Preparation method and application of composite nicotine salt and electronic tobacco tar

Abstract

The invention relates to a preparation method and application of composite nicotine salt and electronic tobacco tar. The composite nicotine salt is prepared from the following raw materials: 40-60 parts by weight of organic acid and 40-60 parts by weight of nicotine; and the organic acid is composed of benzoic acid, linolenic acid, linoleic acid, citric acid, malic acid, ascorbic acid and other organic acids. According to the organic acid disclosed by the invention, the irritation of the nicotine can be remarkably reduced through an appropriate proportion, the formed nicotine salt generates fragrance similar to the combusted natural tobacco during smoking, the nicotine salt is proportioned with a proper diluent, the diluent is composed of glycerol, propylene glycol, squalene and squalane,and the electronic tobacco tar is prepared and can be directly applied to electronic cigarette atomizers. According to the preparation method and the application in the invention, the fragrance of thecomposite nicotine salt is closer to that of the traditional cigarette, the smoking addiction relief effect is better, and the use safety is higher.

Description

technical field

[0001] The invention belongs to the technical field of electronic cigarettes, and in particular relates to a preparation method and application of electronic cigarette oil compounded with nicotine salt solution. Background technique

[0002] E-cigarettes are electronic products that mimic cigarettes and have the same look, smoke, taste and feel as cigarettes. It is a product that allows users to inhale after turning liquid nicotine salt into steam by means of atomization. The structure of e-cigarette mainly includes three parts: a pipe containing liquid nicotine salt, an evaporator and a battery. The liquid nicotine salt electronic cigarette oil is the key to the smoking quality of electronic cigarettes, and the existing liquid nicotine salt has unsatisfactory fragrance after smoking, effect of relieving smoking addiction and safety of use. Contents of the invention

[0003] In order to solve the above-mentioned problems in the prior art, the present inve...

Examples

Embodiment 1

[0019] This embodiment provides a compound nicotine salt. The raw material components include: 500g of organic acid and 500g of nicotine base. %, citric acid 9%, malic acid 10%, ascorbic acid 1%.

[0020] Further, a method for preparing the compound nicotine salt is provided, comprising the steps of: mixing 100 g of benzoic acid, 50 g of linolenic acid, 250 g of linoleic acid, 45 g of citric acid, 50 g of malic acid, and 5 g of ascorbic acid according to the above mass ratio to obtain a mixed Material S1; mix 250g squalene and 250g squalane uniformly at 1:1 to obtain mixture S2; pour mixture S2 into mixture S1, then add 500g of nicotine base, 250g of glycerol and propylene glycol, and heat Heat to 50°C, stir while heating to fully react, the speed of stirring is 50rpm, that is to say.

Embodiment 2

[0022] This embodiment provides a compound nicotine salt. The raw material components include: 400g of organic acid and 600g of nicotine base. %, citric acid 9%, malic acid 10%, ascorbic acid 1%.

[0023] Further, a method for preparing the compound nicotine salt is provided, comprising the steps of: mixing 80 g of benzoic acid, 40 g of linolenic acid, 200 g of linoleic acid, 36 g of citric acid, 40 g of malic acid, and 4 g of ascorbic acid according to the above mass ratio to obtain a mixed Material S1; mix 250g squalene and 250g squalane uniformly at 1:1 to obtain mixture S2; pour mixture S2 into mixture S1, then add 600g of nicotine base, 250g of glycerol and propylene glycol, and heat Heat to 50°C, stir while heating to fully react, the speed of stirring is 50rpm, that is to say.

Embodiment 3

[0025] This embodiment provides a compound nicotine salt, the raw material components include: 600g of organic acid, 400g of nicotine base, the organic acid is composed of the following components in mass percentage: 20% of benzoic acid, 10% of linolenic acid, 50% of linoleic acid %, citric acid 9%, malic acid 10%, ascorbic acid 1%.

[0026] Further, a method for preparing the compound nicotine salt is provided, comprising the steps of: mixing 120 g of benzoic acid, 60 g of linolenic acid, 600 g of linoleic acid, 54 g of citric acid, 60 g of malic acid, and 6 g of ascorbic acid according to the above mass ratio to obtain a mixed Material S1; mix 250g squalene and 250g squalane uniformly at 1:1 to obtain mixture S2; pour mixture S2 into mixture S1, then add 400g of nicotine base, 250g of glycerol and propylene glycol, and heat Heat to 50°C, stir while heating to fully react, the speed of stirring is 50rpm, that is to say.

technical field

[0001] The invention belongs to the technical field of electronic cigarettes, and in particular relates to a preparation method and application of electronic cigarette oil compounded with nicotine salt solution. Background technique

[0002] E-cigarettes are electronic products that mimic cigarettes and have the same look, smoke, taste and feel as cigarettes. It is a product that allows users to inhale after turning liquid nicotine salt into steam by means of atomization. The structure of e-cigarette mainly includes three parts: a pipe containing liquid nicotine salt, an evaporator and a battery. The liquid nicotine salt electronic cigarette oil is the key to the smoking quality of electronic cigarettes, and the existing liquid nicotine salt has unsatisfactory fragrance after smoking, effect of relieving smoking addiction and safety of use. Contents of the invention

[0003] In order to solve the above-mentioned problems in the prior art, the present inve...

Examples

Embodiment 1

[0019] This embodiment provides a compound nicotine salt. The raw material components include: 500g of organic acid and 500g of nicotine base. %, citric acid 9%, malic acid 10%, ascorbic acid 1%.

[0020] Further, a method for preparing the compound nicotine salt is provided, comprising the steps of: mixing 100 g of benzoic acid, 50 g of linolenic acid, 250 g of linoleic acid, 45 g of citric acid, 50 g of malic acid, and 5 g of ascorbic acid according to the above mass ratio to obtain a mixed Material S1; mix 250g squalene and 250g squalane uniformly at 1:1 to obtain mixture S2; pour mixture S2 into mixture S1, then add 500g of nicotine base, 250g of glycerol and propylene glycol, and heat Heat to 50°C, stir while heating to fully react, the speed of stirring is 50rpm, that is to say.

Embodiment 2

[0022] This embodiment provides a compound nicotine salt. The raw material components include: 400g of organic acid and 600g of nicotine base. %, citric acid 9%, malic acid 10%, ascorbic acid 1%.

[0023] Further, a method for preparing the compound nicotine salt is provided, comprising the steps of: mixing 80 g of benzoic acid, 40 g of linolenic acid, 200 g of linoleic acid, 36 g of citric acid, 40 g of malic acid, and 4 g of ascorbic acid according to the above mass ratio to obtain a mixed Material S1; mix 250g squalene and 250g squalane uniformly at 1:1 to obtain mixture S2; pour mixture S2 into mixture S1, then add 600g of nicotine base, 250g of glycerol and propylene glycol, and heat Heat to 50°C, stir while heating to fully react, the speed of stirring is 50rpm, that is to say.

Embodiment 3

[0025] This embodiment provides a compound nicotine salt, the raw material components include: 600g of organic acid, 400g of nicotine base, the organic acid is composed of the following components in mass percentage: 20% of benzoic acid, 10% of linolenic acid, 50% of linoleic acid %, citric acid 9%, malic acid 10%, ascorbic acid 1%.

[0026] Further, a method for preparing the compound nicotine salt is provided, comprising the steps of: mixing 120 g of benzoic acid, 60 g of linolenic acid, 600 g of linoleic acid, 54 g of citric acid, 60 g of malic acid, and 6 g of ascorbic acid according to the above mass ratio to obtain a mixed Material S1; mix 250g squalene and 250g squalane uniformly at 1:1 to obtain mixture S2; pour mixture S2 into mixture S1, then add 400g of nicotine base, 250g of glycerol and propylene glycol, and heat Heat to 50°C, stir while heating to fully react, the speed of stirring is 50rpm, that is to say.

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