Whole nutrient powder dry-wet composite technology
Through the dry and wet-combination process of full nutrition powder and combined with maltodextrin, the problems of poor mixing uniformity and insufficient stability in the dry process are solved, the cost of the wet process is reduced, and the use of trace minerals and oils is compounded. Improves the absorption efficiency and bone health of nutrient powder.
Patent Information
- Application Number
- CN202411161581.7
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-08-22
- Publication Date
- 2024-12-17
- Estimated Expiration
- Not applicable · inactive patent
AI Technical Summary
In the production of nutrient powder, dry and wet processes have problems such as poor mixing uniformity, slow dissolution speed and insufficient liquid stability. Vitamins with high cost and unstable wet processes are easily destroyed.
Using the wet and dry process of full nutrition powder, purified water and casein are added to the mixing equipment for stirring, nutrients and oil are added, and the oil and water emulsion is formed and dissolved with vitamins, emulsification and homogenization are carried out, and then spray-drying is carried out, combined with malt Mix dextrin to form a powder.
It improves mixing uniformity and dissolution speed, enhances liquid stability, reduces production costs, and promotes the absorption of vitamins and bone health through the use of compounded trace minerals and oils.
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Figure CN119138627A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of nutritional powder, in particular to a dry-wet compounding process of a complete nutritional powder. Background Art
[0002] Nutritional powder mainly includes macronutrients such as carbohydrates, fats, proteins, and various vitamins. Currently, there are two main production processes for nutritional powder: dry process and wet process.
[0003] Dry process: Put various nutrients together and mix them in a dry state. The mixing uniformity is relatively poor, the dissolution speed is slow when adding water to dissolve, and the liquid stability after dissolution is poor;
[0004] Wet process: various nutrients are added to water, mixed in a liquid state, and then dried by spray drying or other methods. This method is costly and some unstable vitamins, such as vitamin D and vitamin A, will be destroyed to a certain extent. Summary of the invention
[0005] In view of the problems existing in the existing multi-source power grid information fusion based on the Internet of Things, the present invention is proposed.
[0006] Therefore, the problem to be solved by the present invention is that both the dry process and the wet process have some limitations.
[0007] In order to solve the above technical problems, the present invention provides the following technical solutions:
[0008] In a first aspect, an embodiment of the present invention provides a dry-wet compounding process for a complete nutrient powder, which comprises the following steps:
[0009] Add purified water and casein into a mixing device, stir through the mixing device, and then add nutrients until stirring is sufficient or reaches a predetermined time to obtain a mixed solution;
[0010] The oil is heated, and after the oil temperature reaches a preset value, purified water and succinic acid monoglyceride are added, and then stirred to obtain an oil-water emulsion;
[0011] The mixed solution and the oil-water emulsion are mixed together and emulsified to obtain an emulsion;
[0012] Dissolve fat-soluble vitamins and water-soluble vitamins in purified water, and then add them to the emulsion to make a fixed volume;
[0013] The fixed volume liquid is homogenized, sterilized and spray-dried to obtain a powder;
[0014] The powder is mixed with the remaining maltodextrin to obtain a nutritional powder.
[0015] As a preferred solution of the dry-wet composite process of the complete nutrient powder of the present invention, when the purified water and casein are mixed, the temperature of the mixing equipment is set to 30-65° C. and the stirring time is 10-50 min;
[0016] Among them, the ratio of purified water to casein is 6:4;
[0017] After adding nutrients, the mixing equipment is set to a temperature of 30-65°C and a stirring time of 5-25 minutes.
[0018] As a preferred solution of the dry-wet compounding process of the complete nutrient powder of the present invention, the nutrients include the following components by weight:
[0019] Concentrated whey protein 50-70g, microcrystalline cellulose 6-8g, galactomannan 35-45g, inulin 25-30g, maltodextrin 0-570g, choline chloride 2-3g, potassium citrate 5-15g, sodium citrate 5-15g, edible salt 5-8g, complex trace minerals 6.8g, and hydrogen phosphate 2-3g.
[0020] As a preferred solution of the dry-wet compounding process of the complete nutrient powder of the present invention, the compounded trace minerals include the following components by weight:
[0021] Magnesium sulfate 1.6-2.4g, ferrous sulfate 0.8-1.2g, zinc sulfate 0.8-1.2g, copper sulfate 0.2-0.6g, manganese sulfate 0.1-0.3g, potassium iodide 0.05-0.15g, sodium selenite 0.05-0.15g.
[0022] As a preferred embodiment of the dry-wet composite process of the complete nutrient powder of the present invention, the oil comprises sunflower oil, medium-chain triglycerides and low-erucic acid rapeseed oil;
[0023] Sunflower oil accounts for 0.1-0.4;
[0024] The proportion of medium-chain triglycerides is 0.2-0.5;
[0025] The proportion of low-erucic acid rapeseed oil is 0.4-0.5.
[0026] As a preferred solution of the dry-wet composite process of the complete nutrient powder of the present invention, wherein: when the oil is heated, it is stirred by a stirring device, and the preset value of the oil temperature is set to 50-80°C;
[0027] When purified water and succinic acid monoglyceride are added to the oil, the proportion of purified water is 1%, the proportion of succinic acid monoglyceride is 1-8%, and stirring is performed by a stirring device, and the stirring time is set to 5-40 minutes.
[0028] As a preferred solution of the dry-wet composite process of the complete nutrient powder of the present invention, the steps of making the emulsion are as follows:
[0029] The air in the emulsification tank is discharged by nitrogen purging, and then nitrogen is filled into the emulsification tank for gas replacement;
[0030] Add the mixed solution and the oil-water emulsion into an emulsification tank;
[0031] Turn on the stirring equipment, perform emulsification operation, and set the temperature to 30-65℃.
[0032] As a preferred embodiment of the dry-wet composite process of the complete nutrient powder of the present invention, when the fat-soluble vitamins are dissolved in purified water, a co-solvent is added to the purified water;
[0033] The cosolvent is lecithin or glyceride;
[0034] The fat-soluble vitamins include the following components by weight:
[0035] Vitamin A: 900 μg;
[0036] Vitamin D: 15-20 μg;
[0037] Vitamin E: 10 mg;
[0038] The water-soluble vitamins include the following components by weight:
[0039] Vitamin B1: 1.1 mg;
[0040] Vitamin B2: 1.3 mg;
[0041] Vitamin B3: 16 mg;
[0042] Vitamin B5: 5 mg;
[0043] Vitamin B6: 1.3-1.7 mg;
[0044] Vitamin B7: 30 μg;
[0045] Vitamin B9: 400μg.
[0046] As a preferred solution of the dry-wet composite process of the complete nutrient powder of the present invention, wherein: the liquid after volume adjustment is homogenized twice, wherein the first homogenization pressure is 100-300 bar, and the second homogenization pressure is 30-60 bar;
[0047] After the secondary homogenization treatment, the liquid is input into the sterilizer and sterilized at a temperature of 75-85°C for 25-40 seconds.
[0048] After sterilization, the water in the liquid is removed by an evaporator to increase the solid content and the density of the liquid until the density of the liquid reaches 1.07-1.15;
[0049] The concentrated liquid is spray-dried to form a powdery product to obtain a powder.
[0050] As a preferred solution of the dry-wet compounding process of the complete nutrient powder of the present invention, when the powder is mixed with the remaining maltodextrin, the mixing time is set to 15-45 minutes and the rotation speed is set to 45-120 revolutions / min.
[0051] The beneficial effects of the present invention are:
[0052] By combining the dry process with the wet process, certain nutrients are pre-mixed in a wet state and then combined with the dry-mixed nutrients, which significantly improves the mixing uniformity and avoids the problem of uneven mixing in the dry process. When adding water to dissolve, the dissolution speed is faster due to more uniform mixing, and the liquid stability after dissolution is better, which solves the problems of poor solubility and insufficient stability in the dry process. Secondly, compared with the traditional wet process, the dry-wet composite process may reduce the dependence on high-cost equipment, such as spray drying, thereby reducing the overall production cost.
[0053] By adding complex trace minerals and using magnesium sulfate, it helps vasodilation, and magnesium sulfate works together with calcium sulfate to help maintain bone strength and density. Secondly, the use of oils and fats provides the human body with essential fatty acids, and when used in combination with fat-soluble vitamins and water-soluble vitamins, it can help the human body absorb fat-soluble vitamins and water-soluble vitamins. BRIEF DESCRIPTION OF THE DRAWINGS
[0054] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following briefly introduces the drawings required for describing the embodiments. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work. Among them:
[0055] Figure 1 This is a flow chart of the dry-wet compounding process of complete nutrient powder. DETAILED DESCRIPTION
[0056] In order to make the above-mentioned purposes, features and advantages of the present invention more obvious and easy to understand, the specific implementation methods of the present invention are described in detail below in conjunction with the drawings of the specification. Obviously, the described embodiments are part of the embodiments of the present invention, but not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary persons in the art without creative work should fall within the scope of protection of the present invention.
[0057] In the following description, many specific details are set forth to facilitate a full understanding of the present invention, but the present invention may also be implemented in other ways different from those described herein, and those skilled in the art may make similar generalizations without violating the connotation of the present invention. Therefore, the present invention is not limited to the specific embodiments disclosed below.
[0058] Secondly, the term "one embodiment" or "embodiment" as used herein refers to a specific feature, structure, or characteristic that may be included in at least one implementation of the present invention. The term "in one embodiment" that appears in different places in this specification does not necessarily refer to the same embodiment, nor does it refer to a separate or selective embodiment that is mutually exclusive with other embodiments.
[0059] The present invention is described in detail with reference to schematic diagrams. When describing the embodiments of the present invention, for the sake of convenience, the cross-sectional diagrams showing the device structure will not be partially enlarged according to the general scale, and the schematic diagrams are only examples, which should not limit the scope of protection of the present invention. In addition, in actual production, the three-dimensional dimensions of length, width and depth should be included.
[0060] At the same time, in the description of the present invention, it should be noted that the directions or positional relationships indicated by the terms "upper, lower, inner and outer" are based on the directions or positional relationships shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific direction, be constructed and operated in a specific direction, and therefore cannot be understood as limiting the present invention. In addition, the terms "first, second or third" are only used for descriptive purposes and cannot be understood as indicating or implying relative importance.
[0061] In the present invention, unless otherwise clearly specified and limited, the terms "install, connect, connect" should be understood in a broad sense, for example: it can be a fixed connection, a detachable connection or an integral connection; it can also be a mechanical connection, an electrical connection or a direct connection, or it can be indirectly connected through an intermediate medium, or it can be the internal communication of two components. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.
[0062] Example 1
[0063] Reference Figure 1, which is the first embodiment of the present invention, provides a dry-wet compounding process for a complete nutrient powder, comprising the following steps:
[0064] S1. Add purified water and casein into a mixing device, stir through the mixing device, and then add nutrients until stirring is sufficient or reaches a predetermined time to obtain a mixed solution.
[0065] When the purified water and casein are mixed, the temperature of the mixing equipment is set to 30-65°C and the stirring time is 10-50 minutes;
[0066] Among them, the ratio of purified water to casein is 6:4;
[0067] After adding nutrients, the mixing equipment is set to a temperature of 30-65°C and the stirring time is 5-25 minutes.
[0068] The nutrients include the following components by weight:
[0069] Concentrated whey protein 50g, microcrystalline cellulose 6g, galactomannan 35g, inulin 25g, maltodextrin 0g, choline chloride 2g, potassium citrate 5g, sodium citrate 5g, table salt 5g, complex trace minerals 6.8g, and hydrogen phosphate 2g.
[0070] The compound trace minerals include the following components by weight:
[0071] Magnesium sulfate 1.6-2.4g, ferrous sulfate 0.8-1.2g, zinc sulfate 0.8-1.2g, copper sulfate 0.2-0.6g, manganese sulfate 0.1-0.3g, potassium iodide 0.05-0.15g, sodium selenite 0.05-0.15g.
[0072] S2. Heat the oil, add purified water and succinic acid monoglyceride after the oil temperature reaches a preset value, and stir to obtain an oil-water emulsion.
[0073] The oils include sunflower oil, medium chain triglycerides and low-erucic acid rapeseed oil; wherein,
[0074] Sunflower oil accounts for 0.1-0.4;
[0075] The proportion of medium-chain triglycerides is 0.2-0.5;
[0076] The proportion of low-erucic acid rapeseed oil is 0.4-0.5.
[0077] When heating the grease, the grease is stirred by a stirring device, and the preset value of the oil temperature is set to 50-80° C. In this embodiment, the preset value of the oil temperature is 60° C.;
[0078] When purified water and succinic acid monoglyceride are added to the oil, the proportion of purified water is 1%, the proportion of succinic acid monoglyceride is 1-8%, and stirring is performed by a stirring device, and the stirring time is set to 5-40 minutes.
[0079] S3, mixing the mixed solution and the oil-water emulsion together, and emulsifying them to obtain an emulsion.
[0080] The preparation steps of the emulsion are:
[0081] The air in the emulsification tank is discharged by nitrogen purging, and then nitrogen is filled into the emulsification tank for gas replacement;
[0082] Add the mixed solution and the oil-water emulsion into an emulsification tank;
[0083] Turn on the stirring equipment, perform emulsification operation, and set the temperature to 30-65℃.
[0084] S4. Dissolve fat-soluble vitamins and water-soluble vitamins in purified water, and then add them to the emulsion to make up the volume.
[0085] When dissolving fat-soluble vitamins in purified water, add a cosolvent to the purified water;
[0086] The cosolvent is lecithin or glyceride;
[0087] The fat-soluble vitamins include the following components by weight:
[0088] Vitamin A: 900 μg;
[0089] Vitamin D: 15-20 μg;
[0090] Vitamin E: 10 mg;
[0091] The water-soluble vitamins include the following components by weight:
[0092] Vitamin B1: 1.1 mg;
[0093] Vitamin B2: 1.3 mg;
[0094] Vitamin B3: 16 mg;
[0095] Vitamin B5: 5 mg;
[0096] Vitamin B6: 1.3-1.7 mg;
[0097] Vitamin B7: 30 μg;
[0098] Vitamin B9: 400μg.
[0099] S5. The fixed volume liquid is homogenized, sterilized and spray-dried to obtain a powder.
[0100] The liquid after volume adjustment is homogenized twice, wherein the first homogenization pressure is 100-300 bar and the second homogenization pressure is 30-60 bar;
[0101] After the secondary homogenization treatment, the feed liquid is input into the sterilizer and sterilized at a temperature of 75-85°C for 25-40 seconds. In this embodiment, the temperature is set to 75°C for 25 seconds.
[0102] After sterilization, the water in the liquid is removed by an evaporator to increase the solid content and the density of the liquid until the density of the liquid reaches 1.07-1.15;
[0103] The concentrated liquid is spray-dried to form a powdery product to obtain a powder.
[0104] S6. Mix the powder with the remaining maltodextrin to obtain nutritional powder.
[0105] When dry mixing the powder with the remaining maltodextrin, set the mixing time to 15-45 min and the speed to 45-120 rpm;
[0106] At this time, the remaining maltodextrin was 570 g.
[0107] The oil embedding rate of the spray-dried powder was tested to be 99.5%. The spray-dried powder dissolved quickly after being mixed with warm water, and the system was stable.
[0108] Example 2
[0109] Reference Figure 1 , which is the second embodiment of the present invention, provides a dry-wet compounding process for a complete nutrient powder, comprising the following steps:
[0110] S1. Add purified water and casein into a mixing device, stir through the mixing device, and then add nutrients until stirring is sufficient or reaches a predetermined time to obtain a mixed solution.
[0111] When the purified water and casein are mixed, the temperature of the mixing equipment is set to 30-65°C and the stirring time is 10-50 minutes;
[0112] Among them, the ratio of purified water to casein is 6:4;
[0113] After adding nutrients, the mixing equipment is set to a temperature of 30-65°C and a stirring time of 5-25 minutes.
[0114] The nutrients include the following components by weight:
[0115] Concentrated whey protein 60g, microcrystalline cellulose 7g, galactomannan 40g, inulin 27g, maltodextrin 270g, choline chloride 2g, potassium citrate 10g, sodium citrate 10g, table salt 7g, complex trace minerals 6.8g, and hydrogen phosphate 2g.
[0116] The compound trace minerals include the following components by weight:
[0117] Magnesium sulfate 1.6-2.4g, ferrous sulfate 0.8-1.2g, zinc sulfate 0.8-1.2g, copper sulfate 0.2-0.6g, manganese sulfate 0.1-0.3g, potassium iodide 0.05-0.15g, sodium selenite 0.05-0.15g.
[0118] S2. Heat the oil, add purified water and succinic acid monoglyceride after the oil temperature reaches a preset value, and stir to obtain an oil-water emulsion.
[0119] The oils include sunflower oil, medium chain triglycerides and low-erucic acid rapeseed oil; wherein,
[0120] Sunflower oil accounts for 0.1-0.4;
[0121] The proportion of medium-chain triglycerides is 0.2-0.5;
[0122] The proportion of low-erucic acid rapeseed oil is 0.4-0.5.
[0123] When heating the grease, the grease is stirred by a stirring device, and the preset value of the oil temperature is set to 50-80° C. In this embodiment, the preset value of the oil temperature is 65° C.;
[0124] When purified water and succinic acid monoglyceride are added to the oil, the proportion of purified water is 1%, the proportion of succinic acid monoglyceride is 1-8%, and stirring is performed by a stirring device, and the stirring time is set to 5-40 minutes.
[0125] S3, mixing the mixed solution and the oil-water emulsion together, and emulsifying them to obtain an emulsion.
[0126] The steps of making the emulsion are:
[0127] The air in the emulsification tank is discharged by nitrogen purging, and then nitrogen is filled into the emulsification tank for gas replacement;
[0128] Add the mixed solution and the oil-water emulsion into an emulsification tank;
[0129] Turn on the stirring equipment, perform emulsification operation, and set the temperature to 30-65℃.
[0130] S4. Dissolve fat-soluble vitamins and water-soluble vitamins in purified water, and then add them to the emulsion to make up the volume.
[0131] When dissolving fat-soluble vitamins in purified water, add a cosolvent to the purified water;
[0132] The cosolvent is lecithin or glyceride;
[0133] The fat-soluble vitamins include the following components by weight:
[0134] Vitamin A: 900 μg;
[0135] Vitamin D: 15-20 μg;
[0136] Vitamin E: 10 mg;
[0137] The water-soluble vitamins include the following components by weight:
[0138] Vitamin B1: 1.1 mg;
[0139] Vitamin B2: 1.3 mg;
[0140] Vitamin B3: 16 mg;
[0141] Vitamin B5: 5 mg;
[0142] Vitamin B6: 1.3-1.7 mg;
[0143] Vitamin B7: 30 μg;
[0144] Vitamin B9: 400μg.
[0145] S5. The fixed volume liquid is homogenized, sterilized and spray-dried to obtain a powder.
[0146] The liquid after volume adjustment is homogenized twice, wherein the first homogenization pressure is 100-300 bar and the second homogenization pressure is 30-60 bar;
[0147] After the secondary homogenization treatment, the feed liquid is input into the sterilizer and sterilized at a temperature of 75-85°C for 25-40 seconds. In this embodiment, the temperature is set to 75°C for 35 seconds.
[0148] After sterilization, the water in the liquid is removed by an evaporator to increase the solid content and the density of the liquid until the density of the liquid reaches 1.07-1.15;
[0149] The concentrated liquid is spray-dried to form a powdery product to obtain a powder.
[0150] S6. Mix the powder with the remaining maltodextrin to obtain nutritional powder.
[0151] When dry mixing the powder with the remaining maltodextrin, set the mixing time to 15-45 min and the speed to 45-120 rpm;
[0152] At this time, the remaining maltodextrin was 300 g.
[0153] The oil embedding rate of the spray-dried powder was tested to be 99.3%. The final product dissolved quickly after being mixed with warm water, and the system was stable.
[0154] Example 3
[0155] Reference Figure 1 , which is the third embodiment of the present invention, provides a dry-wet compounding process for a complete nutrient powder, comprising the following steps:
[0156] S1. Add purified water and casein into a mixing device, stir through the mixing device, and then add nutrients until stirring is sufficient or reaches a predetermined time to obtain a mixed solution.
[0157] When the purified water and casein are mixed, the temperature of the mixing equipment is set to 30-65°C and the stirring time is 10-50 minutes;
[0158] Among them, the ratio of purified water to casein is 6:4;
[0159] After adding nutrients, the mixing equipment is set to a temperature of 30-65°C and a stirring time of 5-25 minutes.
[0160] The nutrients include the following components by weight:
[0161] Concentrated whey protein 65g, microcrystalline cellulose 8g, galactomannan 40g, inulin 30g, maltodextrin 450g, choline chloride 3g, potassium citrate 12g, sodium citrate 12g, table salt 7g, complex trace minerals 6.8g, and hydrogen phosphate 3g.
[0162] The compound trace minerals include the following components by weight:
[0163] Magnesium sulfate 1.6-2.4g, ferrous sulfate 0.8-1.2g, zinc sulfate 0.8-1.2g, copper sulfate 0.2-0.6g, manganese sulfate 0.1-0.3g, potassium iodide 0.05-0.15g, sodium selenite 0.05-0.15g.
[0164] S2. Heat the oil, add purified water and succinic acid monoglyceride after the oil temperature reaches a preset value, and stir to obtain an oil-water emulsion.
[0165] The oils include sunflower oil, medium chain triglycerides and low-erucic acid rapeseed oil; wherein,
[0166] Sunflower oil accounts for 0.1-0.4;
[0167] The proportion of medium-chain triglycerides is 0.2-0.5;
[0168] The proportion of low-erucic acid rapeseed oil is 0.4-0.5.
[0169] When heating the grease, the grease is stirred by a stirring device, and the preset value of the oil temperature is set to 50-80° C. In this embodiment, the preset value of the oil temperature is 70° C.;
[0170] When purified water and succinic acid monoglyceride are added to the oil, the proportion of purified water is 1%, the proportion of succinic acid monoglyceride is 1-8%, and stirring is performed by a stirring device, and the stirring time is set to 5-40 minutes.
[0171] S3, mixing the mixed solution and the oil-water emulsion together, and emulsifying them to obtain an emulsion.
[0172] The steps of making the emulsion are:
[0173] The air in the emulsification tank is discharged by nitrogen purging, and then nitrogen is filled into the emulsification tank for gas replacement;
[0174] Add the mixed solution and the oil-water emulsion into an emulsification tank;
[0175] Turn on the stirring equipment, perform emulsification operation, and set the temperature to 30-65℃.
[0176] S4. Dissolve the fat-soluble vitamins and water-soluble vitamins in purified water, and then add them to the emulsion to make up the volume.
[0177] When dissolving fat-soluble vitamins in purified water, add a cosolvent to the purified water;
[0178] The cosolvent is lecithin or glyceride;
[0179] The fat-soluble vitamins include the following components by weight:
[0180] Vitamin A: 900 μg;
[0181] Vitamin D: 15-20 μg;
[0182] Vitamin E: 10 mg;
[0183] The water-soluble vitamins include the following components by weight:
[0184] Vitamin B1: 1.1 mg;
[0185] Vitamin B2: 1.3 mg;
[0186] Vitamin B3: 16 mg;
[0187] Vitamin B5: 5 mg;
[0188] Vitamin B6: 1.3-1.7 mg;
[0189] Vitamin B7: 30 μg;
[0190] Vitamin B9: 400μg.
[0191] S5. The fixed volume liquid is homogenized, sterilized and spray-dried to obtain a powder.
[0192] The liquid after volume adjustment is homogenized twice, wherein the first homogenization pressure is 100-300 bar and the second homogenization pressure is 30-60 bar;
[0193] After the secondary homogenization treatment, the feed liquid is input into the sterilizer and sterilized at a temperature of 75-85°C for 25-40 seconds. In this embodiment, the temperature is set to 80°C for 40 seconds.
[0194] After sterilization, the water in the liquid is removed by an evaporator to increase the solid content and the density of the liquid until the density of the liquid reaches 1.07-1.15;
[0195] The concentrated liquid is spray-dried to form a powdery product to obtain a powder.
[0196] S6. Mix the powder with the remaining maltodextrin to obtain nutritional powder.
[0197] When dry mixing the powder with the remaining maltodextrin, set the mixing time to 15-45 min and the speed to 45-120 rpm;
[0198] At this time, the remaining maltodextrin was 120 g.
[0199] The oil embedding rate of the spray-dried powder was tested to be 98.1%. The spray-dried powder dissolved quickly after being mixed with warm water, and the system was stable.
[0200] Example 4
[0201] Reference Figure 1 , which is the third embodiment of the present invention, provides a dry-wet compounding process for a complete nutrient powder, comprising the following steps:
[0202] S1. Add purified water and casein into a mixing device, stir through the mixing device, and then add nutrients until stirring is sufficient or reaches a predetermined time to obtain a mixed solution.
[0203] When the purified water and casein are mixed, the temperature of the mixing equipment is set to 30-65°C and the stirring time is 10-50 minutes;
[0204] Among them, the ratio of purified water to casein is 6:4;
[0205] After adding nutrients, the mixing equipment is set to a temperature of 30-65°C and a stirring time of 5-25 minutes.
[0206] The nutrients include the following components by weight:
[0207] Concentrated whey protein 70g, microcrystalline cellulose 8g, galactomannan 45g, inulin 30g, maltodextrin 570g, choline chloride 3g, potassium citrate 15g, sodium citrate 15g, edible salt 8g, complex trace minerals 6.8g, and hydrogen phosphate 3g.
[0208] The compound trace minerals include the following components by weight:
[0209] Magnesium sulfate 1.6-2.4g, ferrous sulfate 0.8-1.2g, zinc sulfate 0.8-1.2g, copper sulfate 0.2-0.6g, manganese sulfate 0.1-0.3g, potassium iodide 0.05-0.15g, sodium selenite 0.05-0.15g.
[0210] S2. Heat the oil, add purified water and succinic acid monoglyceride after the oil temperature reaches a preset value, and stir to obtain an oil-water emulsion.
[0211] The oils include sunflower oil, medium chain triglycerides and low-erucic acid rapeseed oil; wherein,
[0212] Sunflower oil accounts for 0.1-0.4;
[0213] The proportion of medium-chain triglycerides is 0.2-0.5;
[0214] The proportion of low-erucic acid rapeseed oil is 0.4-0.5.
[0215] When heating the grease, the grease is stirred by a stirring device, and the preset value of the oil temperature is set to 50-80° C. In this embodiment, the preset value of the oil temperature is 80° C.;
[0216] When purified water and succinic acid monoglyceride are added to the oil, the proportion of purified water is 1%, the proportion of succinic acid monoglyceride is 1-8%, and stirring is performed by a stirring device, and the stirring time is set to 5-40 minutes.
[0217] S3, mixing the mixed solution and the oil-water emulsion together, and emulsifying them to obtain an emulsion.
[0218] The steps of making the emulsion are:
[0219] The air in the emulsification tank is discharged by nitrogen purging, and then nitrogen is filled into the emulsification tank for gas replacement;
[0220] Add the mixed solution and the oil-water emulsion into an emulsification tank;
[0221] Turn on the stirring equipment, perform emulsification operation, and set the temperature to 30-65℃.
[0222] S4. Dissolve the fat-soluble vitamins and water-soluble vitamins in purified water, and then add them to the emulsion to make up the volume.
[0223] When dissolving fat-soluble vitamins in purified water, add a cosolvent to the purified water;
[0224] The cosolvent is lecithin or glyceride;
[0225] The fat-soluble vitamins include the following components by weight:
[0226] Vitamin A: 900 μg;
[0227] Vitamin D: 15-20 μg;
[0228] Vitamin E: 10 mg;
[0229] The water-soluble vitamins include the following components by weight:
[0230] Vitamin B1: 1.1 mg;
[0231] Vitamin B2: 1.3 mg;
[0232] Vitamin B3: 16 mg;
[0233] Vitamin B5: 5 mg;
[0234] Vitamin B6: 1.3-1.7 mg;
[0235] Vitamin B7: 30 μg;
[0236] Vitamin B9: 400μg.
[0237] S5. The fixed volume liquid is homogenized, sterilized and spray-dried to obtain a powder.
[0238] The liquid after volume adjustment is homogenized twice, wherein the first homogenization pressure is 100-300 bar and the second homogenization pressure is 30-60 bar;
[0239] After the secondary homogenization treatment, the feed liquid is input into the sterilizer and sterilized at a temperature of 75-85°C for 25-40 seconds. In this embodiment, the temperature is set to 85°C for 35 seconds.
[0240] After sterilization, the water in the liquid is removed by an evaporator to increase the solid content and the density of the liquid until the density of the liquid reaches 1.07-1.15;
[0241] The concentrated liquid is spray-dried to form a powdery product to obtain a powder.
[0242] S6. Mix the powder with the remaining maltodextrin to obtain nutritional powder.
[0243] When dry mixing the powder with the remaining maltodextrin, set the mixing time to 15-45 min and the speed to 45-120 rpm;
[0244] At this time, the remaining maltodextrin was 0 g.
[0245] The oil embedding rate of the spray-dried powder was tested to be 97.2%. The spray-dried powder dissolved quickly after being mixed with warm water, and the system was stable.
[0246] Table 1: Ingredients of Examples 1 to 4
[0247] Ingredients / g Example 1 Example 2 Example 3 Example 4 Maltodextrin dry process 0 270 450 570 Maltodextrin wet process 570 300 120 0 Whey Protein Concentrate 50 60 68 70 Microcrystalline Cellulose 7.67 7 8 8 Galactomannan 35 40 40 45 Inulin 25 27 30 30 Choline chloride 2 2 3 3 Potassium Citrate 5 10 12 15 Sodium Citrate 5 10 12 15 Salt 5 7 7 8 Complex trace minerals 6.8 6.8 6.8 6.8 Hydrogen Phosphate 2 2 3 3
[0248] Comparative Example 1: The compounded trace minerals in Example 4 were deleted, and other ingredients and production process remained unchanged to obtain nutritional powder.
[0249] Comparative Example 2: The oil in Example 4 was deleted, and an emulsifier (lecithin / monoglyceride / diglyceride) was used, while other ingredients and production process remained unchanged to obtain a nutritional powder.
[0250] Comparative Example 3: When mixing the powder with the remaining maltodextrin, wet mixing is adopted, and other production processes remain unchanged to obtain nutritional powder.
[0251] Table 2: Differences between Example 4 and Comparative Examples:
[0252] Nutritional Information Absorption efficiency Oil embedding rate Example 4 99.7% 99.4% 97.2% Comparative Example 1 65.5% 76.4% 96.7% Comparative Example 2 76.7% 97.5% 96.4% Comparative Example 3 71.5% 70.5% 96.2%
[0253] It can be seen from Table 2 that in the absence of compound trace minerals, necessary trace elements will be lacking. Secondly, compound trace minerals can help vasodilation, thereby increasing absorption efficiency. Secondly, when emulsifiers are used instead of oils, they are mainly used to stabilize the emulsified system, but reduce nutritional costs. Secondly, the use of oils can also increase taste and satiety, and the use of emulsifiers, although they can help disperse fat-soluble vitamins, cannot effectively protect them and can easily cause vitamin damage. The use of comparative example 3 will increase production costs. Secondly, it will cause damage to some vitamins. In addition, Example 4 can also achieve a similar oil encapsulation rate by using less raw materials than comparative examples 1-3.
[0254] In summary, the purpose of the wet process of this product is mainly to make vegetable oil into fat powder through processes such as embedding and spray drying. In the wet process, the remaining nutrients except maltodextrin are added in the wet process part, among which protein can help to increase the embedding rate of fat. Vitamins and minerals are low in weight, and the added cost of adding them to the wet process is very small. Micronutrients such as vitamins and minerals are added to the wet part, and after dissolution, emulsification, homogenization, spray drying, etc., the content in the finished product is more uniform than that added by the dry method, and fat-soluble vitamins and water-soluble vitamins are added under nitrogen protection after emulsification. During the whole process, the content of each vitamin is relatively stable, and the loss rate is small. The process loss of vitamin A and vitamin D is about 10%, and there is no loss of other vitamins.
[0255] By combining the dry process with the wet process, certain nutrients are pre-mixed in a wet state and then combined with the dry-mixed nutrients, which significantly improves the mixing uniformity and avoids the problem of uneven mixing in the dry process. When adding water to dissolve, the dissolution speed is faster due to more uniform mixing, and the liquid stability after dissolution is better, which solves the problems of poor solubility and insufficient stability in the dry process. Secondly, compared with the traditional wet process, the dry-wet composite process may reduce the dependence on high-cost equipment, such as spray drying, thereby reducing the overall production cost.
[0256] By adding complex trace minerals and using magnesium sulfate, it helps vasodilation, and magnesium sulfate works together with calcium sulfate to help maintain bone strength and density. Secondly, the use of oils and fats provides the human body with essential fatty acids, and when used in combination with fat-soluble vitamins and water-soluble vitamins, it can help the human body absorb fat-soluble vitamins and water-soluble vitamins.
[0257] It should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention rather than to limit it. Although the present invention has been described in detail with reference to the preferred embodiments, those skilled in the art should understand that the technical solutions of the present invention can be modified or replaced by equivalents without departing from the spirit and scope of the technical solutions of the present invention, which should all be included in the scope of the present invention.
Claims
1. A dry-wet composite process for a complete nutrient powder, characterized in that: The following steps are included: Add purified water and casein into a mixing device, stir through the mixing device, and then add nutrients until stirring is sufficient or reaches a predetermined time to obtain a mixed solution; The oil is heated, and after the oil temperature reaches a preset value, purified water and succinic acid monoglyceride are added, and then stirred to obtain an oil-water emulsion; The mixed solution and the oil-water emulsion are mixed together and emulsified to obtain an emulsion; Dissolve fat-soluble vitamins and water-soluble vitamins in purified water, and then add them to the emulsion to make a fixed volume; The fixed volume liquid is homogenized, sterilized and spray-dried to obtain a powder; The powder is mixed with the remaining maltodextrin to obtain a nutritional powder.
2. The dry-wet composite process of the complete nutrient powder according to claim 1, characterized in that: When the purified water and casein are mixed, the temperature of the mixing equipment is set to 30-65°C and the stirring time is 10-50 minutes; Among them, the ratio of purified water to casein is 6:4; After adding nutrients, the mixing equipment is set to a temperature of 30-65°C and a stirring time of 5-25 minutes.
3. The dry-wet composite process of the complete nutrient powder according to claim 2, characterized in that: The nutrients include the following components by weight: Concentrated whey protein 50-70g, microcrystalline cellulose 6-8g, galactomannan 35-45g, inulin 25-30g, maltodextrin 0-570g, choline chloride 2-3g, potassium citrate 5-15g, sodium citrate 5-15g, edible salt 5-8g, complex trace minerals 6.8g, and hydrogen phosphate 2-3g.
4. The dry-wet composite process of the complete nutrient powder according to claim 3, characterized in that: The compound trace minerals include the following components by weight: Magnesium sulfate 1.6-2.4g, ferrous sulfate 0.8-1.2g, zinc sulfate 0.8-1.2g, copper sulfate 0.2-0.6g, manganese sulfate 0.1-0.3g, potassium iodide 0.05-0.15g, sodium selenite 0.05-0.15g.
5. The dry-wet composite process of the complete nutrient powder according to claim 4, characterized in that: The oils include sunflower oil, medium chain triglycerides and low-erucic acid rapeseed oil; wherein, Sunflower oil accounts for 0.1-0.4; The proportion of medium-chain triglycerides is 0.2-0.5; The proportion of low-erucic acid rapeseed oil is 0.4-0.
5.
6. The dry-wet composite process of the complete nutrient powder according to claim 5, characterized in that: When heating the grease, stir it with a stirring device, and set the preset value of the oil temperature to 50-80°C; When purified water and succinic acid monoglyceride are added to the oil, the proportion of purified water is 1%, the proportion of succinic acid monoglyceride is 1-8%, and stirring is performed by a stirring device, and the stirring time is set to 5-40 minutes.
7. The dry-wet composite process of the complete nutrient powder according to claim 6, characterized in that: The preparation steps of the emulsion are: The air in the emulsification tank is discharged by nitrogen purging, and then nitrogen is filled into the emulsification tank for gas replacement; Add the mixed solution and the oil-water emulsion into an emulsification tank; Turn on the stirring equipment, perform emulsification operation, and set the temperature to 30-65℃.
8. The dry-wet composite process of the complete nutrient powder according to claim 7, characterized in that: When dissolving fat-soluble vitamins in purified water, add a cosolvent to the purified water; The cosolvent is lecithin or glyceride; The fat-soluble vitamins include the following components by weight: Vitamin A: 900 μg; Vitamin D: 15-20 μg; Vitamin E: 10 mg; The water-soluble vitamins include the following components by weight: Vitamin B1: 1.1 mg; Vitamin B2: 1.3 mg; Vitamin B3: 16 mg; Vitamin B5: 5 mg; Vitamin B6: 1.3-1.7 mg; Vitamin B7: 30 μg; Vitamin B9: 400μg.
9. The dry-wet composite process of the complete nutrient powder according to claim 8, characterized in that: The liquid after volume adjustment is homogenized twice, wherein the first homogenization pressure is 100-300 bar and the second homogenization pressure is 30-60 bar; After the secondary homogenization treatment, the liquid is input into the sterilizer and sterilized at a temperature of 75-85°C for 25-40 seconds. After sterilization, the water in the liquid is removed by an evaporator to increase the solid content and the density of the liquid until the density of the liquid reaches 1.07-1.15; The concentrated liquid is spray-dried to form a powdery product to obtain a powder.
10. The dry-wet compounding process of the complete nutrient powder according to claim 9, characterized in that: When mixing the powder with the remaining maltodextrin, set the mixing time to 15-45 minutes and the speed to 45-120 revolutions per minute.
Citation Information
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