Edible film and production method thereof

The edible film composition, featuring water-soluble and water-insoluble plant fibers and alpha starch, addresses the challenges of ductility and taste in existing edible films, resulting in a high-quality film with excellent texture and flavor.

JP2025058911AActive Publication Date: 2025-04-09ESU TECH CO LTD
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Patent Information

Application Number
JP2024128583
Authority / Receiving Office
JP · JP
Patent Type
Applications
Current Assignee / Owner
Priority Date
2023-09-28
Filing Date
2024-08-02
Publication Date
2025-04-09
Estimated Expiration
2044-08-02

AI Technical Summary

Technical Problem

Existing edible films struggle to achieve both excellent ductility during manufacturing and a firm taste without increasing moisture levels, leading to issues like stickiness and poor texture.

Method used

A composition for edible films that includes both water-soluble and water-insoluble plant fibers, with a liquid component that does not use water, and alpha starch, which allows for excellent ductility and a firm taste.

Benefits of technology

The edible film achieves excellent ductility during manufacturing, ensuring a high-quality film with a firm taste and improved texture, preventing stickiness and thermal degradation.

✦ Generated by Eureka AI based on patent content.

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Abstract

To provide an edible film including a composition superior in ductility while being produced without increasing a moisture content and superior in a bodied feeling allowing the taste to be fully savored and a production method thereof.SOLUTION: An edible film contains water-soluble vegetable fiber and water-insoluble vegetable fiber in a total amount of 5 wt.% or more, where the blend ratio of the water-soluble vegetable fiber and the water-insoluble vegetable fiber is, in weight ratio, 10-150 pts.wt. of the water-insoluble vegetable fiber relative to 100 pts.wt. of the water-soluble vegetable fiber. A production method of the edible film includes: a mixing step of mixing solid components; a permeation step of adding the mix obtained in the mixing step to a liquid component and permeating the liquid component into the mix to obtain the permeated product; and a filming step of rolling the permeated product to obtain a film.SELECTED DRAWING: None
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Description

[Technical field]

[0001] The present invention relates to an edible film and a method for producing the same, and more specifically, to an edible film having a composition that provides excellent spreadability during production without increasing the moisture content, and an excellent body that allows the flavor to be fully enjoyed, and a method for producing the same. [Background technology]

[0002] Various proposals have been made regarding edible films, and they are used in a variety of fields, including various luxury items, sweets, and pharmaceuticals. Among these fields of application, in the case of various luxury items and sweets, it is important to fully enjoy the flavor, so it is necessary to incorporate a sufficient amount of extracts that bring out the flavor. However, when a sufficient amount of these extracts is added, there are problems such as excess moisture, which increases the cost of drying, and the use of extract powders results in poor ductility when producing a film, making it impossible to produce an edible film of uniform thickness. Accordingly, various proposals have been made to solve the problems with formability, such as the ductility, of edible films. For example, Patent Document 1 proposes a laminated edible film that is water-insoluble and has improved strength. Specifically, the proposed laminated edible film is a water-insoluble edible film formed by laminating two edible films, an acidic film made of polysaccharides soluble in the acidic range and an alkaline film made of polysaccharides soluble in the alkaline range, and the acidic and alkaline components contained in the film react and are neutralized between the layers of the acidic and alkaline films, making the laminated film insoluble in water. Patent Document 2 also proposes an edible sheet and its manufacturing method that can be efficiently and inexpensively produced, in which the thickness can be easily controlled and thinned for use in various applications, and in which thermal deterioration of food ingredients that are easily degraded in taste and flavor by heating is suppressed. Specifically, the proposed edible sheet is a sheet-shaped thermocompression molded product of a raw material composition containing pregelatinized starch, in which the raw material composition contains at least one food ingredient belonging to vegetables, including potatoes, fruit vegetables, grains, legumes, leafy vegetables, stem vegetables, flower vegetables, and root vegetables, fruits, seaweed, or seafood. [Prior art documents] [Patent documents]

[0003] [Patent Document 1] JP 2013-99342 A [Patent Document 2] JP 2022-100790 A Summary of the Invention [Problem to be solved by the invention]

[0004] However, even with the above proposals, it has not yet been possible to provide an edible film itself that fully exhibits flavor. In addition, although increasing the water content in the liquid composition for film before molding may improve moldability, which is one of the conventional problems, on the other hand, the increased water content causes problems such as the finished film being sticky and the drying process being lengthy. The reason why the above proposals cannot solve the problem is that the problem of poor spreadability when the composition is adjusted to fully exhibit flavor has not been solved, and as a result, it is currently not possible to obtain a good quality edible film. In short, there is currently a demand for the development of an edible film that allows the flavor to be fully enjoyed and has a composition that is excellent in stretchability during production.

[0005] Therefore, an object of the present invention is to provide an edible film having a composition with excellent spreadability during production without increasing the moisture content, and an excellent body that allows the flavor to be fully enjoyed, and a method for producing the same. [Means for solving the problem]

[0006] As a result of intensive research into solving the above problems, the inventors discovered that the above object could be achieved by containing both water-soluble plant fiber and water-insoluble plant fiber, and not using water as a liquid component. Further intensive research led to the completion of the present invention. That is, the present invention provides the following inventions. 1. The composition comprises an edible film composition containing a liquid component and a solid component, The food product contains both water-soluble plant fiber and water-insoluble plant fiber as the solid component, An edible film that does not use water as the liquid component, The total amount of water-soluble plant fiber and water-insoluble plant fiber derived from the above food is 5% by weight or more, The blending ratio of the water-soluble plant fiber derived from the food to the water-insoluble plant fiber is 100 parts by weight of the water-soluble plant fiber to 10 to 500 parts by weight of the water-insoluble plant fiber. Edible film. 2. The edible film according to 1, further comprising pregelatinized starch in an amount of 10 to 30% by weight based on the total weight of the edible film. 3. The edible film according to 1, wherein the blending ratio of the liquid component to the solid component is 100 parts by weight of the liquid component to 200 to 500 parts by weight of the solid component. 4. A mixing step of mixing solid components; a permeation step of adding the mixture obtained in the mixing step to a liquid component not containing water, and permeating the liquid component into the mixture to obtain a permeate; and The film-forming process involves rolling the permeate to obtain a film. 1. A method for producing an edible film according to claim 1, comprising: Effect of the Invention

[0007] The edible film of the present invention has a composition that provides excellent spreadability during production, and has an excellent body that allows the flavor to be fully enjoyed. Furthermore, according to the method for producing an edible film of the present invention, a high-quality edible film having excellent ductility can be efficiently produced. DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS

[0008] The present invention will now be described in further detail. The edible film of the present invention comprises an edible film composition containing a liquid component and a solid component, the solid component being a food product containing both water-soluble plant fiber and water-insoluble plant fiber, and the liquid component being water-free. The present invention will be described in detail below.

[0009] <Edible film composition> [Liquid component] The liquid component used in the present invention may have any fluidity, including a viscous paste, but water is not used in the present invention. The liquid component is not particularly limited as long as it is a liquid component other than water, and an extract component, other liquid component, etc. can be used. The above extract components are components for imparting a desired taste, and specific examples include plum extract; various fruit juices; various plant extracts; seafood extracts; and animal-derived extracts such as beef extract, pork extract, and chicken extract. Other liquid components include glycerin, starch syrup, isomerized liquid sugar, sugar alcohols, and the like.

[0010] [Solid component] The solid components used in the present invention include foods containing both the water-soluble plant fibers and the water-insoluble plant fibers, as well as bases, other solid components, and the like. As the base, the following film materials can generally be used, each of which can be used alone or in combination of two or more kinds, and each of which can be a commercially available product. Polyvinylpyrrolidone, polyvinyl alcohol, sodium polyacrylate, carboxymethylcellulose, starch, xanthan gum, karaya gum, sodium alginate, methylcellulose, carboxyvinyl polymer, agar, hydroxypropyl cellulose, hydroxypropyl methylcellulose phthalate (HPMCP), cellulose acetate phthalate (also known as cellulose acetate phthalate, CAP), carboxymethylethylcellulose (CMEC), ethylcellulose, hydroxyethylcellulose, hydroxypropylmethylcellulose, carboxyvinyl polymer (product name: Carbopol, manufactured by BF Goodrich Co.), tragacanth, gum arabic, locust bean gum, guar gum, carrageenan, dextrin, dextran, amylose, potassium carboxymethylcellulose, carbo Examples of suitable materials include sodium carboxymethylcellulose, calcium carboxymethylcellulose, pullulan, chitosan, starch, polyvinyl alcohol, carboxymethylethylcellulose, sodium carboxymethylstarch, Plantago seed coat, galactomannan, Eudragit, casein, sodium alginate, alkyl alginate ester, gelatin, shellac resins (shellac, white transparent shellac), starch, cellulose acetate, hydroxyethyl methylcellulose, water-insoluble methacrylic acid copolymer, ethyl methacrylate-trimethylammonium ethyl methacrylate chloride copolymer, dimethylaminoethyl methacrylate-methyl methacrylate copolymer, pullulan, hydroxypropyl methylcellulose (HPMC), methylcellulose, acrylic acid, methyl methacrylate copolymer, hydroxyethyl cellulose, polyethylene glycol, etc.

[0011] [Water-soluble vegetable fiber] The water-soluble plant fiber used in the present invention can be contained in food or can be used in food, and various types of plant fiber can be used without any particular limitation as long as it is water-soluble plant fiber. Food or food additives containing such water-soluble plant fiber can also be contained in the edible film of the present invention. Specifically, pectin, alginic acid, gums (xanthan gum, guar gum, gum arabic), methylcellulose, hydroxypropyl methylcellulose, glucomannan, cellulose, gluten, pullulan, soybean polysaccharides, various fruit-derived plant fibers etc. [Water-insoluble vegetable fiber] The water-insoluble plant fiber used in the present invention is not particularly limited as long as it is contained in food or can be used in food, and various types of plant fiber that do not dissolve in water can be used. By using a food or food additive containing such water-insoluble plant fiber, it can also be incorporated into the edible film of the present invention. Specific examples include cellulose, hemicellulose, lignin, chitin, and the like. [Other solid components] The other solid component may be pregelatinized starch, and in the present invention, in addition to the water-soluble plant fiber and the water-insoluble plant fiber, pregelatinized starch is preferably contained. Commercially available pregelatinized starch may be used as the pregelatinized starch. The amount of pregelatinized starch in the edible film is preferably 10 to 30% by weight based on the total weight of the edible film, in order to improve the spreadability and to give the edible film a good texture that is neither sticky nor papery, and more preferably 15 to 25% by weight.

[0012] [The above foods and their contents] Specific examples of the food containing both the water-soluble plant fiber and the water-insoluble plant fiber used as the solid component in the present invention include the following: "VITACEL AF401 (Apple Fiber)" product name, VITACEL series manufactured by Rettenmaier Co., Ltd.; "NUTRAVA (registered trademark) Citrus Fiber" sold by Sansho Co., Ltd.; Citri-Fi (registered trademark, sold by Torigoe Flour Milling Co., Ltd.), etc. The blending ratio of the water-soluble plant fiber and the water-insoluble plant fiber, i.e., the blending ratio of the insoluble dietary fiber and the water-soluble dietary fiber in the food, is preferably 10 to 500 parts by weight of the water-insoluble plant fiber to 100 parts by weight of the water-soluble plant fiber, more preferably 50 to 500. By using the mixture in this range, the desired effect can be obtained. Furthermore, the total amount of the insoluble dietary fiber and the water-soluble dietary fiber used, i.e., the total amount of the insoluble dietary fiber and the water-soluble dietary fiber in the food, is preferably 5% by weight or more, more preferably 5 to 20% by weight, and most preferably 5 to 15% by weight, of the entire edible film.

[0013] [Other ingredients] In the present invention, in addition to the water-soluble vegetable fibers and the water-insoluble vegetable fibers, various components that can usually be used in this type of edible film can be used. Examples of the other components include the following. When these are used, if they are liquid components, they are used as the liquid components, and if they are solid components, they are used as the solid components. Acidulants such as citric acid; flavoring agents such as plum salt; umami seasonings such as sodium glutamate and sodium inosinate; binders such as tragacanth powder, gum arabic, and corn starch; excipients such as crystalline cellulose; disintegrants such as corn starch; lubricants such as magnesium stearate; sweeteners such as sucrose, lactose, fructose or saccharin, aspartame, sucralose, stevia, and acesulfame potassium; flavorings such as peppermint, peppermint oil, cherry flavor, orange oil, and fennel oil; preservatives such as benzoic acid, sodium benzoate, benzyl benzoate, ethyl parahydroxybenzoate, butyl parahydroxybenzoate, and propyl parahydroxybenzoate; opacifying agents such as titanium oxide; colorants such as ferric oxide and yellow ferric oxide; various medicinal ingredients, etc.

[0014] (Ratio of liquid component to solid component) The mixing ratio of the liquid component to the solid component is preferably 100 parts by weight of the liquid component to 200 to 500 parts by weight of the solid component, and more preferably 300 to 450 parts by weight of the liquid component.

[0015] [Method for producing edible film of the present invention] The edible film of the present invention can be obtained by carrying out the following production method. That is, the production method of the present invention is a mixing step of mixing the solid components and separately mixing the water-free liquid components; a permeation step of adding the mixture obtained in the mixing step to a mixture of liquid components to permeate the mixture with the liquid components to obtain a permeate; and The film-forming process involves rolling the permeate to obtain a film. This can be implemented by executing: Details are provided below. (Mixing process) In the present invention, it is important to mix the solid component and the liquid component separately and then mix the mixture of the two. The mixing method for mixing the solid components in the mixing step is not particularly limited, and can be performed using various mixers depending on the amount of the solid components. The mixing time is also not particularly limited, and mixing can be performed according to a conventional method to the extent that the solid components (all the above-mentioned solid components are powders) are sufficiently dispersed and mixed. The method for mixing the liquid components is not particularly limited, and can be performed using various mixers depending on the amount of the solid components. The mixing time is also not particularly limited, and mixing may be performed to a degree that allows sufficient dispersion and mixing according to a conventional method. (Infiltration process) The mixture of solid components mixed in the above mixing step is poured into the mixture of liquid components, and the two are mixed to allow the mixture of liquid components to penetrate into the mixture of solid components. It is preferable to mix the two when penetrating. Penetration and mixing may be performed to the extent that the liquid component and the solid component are lightly combined. Such penetration and mixing may be performed using a normal stirring mixer or the like. (Film making process) In this step, first, the mixture of the solid component and the liquid component obtained in the above-mentioned penetration step is placed in a bag, for example an aluminum bag, and after sealing, it is steamed for 10 to 60 minutes. After steaming, the product is sandwiched between release paper or the like and rolled in a rolling machine in a conventional manner. This rolling is continued until a desired thickness is reached, and the edible film of the present invention can be obtained. (Other processes) In the present invention, in addition to the above-mentioned steps, other steps can be appropriately carried out without departing from the spirit of the present invention. The edible film of the present invention can be obtained by carrying out the production method of the present invention. The edible film of the present invention obtained by the above steps contains the above-mentioned components. The thickness is not particularly limited, but from the viewpoint of maintaining the texture, it is preferably in the range of 0.01 mm to 10 mm, and more preferably 0.1 to 5 mm.

[0016] [Usage, effects] The edible film of the present invention can be used by cutting it to a desired size and eating it in the same way as ordinary snacks. The edible film of the present invention is constructed as described above, and therefore can be manufactured with excellent spreadability. It also has an excellent texture, is neither papery nor sticky, dissolves well in the mouth, and has a savory flavor. The reason for such effects is unclear, but it is believed that the insoluble dietary fiber and soluble dietary fiber improve the balance between the skeletal components and the water-retaining components, resulting in soft physical properties and improved processability when rubbing into a sheet. EXAMPLES

[0017] The present invention will be described in more detail below with reference to examples and comparative examples, but the present invention is not limited to these in any way. [Examples 1-2] Edible films were prepared as follows, using the compositions shown in Table 1. Note that in the following examples, the work was done manually because the amounts involved were small, but each work may be done using machinery. (Mixing process) The solid ingredients in Table 1 were mixed using a spoon until the solid ingredients were thoroughly dispersed and mixed. Separately, the liquid ingredients in Table 1 were mixed using a spoon until they were thoroughly dispersed and mixed. (Infiltration process) The mixture of solid components mixed in the above mixing step was poured into the mixture of liquid components, and the two were mixed to allow the mixture of liquid components to permeate into the mixture of solid components. During permeation, the mixture was kneaded at the same time to mix, and a ball-like mixture was obtained. (Film making process) Next, the mixture of the solid and liquid components was placed in an aluminum bag or the like, sealed, and then steamed for 20 minutes. After steaming, the pieces were sandwiched between release paper and rolled using a rolling pin to obtain an edible film with a thickness of 2.5 mm. The obtained edible film was subjected to the following evaluations, and the results are shown in Table 2. Texture testing; For the sensory evaluation, 10 monitors were prepared and asked to eat the obtained edible film and evaluate it based on the following evaluation criteria. Extensibility: Determined whether the film had good extensibility during the film-making process. : Good stretchability and good stretchability. ◯: Although it was a little sticky, it was possible to stretch it to the specified thickness. △: Somewhat hard or viscous, some parts not stretchable, or some parts not moldable. ×: Hard and not stretchable or could not be molded. (Sensory evaluation) Stickiness: Determined by whether or not the sample is sticky when touched with the hand. ◎: Not sticky when touched. O: There was almost no stickiness when touched. △: It was slightly sticky when touched. ×: Sticky to the touch. Adhesion to teeth: Adhesion to teeth was evaluated when biting with teeth. ◎: Did not stick to teeth. ○: It was difficult to stick to my teeth. △: Some of it got on my teeth. ×: Got on my teeth. Hardness: judged as to whether it could be bitten off with teeth. ◎: Very easy to bite through. 〇: It was easy to bite through. △: It was a little difficult to bite through. ×: It was difficult to bite through. Meltability in the mouth: The degree to which the product melts in the mouth when placed in the mouth was judged. ◎: Very melt-in-the-mouth. 〇: Melts easily in the mouth. △: Somewhat difficult to melt in the mouth. ×: Does not melt in the mouth. Taste and aroma: The taste and aroma were judged when the sample was placed in the mouth. ◎: Strong taste and aroma. 〇: The taste and aroma were easily noticeable. △: The taste and aroma were somewhat weak. ×: No taste or aroma.

[0018] [Comparative Examples 1-2] Edible films were produced and tested in the same manner as in Example 1, except that the compositions were as shown in Table 1. The results are shown in Tables 1 and 2.

[0019] [Table 1]

[0020] [Table 2]

[0021] As shown in Table 2, the following can be seen: Both Example 1 and Example 2 were favorable in all evaluation items. In particular, Example 1 was highly evaluated in both workability and sensory test. On the other hand, Comparative Examples 1 and 2 were inferior to Examples 1 and 2 in the sensory evaluation, and were found to have poor workability.

Claims

1. The composition comprises an edible film composition containing a liquid component and a solid component, The food product contains both water-soluble plant fiber and water-insoluble plant fiber as the solid component, An edible film that does not use water as the liquid component, The food product contains water-soluble plant fiber and water-insoluble plant fiber derived from the food product in a total amount of 5% by weight or more, The blending ratio of the water-soluble plant fiber derived from the food to the water-insoluble plant fiber is 100 parts by weight of the water-soluble plant fiber to 10 to 500 parts by weight of the water-insoluble plant fiber. Edible film.

2. 2. The edible film according to claim 1, further comprising pregelatinized starch in an amount of 10 to 30% by weight based on the total weight of the edible film.

3. 2. The edible film according to claim 1, wherein the blending ratio of said liquid component to said solid component is 100% by weight of said liquid component to 200 to 500% by weight of said solid component.

4. a mixing step of mixing the solid components and separately mixing the water-free liquid components; a permeation step of adding the mixture obtained in the mixing step to a mixture of liquid components to permeate the mixture with the liquid components to obtain a permeate; and The film-forming process involves rolling the permeate to obtain a film. The method for producing an edible film according to claim 1, comprising:

Citation Information

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