Crystallization device for producing isophthalic acid-5-sodium sulfonate

Abstract

The utility model discloses a crystallization device for producing isophthalic acid-5-sodium sulfonate, and mainly relates to a sodium sulfonate crystallization device. Comprising a bottom plate, an auxiliary structure and two adjusting structures, the upper surface of the bottom plate is fixedly connected with a vertical rod, one side of the vertical rod is provided with a tank body, the tank body is connected with the vertical rod through the auxiliary structure, the arc surface of the vertical rod is provided with the auxiliary structure, the auxiliary structure comprises a rotating ring, and the rotating ring is rotationally connected with the vertical rod; the arc surface of the rotating ring is fixedly connected with a connecting frame, the end, away from the rotating ring, of the connecting frame is fixedly connected with the tank body, a servo motor is installed at the upper end of the vertical rod, the output end of the servo motor is fixedly connected with a rotating disc, and the arc surface of the rotating disc is fixedly connected with a plurality of fixing plates. The heating and cooling device has the advantages that heating and cooling of sodium sulfonate can be conveniently completed in the same procedure, and a sodium sulfonate solution does not need to be moved to a fixed position for cooling.

Description

Technical Field

[0001] This utility model relates to the technical field of sodium sulfonate crystallization apparatus, and more particularly to a crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate. Background Technology

[0002] Sodium sulfonate is a common surfactant widely used in detergents, emulsifiers, and wetting agents. Crystallization is a crucial step in its production. Crystallization equipment is used to separate and purify sodium sulfonate from solution to ensure the quality and purity of the final product.

[0003] Existing technologies, such as the utility model patent with publication number CN220257210U, disclose a recrystallization device. This patent employs a crystallization kettle, a recrystallization unit, and a tilting unit. A filter barrel is provided inside the crystallization kettle, with uniformly distributed through holes on its bottom surface. The recrystallization unit includes a vertical arm, a horizontal arm, a ring body, a rotating shaft, a stirring fan blade assembly, a motor mounting frame, and a stirring motor. The upper left and right sides of the filter barrel are fixedly connected to the bottom ends of the vertical arm, and the upper outer ends of the vertical arm are fixedly connected to both ends of the horizontal arm. A ring body is provided in the middle of the horizontal arm, and a rotating shaft is inserted inside the ring body. The bottom end of the rotating shaft is fixedly connected to the stirring fan blade assembly. Utilizing the dissolving properties, a saturated sodium benzenesulfinate solution is injected into the crystallization kettle, and the solution is heated and distilled, causing the sodium benzenesulfinate to recrystallize in the solution. Then, the sodium benzenesulfinate is obtained by lifting and tilting through the filter barrel, resulting in a significant improvement in efficiency.

[0004] The inventors discovered through daily use that crystallization in existing technologies is a process closely related to temperature and concentration, typically requiring precise temperature control. In traditional crystallization apparatus, simultaneous heating and cooling within a single process is impossible, necessitating staged processes. This increases process complexity and makes precise temperature gradient control difficult, impacting the crystallization efficiency and quality of sodium sulfonate. Sodium sulfonate crystallization usually requires lengthy heating and cooling processes. Traditional apparatus requires multiple temperature change stages to complete crystallization, which not only increases operation time but also reduces production efficiency.

[0005] This application provides another technical solution to this technical problem, aiming to provide those skilled in the art with multiple options for solving the problem. Utility Model Content

[0006] The purpose of this invention is to address the shortcomings of existing technologies by proposing a crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate.

[0007] To achieve the above objectives, this utility model adopts the following technical solution: It includes a base plate, an auxiliary structure, and two adjustment structures. A vertical rod is fixedly connected to the upper surface of the base plate. A tank is provided on one side of the vertical rod. The tank is connected to the vertical rod via the auxiliary structure. The auxiliary structure includes a rotating ring, which is rotatably connected to the vertical rod. A connecting frame is fixedly connected to the rotating ring's arc surface. The end of the connecting frame away from the rotating ring is fixedly connected to the tank. A servo motor is installed at the upper end of the vertical rod, and the output end of the servo motor is fixedly connected to... The device includes a turntable with several fixed rods fixedly connected to its arc surface. These fixed rods are fixedly connected to a rotating ring. Cooling and heating seats are respectively provided on the upper sides of the base plate. Both the heating and cooling seats are connected to the base plate via an adjustment structure. Several heating rods are installed inside the heating seat, and several connecting rods are fixedly connected inside the cooling seat. The connecting rods are grouped into sets of four, and a fixed ring is fixedly connected to one end of each of the four connecting rods that are close to each other. A drive shaft is installed inside the fixed ring, and several fan blades are installed on the arc surface of the drive shaft.

[0008] The aforementioned components achieve the following effect: When crystallization of sodium sulfonate is required, the material is placed into the tank, and then the servo motor is started. The servo motor drives the turntable to rotate, the turntable moves the fixed rod, the fixed rod moves the rotating ring, the rotating ring moves the connecting frame, and the connecting frame moves the tank. The tank then moves to the heating base for heating and melting. After the raw material melts, the process continues. The servo motor is then started, and the tank is moved to the cooling base for cooling and crystallization.

[0009] Preferably, a plurality of the fan blades are evenly distributed on the drive shaft, and the fan blades are plastic blades.

[0010] The effect achieved by the above components is that the plastic material is relatively inexpensive, which can greatly reduce the manufacturing cost of the fan blades.

[0011] Preferably, the cross-section of the fixing rod is "L" shaped, and the fixing rod is a stainless steel rod.

[0012] The effect achieved by the above components is that the stainless steel material can increase the service life of the fixing rod and prevent the fixing rod from rusting during use.

[0013] Preferably, the connecting frame is a titanium alloy frame, and the cross-section of the connecting frame is triangular.

[0014] Preferably, the base plate has adjustment structures on both sides, each adjustment structure including a connecting plate, the connecting plate being fixedly connected to the base plate, and a sleeve plate being fixedly connected to the upper surface of both the base plate and the connecting plate. A sliding plate is slidably connected to the inner wall of the sleeve plate, and two sets of sliding plates are fixedly connected to the heating seat and the cooling seat respectively. A plurality of insertion holes are opened on the inner wall of the sliding plate, and an insertion rod is slidably connected to the inner wall of the sliding plate. The insertion rod is slidably connected to the insertion hole.

[0015] The effect achieved by the above components is as follows: when it is necessary to adjust the height of the heating base and the cooling base, pull the plug rod to move it, separate the plug rod from the socket, and then pull the slide plate to move it. The slide plate moves the heating base and the cooling base. The slide plate slides on the inner wall of the sleeve plate. After moving to the appropriate position, pull the plug rod to move it, align the plug rod with the sleeve plate and the appropriate socket, and then insert the plug rod to fix it.

[0016] Preferably, limit rods are fixedly connected to both sides of the slide plate, and the limit rods are slidably connected to the sleeve plate.

[0017] The effect achieved by the above components is that the limiting rod can limit the skateboard, prevent the skateboard from deviating when sliding, and improve the stability of the skateboard.

[0018] Preferably, a spring is fitted onto the arc surface of the insertion rod, and the two ends of the spring are fixedly connected to the insertion rod and the sleeve plate, respectively.

[0019] The effect achieved by the above components is as follows: when it is necessary to insert a plug for fixation, the plug is pulled to move it, the plug causes the spring to stretch, then the plug is aligned with the appropriate plug hole, and then the plug is inserted for fixation.

[0020] In summary, the beneficial effects of this utility model are as follows:

[0021] In this invention, by swapping the auxiliary structure, crystallization in the prior art is a process closely related to temperature and concentration, typically requiring precise temperature control. In traditional crystallization apparatus, simultaneous heating and cooling within a single process is impossible, necessitating staged processes. This increases process complexity and makes precise temperature gradient control difficult, thus affecting the crystallization efficiency and quality of sodium sulfonate. Sodium sulfonate crystallization usually requires a lengthy heating and cooling process. Traditional apparatus requires multiple temperature change stages to complete crystallization, increasing operation time and reducing production efficiency. This new apparatus allows for convenient heating and cooling of sodium sulfonate within a single process, eliminating the need to move the sodium sulfonate solution to a fixed location for cooling.

[0022] In this invention, the height of the cooling seat and the heating seat can be quickly and easily adjusted by adjusting the adjustment structure, which can meet the needs of various tank models. Attached Figure Description

[0023] Appendix Figure 1 This is a schematic diagram of the crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate provided by this utility model.

[0024] Appendix Figure 2 for Figure 1 The diagram shows the auxiliary structure.

[0025] Appendix Figure 3 for Figure 2 The diagram shows a partial structural representation.

[0026] Appendix Figure 4 for Figure 1 The diagram shows the adjustment structure.

[0027] The following are the labels shown in the attached diagram: 1. Base plate; 2. Upright pole; 3. Auxiliary structure; 301. Rotary ring; 302. Connecting frame; 303. Servo motor; 304. Turntable; 305. Fixing rod; 306. Heating seat; 307. Heating rod; 308. Cooling seat; 309. Drive shaft; 310. Connecting rod; 311. Fixing ring; 312. Fan blade; 4. Adjustment structure; 41. Connecting plate; 42. Sleeve plate; 43. Insert rod; 44. Spring; 45. Limiting rod; 46. Insertion hole; 47. Slide plate; 5. Tank body. Detailed Implementation

[0028] The present invention will be further illustrated below with reference to specific embodiments. It should be understood that these embodiments are for illustrative purposes only and are not intended to limit the scope of the present invention. Furthermore, it should be understood that after reading the teachings of this invention, those skilled in the art can make various alterations or modifications to the present invention, and these equivalent forms also fall within the scope defined by the appended claims.

[0029] Reference Figure 1 As shown, this utility model provides a technical solution: a crystallization device for the production of sodium isophthalic acid-5-sulfonate, including a base plate 1, an auxiliary structure 3 and two adjustment structures 4. A vertical rod 2 is fixedly connected to the upper surface of the base plate 1. A tank 5 is provided on one side of the vertical rod 2. The tank 5 is connected to the vertical rod 2 by means of the auxiliary structure 3. The arc surface of the vertical rod 2 is provided with the auxiliary structure 3. Adjustment structures 4 are provided on both sides of the base plate 1.

[0030] The specific settings and functions of its auxiliary structure 3 and adjustment structure 4 will be discussed below.

[0031] Reference Figure 2 , Figure 3As shown in this embodiment: the auxiliary structure 3 includes a rotating ring 301, which is rotatably connected to the upright 2. A connecting frame 302 is fixedly connected to the arc surface of the rotating ring 301. The end of the connecting frame 302 away from the rotating ring 301 is fixedly connected to the tank body 5. A servo motor 303 is installed at the upper end of the upright 2. A turntable 304 is fixedly connected to the output end of the servo motor 303. Several fixing rods 305 are fixedly connected to the arc surface of the turntable 304. The fixing rods 305 are fixedly connected to the rotating ring 301. The upper sides of the base plate 1 are respectively provided with... There are cooling base 308 and heating base 306. Both heating base 306 and cooling base 308 are connected to base plate 1 by means of adjustment structure 4. Several heating rods 307 are installed inside the heating base 306. Several connecting rods 310 are fixedly connected inside the cooling base 308. The several connecting rods 310 are divided into groups of four. A fixing ring 311 is fixedly connected to one end of the four connecting rods 310 that are close to each other. A drive shaft 309 is installed inside the fixing ring 311. Several fan blades 312 are installed on the arc surface of the drive shaft 309. When sodium sulfonate needs to be crystallized, the material is placed in tank 5, and then the servo motor 303 is started. The servo motor 303 drives the turntable 304 to rotate, the turntable 304 drives the fixed rod 305 to move, the fixed rod 305 drives the rotating ring 301 to rotate, the rotating ring 301 drives the connecting frame 302 to move, and the connecting frame 302 drives the tank 5 to rotate. Then the tank 5 moves to the heating seat 306 for heating and melting. After the raw material melts, the process continues. The servo motor 303 is started, and then the tank 5 is moved to the cooling seat 308 for cooling and crystallization. Several fan blades 312 are evenly distributed on the drive shaft 309. The fan blades 312 are plastic blades. Plastic material is relatively inexpensive, which can greatly reduce the manufacturing cost of the fan blades 312. The fixed rod 305 has an "L" shaped cross section and is made of stainless steel. The stainless steel material can increase the service life of the fixing rod 305 and prevent the fixing rod 305 from rusting during use. The connecting frame 302 is a titanium alloy frame with a trident-shaped cross section.

[0032] Reference Figure 4As shown in this embodiment: the adjustment structure 4 includes a connecting plate 41, which is fixedly connected to the base plate 1. A sleeve plate 42 is fixedly connected to the upper surface of both the base plate 1 and the connecting plate 41. A sliding plate 47 is slidably connected to the inner wall of the sleeve plate 42. The two sets of sliding plates 47 are fixedly connected to the heating seat 306 and the cooling seat 308 respectively. Several insertion holes 46 are opened on the inner wall of the sliding plate 47. An insertion rod 43 is slidably connected to the inner wall of the sliding plate 47. The insertion rod 43 is slidably connected to the insertion hole 46. When the height of the heating base 306 and the cooling base 308 needs to be adjusted, pull the insertion rod 43 to move it, separating the insertion rod 43 from the insertion hole 46. Then pull the sliding plate 47 to move it, causing the heating base 306 and the cooling base 308 to move. The sliding plate 47 slides on the inner wall of the sleeve plate 42. After moving to the appropriate position, pull the insertion rod 43 to move it, aligning the insertion rod 43 with the sleeve plate 42 and the insertion hole 46. Then insert the insertion rod 43 to fix it. Limiting rods 45 are fixedly connected to both sides of the sliding plate 47, and the limiting rods 45 are slidably connected to the sleeve plate 42. The limiting rods 45 can limit the sliding plate 47 to prevent it from deviating during sliding, thus improving the stability of the sliding plate 47. A spring 44 is sleeved on the arc surface of the insertion rod 43, and the two ends of the spring 44 are fixedly connected to the insertion rod 43 and the sleeve plate 42, respectively. When it is necessary to insert the plug rod 43 for fixation, pull the plug rod 43 to move it. The plug rod 43 drives the spring 44 to stretch. Then, align the plug rod 43 with the appropriate socket 46 and insert the plug rod 43 for fixation.

[0033] Detailed Instructions for Use: When crystallizing sodium sulfonate, place the material into tank 5, then start the servo motor 303. The servo motor 303 drives the turntable 304 to rotate, which in turn moves the fixed rod 305. The fixed rod 305 then drives the rotating ring 301 to rotate, which in turn moves the connecting frame 302. The connecting frame 302 then rotates the tank 5, moving it to the heating seat 306 for heating and melting. After the raw material melts, continue heating. Then, start the servo motor 303 again and move the tank 5 to the cooling seat 308 for cooling and crystallization. The plastic material is relatively inexpensive, which can greatly reduce the manufacturing cost of the fan blade 312. The stainless steel material increases the service life of the fixed rod 305 and prevents it from rusting during use.

[0034] When the height of the heating base 306 and the cooling base 308 needs to be adjusted, pull the insertion rod 43 to move it, separating the insertion rod 43 from the insertion hole 46. Then pull the sliding plate 47 to move it, causing the heating base 306 and the cooling base 308 to move. The sliding plate 47 slides on the inner wall of the sleeve plate 42. After moving to the appropriate position, pull the insertion rod 43 to move it, aligning the insertion rod 43 with the sleeve plate 42 and the insertion hole 46. Then insert the insertion rod 43 to fix it. The limiting rod 45 can limit the sliding plate 47 to prevent it from deviating when sliding, thus improving the stability of the sliding plate 47. When it is necessary to insert the insertion rod 43 to fix it, pull the insertion rod 43 to move it, causing the spring 44 to stretch. Then align the insertion rod 43 with the appropriate insertion hole 46 and insert the insertion rod 43 to fix it.

Claims

1. A crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate, comprising a base plate (1), an auxiliary structure (3), and two regulating structures (4), characterized in that: A vertical rod (2) is fixedly connected to the upper surface of the base plate (1). A tank (5) is provided on one side of the vertical rod (2). The tank (5) is connected to the vertical rod (2) by means of an auxiliary structure (3). An auxiliary structure (3) is provided on the arc surface of the vertical rod (2). The auxiliary structure (3) includes a rotating ring (301). The rotating ring (301) is rotatably connected to the vertical rod (2). A connecting frame (302) is fixedly connected to the arc surface of the rotating ring (301). The end of the connecting frame (302) away from the rotating ring (301) is fixedly connected to the tank (5). A servo motor (303) is installed at the upper end of the vertical rod (2). A turntable (304) is fixedly connected to the output end of the servo motor (303). Several fixed rods (3) are fixedly connected to the arc surface of the turntable (304). 05), the fixed rod (305) is fixedly connected to the rotating ring (301), and a cooling seat (308) and a heating seat (306) are respectively provided on the upper sides of the base plate (1). The heating seat (306) and the cooling seat (308) are both connected to the base plate (1) by means of the adjustment structure (4). Several heating rods (307) are installed inside the heating seat (306), and several connecting rods (310) are fixedly connected inside the cooling seat (308). The several connecting rods (310) are divided into groups of four. A fixed ring (311) is fixedly connected to one end of the four connecting rods (310) that are close to each other. A drive shaft (309) is installed inside the fixed ring (311), and several fan blades (312) are installed on the arc surface of the drive shaft (309).

2. The crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate according to claim 1, characterized in that, Several fan blades (312) are evenly distributed on the drive shaft (309), and the fan blades (312) are plastic blades.

3. The crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate according to claim 1, characterized in that, The cross-section of the fixing rod (305) is "L" shaped, and the fixing rod (305) is a stainless steel rod.

4. The crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate according to claim 1, characterized in that, The connecting frame (302) is a titanium alloy frame, and the cross-section of the connecting frame (302) is triangular.

5. The crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate according to claim 1, characterized in that, The base plate (1) is provided with adjustment structures (4) on both sides. The adjustment structure (4) includes a connecting plate (41). The connecting plate (41) is fixedly connected to the base plate (1). The upper surfaces of the base plate (1) and the connecting plate (41) are fixedly connected with sleeve plates (42). The inner wall of the sleeve plate (42) is slidably connected with a sliding plate (47). The two sets of sliding plates (47) are fixedly connected to the heating seat (306) and the cooling seat (308) respectively. The inner wall of the sliding plate (47) is provided with several insertion holes (46). The inner wall of the sliding plate (47) is slidably connected with an insertion rod (43). The insertion rod (43) is slidably connected to the insertion hole (46).

6. The crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate according to claim 5, characterized in that, Limiting rods (45) are fixedly connected to both sides of the sliding plate (47), and the limiting rods (45) are slidably connected to the sleeve plate (42).

7. The crystallization apparatus for the production of sodium isophthalic acid-5-sulfonate according to claim 5, characterized in that, The arc surface of the insertion rod (43) is fitted with a spring (44), and the two ends of the spring (44) are fixedly connected to the insertion rod (43) and the sleeve plate (42) respectively.

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