hinged to a support column connected to an electric push rod.

[0008] Preferably, the bottom end of the movable block is hinged to a movable rod, and the end of the movable rod away from the movable block is hinged to a movable plate on which a movable wheel is installed.

[0009] Preferably, the auxiliary component includes a mounting plate fixedly connected to the side of the mounting bracket and a first hydraulic rod mounted on the bottom end of the mounting plate.

[0010] Preferably, the driving end of the first hydraulic rod is fixedly connected to a sealing cover, the top of the sealing cover is equipped with the fixed end of the drive motor, and the driving end of the drive motor is fixedly connected to the stirring rod through the sealing cover.

[0011] Compared with the prior art, the technical effects and advantages of this utility model are as follows:

[0012] This adamantane amination process reactor benefits from the design of servo motors and adjustment components. By activating the first hydraulic rod of the auxiliary component to raise the sealing cover, activating the stepper motor to rotate the reactor to a certain angle, activating the second hydraulic rod to move the limiting plate horizontally, allowing the cleaning brush to embed into the reactor, and activating the servo motor to rotate the cleaning brush on the side of the linkage plate, the reactor is automatically cleaned. Compared with the existing cleaning methods, this device can automatically clean the reactor, making the cleaning operation more time-saving and labor-saving. Furthermore, the design of the adjustment components facilitates the movement of the device and ensures its stability during use.

[0013] The adamantane amination process reactor can automatically clean the reactor, making the cleaning operation more time-saving and labor-saving. Attached Figure Description

[0014] To more clearly illustrate the specific embodiments of this utility model or the technical solutions in the prior art, the drawings used in the description of the specific embodiments or the prior art will be briefly introduced below. Obviously, the drawings described below are some embodiments of this utility model. For those skilled in the art, other drawings can be obtained from these drawings without creative effort.

[0015] Figure 1 This is a schematic diagram of the structure of this utility model;

[0016] Figure 2 This is a partial cross-sectional view of the reactor of this utility model;

[0017] Figure 3 This is a cross-sectional view of the connection of the adjustment component of this utility model.

[0018] Explanation of reference numerals in the attached figures:

[0019] In the diagram: 1. Base; 2. Reactor; 3. Heating assembly; 4. Adjustment assembly; 41. Electric push rod; 42. Mounting box; 43. Support column; 44. Moving rod; 45. Movable block; 46. Guide rod; 47. Movable rod; 48. Moving plate; 5. Auxiliary assembly; 51. Sealing cover; 52. Mounting plate; 53. First hydraulic rod; 54. Drive motor; 55. Stirring rod; 6. Stepper motor; 7. Mounting bracket; 8. Second hydraulic rod; 9. Limiting plate; 10. Servo motor; 11. Linkage plate; 12. Cleaning brush; 13. Drive shaft; 14. Gear. Detailed Implementation

[0020] In the following description, numerous specific details are set forth in order to provide a more thorough understanding of the present invention. However, it will be apparent to those skilled in the art that the present invention can be practiced without one or more of these details. In other instances, certain technical features well-known in the art have not been described in order to avoid confusion with the present invention.

[0021] Unless otherwise defined, the directions mentioned herein, such as up, down, left, right, front, back, inside, and outside, are based on the directions shown in the figures of this utility model, and are explained here together.

[0022] The connection method can be any existing method, such as bonding, welding, or bolting, depending on the actual needs. Techniques, methods, and equipment known to those skilled in the art may not be discussed in detail; however, where appropriate, such techniques, methods, and equipment should be considered part of the specification. The proportions of the components in the accompanying drawings are for reference only and can be adjusted to a certain extent according to the actual use.

[0023] Examples, such as Figures 1 to 3 As shown, the bottom of the reactor 2 is provided with an L-shaped base 1, and an adjustment component 4 and an auxiliary component 5 are installed on the side of the base 1. The top of the base 1 is fixedly connected to a mounting bracket 7, and two drive shafts 13 connected to the reactor 2 are rotatably connected to the inner side of the mounting bracket 7. The top of the sealing cover 51 is connected to an exhaust pipe that communicates with the outside. The fixed end of the stepper motor 6 is installed on the side of the mounting bracket 7, and gears 14 are installed on the drive end of the stepper motor 6 and the outer periphery of the drive shafts 13. The two gears 14 are meshed together. The side of the reactor 2... A heating component 3 is installed on the surface of the container. The fixed end of the second hydraulic rod 8 is installed on the side of the mounting frame 7. The design of the second hydraulic rod 8 is to drive the cleaning brush 12 to be embedded in the reactor 2. The driving end of the second hydraulic rod 8 passes through the mounting frame 7 and is fixedly connected to the limiting plate 9. The fixed end of the servo motor 10 is installed on the side of the limiting plate 9. The design of the servo motor 10 is to drive the cleaning brush 12 to rotate, thereby realizing the cleaning operation of the reactor 2. The driving end of the servo motor 10 is fixedly connected to the L-shaped linkage plate 11, and the cleaning brush 12 is glued to the side of the linkage plate 11.

[0024] The adjustment assembly 4 includes two mounting boxes 42 embedded in the top of the base 1, an electric push rod 41 mounted on the top of the mounting box 42, and a guide rod 46 fixedly connected to the inside of the mounting box 42. A movable block 45 is slidably connected to the outer periphery of the guide rod 46. By activating the electric push rod 41, the moving wheel can be driven to adjust its position, making the device easy to move and ensuring the stability of the device. The electric push rod 41 drives the support column 43 to rise, so that the linkage plate 48 drives the moving wheel to contact the ground. The bottom of the mounting box 42 is an open design. The top of the movable block 45 is hinged to a moving rod 44. One end of the moving rod 44 is hinged to the support column 43 connected to the electric push rod 41. The bottom of the movable block 45 is hinged to a moving rod 47. The end of the moving rod 47 away from the movable block 45 is hinged to the moving plate 48 on which the moving wheel is mounted.

[0025] The auxiliary component 5 includes a mounting plate 52 fixedly connected to the side of the mounting frame 7 and a first hydraulic rod 53 installed at the bottom of the mounting plate 52. A sealing gasket is glued to the bottom of the sealing cover 51. The design of the first hydraulic rod 53 facilitates the feeding and cleaning of the reactor 2. The driving end of the first hydraulic rod 53 is fixedly connected to the sealing cover 51. The top of the sealing cover 51 is equipped with the fixed end of the drive motor 54, and the driving end of the drive motor 54 passes through the sealing cover 51 and is fixedly connected to the stirring rod 55.

[0026] Heating component 3, electric push rod 41, first hydraulic rod 53, drive motor 54, stepper motor 6, second hydraulic rod 8, and servo motor 10 are all conventional instruments. Their working principles, dimensions, and models are irrelevant to the function of this application, so they will not be described in detail. They are all controlled by remote control switches. The control method of this utility model is through a controller. The control circuit of the controller can be implemented by simple programming by those skilled in the art. The power supply is also common knowledge in the art. Furthermore, this utility model is mainly used to protect mechanical devices, so the control method and circuit connection will not be explained in detail. The scale of the attached drawings is for reference only and can be adjusted to a certain extent according to the actual use.

[0027] Working principle

[0028] In operation, the adamantane amination process reactor is used to feed material into the reactor 2. The drive motor 54 is started to rotate the stirring rod 55, thereby carrying out the processing reaction. After processing, the first hydraulic rod 53 is started to raise the sealing cover 51. The stepper motor 6 is started to rotate the drive shaft 13, causing the reactor 2 to rotate to a certain angle for material discharge. After material discharge, the stepper motor 6 is started to rotate the reactor 2 to a certain angle. The second hydraulic rod 8 is started to move the limiting plate 9 horizontally, so that the cleaning brush 12 is embedded in the reactor 2. The servo motor 10 is started to rotate the cleaning brush 12 on the side of the linkage plate 11. During the rotation, cleaning water can be added as needed to achieve the effect of automatic cleaning.

[0029] It should be noted that, in this document, relational terms such as "one" and "two" are used merely to distinguish one entity or operation from another, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Furthermore, the terms "comprising," "including," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to such a process, method, article, or apparatus. Without further limitations, the phrase "comprising an element defined as..." does not exclude the presence of other identical elements in the process, method, article, or apparatus that includes said element.

[0030] Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the present invention, the scope of which is defined by the appended claims and their equivalents.

Claims

1. A reaction apparatus for adamantane amination process, comprising a reaction vessel (2) for adamantane amination reaction, wherein the bottom end of the reaction vessel (2) is provided with an L-shaped base (1), and an adjustment component (4) is installed on the side of the base (1), and an auxiliary component (5) is installed on the side of the base (1), characterized in that: The top of the base (1) is fixedly connected to the mounting bracket (7), and the inner side of the mounting bracket (7) is rotatably connected to two drive shafts (13) connected to the reactor (2). The side of the mounting bracket (7) is equipped with the fixed end of the stepper motor (6), and the drive end of the stepper motor (6) and the outer periphery of the drive shaft (13) are both equipped with gears (14). The two gears (14) are meshed together. The side of the reactor (2) is equipped with a heating assembly (3). The side of the mounting bracket (7) is equipped with the fixed end of the second hydraulic rod (8), and the drive end of the second hydraulic rod (8) passes through the mounting bracket (7) and is fixedly connected to the limiting plate (9). The side of the limiting plate (9) is equipped with the fixed end of the servo motor (10), and the drive end of the servo motor (10) is fixedly connected to the L-shaped linkage plate (11). The side of the linkage plate (11) is bonded with a cleaning brush (12).

2. The adamantaneamine amination process reaction apparatus according to claim 1, characterized in that: The adjustment assembly (4) includes two mounting boxes (42) embedded in the top of the base (1), an electric push rod (41) mounted on the top of the mounting box (42), and a guide rod (46) fixedly connected to the inside of the mounting box (42).

3. The adamantaneamine amination process reaction apparatus according to claim 2, characterized in that: The guide rod (46) is slidably connected to a movable block (45) on its outer periphery, and the top of the movable block (45) is hinged to a moving rod (44) via a hinge. One end of the moving rod (44) is hinged to a support column (43) connected to an electric push rod (41).

4. The adamantane amination process reaction apparatus according to claim 3, characterized in that: The bottom end of the movable block (45) is hinged to a movable rod (47), and the end of the movable rod (47) away from the movable block (45) is hinged to a movable plate (48) on which a movable wheel is installed.

5. The adamantaneamine amination process reaction apparatus according to claim 1, characterized in that: The auxiliary component (5) includes a mounting plate (52) fixedly connected to the side of the mounting bracket (7) and a first hydraulic rod (53) mounted on the bottom of the mounting plate (52).

6. The adamantaneamine amination process reaction apparatus according to claim 5, characterized in that: The first hydraulic rod (53) has a sealing cover (51) fixedly connected to its driving end. The top of the sealing cover (51) has a fixed end of a drive motor (54) installed on it, and the driving end of the drive motor (54) is fixedly connected to a stirring rod (55) through the sealing cover (51).

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