Reaction kettle for preparing high-purity silicon carbide

Abstract

The utility model discloses a reaction kettle for preparing high purity silicon carbide, which comprises a reaction kettle body, the upper surface of the reaction kettle body is fixedly connected with a motor, the output end of the motor is fixedly connected with a rotating rod, the side inner wall of the rotating rod is fixedly connected with a clamping block, the side surface of the clamping block is fixedly connected with a connecting cylinder, and the connecting cylinder is fixedly connected with a rotating shaft. A butt joint rod is slidably connected to the side inner wall of the connecting cylinder, a rotating plate is fixedly connected to one end of the butt joint rod, a feeding port is fixedly connected to the upper surface of the reaction kettle body, an electric telescopic rod is fixedly connected to the side surface of the feeding port, and a sliding block is fixedly connected to the output end of the electric telescopic rod. By means of the components, the rotating plate can be used for dredging the feeding port to prevent silicon carbide from blocking the feeding port, connection between the rotating plate and the motor is removed after blanking is completed, and the rotating plate is used for blocking the feeding port to prevent harmful gas in the reaction kettle from flowing out, polluting the environment, causing energy loss and reducing the purification effect.

Description

Technical Field

[0001] This utility model relates to the field of reaction vessel technology, and in particular to a reaction vessel for preparing high-purity silicon carbide. Background Technology

[0002] Existing reactors used for preparing high-purity silicon carbide employ cleaning components to clean the inner walls of the reactor, preventing the raw liquid and purified material from adhering to the wall surface and becoming difficult to clean, thus reducing the purification quality. A feed paddle is used to unclog the inlet, ensuring smooth silicon carbide flow. However, the feed paddle continues to rotate during the purification process, causing harmful gases generated during purification to be released from the inlet and generating significant heat. For example, a silicon carbide purification device disclosed in Chinese Patent Application No. CN202321553614.3, while using a discharge assembly to guide the feed pipe and prevent silicon carbide from sticking and condensing after entering the separation liquid, and also preventing feed blockage and making the silicon carbide flow more uniform and smooth, improving the purification effect, cannot completely seal the inlet. This results in harmful gases generated during purification being discharged from the feed pipe, polluting the environment. Simultaneously, the gases carry a large amount of heat and dissipate from the reactor, causing energy loss, reducing energy utilization efficiency, and lowering the purification quality, thus limiting its application. Utility Model Content

[0003] The purpose of this invention is to at least solve one of the technical problems existing in the prior art, and to provide a reaction vessel for preparing high-purity silicon carbide. A motor can simultaneously drive a rotating plate and a stirring paddle to rotate, causing the rotating plate to rotate within the feed inlet. This prevents silicon carbide from accumulating in the feed inlet during the feeding process, making the feeding smoother. After feeding is complete, the rotating plate can be disconnected from the motor, and the feed inlet can be sealed with the rotating plate to prevent harmful gases generated during purification from escaping from the feed inlet and polluting the environment, as well as heat loss, which would reduce purification efficiency. Furthermore, the reaction vessel can be placed on a support base during use, and pressing the slider causes a limiting block to extend from the support base to limit and fix the reaction vessel, improving the stability of the reaction vessel during use.

[0004] This utility model also provides a reaction vessel for preparing high-purity silicon carbide, comprising: a reaction vessel body, a discharge port fixedly connected to the lower surface of the reaction vessel body, a motor fixedly connected to the upper surface of the reaction vessel body, a rotating rod fixedly connected to the output end of the motor, a locking block fixedly connected to the inner side wall of the rotating rod, a connecting cylinder fixedly connected to the side surface of the locking block, a docking rod slidably connected to the inner side wall of the connecting cylinder, a rotating plate fixedly connected to one end of the docking rod, a feed port fixedly connected to the upper surface of the reaction vessel body, an electric telescopic rod fixedly connected to the side surface of the feed port, and a sliding block fixedly connected to the output end of the electric telescopic rod;

[0005] A driving bevel gear is fixedly connected to the side surface of the rotating rod. A driven bevel gear meshes with the side surface of the driving bevel gear. An agitator is fixedly connected to the surface of the driven bevel gear. A cleaning plate is fixedly connected to the side surface of the agitator. A scraper is fixedly connected to the side surface of the cleaning plate. These components allow the rotating plate to be disconnected from the motor after material discharge, and the rotating plate can block the inlet, preventing harmful gases from escaping from the reactor, thus avoiding environmental pollution and energy loss.

[0006] According to the present invention, a reaction vessel for preparing high-purity silicon carbide is provided, wherein a support base is fixedly connected to the lower surface of the reaction vessel body, and a limiting block is fixedly connected to the side surface of the reaction vessel body. The support base and the limiting block ensure the stability of the reaction vessel during use.

[0007] According to the present invention, a reaction vessel for preparing high-purity silicon carbide is provided, wherein a slider is slidably connected to the inner side wall of the support base, and the lower surface of the reaction vessel body is slidably connected to the slider. When the reaction vessel body is placed on the support base, the slider is pressed down, causing it to slide into the support base.

[0008] According to the present invention, a reaction vessel for preparing high-purity silicon carbide is provided, wherein a sliding rod is fixedly connected to the side surface of the slider, and a sliding groove plate is slidably connected to the side surface of the sliding rod. The slider moves the sliding groove plate via the sliding rod.

[0009] According to the present invention, a reaction vessel for preparing high-purity silicon carbide is provided, wherein the upper surface of the sliding plate is fixedly connected to a limiting block, and the side surface of the limiting block is slidably connected to a support base. The sliding plate drives the limiting block to extend from the support base to fix the reaction vessel body.

[0010] According to the present invention, a reaction vessel for preparing high-purity silicon carbide is provided, wherein a spring is fixedly connected to the side surface of the slider, and the end of the spring away from the slider is fixedly connected to a support base. After the reaction vessel is removed, the spring pushes the slider back to its original position.

[0011] According to the present invention, a reaction vessel for preparing high-purity silicon carbide is provided, wherein the side surface of the connecting cylinder is rotatably connected to the sliding block, the side surface of the clamping block is slidably connected to the rotating rod during operation, and the side surface of the rotating plate is rotatably connected to the feed inlet. This allows the rotating plate to rotate inside the feed inlet, preventing silicon carbide from accumulating in the feed inlet.

[0012] According to the present invention, a reaction vessel for preparing high-purity silicon carbide is provided, wherein the side surface of the cleaning plate is rotatably connected to the reaction vessel body, and the upper bottom wall of the reaction vessel body is rotatably connected to the scraper. The cleaning plate and scraper can be used to clean the interior of the reaction vessel body, thereby improving the purification effect.

[0013] Beneficial effects:

[0014] Compared with existing technologies, a motor can simultaneously drive the rotating plate and the stirring paddle to rotate, causing the rotating plate to rotate in the feed inlet. This prevents silicon carbide from accumulating in the feed inlet during the feeding process, making the feeding smoother. After feeding is completed, the rotating plate can be disconnected from the motor, and the feed inlet can be sealed with the rotating plate to prevent harmful gases generated during the purification process from being discharged from the feed inlet and polluting the environment, as well as carrying away heat and reducing purification efficiency. At the same time, the reactor can be placed on the support base during use, and the sliding block can be pressed to extend the limiting block from the support base to limit and fix the reactor, improving the stability of the reactor during use. Attached Figure Description

[0015] The present invention will be further described below with reference to the accompanying drawings and embodiments;

[0016] Figure 1 This is an overall structural diagram of the reaction vessel used in the preparation of high-purity silicon carbide according to this utility model;

[0017] Figure 2 This is a cross-sectional view of the reaction vessel used in the preparation of high-purity silicon carbide according to this utility model;

[0018] Figure 3 This invention relates to a reaction vessel for preparing high-purity silicon carbide. Figure 2 Partial structural diagram at point A in the middle;

[0019] Figure 4 This is a structural diagram of the rotating plate of the reaction vessel used in the preparation of high-purity silicon carbide according to this utility model;

[0020] Figure 5 This is a structural diagram of the stirring paddle of the reaction vessel used in the preparation of high-purity silicon carbide according to this utility model;

[0021] Figure 6 This is a structural diagram of the limiting block of the reaction vessel used in the preparation of high-purity silicon carbide according to this utility model.

[0022] Legend:

[0023] 1. Reactor body; 2. Support base; 3. Motor; 4. Driving bevel gear; 5. Rotating rod; 6. Driven bevel gear; 7. Inlet; 8. Limiting block; 9. Stirring paddle; 10. Cleaning plate; 11. Scraper; 12. Outlet; 13. Rotating plate; 14. Sliding block; 15. Electric telescopic rod; 16. Connecting cylinder; 17. Connecting rod; 18. Locking block; 19. Sliding groove plate; 20. Sliding rod; 21. Spring; 22. Sliding block. Detailed Implementation

[0024] This section will describe in detail the specific embodiments of the present utility model. The preferred embodiments of the present utility model are shown in the accompanying drawings. The purpose of the drawings is to supplement the textual description with graphics, so that people can intuitively and vividly understand each technical feature and the overall technical solution of the present utility model, but they should not be construed as limiting the scope of protection of the present utility model.

[0025] Reference Figure 1-6 This utility model discloses a reactor for preparing high-purity silicon carbide, comprising: a reactor body 1, with a discharge port 12 fixedly connected to the lower surface of the reactor body 1 to discharge purified silicon carbide; a motor 3 fixedly connected to the upper surface of the reactor body 1 to provide power for the rotation of a rotating rod 5; the output end of the motor 3 is fixedly connected to the rotating rod 5, driving the active bevel gear 4 and the connected locking block 18 to rotate; the locking block 18 is fixedly connected to the inner side wall of the rotating rod 5, and the side surface of the locking block 18 is slidably connected to the rotating rod 5 during operation, allowing it to engage with the rotating rod 5; and it drives the rotating plate 13 to rotate through a connecting cylinder 16 and a docking rod 17; the side surface of the locking block 18 is fixedly connected to the connecting cylinder 16, and the side surface of the connecting cylinder 16 is rotatably connected to a sliding block 14, allowing it to slide along the docking rod 17, so that the locking block 18 engages with the rotating rod 5. The connecting rod 5 drives the docking rod 17 to rotate. The docking rod 17 is slidably connected to the inner side wall of the connecting cylinder 16. The connecting cylinder 16 drives the rotating plate 13 to rotate. One end of the docking rod 17 is fixedly connected to the rotating plate 13. The side surface of the rotating plate 13 is rotatably connected to the feed port 7 to clear the feed port 7 and prevent silicon carbide from blocking the feed port 7. After the material is discharged, the feed port 7 is closed to prevent the emission of harmful gases inside the reactor body 1 during purification and to reduce heat loss. The upper surface of the reactor body 1 is fixedly connected to the feed port 7, which can add silicon carbide into the reactor body 1. The side surface of the feed port 7 is fixedly connected to the electric telescopic rod 15, which drives the sliding block 14 to move. The output end of the electric telescopic rod 15 is fixedly connected to the sliding block 14, which drives the locking block 18 to lock into the rotating rod 5.

[0026] A drive bevel gear 4 is fixedly connected to the side surface of the rotating rod 5, which drives the driven bevel gear 6 to rotate. The driven bevel gear 6 meshes with the side surface of the drive bevel gear 4, which drives the stirring paddle 9 to rotate. The stirring paddle 9 is fixedly connected to the surface of the driven bevel gear 6, which mixes and stirs the solution and silicon carbide inside the reactor body 1 to improve the purification effect. A cleaning plate 10 is fixedly connected to the side surface of the stirring paddle 9. The side surface of the cleaning plate 10 is rotatably connected to the reactor body 1 to clean the inner wall of the reactor body 1, preventing the original solution and purified material from adsorbing on the wall surface and improving the purification effect. A scraper 11 is fixedly connected to the side surface of the cleaning plate 10. The upper bottom wall of the reactor body 1 is rotatably connected to the scraper 11 to scrape off the purified silicon carbide on the lower bottom wall of the reactor body 1, making it easier to discharge the silicon carbide at the end.

[0027] A support base 2 is fixedly connected to the lower surface of the reactor body 1, supporting the reactor body 1 and, together with a limiting block 8, fixing the reactor body 1 to ensure stability during use. A limiting block 8 is fixedly connected to the side surface of the reactor body 1 to limit and fix the reactor body 1, enhancing stability during use. A slider 22 is slidably connected to the inner side wall of the support base 2. When the reactor body 1 presses the slider 22, the slider 22 will cause the slider rod 20 to slide into the support base 2. The lower surface of the reactor body 1 is slidably connected to the slider 22, and a sliding rod 20 is fixedly connected to the side surface of the slider 22. The rod 20 slides along the groove on the surface of the slide plate 19 and drives the slide plate 19 to move. The slide plate 19 is slidably connected to the side surface of the rod 20. The slide plate 19 is provided with a groove on its surface. Under the action of the rod 20, it slides and can drive the limiting block 8 to extend out of the support seat 2. The upper surface of the slide plate 19 is fixedly connected to the limiting block 8. The side surface of the limiting block 8 is slidably connected to the support seat 2. The side surface of the slider 22 is fixedly connected to the spring 21. After the reactor body 1 is removed from the support seat 2, the slider 22 is driven to reset, so that the limiting block 8 is retracted into the support seat 2. The end of the spring 21 away from the slider 22 is fixedly connected to the support seat 2.

[0028] Working principle: Before use, place the reactor body 1 on the support base 2. The reactor body 1 will press the slider 22 into the support base 2, and at the same time drive the slider 20 to slide along the groove on the slide plate 19. This causes the slide plate 19 to drive the limiting block 8 to extend from the support base 2 and limit and fix the reactor body 1. After the reactor body 1 is removed, the spring 21 will drive the slider 22 to reset and retract the limiting block 8 into the support base 1. Then, start the motor 3, which will drive the rotating rod 5 to rotate. The rotating rod 5 drives the rotating plate 13 to rotate in the feed port 7 through the locking block 18, connecting cylinder 16 and docking rod 17. This prevents the silicon carbide added to the reactor body 1 through the feed port 7 from blocking the feed port 7. After stopping the feeding, use... The electric telescopic rod 15 drives the sliding block 14 to pull the connecting cylinder 16, causing the locking block 18 to slide out of the rotating rod 5, releasing the connection between the locking block 18 and the rotating rod 5, stopping the rotating plate 13 from rotating, and sealing the feed port 7 to prevent the gas generated during the purification process from being discharged from the feed port 7, effectively reducing heat emission. At the same time, the active bevel gear 4, driven by the rotating rod 5, drives the stirring paddle 9 to rotate through the driven bevel gear 6 to stir the solution inside the reactor body 1, and drives the cleaning plate 10 and scraper 11 to clean the inner wall and bottom wall of the reactor body 1 respectively, scraping off the original liquid and purified material adsorbed on the inner wall and bottom wall to ensure the purification effect of silicon carbide. Finally, the material is discharged from the discharge port 12, completing the purification.

[0029] The embodiments of the present utility model have been described in detail above with reference to the accompanying drawings. However, the present utility model is not limited to the above embodiments. Within the scope of knowledge possessed by those skilled in the art, various changes can be made without departing from the spirit of the present utility model.

Claims

1. A reaction vessel for preparing high-purity silicon carbide, characterized in that, include: The reactor body (1) has a discharge port (12) fixedly connected to its lower surface, a motor (3) fixedly connected to its upper surface, a rotating rod (5) fixedly connected to the output end of the motor (3), a locking block (18) fixedly connected to the inner side wall of the rotating rod (5), a connecting cylinder (16) fixedly connected to the side surface of the locking block (18), a docking rod (17) slidably connected to the inner side wall of the connecting cylinder (16), a rotating plate (13) fixedly connected to one end of the docking rod (17), a feed inlet (7) fixedly connected to the upper surface of the reactor body (1), an electric telescopic rod (15) fixedly connected to the side surface of the feed inlet (7), and a sliding block (14) fixedly connected to the output end of the electric telescopic rod (15). The rotating rod (5) is fixedly connected to a driving bevel gear (4), the driving bevel gear (4) is meshed with a driven bevel gear (6) on the side surface, the driven bevel gear (6) is fixedly connected to a stirring paddle (9), the stirring paddle (9) is fixedly connected to a cleaning plate (10) on the side surface, and the cleaning plate (10) is fixedly connected to a scraper (11) on the side surface.

2. The reaction vessel for preparing high-purity silicon carbide according to claim 1, characterized in that, A support base (2) is fixedly connected to the lower surface of the reactor body (1), and a limit block (8) is fixedly connected to the side surface of the reactor body (1).

3. The reaction vessel for preparing high-purity silicon carbide according to claim 2, characterized in that, The inner side wall of the support base (2) is slidably connected to a slider (22), and the lower surface of the reactor body (1) is slidably connected to the slider (22).

4. The reaction vessel for preparing high-purity silicon carbide according to claim 3, characterized in that, The slider (22) is fixedly connected to a slide rod (20) on its side surface, and the slide rod (20) is slidably connected to a slide groove plate (19) on its side surface.

5. A reaction vessel for preparing high-purity silicon carbide according to claim 4, characterized in that, The upper surface of the slide plate (19) is fixedly connected to the limiting block (8), and the side surface of the limiting block (8) is slidably connected to the support base (2).

6. The reaction vessel for preparing high-purity silicon carbide according to claim 3, characterized in that, A spring (21) is fixedly connected to the side surface of the slider (22), and the end of the spring (21) away from the slider (22) is fixedly connected to the support base (2).

7. The reaction vessel for preparing high-purity silicon carbide according to claim 1, characterized in that, The side surface of the connecting cylinder (16) is rotatably connected to the sliding block (14), the side surface of the locking block (18) is slidably connected to the rotating rod (5) during operation, and the side surface of the rotating plate (13) is rotatably connected to the feed port (7).

8. A reaction vessel for preparing high-purity silicon carbide according to claim 1, characterized in that, The side surface of the cleaning plate (10) is rotatably connected to the reactor body (1), and the upper bottom wall of the reactor body (1) is rotatably connected to the scraper (11).

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