A production temperature monitoring method and system for chemical rubber accelerator
By redundant processing and temperature trend analysis of the fluid temperature data of the rubber accelerator in the chemical reactor, and adjusting the valve opening of the heating and cooling medium, the problem of unstable temperature control in the chemical reactor is solved, and the precise temperature adjustment and improvement of the finished product purity is achieved in the rubber accelerator production process.
Patent Information
- Application Number
- CN202410561164.5
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-05-08
- Publication Date
- 2025-03-04
- Estimated Expiration
- 2044-05-08
AI Technical Summary
During the production process of rubber accelerators, the temperature control in the chemical reactor is unstable, resulting in insufficient reaction and the purity of the finished product cannot meet the standard.
By collecting the fluid temperature data of the rubber accelerator in the chemical reactor, performing redundant processing to remove noise, determining the temperature turbulence coefficient, and monitoring the opening of the temperature control valve, inferring the temperature trend characteristics, and adjusting the valve opening of the heating and cooling medium based on these characteristics to achieve pre-adjustment of the rubber accelerator production temperature.
The temperature control accuracy and stability of rubber accelerators in chemical reactors are improved, ensuring sufficient reaction and the purity of the finished product reaches the standard.
Smart Images

Figure CN118394157B_ABST
Abstract
Description
Technical Field
[0001] The present application relates to the technical field of production temperature monitoring, and more specifically, to a production temperature monitoring method and system for chemical rubber accelerators. Background Art
[0002] Rubber accelerators are a type of chemical used to accelerate the vulcanization reaction of rubber. They can promote the cross-linking between rubber molecules and improve the mechanical strength, wear resistance and aging resistance of rubber products. Common rubber accelerators include sulfurized phenol compounds and peroxide accelerators. They are widely used in the rubber industry according to different vulcanization mechanisms and application requirements, such as in the production process of tires, rubber tubes and other products.
[0003] In the production process of rubber accelerators, temperature control in chemical reactors is crucial, and is usually controlled by advanced temperature monitoring and control systems. In the production process, the reaction temperature is controlled by monitoring the temperature of the rubber accelerator inside the chemical reactor and adjusting the flow of the heating or cooling medium. This ensures that the reaction can be carried out under ideal temperature conditions and the cross-linking and bonding of the rubber accelerator molecules can reach the optimal state. However, the supply of heating and cooling media will be unstable during the production temperature control process, and the temperature distribution of the rubber accelerator in the chemical reactor will be uneven. These will lead to insufficient reaction of the rubber accelerator in the chemical reactor, so that the purity of the finished rubber accelerator does not meet the established standards. Therefore, how to control the valve opening of the heating medium and cooling medium in the chemical reactor through the temperature characteristics of the rubber accelerator during production to achieve pre-adjustment of the production temperature of the rubber accelerator is a difficult problem faced by the industry. Summary of the invention
[0004] The present application provides a production temperature monitoring method and system for a chemical rubber accelerator, which can control the valve opening of a heating medium and a cooling medium in a chemical reactor based on the temperature characteristics of the rubber accelerator to achieve pre-adjustment of the production temperature of the rubber accelerator.
[0005] In a first aspect, the present application provides a method for monitoring the production temperature of a chemical rubber accelerator, comprising the following steps:
[0006] Collect the temperature data of the fluid state of the rubber accelerator in the chemical reactor during production, and then obtain the fluid temperature data of the rubber accelerator;
[0007] Eliminating the fluid temperature data of the rubber accelerator according to the data collection time point to obtain the fluid temperature redundant data of the rubber accelerator, and determining the temperature turbulence coefficient of the rubber accelerator in the chemical reactor through the fluid temperature redundant data;
[0008] Monitor the valve opening of the temperature control valve in the chemical reactor during production, determine the temperature trend characteristics of the rubber accelerator according to the valve opening and the heating state of the rubber accelerator at the current moment, and determine the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data;
[0009] According to the production temperature monitoring characteristics and the rubber accelerator reaction temperature range, an adjustment signal for the rubber accelerator production temperature is sent to an industrial monitoring and dispatching center.
[0010] In some embodiments, the temperature data of the fluid state of the rubber accelerator in the chemical reactor during production is collected by a thermistor sensor.
[0011] In some embodiments, the fluid temperature data of the rubber accelerator is redundantly eliminated according to the data acquisition time point to obtain the redundantly eliminated fluid temperature data of the rubber accelerator, specifically comprising:
[0012] For each data collection time point, obtaining the fluid temperature value of the rubber accelerator corresponding to the data collection time point in the fluid temperature data;
[0013] Determine the fluid temperature redundant value corresponding to the data collection time point according to the fluid temperature value of the rubber accelerator corresponding to the data collection time point and the preset temperature redundant adjustment item, and then obtain the fluid temperature redundant value corresponding to each data collection time point;
[0014] The fluid temperature redundant data of the rubber accelerator is determined by the fluid temperature redundant values corresponding to all data collection time points.
[0015] In some embodiments, determining the temperature turbulence coefficient of the rubber accelerator in the chemical reactor by using the fluid temperature redundant data specifically includes:
[0016] Performing data clustering on the redundant data of fluid temperature to obtain a plurality of redundant data clusters of fluid temperature;
[0017] Determine the temperature turbulence value of each fluid temperature redundant data cluster;
[0018] The temperature turbulence coefficient of the rubber accelerator in the chemical reactor is determined based on the temperature turbulence values of all fluid temperature redundant data clusters.
[0019] In some embodiments, the valve opening of the temperature control valve in the chemical reactor during production is monitored by an angle sensor.
[0020] In some embodiments, determining the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data specifically includes:
[0021] Get a pre-trained production temperature prediction model;
[0022] The temperature trend characteristics and the fluid temperature data are used as input data, and the temperature turbulence coefficient is used as a prediction weight to input into the production temperature prediction model for prediction, thereby obtaining a prediction result;
[0023] The prediction results are used as production temperature monitoring features of rubber accelerators in chemical reactors.
[0024] In some embodiments, sending a rubber accelerator production temperature adjustment signal to an industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the rubber accelerator reaction temperature range specifically includes:
[0025] When the production temperature monitoring characteristic is not in the rubber accelerator reaction temperature interval, if the production temperature monitoring characteristic is higher than the interval upper limit of the rubber accelerator reaction temperature interval, a production temperature reduction signal is sent to the industrial monitoring and dispatching center;
[0026] If the production temperature monitoring characteristic is lower than the lower limit of the rubber accelerator reaction temperature range, a production temperature increase signal is sent to the industrial monitoring and dispatching center;
[0027] When the production temperature monitoring characteristic is in the rubber accelerator reaction temperature range, a production temperature stable signal is sent to the industrial monitoring and dispatching center.
[0028] In a second aspect, the present application provides a production temperature monitoring system for a chemical rubber accelerator, including a production temperature control unit, wherein the production temperature control unit includes:
[0029] The monitoring module is used to collect the temperature data of the fluid state of the rubber accelerator in the chemical reactor during production, and then obtain the fluid temperature data of the rubber accelerator;
[0030] A processing module, used for performing redundancy elimination on the fluid temperature data of the rubber accelerator according to the data collection time point to obtain the fluid temperature redundancy eliminated data of the rubber accelerator, and determining the temperature turbulence coefficient of the rubber accelerator in the chemical reactor through the fluid temperature redundancy eliminated data;
[0031] The processing module is also used to monitor the valve opening of the temperature control valve in the chemical reactor during production, determine the temperature trend characteristics of the rubber accelerator according to the valve opening and the heating state of the rubber accelerator at the current moment, and determine the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data;
[0032] The regulating module is used to send a regulating signal of the rubber accelerator production temperature to the industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the rubber accelerator reaction temperature range.
[0033] In a third aspect, the present application provides a computer device, comprising a memory and a processor, wherein the memory is used to store a computer program, and the processor is used to call and run the computer program from the memory, so that the computer device executes the above-mentioned production temperature monitoring method of chemical rubber accelerator.
[0034] In a fourth aspect, the present application provides a computer-readable storage medium, in which instructions or codes are stored. When the instructions or codes are run on a computer, the computer implements the above-mentioned production temperature monitoring method of chemical rubber accelerator when executing.
[0035] The technical solution provided by the embodiments disclosed in this application has the following beneficial effects:
[0036] The present application provides a method and system for monitoring the production temperature of a chemical rubber accelerator. The method and system collect temperature data of the fluid state of the rubber accelerator in a chemical reactor during production to obtain the fluid temperature data of the rubber accelerator; perform redundancy elimination on the fluid temperature data of the rubber accelerator according to the data collection time point to obtain the fluid temperature redundancy elimination data of the rubber accelerator, and determine the temperature turbulence coefficient of the rubber accelerator in the chemical reactor through the fluid temperature redundancy elimination data; monitor the valve opening of the temperature control valve in the chemical reactor during production, determine the temperature trend characteristics of the rubber accelerator according to the valve opening and the heating state of the rubber accelerator at the current moment, and determine the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data; and send an adjustment signal for the production temperature of the rubber accelerator to an industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the reaction temperature range of the rubber accelerator.
[0037] It can be seen that in the present application, the valve opening of the heating medium and the cooling medium in the chemical reactor can be controlled based on the temperature characteristics of the rubber accelerator to achieve pre-adjustment of the production temperature of the rubber accelerator; wherein, firstly, the noise and abnormal values in the fluid temperature data can be removed by redundancy, so as to improve the accuracy and reliability of the fluid temperature data, thereby obtaining the fluid temperature redundancy data, and determining the temperature turbulence coefficient based on the fluid temperature redundancy data, and the temperature turbulence coefficient can better measure the temperature fluctuation characteristics of the rubber accelerator in the chemical reactor; then, by collecting the valve opening of the temperature control valve and the heating state of the rubber accelerator, the temperature trend characteristics of the rubber accelerator can be inferred in real time, so based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data, the production temperature monitoring characteristics of the rubber accelerator can be timely predicted, so as to adjust the production temperature in the production process in time; finally, the production temperature monitoring characteristics are compared with the reaction temperature range, and different production temperature adjustment signals are sent to the industrial monitoring and dispatching center according to the comparison results, so as to change the opening of the cooling medium valve and the temperature control valve in the chemical reactor according to the production temperature adjustment signal to control the production temperature of the rubber accelerator in the chemical reactor. In summary, the technical solution provided in the present application can control the valve opening of the heating medium and the cooling medium in the chemical reaction kettle based on the temperature characteristics of the rubber accelerator, so as to achieve pre-adjustment of the production temperature of the rubber accelerator. BRIEF DESCRIPTION OF THE DRAWINGS
[0038] In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present application. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative labor.
[0039] Figure 1 is an exemplary flow chart of a method for monitoring the production temperature of a chemical rubber accelerator according to some embodiments of the present application;
[0040] Figure 2 is an exemplary flow chart for determining fluid temperature redundant data according to some embodiments of the present application;
[0041] Figure 3 is an exemplary flow chart of determining temperature trend characteristics according to some embodiments of the present application;
[0042] Figure 4 is a schematic diagram of exemplary hardware and / or software for producing a temperature control unit according to some embodiments of the present application;
[0043] Figure 5It is a structural schematic diagram of a computer device for implementing a method for monitoring the production temperature of a chemical rubber accelerator according to some embodiments of the present application. DETAILED DESCRIPTION
[0044] The following will be combined with the drawings in the embodiments of the present application to clearly and completely describe the technical solutions in the embodiments of the present application. Obviously, the described embodiments are only part of the embodiments of the present application, not all of the embodiments. Based on the embodiments in the present application, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of this application.
[0045] The embodiment of the present application provides a production temperature monitoring method and system for chemical rubber accelerators, the core of which is to collect temperature data of the fluid state of the rubber accelerator in the chemical reactor during production, and then obtain the fluid temperature data of the rubber accelerator; perform redundant elimination of the fluid temperature data of the rubber accelerator according to the data collection time point to obtain the redundant elimination data of the fluid temperature of the rubber accelerator, and determine the temperature turbulence coefficient of the rubber accelerator in the chemical reactor through the redundant elimination data of the fluid temperature; monitor the valve opening of the temperature control valve in the chemical reactor during production, determine the temperature trend characteristics of the rubber accelerator according to the valve opening and the heating state of the rubber accelerator at the current moment, and determine the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data; send the adjustment signal of the production temperature of the rubber accelerator to the industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the reaction temperature range of the rubber accelerator. The above scheme can be used to control the valve opening of the heating medium and the cooling medium in the chemical reactor based on the temperature characteristics of the rubber accelerator to achieve pre-adjustment of the production temperature of the rubber accelerator.
[0046] In order to better understand the above technical solution, the above technical solution will be described in detail below in conjunction with the accompanying drawings and specific implementation methods. Figure 1 , which is an exemplary flow chart of a method for monitoring the production temperature of a chemical rubber accelerator according to some embodiments of the present application. The method 100 for monitoring the production temperature of a chemical rubber accelerator mainly includes the following steps:
[0047] In step 101, temperature data of the fluid state of the rubber accelerator in the chemical reaction kettle during production is collected to obtain fluid temperature data of the rubber accelerator.
[0048] In some embodiments, the temperature data of the fluid state of the rubber accelerator in the chemical reactor during production is collected by a thermistor sensor; it should be noted that the rubber accelerator described in the present application is a sulfurized phenol compound, which is usually in a fluid (liquid) state when reacting in a chemical reactor; in specific implementation, first, the thermistor sensor is installed inside the chemical reactor to ensure that it can accurately measure the temperature of the rubber accelerator; then, the thermistor sensor is connected to a temperature data acquisition system, which can be achieved by connecting the wire of the thermistor sensor to a temperature data acquisition device or a control device such as a PLC (programmable logic controller); finally, the temperature data acquisition system is started to start recording the temperature data of the fluid state of the rubber accelerator, thereby obtaining the fluid temperature data of the rubber accelerator, that is, the fluid temperature data represents the temperature data of the rubber accelerator in the fluid state.
[0049] In step 102, the fluid temperature data of the rubber accelerator is redundantly eliminated according to the data collection time point to obtain the redundant temperature data of the rubber accelerator, and the temperature turbulence coefficient of the rubber accelerator in the chemical reactor is determined by the redundant temperature data of the fluid.
[0050] Preferably, in some embodiments, reference Figure 2 As shown in FIG. 1 , this figure is an exemplary flow chart for determining redundant data of fluid temperature in some embodiments of the present application. In this embodiment, redundant data of the fluid temperature of the rubber accelerator is obtained according to the data acquisition time point, and the following steps can be used to obtain the redundant data of the fluid temperature of the rubber accelerator:
[0051] First, in step 1021, for each data collection time point, the fluid temperature value of the rubber accelerator corresponding to the data collection time point in the fluid temperature data is obtained;
[0052] Then, in step 1022, the fluid temperature redundant value corresponding to the data collection time point is determined according to the fluid temperature value of the rubber accelerator corresponding to the data collection time point and the preset temperature redundant adjustment item, so as to obtain the fluid temperature redundant value corresponding to each data collection time point;
[0053] Finally, in step 1023, the fluid temperature redundant data of the rubber accelerator is determined from the fluid temperature redundant values corresponding to all data collection time points.
[0054] It should be noted that, in the present application, the fluid temperature redundant data is data composed of fluid temperature redundant values in chronological order, and the fluid temperature redundant values represent the fluid temperature values after the redundant operation to remove the interference noise; in specific implementation, first, the acquisition time point when the thermistor sensor is monitoring, that is, the data acquisition time point, can be obtained, and for each data acquisition time point, the fluid temperature value of the rubber accelerator corresponding to the data acquisition time point is obtained in the fluid temperature data; then, a temperature redundant adjustment item can be preset according to the historical experimental data, and the temperature redundant adjustment item is used to control the redundant accuracy, so as to obtain the fluid temperature value of the rubber accelerator corresponding to the data acquisition time point before the data acquisition time point, and then the data can be obtained. The redundant value of the fluid temperature corresponding to the collection time point, for example, the redundant value of the fluid temperature corresponding to the nth data collection time point = the redundant adjustment item of the temperature * the fluid temperature value of the rubber accelerator corresponding to the nth data collection time point + (1-the redundant adjustment item of the temperature) * the fluid temperature value of the rubber accelerator corresponding to the n-1th data collection time point, wherein when the value of n is 1, the fluid temperature value of the rubber accelerator corresponding to the n-1 data collection time point is set to a default value, which can be preset by experience. The redundant value of the fluid temperature corresponding to each data collection time point can be obtained by the above method; finally, the redundant value of the fluid temperature corresponding to all the data collection time points can be used to form the redundant data of the fluid temperature of the rubber accelerator in chronological order.
[0055] Preferably, in some embodiments, the temperature turbulence coefficient of the rubber accelerator in the chemical reactor can be determined by the fluid temperature redundant data in the following manner, namely:
[0056] Performing data clustering on the redundant data of fluid temperature to obtain a plurality of redundant data clusters of fluid temperature;
[0057] Determine the temperature turbulence value of each fluid temperature redundant data cluster;
[0058] The temperature turbulence coefficient of the rubber accelerator in the chemical reactor is determined based on the temperature turbulence values of all fluid temperature redundant data clusters.
[0059] It should be noted that, in the present application, the temperature turbulence coefficient is an indicator used to represent the degree of temperature fluctuation of the rubber accelerator in the fluid state in the chemical reactor, and the temperature turbulence value represents the degree of fluctuation of the overall temperature value of the fluid temperature redundant data cluster; in specific implementation, first, the fluid temperature redundant data can be clustered by the K-means clustering algorithm to obtain multiple fluid temperature redundant data clusters; then, for each fluid temperature redundant data cluster, the ratio of the total number of data in the fluid temperature redundant data cluster to the total number of data of the fluid temperature redundant data cluster of the rubber accelerator can be used as the temperature turbulence value of the fluid temperature redundant data cluster, thereby obtaining the temperature turbulence value of each fluid temperature redundant data cluster; finally, for each fluid temperature redundant data cluster, the product of the temperature turbulence value of the fluid temperature redundant data cluster and its logarithm is calculated, and the sum of all calculation results is dimensionally eliminated, and the final result after dimension elimination is used as the temperature turbulence coefficient of the rubber accelerator in the chemical reactor.
[0060] In addition, it should be noted that noise and outliers in the fluid temperature data can be removed through redundancy elimination, which is convenient for improving the accuracy and reliability of the fluid temperature data, thereby obtaining fluid temperature redundant data, and determining the temperature turbulence coefficient based on the fluid temperature redundant data. The temperature turbulence coefficient can better measure the temperature fluctuation characteristics of the rubber accelerator in the chemical reactor.
[0061] In step 103, the valve opening of the temperature control valve in the chemical reactor during production is monitored, and the temperature trend characteristics of the rubber accelerator are determined based on the valve opening and the heating state of the rubber accelerator at the current moment. The production temperature monitoring characteristics of the rubber accelerator in the chemical reactor are determined based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data.
[0062] In some embodiments, the valve opening of the temperature control valve in the chemical reactor during production is monitored by an angle sensor; in specific implementation, first, the angle sensor is installed on the rotating part of the temperature control valve in the chemical reactor to monitor the valve opening angle in real time; then, the data acquisition system is started to collect the angle data of the valve opening of the temperature control valve, that is, the valve opening of the temperature control valve in the chemical reactor during production, and the valve opening represents the opening angle of the temperature control valve; it should be noted that when the valve opening of the temperature control valve increases, it indicates that the supply of the heating medium will increase, and the fluid temperature of the rubber accelerator in the chemical reactor will rise; conversely, when the valve opening of the temperature control valve decreases, it indicates that the supply of the heating medium will decrease, and the fluid temperature of the rubber accelerator in the chemical reactor will decrease.
[0063] Preferably, in some embodiments, reference Figure 3As shown in FIG. 1 , this figure is an exemplary flow chart for determining temperature trend characteristics in some embodiments of the present application. In this embodiment, the temperature trend characteristics of the rubber accelerator are determined according to the valve opening and the heating state of the rubber accelerator at the current moment, which can be achieved by the following steps:
[0064] First, in step 1031, the flow rate of the heating medium supplied to the chemical reaction kettle is determined according to the valve opening;
[0065] Then, in step 1032, the temperature change trend of the rubber accelerator is simulated based on the heating state of the rubber accelerator at the current moment to obtain the fluid temperature trend of the rubber accelerator in the chemical reactor;
[0066] Finally, in step 1033, the temperature trend characteristics of the rubber accelerator are determined by the flow rate of the heating medium and the fluid temperature trend quantity of the rubber accelerator in the chemical reactor.
[0067] It should be noted that, in the present application, the temperature trend characteristic of the rubber accelerator is a characteristic used to describe the temperature change trend of the fluid of the rubber accelerator, and the fluid temperature trend quantity represents the temperature change quantity of the fluid of the rubber accelerator in the chemical reactor. In specific implementation, first, the cross-sectional area of the temperature control valve opening can be calculated according to the valve opening, and the flow rate of the heating medium can be obtained, so that the heating medium flow rate in the chemical reactor can be calculated, wherein the heating medium flow rate = the cross-sectional area of the temperature control valve opening * the flow rate of the heating medium; then, the heating state of the rubber accelerator at the current moment can be input into the simulation software to simulate the temperature change trend of the rubber accelerator, so as to obtain the fluid temperature trend quantity of the rubber accelerator in the chemical reactor, and the heating state refers to whether the rubber accelerator is being heated in the chemical reactor, as well as the intensity and duration of the heating, and different heating states will affect the change trend of the fluid temperature of the rubber accelerator; finally, the fluid temperature rise of the rubber accelerator in the chemical reactor can be calculated according to the heating medium flow rate, so that the sum of the fluid temperature rise and the fluid temperature trend quantity of the rubber accelerator can be taken as the value of the temperature trend characteristic of the rubber accelerator.
[0068] In some embodiments, the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor can be determined based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data in the following manner, namely:
[0069] Get a pre-trained production temperature prediction model;
[0070] The temperature trend characteristics and the fluid temperature data are used as input data, and the temperature turbulence coefficient is used as a prediction weight to input into the production temperature prediction model for prediction, thereby obtaining a prediction result;
[0071] The prediction results are used as production temperature monitoring features of rubber accelerators in chemical reactors.
[0072] In the specific implementation, first, in this application, a production temperature prediction model is constructed and trained based on machine learning technology, and a production temperature prediction model can also be constructed and trained based on methods such as statistical regression analysis, which is not limited here; then, the temperature trend characteristics and fluid temperature data are used as input data, and the temperature turbulence coefficient is used as the prediction weight to input into the production temperature prediction model for prediction. The production temperature prediction model will calculate according to the input data and the prediction weight to obtain the prediction result; finally, the prediction result can be used as the production temperature monitoring feature of the rubber accelerator in the chemical reactor, and the production temperature monitoring feature indicates the fluid temperature value that the rubber accelerator in the chemical reactor may reach during production.
[0073] It should be noted that by collecting the valve opening of the temperature control valve and the heating status of the rubber accelerator, the temperature trend characteristics of the rubber accelerator can be inferred in real time. Therefore, based on the temperature trend characteristics, temperature turbulence coefficient and fluid temperature data, the production temperature monitoring characteristics of the rubber accelerator can be predicted in time, which is convenient for timely adjustment of the production temperature in the production process.
[0074] In step 104, a signal for adjusting the production temperature of the rubber accelerator is sent to an industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the reaction temperature range of the rubber accelerator.
[0075] In some embodiments, the following method can be used to send a rubber accelerator production temperature adjustment signal to the industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the rubber accelerator reaction temperature range, namely:
[0076] When the production temperature monitoring characteristic is not in the rubber accelerator reaction temperature interval, if the production temperature monitoring characteristic is higher than the interval upper limit of the rubber accelerator reaction temperature interval, a production temperature reduction signal is sent to the industrial monitoring and dispatching center;
[0077] If the production temperature monitoring characteristic is lower than the lower limit of the rubber accelerator reaction temperature range, a production temperature increase signal is sent to the industrial monitoring and dispatching center;
[0078] When the production temperature monitoring characteristic is in the rubber accelerator reaction temperature range, a production temperature stable signal is sent to the industrial monitoring and dispatching center.
[0079] It should be noted that, in the present application, the rubber accelerator reaction temperature range refers to the production temperature range required for preparing a rubber accelerator that meets the established standards, and the rubber accelerator reaction temperature range can be obtained through literature data; in specific implementation, first, it is determined whether the production temperature monitoring characteristics are in the rubber accelerator reaction temperature range, and based on the judgment result, a rubber accelerator production temperature adjustment signal is sent to the industrial monitoring and dispatching center to achieve pre-adjustment of the production temperature of the rubber accelerator in the chemical reactor.
[0080] In the above embodiment, a signal for adjusting the production temperature of the rubber accelerator is sent to the industrial monitoring and dispatching center according to the judgment result; in specific implementation, when the production temperature monitoring characteristic is not in the reaction temperature interval of the rubber accelerator, if the production temperature monitoring characteristic is higher than the upper limit of the reaction temperature interval of the rubber accelerator, it means that the production temperature monitoring characteristic is too high, which will cause the rubber accelerator to overheat or react uncontrollably at this temperature. In this case, a production temperature reduction signal should be sent to the industrial monitoring and dispatching center to open the valve of the cooling medium in the chemical reactor, increase the supply of the cooling medium, and reduce the fluid temperature of the rubber accelerator in the reactor; if the production temperature monitoring characteristic is lower than the upper limit of the reaction temperature interval of the rubber accelerator, The lower limit of the rubber accelerator reaction temperature range indicates that the production temperature monitoring characteristic is too low, which will affect the reaction rate or cause incomplete reaction. In this case, a production temperature increase signal is sent to the industrial monitoring and dispatching center, thereby increasing the valve opening of the temperature control valve in the chemical reactor and increasing the supply of heating medium to increase the fluid temperature of the rubber accelerator in the reactor. When the production temperature monitoring characteristic is in the rubber accelerator reaction temperature range, it means that the current production temperature monitoring characteristic is in a suitable range and the rubber accelerator reaction conditions are good. In this case, a production temperature stabilization signal is sent to the industrial monitoring and dispatching center, and the valve opening of the current temperature control valve is kept unchanged to maintain the existing heating state.
[0081] It can be seen that in the present application, the valve opening of the heating medium and the cooling medium in the chemical reactor can be controlled based on the temperature characteristics of the rubber accelerator to achieve pre-adjustment of the production temperature of the rubber accelerator; wherein, firstly, the noise and abnormal values in the fluid temperature data can be removed by redundancy, so as to improve the accuracy and reliability of the fluid temperature data, thereby obtaining the fluid temperature redundancy data, and determining the temperature turbulence coefficient based on the fluid temperature redundancy data, and the temperature turbulence coefficient can better measure the temperature fluctuation characteristics of the rubber accelerator in the chemical reactor; then, by collecting the valve opening of the temperature control valve and the heating state of the rubber accelerator, the temperature trend characteristics of the rubber accelerator can be inferred in real time, so based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data, the production temperature monitoring characteristics of the rubber accelerator can be timely predicted, so as to adjust the production temperature in the production process in time; finally, the production temperature monitoring characteristics are compared with the reaction temperature range, and different production temperature adjustment signals are sent to the industrial monitoring and dispatching center according to the comparison results, so as to change the opening of the cooling medium valve and the temperature control valve in the chemical reactor according to the production temperature adjustment signal to control the production temperature of the rubber accelerator in the chemical reactor. In summary, the technical solution provided in the present application can control the valve opening of the heating medium and the cooling medium in the chemical reaction kettle based on the temperature characteristics of the rubber accelerator, so as to achieve pre-adjustment of the production temperature of the rubber accelerator.
[0082] In addition, in another aspect of the present application, in some embodiments, the present application provides a production temperature monitoring system for a chemical rubber accelerator, the production temperature monitoring system for a chemical rubber accelerator includes a production temperature control unit, referring to Figure 4 , which is a schematic diagram of exemplary hardware and / or software of a production temperature control unit according to some embodiments of the present application, the production temperature control unit 400 includes: a monitoring module 401, a processing module 402 and an adjustment module 403, which are described as follows:
[0083] Monitoring module 401, in this application, monitoring module 401 is mainly used to collect temperature data of the fluid state of the rubber accelerator in the chemical reactor during production, and then obtain the fluid temperature data of the rubber accelerator;
[0084] Processing module 402, in the present application, is used to perform redundant elimination of the fluid temperature data of the rubber accelerator according to the data collection time point to obtain the redundant eliminated data of the fluid temperature of the rubber accelerator, and determine the temperature turbulence coefficient of the rubber accelerator in the chemical reactor through the redundant eliminated data of the fluid temperature;
[0085] It should be noted that the processing module 402 in the present application is also used to monitor the valve opening of the temperature control valve in the chemical reactor during production, determine the temperature trend characteristics of the rubber accelerator according to the valve opening and the heating state of the rubber accelerator at the current moment, and determine the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data;
[0086] The regulating module 403 in the present application is mainly used to send a regulating signal of the rubber accelerator production temperature to the industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the rubber accelerator reaction temperature range.
[0087] The above describes in detail the examples of the production temperature monitoring method and system of the chemical rubber accelerator provided in the embodiments of the present application. It can be understood that in order to realize the above functions, the corresponding device includes hardware structures and / or software modules corresponding to the execution of each function. It should be easily appreciated by those skilled in the art that, in combination with the units and algorithm steps of each example described in the embodiments disclosed herein, the present application can be implemented in the form of hardware or a combination of hardware and computer software. Whether a function is executed in the form of hardware or computer software driving hardware depends on the specific application and design constraints of the technical solution. Professional and technical personnel can use different methods to implement the described functions for each specific application, but such implementation should not be considered to be beyond the scope of the present application.
[0088] In some embodiments, the present application also provides a computer device, which includes a memory and a processor, wherein the memory is used to store a computer program, and the processor is used to call and run the computer program from the memory, so that the computer device executes the above-mentioned production temperature monitoring method of chemical rubber accelerator.
[0089] In some embodiments, reference Figure 5 , the dotted line in the figure indicates that the unit or the module is optional, and the figure is a schematic diagram of the structure of a computer device for a method for monitoring the production temperature of a chemical rubber accelerator provided in an embodiment of the present application. The method for monitoring the production temperature of a chemical rubber accelerator described in the above embodiment can be Figure 5 The computer device 500 shown in the figure is implemented, and the computer device 500 includes at least one processor 501, a memory 502 and at least one communication unit 505. The computer device 500 can be a terminal device, a server or a chip.
[0090] The processor 501 may be a general-purpose processor or a special-purpose processor. For example, the processor 501 may be a central processing unit (CPU), which may be used to control the computer device 500, execute software programs, and process data of the software programs. The computer device 500 may also include a communication unit 505 to implement signal input (reception) and output (transmission).
[0091] For example, the computer device 500 may be a chip, the communication unit 505 may be an input and / or output circuit of the chip, or the communication unit 505 may be a communication interface of the chip, and the chip may be a component of a terminal device, a network device, or other devices.
[0092] For another example, the computer device 500 may be a terminal device or a server, and the communication unit 505 may be a transceiver of the terminal device or the server, or the communication unit 505 may be a transceiver circuit of the terminal device or the server.
[0093] The computer device 500 may include one or more memories 502, on which a program 504 is stored. The program 504 can be executed by the processor 501 to generate instructions 503, so that the processor 501 performs the method described in the above method embodiment according to the instructions 503. Optionally, data (such as a target audit model) can also be stored in the memory 502. Optionally, the processor 501 can also read the data stored in the memory 502, and the data can be stored at the same storage address as the program 504, or the data can be stored at a different storage address from the program 504.
[0094] The processor 501 and the memory 502 may be provided separately or integrated together, for example, integrated on a system on chip (SOC) of the terminal device.
[0095] It should be understood that each step of the above method embodiment can be completed by a hardware-based logic circuit or software-based instructions in the processor 501. The processor 501 can be a central processing unit, a digital signal processor (DSP), an application specific integrated circuit (ASIC), a field programmable gate array (FPGA) or other programmable logic devices, such as discrete gates, transistor logic devices or discrete hardware components.
[0096] Those skilled in the art will appreciate that the embodiments of the present application may be provided as methods, systems, or computer program products. Therefore, the present application may adopt the form of a complete hardware embodiment, a complete software embodiment, or an embodiment combining software and hardware. Moreover, the present application may adopt the form of a computer program product implemented on one or more computer-usable storage media (including but not limited to disk storage, CD-ROM, optical storage, etc.) containing computer-usable program codes.
[0097] For example, in some embodiments, the present application also provides a computer-readable storage medium, in which instructions or codes are stored. When the instructions or codes are executed on a computer, the computer implements the above-mentioned production temperature monitoring method of chemical rubber accelerators.
[0098] Although the preferred embodiments of the present application have been described, those skilled in the art may make other changes and modifications to these embodiments once they have learned the basic creative concept. Therefore, the appended claims are intended to be interpreted as including the preferred embodiments and all changes and modifications falling within the scope of the present application.
[0099] Obviously, those skilled in the art can make various changes and modifications to the present application without departing from the spirit and scope of the present application. Thus, if these modifications and variations of the present application fall within the scope of the claims of the present application and their equivalents, the present application is also intended to include these modifications and variations.
Claims
1. A method for monitoring the production temperature of a chemical rubber accelerator, characterized in that: The steps include: Collect the temperature data of the fluid state of the rubber accelerator in the chemical reactor during production to obtain the fluid temperature data of the rubber accelerator; Eliminating the fluid temperature data of the rubber accelerator according to the data collection time point to obtain the fluid temperature redundant data of the rubber accelerator, and determining the temperature turbulence coefficient of the rubber accelerator in the chemical reactor through the fluid temperature redundant data; Monitor the valve opening of the temperature control valve in the chemical reactor during production, determine the temperature trend characteristics of the rubber accelerator according to the valve opening and the heating state of the rubber accelerator at the current moment, and determine the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data; Sending a rubber accelerator production temperature adjustment signal to an industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the rubber accelerator reaction temperature range; The temperature trend characteristics of the rubber accelerator are determined according to the valve opening and the heating state of the rubber accelerator at the current moment by the following steps: Determining the flow rate of the heating medium supplied to the chemical reaction kettle according to the valve opening; Based on the heating state of the rubber accelerator at the current moment, the temperature change trend of the rubber accelerator is simulated to obtain the fluid temperature trend of the rubber accelerator in the chemical reactor; Determining the temperature trend characteristics of the rubber accelerator by the flow rate of the heating medium and the fluid temperature trend quantity of the rubber accelerator in the chemical reactor; Wherein, the temperature turbulence coefficient is used to indicate the degree of temperature fluctuation in the fluid state of the rubber accelerator in the chemical reactor; Wherein, determining the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data specifically includes: Get a pre-trained production temperature prediction model; The temperature trend characteristics and the fluid temperature data are used as input data, and the temperature turbulence coefficient is used as a prediction weight to input into the production temperature prediction model for prediction, thereby obtaining a prediction result; The prediction result is used as a production temperature monitoring feature of the rubber accelerator in the chemical reactor; Wherein, determining the temperature turbulence coefficient of the rubber accelerator in the chemical reactor by using the fluid temperature redundant data specifically includes: Performing data clustering on the redundant data of fluid temperature to obtain a plurality of redundant data clusters of fluid temperature; Determine the temperature turbulence value of each fluid temperature redundant data cluster; Determine the temperature turbulence coefficient of the rubber accelerator in the chemical reactor according to the temperature turbulence value of all fluid temperature redundant data clusters; Among them, the temperature turbulence value represents the degree of fluctuation of the overall temperature value of the fluid temperature redundant data cluster; in specific implementation, the fluid temperature redundant data is clustered to obtain multiple fluid temperature redundant data clusters; for each fluid temperature redundant data cluster, the ratio of the total number of data in the fluid temperature redundant data cluster to the total number of data of the fluid temperature redundant data cluster of the rubber accelerator is used as the temperature turbulence value of the fluid temperature redundant data cluster, thereby obtaining the temperature turbulence value of each fluid temperature redundant data cluster; for each fluid temperature redundant data cluster, the product of the temperature turbulence value of the fluid temperature redundant data cluster and its logarithm is calculated, and the sum of all calculation results is dimensionally eliminated, and the final result after dimension elimination is used as the temperature turbulence coefficient of the rubber accelerator in the chemical reactor.
2. The method according to claim 1, characterized in that The temperature data of the rubber accelerator fluid state in the chemical reactor during production is collected through thermistor sensors.
3. The method according to claim 1, characterized in that The fluid temperature data of the rubber accelerator is redundantly eliminated according to the data acquisition time point to obtain the redundantly eliminated fluid temperature data of the rubber accelerator, which specifically includes: For each data collection time point, obtaining the fluid temperature value of the rubber accelerator corresponding to the data collection time point in the fluid temperature data; Determine the fluid temperature redundant value corresponding to the data collection time point according to the fluid temperature value of the rubber accelerator corresponding to the data collection time point and the preset temperature redundant adjustment item, and then obtain the fluid temperature redundant value corresponding to each data collection time point; The fluid temperature redundant data of the rubber accelerator is determined by the fluid temperature redundant values corresponding to all data collection time points.
4. The method according to claim 1, characterized in that The valve opening of the temperature control valve in the chemical reactor during production is monitored by an angle sensor.
5. The method according to claim 1, characterized in that Sending a rubber accelerator production temperature adjustment signal to the industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the rubber accelerator reaction temperature range specifically includes: When the production temperature monitoring characteristic is not in the rubber accelerator reaction temperature interval, if the production temperature monitoring characteristic is higher than the interval upper limit of the rubber accelerator reaction temperature interval, a production temperature reduction signal is sent to the industrial monitoring and dispatching center; If the production temperature monitoring characteristic is lower than the lower limit of the rubber accelerator reaction temperature range, a production temperature increase signal is sent to the industrial monitoring and dispatching center; When the production temperature monitoring characteristic is in the rubber accelerator reaction temperature range, a production temperature stable signal is sent to the industrial monitoring and dispatching center.
6. A production temperature monitoring system for a chemical rubber accelerator, which adopts the method described in any one of claims 1 to 5 to perform production temperature monitoring, and the production temperature monitoring system for a chemical rubber accelerator includes a production temperature control unit, characterized in that: The production temperature control unit comprises: The monitoring module is used to collect the temperature data of the fluid state of the rubber accelerator in the chemical reactor during production, and then obtain the fluid temperature data of the rubber accelerator; A processing module, used for performing redundancy elimination on the fluid temperature data of the rubber accelerator according to the data collection time point to obtain the fluid temperature redundancy eliminated data of the rubber accelerator, and determining the temperature turbulence coefficient of the rubber accelerator in the chemical reactor through the fluid temperature redundancy eliminated data; The processing module is also used to monitor the valve opening of the temperature control valve in the chemical reactor during production, determine the temperature trend characteristics of the rubber accelerator according to the valve opening and the heating state of the rubber accelerator at the current moment, and determine the production temperature monitoring characteristics of the rubber accelerator in the chemical reactor based on the temperature trend characteristics, the temperature turbulence coefficient and the fluid temperature data; The regulating module is used to send a regulating signal of the rubber accelerator production temperature to the industrial monitoring and dispatching center according to the production temperature monitoring characteristics and the rubber accelerator reaction temperature range.
7. A computer device, characterized in that: The computer device includes a memory and a processor, the memory is used to store a computer program, and the processor is used to call and run the computer program from the memory, so that the computer device executes the production temperature monitoring method of a chemical rubber accelerator according to any one of claims 1 to 5.
8. A computer-readable storage medium, wherein instructions or codes are stored in the computer-readable storage medium. When the instructions or codes are executed on a computer, the computer implements the production temperature monitoring method of a chemical rubber accelerator as described in any one of claims 1 to 5.
Citation Information
Patent Citations
Reaction kettle temperature prediction and control method, device and terminal equipment
CN110716593A
Intelligent wine cabinet temperature control system and control method thereof
CN117348635A