A down quilt fabric capable of preventing insects and mites and its preparation method

By mixing fiber kapok fiber and flax fiber in down duvet fabric and preparing and modifying insect-proof and anti-mites finishing agent, the problem of insufficient anti-drilling and wrinkle properties of existing fabrics is solved, and efficient anti-mite and anti-mite and wrinkle properties are achieved.

CN116289224BActive Publication Date: 2025-07-15GAOFAN (ZHEJIANG) INFORMATION TECH CO LTD
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Patent Information

Application Number
CN202310281832.4
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2023-03-22
Publication Date
2025-07-15
Estimated Expiration
2043-03-22

AI Technical Summary

Technical Problem

After the existing down quilt fabrics are treated with insects and mites, the anti-drilling and anti-wrinkle properties are insufficient, resulting in the down being easily drilled out of the fabric, affecting its use and aesthetics.

Method used

After using kapok fiber and flax fiber mixed fiber, insect-proof and mite-proof finishing agents containing polyglutamic acid, alkyl sulfonate, fatty acid polyol esters, tea saponin, dodecyl dimethylbenzyl ammonium chloride, ethylenediamine diohydroxyphenyl sodium ferric acetate, nanosilver, polyethylene oxide and hexamethyl melamine hexamethyl ether were prepared, and the insect-proof and mite-proof finishing agents were formed by ionizing radiation treatment, combined with nano-scale diatomaceous earth modification treatment loaded with sulfonated phenolic resin.

Benefits of technology

It significantly improves the wrinkle deformation resistance and drilling quilt resistance of the fabric, while maintaining good anti-insect and mites, ensuring the normal use of the down quilt.

✦ Generated by Eureka AI based on patent content.

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Patent Text Reader

Abstract

The present invention discloses a fabric for a duvet that can prevent insects and mites and a preparation method thereof, including blending fibers; weaving; adding alkyl sulfonate and fatty acid polyol ester to polyglutamic acid, heating and then grinding, stirring until dissolved, then adding tea saponin, dodecyl dimethyl benzyl ammonium chloride, sodium ethylenediamine di(o-hydroxyphenyl) acetate ferrate and nano silver, subjecting to ionization radiation treatment after sufficient mixing, and then adding polyethylene oxide and hexahydroxymethylmelamine hexamethyl ether, and obtaining an insect and mite prevention finishing agent after mixing evenly; impregnating and rolling the fabric. For the fabric for a duvet that can prevent insects and mites and the preparation method thereof according to the present invention, nano-level diatomite carrying sulfonated phenolic resin is used to modify the prepared insect and mite prevention finishing agent, which can greatly improve the anti-wrinkle and deformation resistance and anti-feather leakage performance of the fabric while ensuring the insect and mite prevention effect of the fabric, and ensure the normal use of the duvet.
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Description

Technical Field

[0001] The present invention relates to the technical field of duvet fabrics, and particularly relates to an insect-proof and mite-proof duvet fabric and a preparation method thereof. Background Art

[0002] A duvet consists of a core and a fabric. The filling of the core is mainly down. Since the chemical composition of down is a kind of protein and accompanied by animal fat, even after degreasing and washing processes in the pretreatment, the fat and bacteria cannot be completely removed. Therefore, it is necessary to perform insect-proof and mite-proof treatments on the duvet fabric to prevent insects and mites from breeding on the fabric surface or even damaging the internal down through the fabric. Although the existing duvet fabrics have certain insect-proof and mite-proof effects after the treatment, the anti-feather leakage performance and anti-wrinkle performance of the duvet fabrics after the insect-proof and mite-proof treatment still cannot be guaranteed, resulting in the internal filled down being extremely easy to drill out from the fabric, affecting the normal use and aesthetic degree of the duvet. Summary of the Invention

[0003] The main purpose of the present invention is to provide an insect-proof and mite-proof duvet fabric and a preparation method thereof, which can effectively solve the problems in the background art.

[0004] To achieve the above purpose, the technical solution adopted by the present invention is as follows:

[0005] The present invention provides an insect-proof and mite-proof duvet fabric and a preparation method thereof, including the following steps:

[0006] Step S1, fiber blending: Blend kapok fiber and flax fiber in a mass ratio of 1:1.5, and then process them through the processes of blowing, carding, drawing, roving, and spinning to make a blended yarn.

[0007] Step S2, weaving: Weave the blended yarn into a grey fabric by warp and weft knitting, and set it aside.

[0008] Step S3, preparing an insect-proof and mite-proof finishing agent: Add alkyl sulfonate and fatty acid polyol ester to polyglutamic acid, heat it up and then grind it, stir until dissolved, then add saponin, dodecyl dimethyl benzyl ammonium chloride, sodium ferric ethylenediamine di-o-hydroxyphenyl acetate, and nano-silver, mix them fully and then perform ionization radiation treatment, and then add polyethylene oxide and hexamethylol melamine hexamethyl ether, and mix them evenly to obtain the insect-proof and mite-proof finishing agent.

[0009] Step S4, fabric padding: Pad the grey fabric in the insect-proof and mite-proof finishing agent, dry it after impregnation, and then obtain the insect-proof and mite-proof duvet fabric after washing, dehydration, and drying.

[0010] As a further optimization solution of the present invention, the insect and mite proofing agent in step S3 is composed of the following components in parts by weight: 12-15 parts of polyglutamic acid, 3-5 parts of alkyl sulfonate, 0.6-1 part of fatty acid polyol ester, 1-2 parts of tea saponin, 0.1-0.3 part of dodecyl dimethyl benzyl ammonium chloride, 0.1-0.3 part of sodium ferric ethylenediamine di-o-hydroxyphenyl acetate, 0.1-0.2 part of nano silver, 1.0-1.5 parts of polyethylene oxide, and 0.2-0.5 part of hexahydroxymethyl melamine hexamethyl ether.

[0011] As a further optimization solution of the present invention, the ionizing radiation in step S3 is γ-ray, X-ray or electron beam.

[0012] As a further optimization solution of the present invention, the irradiation dose of the ionizing irradiation is 4k-10kGy.

[0013] As a further optimization solution of the present invention, the temperature is raised to 50-55°C in step S3, and the stirring rate is 300-800 r / min.

[0014] As a further optimization solution of the present invention, step S3 further includes: adding nano-sized diatomaceous earth to deionized water, shaking and dispersing, then adding sulfonated phenolic resin and stirring at high speed to mix, obtaining nano-sized diatomaceous earth loaded with sulfonated phenolic resin, adding the nano-sized diatomaceous earth loaded with sulfonated phenolic resin into the insect and mite proofing agent, mixing and stirring, and then washing and centrifuging with absolute ethanol to obtain a modified insect and mite proofing agent.

[0015] As a further optimization solution of the present invention, in step S3, the modified insect and mite proofing agent is used to replace the insect and mite proofing agent in equal amount.

[0016] As a further optimization solution of the present invention, the weight ratio of sulfonated phenolic resin to nano-sized diatomaceous earth in step S4 is 1:(1.2-1.5).

[0017] As a further optimization solution of the present invention, the weight ratio of nano-sized diatomaceous earth to the insect and mite proofing agent in step S4 is 1:(1.5-2).

[0018] The present invention also provides a duvet fabric that can prevent insects and mites, which is produced by the above preparation method of the duvet fabric.

[0019] Compared with the prior art, the present invention has the following beneficial effects:

[0020] In the present invention, an insect - and mite - proofing finishing agent is obtained by adding alkyl sulfonate and fatty acid polyol ester to polyglutamic acid, mixing it with tea saponin, dodecyl dimethyl benzyl ammonium chloride, sodium ferric ethylenediamine di - o - hydroxyphenyl acetate and nano - silver, polyethylene oxide and hexahydroxymethyl melamine hexamethyl ether, and then subjecting the mixture to ionization radiation treatment. Moreover, nano - sized diatomite carrying sulfonated phenolic resin is used to modify the prepared insect - and mite - proofing finishing agent, which can significantly improve the wrinkle - resistant and deformation - resistant properties and anti - feather - leakage properties of the fabric while ensuring the insect - and mite - proofing effect of the fabric, ensuring the normal use of the duvet and preventing the duvet from wrinkling and deforming. Detailed implementation mode

[0021] The following further describes the present application in detail. It is necessary to point out here that the following specific implementation modes are only used to further illustrate the present application and cannot be understood as limiting the protection scope of the present application. Those skilled in the art can make some non - essential improvements and adjustments to the present application based on the above application content.

[0022] Example 1

[0023] A preparation method of an insect - and mite - proof duvet fabric includes the following steps:

[0024] Step S1, fiber blending: Blend kapok fiber and flax fiber in a mass ratio of 1:1.5, and then process them through the processes of blowing, carding, drawing, roving, and spinning to make a blended yarn.

[0025] Step S2, weaving: Weave the blended yarn into a grey fabric through warp - weft knitting and set it aside.

[0026] Step S3, preparing the insect - and mite - proofing finishing agent: By weight, add 3 parts of alkyl sulfonate and 0.6 parts of fatty acid polyol ester to 12 parts of polyglutamic acid, heat up to 50 - 55 °C and then grind, stir at 300 r / min until dissolved, then add 1 part of tea saponin, 0.1 part of dodecyl dimethyl benzyl ammonium chloride, 0.1 part of sodium ferric ethylenediamine di - o - hydroxyphenyl acetate and 0.1 part of nano - silver, fully mix and then subject it to electron beam ionization radiation treatment. Subsequently, add 1.0 part of polyethylene oxide and 0.2 part of hexahydroxymethyl melamine hexamethyl ether, and mix evenly to obtain the insect - and mite - proofing finishing agent, where the irradiation dose of the ionization irradiation is 4 kGy.

[0027] Step S4, fabric padding: Pad the grey fabric in the insect - and mite - proofing finishing agent, dry it after impregnation, and then obtain the insect - and mite - proof duvet fabric after washing, dehydration, and drying.

[0028] Example 2

[0029] A preparation method of an insect - and mite - proof duvet fabric includes the following steps:

[0030] Step S1, blending, kapok fiber and flax fiber are blended in a mass ratio of 1:1.5, and then processed into blended yarn through the steps of cleaning, carding, drawing, roving and spinning;

[0031] Step S2, weaving, weaving the blended yarn into a grey cloth by warp and weft, and setting aside;

[0032] Step S3, preparing an insect-proof and anti-mite finishing agent, by weight, adding 5 parts of alkyl sulfonate and 0.1 parts of fatty acid polyol ester to 15 parts of polyglutamic acid, heating to 50-55° C. and grinding, stirring at 800 r / min until dissolved, then adding 2 parts of tea saponin, 0.3 parts of dodecyl dimethyl benzyl ammonium chloride, 0.3 parts of ethylenediamine di-o-hydroxyphenyl sodium ferric acetate and 0.2 parts of nano silver, mixing well and subjecting to γ-ray ionizing radiation treatment, then adding 1.5 parts of polyethylene oxide and 0.5 parts of hexahydroxymethyl melamine hexamethyl ether, mixing well to obtain an insect-proof and anti-mite finishing agent, wherein the irradiation dose of ionizing radiation is 10 kGy;

[0033] Step S4, fabric padding, padding the grey fabric into the anti-insect and anti-mite finishing agent, drying after the immersion, and obtaining the anti-insect and anti-mite down quilt fabric after washing, dehydration and drying.

[0034] Example 3

[0035] A method for preparing an insect-proof and mite-proof down quilt fabric comprises the following steps:

[0036] Step S1, blending, kapok fiber and flax fiber are blended in a mass ratio of 1:1.5, and then processed into blended yarn through the steps of cleaning, carding, drawing, roving and spinning;

[0037] Step S2, weaving, weaving the blended yarn into a grey cloth by warp and weft, and setting aside;

[0038] Step S3, preparing an insect-proof and anti-mite finishing agent, by weight, adding 4 parts of alkyl sulfonate and 0.8 parts of fatty acid polyol ester to 14 parts of polyglutamic acid, heating to 50-55° C. and grinding, stirring at 600 r / min until dissolved, then adding 1.5 parts of tea saponin, 0.2 parts of dodecyl dimethyl benzyl ammonium chloride, 0.2 parts of ethylenediamine di-o-hydroxyphenyl sodium ferric acetate and 0.15 parts of nano silver, mixing well and subjecting to X-ray ionizing radiation treatment, then adding 1.3 parts of polyethylene oxide and 0.4 parts of hexamethylol melamine hexamethyl ether, mixing evenly to obtain an insect-proof and anti-mite finishing agent, wherein The irradiation dose of the medium ionizing irradiation is 7 kGy, the nano-diatomaceous earth is added to deionized water and shaken for dispersion, and then the sulfonated phenolic resin is added and stirred at high speed to obtain the nano-diatomaceous earth loaded with the sulfonated phenolic resin, the nano-diatomaceous earth loaded with the sulfonated phenolic resin is added to the insect-proof and mite-proof finishing agent, and after mixing and stirring, it is washed and centrifuged with anhydrous ethanol to obtain a modified insect-proof and mite-proof finishing agent, and the modified insect-proof and mite-proof finishing agent is used to replace the insect-proof and mite-proof finishing agent in an equal amount, wherein the weight ratio of the sulfonated phenolic resin to the nano-diatomaceous earth is 1:1.2, and the weight ratio of the nano-diatomaceous earth to the insect-proof and mite-proof finishing agent is 1:1.5;

[0039] Step S4, fabric padding, padding the grey fabric into the anti-insect and anti-mite finishing agent, drying after the immersion, and obtaining the anti-insect and anti-mite down quilt fabric after washing, dehydration and drying.

[0040] Example 4

[0041] A method for preparing an insect-proof and mite-proof down quilt fabric comprises the following steps:

[0042] Step S1, blending, kapok fiber and flax fiber are blended in a mass ratio of 1:1.5, and then processed into blended yarn through the steps of cleaning, carding, drawing, roving and spinning;

[0043] Step S2, weaving, weaving the blended yarn into a grey cloth by warp and weft, and setting aside;

[0044] Step S3, preparing an insect-proof and anti-mite finishing agent, by weight, adding 4 parts of alkyl sulfonate and 0.8 parts of fatty acid polyol ester to 14 parts of polyglutamic acid, heating to 50-55° C. and grinding, stirring at 600 r / min until dissolved, then adding 1.5 parts of tea saponin, 0.2 parts of dodecyl dimethyl benzyl ammonium chloride, 0.2 parts of ethylenediamine di-o-hydroxyphenyl sodium ferric acetate and 0.15 parts of nano silver, mixing well and subjecting to X-ray ionizing radiation treatment, then adding 1.3 parts of polyethylene oxide and 0.4 parts of hexahydroxymethyl melamine hexamethyl ether, mixing evenly to obtain an insect-proof and anti-mite finishing agent , wherein the irradiation dose of the ionizing radiation is 7 kGy, after adding the nano-diatomaceous earth into deionized water and shaking and dispersing, the sulfonated phenolic resin is added and mixed at a high speed to obtain the nano-diatomaceous earth loaded with the sulfonated phenolic resin, the nano-diatomaceous earth loaded with the sulfonated phenolic resin is added into the insect-proof and anti-mite finishing agent, after mixing and stirring, the modified insect-proof and anti-mite finishing agent is washed and centrifuged with anhydrous ethanol to obtain the modified insect-proof and anti-mite finishing agent, and the insect-proof and anti-mite finishing agent is replaced with an equal amount of the modified insect-proof and anti-mite finishing agent, wherein the weight ratio of the sulfonated phenolic resin to the nano-diatomaceous earth is 1:1.5, and the weight ratio of the nano-diatomaceous earth to the insect-proof and anti-mite finishing agent is 1:2;

[0045] Step S4, fabric padding, padding the grey fabric into the anti-insect and anti-mite finishing agent, drying after the immersion, and obtaining the anti-insect and anti-mite down quilt fabric after washing, dehydration and drying.

[0046] Example 5

[0047] A method for preparing an insect-proof and mite-proof down quilt fabric comprises the following steps:

[0048] Step S1, blending, kapok fiber and flax fiber are blended in a mass ratio of 1:1.5, and then processed into blended yarn through the steps of cleaning, carding, drawing, roving and spinning;

[0049] Step S2, weaving, weaving the blended yarn into a grey cloth by warp and weft, and setting aside;

[0050] Step S3, preparing an insect-proof and anti-mite finishing agent, by weight, adding 4 parts of alkyl sulfonate and 0.8 parts of fatty acid polyol ester to 14 parts of polyglutamic acid, heating to 50-55° C. and grinding, stirring at 600 r / min until dissolved, then adding 1.5 parts of tea saponin, 0.2 parts of dodecyl dimethyl benzyl ammonium chloride, 0.2 parts of ethylenediamine di-o-hydroxyphenyl sodium ferric acetate and 0.15 parts of nano silver, mixing well and subjecting to X-ray ionizing radiation treatment, then adding 1.3 parts of polyethylene oxide and 0.4 parts of hexamethylol melamine hexamethylene ether, mixing evenly to obtain an insect-proof and anti-mite finishing agent, wherein the irradiation dose of the ionizing radiation is 7 kGy, after adding the nano-diatomaceous earth into deionized water and shaking and dispersing, the sulfonated phenolic resin is added and mixed at a high speed to obtain the nano-diatomaceous earth loaded with the sulfonated phenolic resin, the nano-diatomaceous earth loaded with the sulfonated phenolic resin is added into the insect-proof and anti-mite finishing agent, after mixing and stirring, the modified insect-proof and anti-mite finishing agent is washed and centrifuged with anhydrous ethanol to obtain the modified insect-proof and anti-mite finishing agent, and the insect-proof and anti-mite finishing agent is replaced with an equal amount of the modified insect-proof and anti-mite finishing agent, wherein the weight ratio of the sulfonated phenolic resin to the nano-diatomaceous earth is 1:1.4, and the weight ratio of the nano-diatomaceous earth to the insect-proof and anti-mite finishing agent is 1:1.8;

[0051] Step S4, fabric padding, padding the grey fabric into the anti-insect and anti-mite finishing agent, drying after the immersion, and obtaining the anti-insect and anti-mite down quilt fabric after washing, dehydration and drying.

[0052] Comparative Example 1

[0053] A method for preparing an insect-proof and mite-proof down quilt fabric comprises the following steps:

[0054] Step S1, blending, kapok fiber and flax fiber are blended in a mass ratio of 1:1.5, and then processed into blended yarn through the steps of cleaning, carding, drawing, roving and spinning;

[0055] Step S2, weaving, weaving the blended yarn into a grey cloth by warp and weft, and setting aside;

[0056] Step S3: Prepare the insect - and mite - proofing finishing agent. By weight, heat 18.8 parts of polyglutamic acid to 50 - 55 °C and then grind it. Stir at 600 r / min until dissolved, and then add 1.5 parts of saponin, 0.2 parts of dodecyldimethylbenzylammonium chloride, 0.2 parts of sodium ethylene diamine di - o - hydroxyphenyl acetic acid ferrate, and 0.15 parts of nano - silver. Subsequently, add 1.3 parts of polyethylene oxide and 0.4 parts of hexahydroxymethylmelamine hexa - methyl ether. After mixing evenly, obtain the insect - and mite - proofing finishing agent. Add nano - sized diatomite to deionized water, shake and disperse it, and then add sulfonated phenolic resin and stir at high speed to mix, obtaining nano - sized diatomite carrying sulfonated phenolic resin. Add the nano - sized diatomite carrying sulfonated phenolic resin into the insect - and mite - proofing finishing agent, mix and stir, and then wash and centrifuge with absolute ethanol to obtain the modified insect - and mite - proofing finishing agent. Replace the insect - and mite - proofing finishing agent with an equal amount of the modified insect - and mite - proofing finishing agent. The weight ratio of sulfonated phenolic resin to nano - sized diatomite is 1:1.4, and the weight ratio of nano - sized diatomite to the insect - and mite - proofing finishing agent is 1:1.8;

[0057] Step S4: Fabric padding. Immerse the grey fabric in the insect - and mite - proofing finishing agent, dry it after impregnation, and then obtain the insect - and mite - proof down quilt fabric after washing, dewatering, and drying.

[0058] Comparative Example 2

[0059] A preparation method of an insect - and mite - proof down quilt fabric includes the following steps:

[0060] Step S1: Fiber blending. Blend kapok fiber and flax fiber in a mass ratio of 1:1.5, and then process them through the processes of blowing, carding, drawing, roving, and spinning to make blended yarn;

[0061] Step S2: Weaving. Weave the blended yarn into grey fabric through warp - weft knitting and set it aside;

[0062] Step S3: Prepare the insect - and mite - proofing finishing agent. The insect - and mite - proofing finishing agent is antibacterial and mite - proofing finishing agent SCJ - 2012, and the antibacterial and mite - proofing finishing agent SCJ - 2012 is treated by X - ray ionization radiation, where the irradiation dose of ionization irradiation is 7 kGy;

[0063] Step S4: Fabric padding. Immerse the grey fabric in the insect - and mite - proofing finishing agent, dry it after impregnation, and then obtain the insect - and mite - proof down quilt fabric after washing, dewatering, and drying.

[0064] Comparative Example 3

[0065] A preparation method of an insect - and mite - proof down quilt fabric includes the following steps:

[0066] Step S1: Fiber blending. Blend kapok fiber and linen fiber in a mass ratio of 1:1.5, and then process them through the processes of blowing, carding, drawing, roving, and spinning to make a blended yarn;

[0067] Step S2: Weaving. Weave the blended yarn through warp and weft knitting to form a grey fabric, and set it aside;

[0068] Step S3: Prepare the insect - and mite - proofing finishing agent. By weight, add 4 parts of alkyl sulfonate and 0.8 parts of fatty acid polyol ester to 14 parts of polyglutamic acid. Heat it to 50 - 55 °C and then grind it. Stir it at 600 r / min until dissolved. Then add 1.5 parts of saponin, 0.2 parts of dodecyl dimethyl benzyl ammonium chloride, 0.2 parts of sodium ferric ethylenediamine di - o - hydroxyphenyl acetate, and 0.15 parts of nano - silver. Subsequently, add 1.3 parts of polyethylene oxide and 0.4 parts of hexahydroxymethyl melamine hexamethyl ether. After mixing evenly, obtain the insect - and mite - proofing finishing agent;

[0069] Step S4: Fabric padding. Pad the grey fabric in the insect - and mite - proofing finishing agent. After impregnation, dry it, and then wash, dehydrate, and dry it to obtain the insect - and mite - proof down comforter fabric.

[0070] Control group

[0071] A preparation method of an insect - and mite - proof down comforter fabric, comprising the following steps:

[0072] Step S1: Fiber blending. Blend kapok fiber and linen fiber in a mass ratio of 1:1.5, and then process them through the processes of blowing, carding, drawing, roving, and spinning to make a blended yarn;

[0073] Step S2: Weaving. Weave the blended yarn through warp and weft knitting to form a grey fabric, and set it aside;

[0074] Step S3: Prepare the insect - and mite - proofing finishing agent. The insect - and mite - proofing finishing agent is antibacterial and mite - proofing finishing agent SCJ - 2012. After mixing evenly, obtain the insect - and mite - proofing finishing agent;

[0075] Step S4: Fabric padding. Pad the grey fabric in the insect - and mite - proofing finishing agent. After impregnation, dry it, and then wash, dehydrate, and dry it to obtain the insect - and mite - proof down comforter fabric.

[0076] The performance of the anti-insect and anti-mite duvet fabrics obtained by the preparation methods of Examples 1-5, Comparative Examples 1-3, and the control group will be tested respectively. The test contents include: (1) Wrinkle resistance test, which is carried out according to the crease recovery angle method in GB / T 3819-1997; (2) Anti-feather leakage performance test, using the rotary box method. The test sample is placed in a rotary box filled with hard rubber balls. The rotary box rotates at a constant speed to bring the rubber balls to a certain height, impacting the test sample package in the box to simulate various squeezing, rubbing, and collision effects suffered by the duvet products during use. Finally, the anti-feather leakage performance of the seamless lattice anti-feather fabric is evaluated according to the feather leakage quality of the test sample; (3) Acaricidal test, referring to the "Test Methods and Evaluation Standards for Acaricidal and Mite-repellent Efficacy" in the letter of Pesticide Inspection (Bioassay) No. 45 in 2003, and entrusting the Institute of Parasitic Diseases Prevention and Control of the Chinese Center for Disease Control and Prevention. The results are shown in the following table:

[0077] Table 1:

[0078]

[0079] Table 2:

[0080]

[0081]

[0082] Based on the above experimental data, the following conclusions are drawn:

[0083] From Examples 1-5, Comparative Examples 1-3, and the control group, it can be seen that the feather leakage quality of the fabrics in Examples 1-2 is below 1000 mg, and the average crease recovery angle of the front and back sides reaches below 120, and the crease recovery angle of the front and back sides is not high. While in Examples 3-5, the crease recovery angle of the front and back sides of the fabrics has increased significantly. In Example 5, the average crease recovery angle of the front and back sides of the fabric reaches 174.1, and the feather leakage quality reaches 640 mg. Comparing Example 5 with Comparative Example 1, Comparative Example 2, or Comparative Example 3, it can be seen that adding alkyl sulfonate and fatty acid polyol ester to the anti-insect and anti-mite finishing agent or modifying the prepared anti-insect and anti-mite finishing agent can improve the anti-feather leakage performance of the fabric while enhancing the wrinkle resistance performance of the fabric. Comparing the control group with Comparative Example 1, Comparative Example 2, or Comparative Example 3 respectively, it can be seen that the crease recovery angle of the fabric in the control group has decreased significantly, and the fabric is extremely prone to feather leakage. It can be seen that adding alkyl sulfonate and fatty acid polyol ester to the anti-insect and anti-mite finishing agent, irradiating it, and then modifying the anti-insect and anti-mite finishing agent with nano-scale diatomaceous earth carrying sulfonated phenolic resin can significantly improve the anti-wrinkle deformation performance and anti-feather leakage performance of the fabric; and it can be seen from Example 5 and Comparative Example 1, Comparative Example 2, or Comparative Example 3 that the modified anti-insect and anti-mite finishing agent can still maintain good acaricidal performance.

[0084] The foregoing has shown and described the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited by the above embodiments, and what is described in the above embodiments and the specification is only to illustrate the principle of the present invention. Without departing from the spirit and scope of the present invention, the present invention will have various changes and improvements, and these changes and improvements fall within the scope of the present invention claimed. The scope of the present invention claimed is defined by the appended claims and their equivalents.

Claims

1. A preparation method of a duvet fabric capable of preventing insects and mites, characterized in that: The following steps are involved: Step S1, blending, kapok fiber and flax fiber are blended in a mass ratio of 1:1.5, and then processed into blended yarn through the steps of cleaning, carding, drawing, roving and spinning; Step S2, weaving, weaving the blended yarn into a grey cloth by warp and weft, and setting aside; Step S3, preparing a modified insect-proof and anti-mite finishing agent, adding alkyl sulfonate and fatty acid polyol ester to polyglutamic acid, grinding after heating, stirring until dissolved, then adding tea saponin, dodecyl dimethyl benzyl ammonium chloride, ethylenediamine di-o-hydroxyphenyl sodium ferric acetate and nano silver, mixing well and then subjecting to ionizing radiation treatment, then adding polyethylene oxide and hexahydroxymethyl melamine hexamethyl ether, mixing evenly to obtain an insect-proof and anti-mite finishing agent; Adding nano-diatomaceous earth to deionized water and shaking to disperse, then adding sulfonated phenolic resin and stirring at high speed to obtain nano-diatomaceous earth loaded with sulfonated phenolic resin, adding the nano-diatomaceous earth loaded with sulfonated phenolic resin to the insect-proof and mite-proof finishing agent, mixing and stirring, then washing with anhydrous ethanol and centrifuging to obtain a modified insect-proof and mite-proof finishing agent; The weight ratio of the sulfonated phenolic resin to the nano-diatomaceous earth is 1:(1.2-1.5), and the weight ratio of the nano-diatomaceous earth to the anti-insect and anti-mite finishing agent is 1:(1.5-2); Step S4, fabric padding, padding the grey fabric into the modified anti-insect and anti-mite finishing agent, drying after the immersion, and obtaining the anti-insect and anti-mite down quilt fabric after washing, dehydration and drying.

2. The preparation method of a down quilt fabric capable of preventing insects and mites according to claim 1, characterized in that: The modified insect and mite proof finishing agent in step S3 is composed of the following components in parts by weight: 12-15 parts of polyglutamic acid, 3-5 parts of alkyl sulfonate, 0.6-1 parts of fatty acid polyol ester, 1-2 parts of tea saponin, 0.1-0.3 parts of dodecyl dimethyl benzyl ammonium chloride, 0.1-0.3 parts of ethylenediamine di-o-hydroxyphenyl sodium ferric acetate, 0.1-0.2 parts of nano silver, 1.0-1.5 parts of polyethylene oxide, and 0.2-0.5 parts of hexamethylol melamine.

3. The preparation method of a down quilt fabric capable of preventing insects and mites according to claim 1, characterized in that: The ionizing radiation in step S3 is gamma rays, X-rays or electron beams.

4. The preparation method of a down quilt fabric capable of preventing insects and mites according to claim 3, characterized in that: The irradiation dose of the ionizing radiation is 4k-10kGy.

5. The preparation method of a down quilt fabric capable of preventing insects and mites according to claim 1, characterized in that: In step S3, the temperature is raised to 50-55° C., and the stirring rate is 300-800 r / min.

6. A duvet fabric that can prevent insects and mites, characterized in that: The down quilt fabric is produced by the preparation method of the down quilt fabric according to any one of claims 1 to 5.

Citation Information

Patent Citations

  • Insect-proof anti-mite type down quilt fabric processing method

    CN107012565A