A kind of smoking particles for heating cigarettes and preparation method thereof
By using natural inorganic mineral particles as the core and the core-shell structure of the composite functional layer outside, the existing heating cigarette suction particles have not high thermal conductivity and easy disintegration, achieving better suction taste and stability, which is suitable for industrial promotion.
Patent Information
- Application Number
- CN202110432291.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2021-04-21
- Publication Date
- 2025-04-22
- Estimated Expiration
- 2041-04-21
AI Technical Summary
The suction particles of existing heated cigarettes are not thermally conductive and easily disintegrate, resulting in poor suction taste.
Natural inorganic mineral particles are used as the core and the core-shell structure of the outer composite functional layer, and the use of adhesives, smoke agents, functional fragrances and auxiliary materials to form suction particles with good thermal conductivity.
It improves the suction taste of the heated cigarette, has good stability, is not easy to disintegrate, and is simple to control costs, which is suitable for industrial promotion.
Abstract
Description
Technical Field
[0001] The present invention relates to the technical field of heated cigarettes, and in particular to a smoking particle for heated cigarettes and a preparation method thereof. Background Art
[0002] Heat-not-burn cigarettes are a type of cigarette made by heating tobacco materials with electronic heating equipment without burning them. During the smoking process, no open flame is used, and tobacco is heated by a special heating source. When heated, nicotine and other substances in the tobacco evaporate to produce smoke to meet the needs of smokers. When smoking this type of cigarette, consumers can not only feel the aroma of tobacco, but also significantly reduce the harmful substances produced by high-temperature pyrolysis of conventional cigarettes during combustion, thus providing consumers with an effective and healthy way to smoke, which is increasingly favored by consumers.
[0003] At present, the main products of heated cigarette cartridges are reconstituted tobacco leaves and smoking particles. The main components of reconstituted tobacco leaves are tobacco powder, adhesives, humectants (propylene glycol and glycerin), enhancers, water, fiber and blended flavors. The finished reconstituted tobacco leaves generally maintain a high moisture content. During the smoking process, the tobacco segment is heated at high temperature. The first thing released is high-temperature water vapor, as well as a small amount of coated tobacco extracts and other characteristic volatile substances, which causes the smoking temperature to be too high and bland. Most of the existing smoking particles use plant-based carriers, which are compounded with tobacco powder, flavors, etc. outside the carrier. However, the plant-based carriers not only have low thermal conductivity, but are also prone to disintegration during the heating process, affecting the smoking taste. Summary of the invention
[0004] In view of the above problems, the purpose of the present invention is to disclose a smoking particle for heated cigarettes and a preparation method thereof, which uses natural inorganic mineral particles as the core, has good thermal conductivity and is not easy to disintegrate. The loaded smoke-generating agent and functional fragrance are heated evenly, which can greatly improve the smoking taste of the heated cigarettes. The preparation method is simple, which is conducive to cost control and is conducive to industrial promotion and use.
[0005] Specifically, the smoking particles for heated cigarettes of the present invention have a core-shell structure with 30-50 mesh natural inorganic mineral particles as the core and a functional layer compounded outside the core.
[0006] Furthermore, the raw materials of the functional layer include: adhesive, smoke generating agent, functional fragrance and auxiliary materials.
[0007] Furthermore, the auxiliary material is one or more of 80-120 mesh natural inorganic mineral particles, tobacco powder, and natural plant powder.
[0008] Furthermore, the functional aroma materials include tobacco extracts, natural plant extracts and related synthetic flavors, etc. The style characteristics of the functional aroma materials include flue-cured tobacco aroma, air-dried tobacco aroma, fresh fragrance, fruity aroma, spicy aroma, woody aroma, green aroma, floral aroma, herbal aroma, bean aroma, cocoa aroma, milk aroma, paste aroma, baked aroma, sweet aroma, etc. as well as other configurable style characteristics.
[0009] Furthermore, the natural inorganic mineral particles are silica-containing mineral particles.
[0010] Furthermore, the natural inorganic mineral particles are any one of river sand, sea sand and mountain sand.
[0011] In addition, the present invention also discloses a method for preparing the above-mentioned smoking particles for heated cigarettes, and the preparation method comprises the following steps:
[0012] S1: Take natural inorganic mineral particles, sieve out natural inorganic mineral particles of 30-50 mesh and 80-120 mesh, wash them clean, and dry them for later use;
[0013] S2: prepare adhesive and functional material, pre-mix the adhesive, and preheat to 40-60°C for standby use;
[0014] S3: Take 30-50 mesh natural inorganic mineral particles and place them in a tray, dry them at 40-60°C for 15-30 minutes, then add them to the disc while they are still hot, spray the adhesive while the disc is rotating, stir them evenly, then add the smoke generating agent, and stir and mix them evenly;
[0015] S4: spraying functional aroma into the rotating disc and stirring to mix;
[0016] S5: Add auxiliary materials to the rotating disc and stir to mix;
[0017] S6: repeat steps S4 and S5, and add a total mass of functional fragrance of 20%-40% of the mass of 30-50 mesh natural inorganic mineral particles, and a total mass of auxiliary materials of 40%-60% of the mass of 30-50 mesh natural inorganic mineral particles;
[0018] S6: Add 1-2 times the mass of 30-50 mesh natural inorganic mineral particles, roll into particles, and bake at 90-105°C for 10-20 minutes;
[0019] S7: Screen the dried particles, select particles with a particle size of 20-30 mesh, and obtain suction particles.
[0020] Furthermore, in the step S3, the mass of the added binder is 1%-6% of the mass of the 30-50 mesh natural inorganic mineral particles, and the mass of the smoke generating agent is 1%-15% of the mass of the 30-50 mesh natural inorganic mineral particles.
[0021] Furthermore, in the step S4, the mass of the added functional fragrance is 2.0%-15% of the mass of the 30-50 mesh natural inorganic mineral particles.
[0022] Furthermore, in the step S5, the mass of the auxiliary material added is 5.0%-20% of the mass of the 30-50 mesh natural inorganic mineral particles.
[0023] Furthermore, the adhesive is a natural adhesive or a composite adhesive, and the composite adhesive includes component A and component B in a mass ratio of 1:(2-8), the component A is a chitosan compound, and the component B is one or more of hydroxymethyl methylcellulose, hydroxypropyl methylcellulose, and hydroxyethyl methylcellulose.
[0024] Furthermore, the adhesive is pre-prepared in step S2 as follows: the adhesive and the smoke generating agent are stirred and mixed at a mass ratio of 1:(8-12), heated in a water bath to a temperature of 40-60° C., and stirred for 15-30 minutes.
[0025] Furthermore, the smoke generating agent is one or more of glycerol and modified glycerol, wherein the modified glycerol can be any existing smoke generating agent, and thus will not be described in detail.
[0026] Beneficial effects of the present invention:
[0027] 1. The present invention discloses a smoking particle for heated cigarettes, which uses natural inorganic mineral particles as the core, has good thermal conductivity, and the loaded smoke-generating agent and functional material fragrance are heated evenly, which can improve the smoking taste of heated cigarettes to a greater extent.
[0028] 2. The smoking particles for heated cigarettes of the present invention are stable in nature and are not prone to disintegration during the smoking and heating process, so they will not bring extra flavor to the smoke and will not affect the taste of the smoke.
[0029] 3. The smoking particles for heated cigarettes of the present invention use natural inorganic mineral particles, which have a heavy specific gravity, are easier to granulate, have a wide source, and a simple preparation process, which is conducive to cost control and is suitable for industrial promotion and use. DETAILED DESCRIPTION
[0030] The present invention will be described in detail below with reference to specific embodiments:
[0031] The invention discloses a smoking particle for heating cigarettes. The smoking particle has a core-shell structure with 30-50 mesh natural inorganic mineral particles as the core and a functional layer compounded outside the core.
[0032] The details are as follows: Embodiment 1
[0033] S1: Take river sand, grind it, pass it through a sieve, and sieve out 40-mesh and 100-mesh river sand particles respectively. After washing it with clean water, dry it at 100℃ for later use.
[0034] S2: prepare adhesive and functional material fragrance;
[0035] The adhesive of this embodiment is specifically prepared as follows: weigh 1g of chitosan into a beaker, add 5g of hydroxypropyl methylcellulose, and add 60g of glycerol, heat in a 50°C water bath with stirring for 20min, and set aside;
[0036] The functional fragrance of this embodiment is tobacco extract, and the amount used is 30g.
[0037] S3: Take 30g of 40-mesh river sand particles and place them in a tray, dry them at 60°C for 20min, then add them to the disc while they are still hot, spray 1.3g of adhesive while the disc is rotating, stir evenly, add 3g of glycerin, and stir to mix;
[0038] S4: Spray 3.4 g of tobacco extract into the rotating disc and stir to mix;
[0039] S5: Add 5 g of 100 mesh river sand particles into the rotating disc and stir to mix;
[0040] S6: repeat steps S4 and S5, adding a total of 10.2 g of tobacco extract and 15 g of 100-mesh river sand particles;
[0041] S6: Add 45g of 100-mesh river sand particles, roll into particles, and bake at 95°C for 10 minutes;
[0042] S7: Sieve the dried particles to select a particle size of 20-30 mesh to obtain suction particles. Embodiment 2
[0043] S1: Take sea sand, pass it through a sieve, and separate out 30-mesh and 80-mesh sea sand particles, wash them with clean water, dry them at 100°C for later use, and crush and screen out 80-mesh bamboo particles.
[0044] S2: prepare adhesive and functional material fragrance;
[0045] The adhesive of this embodiment is specifically prepared as follows: weigh 1g of chitosan into a beaker, add 5g of hydroxymethyl methylcellulose, and add 60g of glycerol, heat in a 60°C water bath with stirring for 30min, and set aside;
[0046] The functional fragrance of this embodiment is a natural plant extract, and the dosage is 30g.
[0047] S3: Take 30g of 30-mesh sea sand particles and place them in a tray, dry them at 50°C for 15min, then add them to the disc while they are still hot, spray 0.8g of adhesive while the disc is rotating, stir evenly, add 4g of glycerin, and stir to mix;
[0048] S4: Spray 4.2 g of natural plant extract into the rotating disc and stir to mix;
[0049] S5: Add 6 g of 100 mesh sea sand particles into the rotating disc and stir to mix;
[0050] S6: repeat steps S4 and S5, adding a total of 12.6 g of tobacco extract and 18 g of 100-mesh sea sand particles;
[0051] S6: add 15g of 100-mesh sea sand particles and 15g of 100-mesh bamboo particles, roll into particles, and bake at 90°C for 20min;
[0052] S7: Sieve the dried particles to select a particle size of 20-30 mesh to obtain suction particles Embodiment 3
[0053] S1: Take mountain sand, sieve it through a sieve, and separate out mountain sand particles of 50 mesh and 120 mesh respectively. After washing with clean water, dry it at 100℃ for later use.
[0054] S2: prepare adhesive and functional material fragrance;
[0055] The adhesive of this embodiment is specifically prepared as follows: weigh 1g of chitosan into a beaker, add 4g of hydroxypropyl methylcellulose, 2g of hydroxyethyl methylcellulose, and 75g of glycerol, and heat in a 40°C water bath with stirring for 30min for later use;
[0056] The functional fragrance of this embodiment is tobacco extract, and the amount used is 30g.
[0057] S3: Take 30g of 50-mesh mountain sand particles and place them in a tray, dry them at 40°C for 30min, then add them to the disc while they are still hot, spray 1.0g of adhesive while the disc is rotating, stir evenly, add 2.8g of glycerin, and stir to mix;
[0058] S4: Spray 3.8 g of tobacco extract into the rotating disc and stir to mix;
[0059] S5: Add 4 g of 100 mesh sand particles into the rotating disc and stir to mix;
[0060] S6: repeat steps S4 and S5, adding a total of 11.4 g of tobacco extract and 12 g of 100 mesh mountain sand particles;
[0061] S6: add 55g of 100-mesh mountain sand particles, roll into particles, and bake at 105°C for 15 minutes;
[0062] S7: Sieve the dried particles to select a particle size of 20-30 mesh to obtain suction particles.
[0063] The above embodiments are only used to illustrate the technical solutions of the present invention and are not intended to limit the present invention. Although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the technical solutions of the present invention may be modified or replaced by equivalents without departing from the purpose and scope of the technical solutions of the present invention, which should be included in the scope of the claims of the present invention. The techniques, shapes, and structural parts not described in detail in the present invention are all known technologies.
Claims
1. A smoking particle for heated cigarettes, characterized in that: The suction particles have a core-shell structure with 30-50 mesh natural inorganic mineral particles as the core and a functional layer compounded outside the core; The natural inorganic mineral particles are any one of river sand, sea sand and mountain sand among silica-containing mineral particles; The raw materials of the functional layer include: adhesive, smoke generating agent, functional fragrance and auxiliary materials; The adhesive is a natural adhesive or a composite adhesive, wherein the composite adhesive comprises a component A and a component B in a mass ratio of 1:(2-8), wherein the component A is a chitosan compound, and the component B is one or more of hydroxymethyl methylcellulose, hydroxypropyl methylcellulose, and hydroxyethyl methylcellulose; The functional aroma is one or more of tobacco extract and natural plant extract; The auxiliary material is one or more of 80-120 mesh natural inorganic mineral particles, tobacco powder, and natural plant powder.
2. The method for preparing smoking particles for heated cigarettes according to claim 1, characterized in that: The preparation method comprises the following steps: S1: Take natural inorganic mineral particles, sieve out natural inorganic mineral particles of 30-50 mesh and 80-120 mesh, wash them clean, and dry them for later use; S2: prepare adhesive and functional material, pre-mix the adhesive, and preheat to 40-60°C for standby use; S3: Take 30-50 mesh natural inorganic mineral particles and place them in a tray, dry them at 40-60°C for 15-30 minutes, then add them to the disc while they are still hot, spray the adhesive while the disc is rotating, stir them evenly, then add the smoke generating agent, and stir and mix them evenly; S4: spraying functional aroma into the rotating disc and stirring to mix; S5: Add auxiliary materials to the rotating disc and stir to mix; S6: repeat steps S4 and S5, and add a total mass of functional fragrance of 20%-40% of the mass of 30-50 mesh natural inorganic mineral particles, and a total mass of auxiliary materials of 40%-60% of the mass of 30-50 mesh natural inorganic mineral particles; S6: Add 1-2 times the mass of 30-50 mesh natural inorganic mineral particles, roll into particles, and bake at 90-105°C for 10-20 minutes; S7: Screen the dried particles, select particles with a particle size of 20-30 mesh, and obtain suction particles.
3. The method for preparing smoking particles for heated cigarettes according to claim 2, characterized in that: The adhesive is prepared in step S2 as follows: the adhesive and the smoke generating agent are stirred and mixed at a mass ratio of 1:(8-12), heated in a water bath to a temperature of 40-60° C., and stirred for 15-30 minutes.
4. The method for preparing smoking particles for heated cigarettes according to claim 2, characterized in that: The smoke generating agent is one or more of glycerol and modified glycerol.
Citation Information
Patent Citations
Method for preparing a suction material for heating non-burning cigarette by centrifugal granulation
CN108936780A
Heating-non-burning cigarette fuming granular material and preparation method thereof
CN109363230A
Smoking particles for heat-not-burn cigarette and preparation method of smoking particles
CN111887468A
Smokeable element
WO2013045944A2
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