AMS monomer resin production wastewater treatment equipment

By designing a device for wastewater treatment for AMS monomer resin production, the problem of solvent precipitation and solid-liquid separation cannot be treated separately, the wastewater recovery rate and catalytic effect are improved, and the solid collection and treatment process is simplified.

CN118420073BActive Publication Date: 2025-02-25PUYANG BINDER CHEM CO LTD
View PDF 1 Cites 0 Cited by

Patent Information

Application Number
CN202410792085.5
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-06-19
Publication Date
2025-02-25
Estimated Expiration
2044-06-19

AI Technical Summary

Technical Problem

In the wastewater treatment of existing AMS monomer resin production, aluminum trichloride solid particles are prone to moisture blocking the pipeline. After solvent storage, it will precipitate and lead to inconsistent concentration, affecting the catalytic effect, and cannot be treated separately after solid-liquid separation, resulting in a decrease in wastewater recovery rate. .

Method used

A wastewater treatment equipment for the production of AMS monomer resin is designed, using components such as reactor body, temperature control pipe, collection pipe and drive wheel, solid-liquid separation through an external pumping mechanism, and solid-liquid separation is achieved using the adjustment wheel and pushing groove mechanism. Classification and treatment of liquid.

Benefits of technology

It effectively solves the problem that solvent precipitation and solid-liquid separation cannot be treated separately, improves wastewater recovery rate, ensures the stability of the catalytic effect, and simplifies the collection and treatment process of solids.

✦ Generated by Eureka AI based on patent content.

Smart Images

  • Figure CN118420073B_ABST
    Figure CN118420073B_ABST
Patent Text Reader

Abstract

The present application relates to the technical field of polymer material preparation, and in particular to wastewater treatment equipment for AMS monomer resin production, which includes a reactor body, wherein a thermostat is embedded inside the reactor body, and a collecting tube is rotatably connected inside the top of the reactor body. The present application transports wastewater into the reactor body through a feed pipe, and an external temperature control mechanism adjusts the temperature of the wastewater through the thermostat. After the solid-liquid separation of the wastewater, the through hole at the corresponding position of the collecting tube is adjusted according to the solid-liquid stratification position of the wastewater, and the servo motor drives the rotating wheel to rotate, and the rotating wheel drives the contact rod to move a certain distance, and the contact rod drives the moving rod to move, and the moving rod drives the top block to move, and the top block moves into the push groove. Under the action of the push groove, the top block drives the adjusting wheel to rotate counterclockwise by 30 degrees, and at this time, the through hole at the corresponding position of the adjusting wheel is opened, and the external pumping mechanism pumps the liquid through the collecting tube, which has the advantage of facilitating solid-liquid classification and processing.
Need to check novelty before this filing date? Find Prior Art

Description

Technical Field

[0001] The present application relates to the technical field of polymer material preparation, and in particular to wastewater treatment equipment for AMS monomer resin production. Background Art

[0002] AMS monomer resin refers to a low molecular weight polymer obtained by polymerization of α-methylstyrene monomer. It is a type of hydrocarbon petroleum resin. AMS monomer resin is a oligomer of methylstyrene. It is an excellent additive for the processing and application of polymer materials. It can be used in plastics, thermoplastic elastomers, rubber processing, adhesives and coatings production. In particular, adding it to rubber can improve the mechanical properties, processing properties and weather resistance of the material.

[0003] In the prior art, aluminum chloride is generally used as a treatment agent in the treatment of AMS monomer resin wastewater. However, the large amount of aluminum chloride solid particles used causes pipeline clogging when encountering moisture, thereby causing a poor catalytic effect. The existing method is to use aluminum chloride particles mixed with solvents.

[0004] Regarding the above-mentioned related technologies, the inventors believe that the following defects exist: the solvent will precipitate after being stored for a period of time, resulting in inconsistent concentrations that affect the catalytic effect, and the existing wastewater cannot be treated separately after solid-liquid separation, resulting in a decrease in wastewater recovery rate and increased production costs. Summary of the invention

[0005] In order to improve the problem that solution precipitation and wastewater cannot be treated separately after solid-liquid separation, the present application provides AMS monomer resin production wastewater treatment equipment.

[0006] The AMS monomer resin production wastewater treatment equipment provided by the present application adopts the following technical scheme: the AMS monomer resin production wastewater treatment equipment comprises a reactor body, wherein a temperature regulating tube is embedded inside the reactor body, a collecting tube is rotatably connected inside the top of the reactor body, the outer wall of the top of the collecting tube is located above the reactor body and is fixedly connected to a driving wheel, the left and right sides of the bottom of the collecting tube are fixedly connected to guide plates, a moving rod is slidably connected inside the collecting tube, a top block is fixedly connected to the outer wall of the bottom end of the moving rod, and six adjusting wheels are connected in an array above the top block, a pushing groove is provided on the inner wall of the adjusting wheel to form a sliding connection with the outer wall of the top block, a limiting ring is fixedly connected to the upper and lower ends of the adjusting wheel on the inner wall of the collecting tube, a pushing frame is fixedly connected to the top wall of the adjusting wheel, and the side wall of the pushing frame is fixedly connected to the guide rod, the inner wall of the limiting ring is located on the outer surface of the guide rod and is fixedly connected to the fixing ring, the outer surface of the guide rod is located between the fixing ring and the pushing frame and is sleeved with a reset spring, the inner wall of the collecting tube is located on the outer surface of the moving rod and is fixedly connected to the limiting ring The top of the collecting tube is located at the outer surface of the moving rod and is rotatably connected with a connecting tube. The top of the moving rod is located at the top of the connecting tube and is fixedly connected with a contact rod. The outer wall of the connecting tube is located at the rear end of the contact rod and is fixedly connected to the supporting frame. The front end of the top of the supporting frame is close to the outer wall of the contact rod and is rotatably connected to a rotating wheel. The right end of the rotating wheel is located at the top of the supporting frame and is fixedly connected to a servo motor. The right side of the driving wheel is meshed with a connecting wheel. The top outer surface of the connecting wheel is meshed with a toothed belt. The inside of the toothed belt is located on the right side of the connecting wheel and is meshed with a driving motor. The outer wall of the driving motor is fixedly connected to the top wall of the reactor body by setting a bearing frame. The right side of the reactor body is connected with an infusion tube through the connection. The right end of the infusion tube is connected with a solvent tank through the connection. The output end of the driving motor is located below the solvent tank and is fixedly connected with a stirring rod. The outer wall of the top end of the stirring rod is located at the inner wall of the solvent tank and is fixedly connected with a scraper. The bottom end of the reactor body is connected with a feeding pipe through the connection. A baffle is inserted in the feeding pipe. The rear end of the baffle is rotatably connected with an adjusting rod. The bottom wall of the reactor body is rotatably connected with the rear end of the adjusting rod by setting a fixed plate.

[0007] Optionally, an interlayer is provided inside the reactor body, the temperature regulating tube is provided in the interlayer, and the liquid inlet and outlet of the temperature regulating tube are respectively provided on the top side wall of the reactor body and the bottom wall of the reactor body.

[0008] Optionally, a bracket is provided on the inner wall of the reactor body at the center of the collecting tube, and six rows of through holes are arranged in an array on the side wall at the bottom end of the collecting tube.

[0009] Optionally, the guide plate extends into the feed pipe at an inclined angle, the guide plate is slidably connected to the inner wall of the reactor body, and a receiving groove engaging with the bottom end of the moving rod is provided at the bottom of the collecting pipe.

[0010] Optionally, the exterior of the regulating wheel is composed of six baffles, a drainage channel is formed between the baffles, the baffles are slidably connected to the inner wall of the collecting tube, the push groove is arranged above the top block, the upper and lower ends of the push groove are composed of vertical grooves, and the center position of the push groove is arranged in a “>” shape.

[0011] Optionally, the guide rod is arranged in an arc shape, the guide rod passes through the fixed ring, the outer wall of the top end of the movable rod and the inner wall of the limit frame form a sliding connection, the connecting pipe is connected to the external pumping mechanism, and the outer wall of the rear end of the connecting pipe is provided with a fixed frame fixedly connected to the top wall of the reactor body.

[0012] Optionally, the contact rod is composed of a plurality of discs, the outer walls of the discs are provided with teeth meshing with the rotating wheel, a support ring is provided on the top of the support frame which is slidably connected to the outer wall of the contact rod, the connecting wheel is composed of two gears of different sizes, and the connecting wheel is rotatably connected to the top wall of the reactor body.

[0013] Optionally, a solenoid valve is provided at the connection between the infusion pipe and the reactor body, a feed pipe is provided at the top of the solvent tank, the outer wall of the stirring rod is composed of spiral blades, the scraper and the inner wall of the solvent tank are slidably connected, the front end of the baffle is engaged with the inner wall of the feed pipe, the bottom of the feed pipe is connected to an external pumping mechanism, the outer wall of the adjusting rod is provided with threads, and the adjusting rod is connected to an external power mechanism.

[0014] The following steps are involved:

[0015] S1. Using catalyst wastewater as raw material, transfer it into the reactor body with a batching pump, drive the collecting tube to rotate with a driving motor to drive the driving wheel, and the collecting tube stirs the raw material through the guide plate. At the same time, the temperature regulating tube adjusts the raw material of the reactor body to 150°C under the action of the external temperature control mechanism, and keeps the temperature for 3 hours to obtain the polyaluminum finished product slurry;

[0016] S2, the driving motor fully stirs the solvent in the solvent tank through the stirring rod, and the solenoid valve sends the solvent in the solvent tank into the reactor body;

[0017] S3. After the wastewater and solvent in the reactor body are fully mixed, the external pumping mechanism pumps the liquid after solid-liquid separation through the collecting pipe;

[0018] S4. The external power mechanism drives the adjusting rod to rotate, and the adjusting rod drives the baffle to disengage the obstruction to the feed pipe. At the same time, the guide plate completely pushes the sediment on the bottom wall of the reactor body to the top of the feed pipe. The external pumping mechanism pumps the solid after solid-liquid separation through the feed pipe and sends it to the drying device to form solid polyaluminium chloride.

[0019] In summary, this application includes the following beneficial technical effects:

[0020] 1. The wastewater is transported to the reactor body through the feed pipe by an external pumping mechanism, and the temperature of the wastewater is adjusted by the external temperature control mechanism through the temperature regulating pipe. After the solid-liquid separation of the wastewater, the through hole at the corresponding position of the collecting pipe is adjusted to open according to the solid-liquid stratification position of the wastewater, and the servo motor drives the rotating wheel to rotate, and the rotating wheel drives the contact rod to move a certain distance, and the contact rod drives the moving rod to move, and the moving rod drives the top block to move, and the top block moves into the pushing groove. Under the action of the pushing groove, the top block drives the adjusting wheel to rotate counterclockwise by 30 degrees. At this time, the through hole at the corresponding position of the adjusting wheel is opened, and the external pumping mechanism pumps the liquid through the collecting pipe, which solves the problem that the existing wastewater cannot be treated separately after solid-liquid separation, resulting in a reduced wastewater recovery rate, and has the advantage of being convenient for solid-liquid classification treatment.

[0021] 2. The toothed belt is driven by a driving motor to rotate, and the toothed belt drives the driving wheel to rotate through the connecting wheel, and the driving wheel drives the collecting tube to rotate, and the collecting tube drives the guide plate to rotate, and the guide plate stirs the wastewater. At the same time, the driving motor drives the stirring rod to rotate, and the stirring rod fully mixes the solvent in the solvent tank. The solenoid valve transports the solvent to the reactor body through the infusion tube until the solvent completely enters the reactor body, and the driving motor stops rotating. This solves the problem of precipitation of the solvent after being stored for a period of time, resulting in inconsistent concentration and affecting the catalytic effect, and has the advantage of uniform solvent mixing.

[0022] 3. The external power mechanism drives the adjusting rod to rotate, and the adjusting rod drives the baffle to block the flow of the feed pipe. After the pumping is completed, the driving motor runs again, and the guide plate pushes the solids at the bottom of the reactor body to the top of the feed pipe. The baffle is separated from the flow blockage of the feed pipe again, and the external pumping mechanism pumps the solids through the feed pipe, which has the advantage of centralized collection. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] Figure 1 It is a schematic diagram of the overall structure in the embodiment of the present application;

[0024] Figure 2 is a schematic diagram of the structure of the support frame in an embodiment of the present application;

[0025] Figure 3 is a schematic diagram of the structure of the baffle in the embodiment of the present application;

[0026] Figure 4 is a schematic diagram of the structure of the stirring rod in the embodiment of the present application;

[0027] Figure 5 is a schematic structural diagram of a rotating wheel in an embodiment of the present application;

[0028] Figure 6 is a schematic structural diagram of a moving rod in an embodiment of the present application;

[0029] Figure 7It is a schematic diagram of the structure of the top block in the embodiment of the present application;

[0030] Figure 8 It is a schematic diagram of the structure of the push slot in the embodiment of the present application;

[0031] Fig. 9 In the embodiment of this application Figure 7 A schematic diagram of the enlarged structure in FIG.

[0032] Figure numerals: 1 reactor body, 2 temperature regulating tube, 3 collecting tube, 4 driving wheel, 5 guide plate, 6 moving rod, 7 top block, 8 adjusting wheel, 9 pushing groove, 10 limiting ring, 11 pushing frame, 12 guide rod, 13 fixing ring, 14 return spring, 15 limiting frame, 16 connecting pipe, 17 contact rod, 18 supporting frame, 19 rotating wheel, 20 servo motor, 21 connecting wheel, 22 toothed belt, 23 driving motor, 24 supporting frame, 25 infusion tube, 26 solvent tank, 27 stirring rod, 28 scraper, 29 feeding pipe, 30 baffle, 31 adjusting rod. DETAILED DESCRIPTION

[0033] The embodiment of the present application discloses an AMS monomer resin production wastewater treatment device, including a reactor body 1, a thermostatic tube 2 is embedded in the reactor body 1, an interlayer is arranged inside the reactor body 1, the thermostatic tube 2 is arranged in the interlayer, the inlet and outlet of the thermostatic tube 2 are respectively arranged on the top side wall of the reactor body 1 and the bottom wall of the reactor body 1, the arrangement of the thermostatic tube 2 facilitates the temperature control of the liquid inside the reactor body 1, a collecting tube 3 is rotatably connected to the top of the reactor body 1, a bracket is arranged on the inner wall of the reactor body 1 at the center position of the collecting tube 3, and six rows of through holes are arranged in an array on the side wall at the bottom end of the collecting tube 3.

[0034] The setting of the through hole is convenient for the pumping mechanism to pump the liquid through the collecting pipe 3. In the initial state, the through holes are all closed. The outer wall of the top end of the collecting pipe 3 is located above the reactor body 1 and is fixedly connected to the driving wheel 4. The left and right sides of the bottom of the collecting pipe 3 are fixedly connected to the guide plates 5. The inside of the collecting pipe 3 is slidably connected to a moving rod 6. The guide plate 5 extends to the inside of the feed pipe 29 at an inclined angle. The guide plate 5 has a stirring effect on the wastewater and is convenient for pushing the solids on the bottom wall of the reactor body 1 to the top of the feed pipe 29. The guide plate 5 is slidably connected to the inner wall of the reactor body 1. The bottom of the collecting pipe 3 is provided with a receiving groove that meshes with the bottom end of the moving rod 6. The setting of the receiving groove facilitates the resetting of the moving rod 6. The outer wall of the bottom end of the moving rod 6 is fixedly connected to a top block 7. The bottom end of the moving rod 6 is located above the top block 7 and is connected to six adjusting wheels 8 in an array.

[0035] The outside of the adjusting wheel 8 is composed of six baffles, and drainage channels are formed between the baffles. The baffles are slidably connected to the inner wall of the collecting pipe 3, and the baffles open and close the through holes on the side walls of the collecting pipe 3. The inner wall of the adjusting wheel 8 is provided with a push groove 9 that is slidably connected to the outer wall of the top block 7. The push groove 9 is arranged above the top block 7. The upper and lower ends of the push groove 9 are composed of vertical grooves. The center position of the push groove 9 is arranged in a “>” shape. The arrangement of the push groove 9 facilitates the moving rod 6 to drive the top block 7 to move up and down. The inner wall of the collecting pipe 3 is located at the upper and lower ends of the adjusting wheel 8, and the limiting ring 10 is fixedly connected. The top wall of the adjusting wheel 8 is fixedly connected to a push frame 11, and the side wall of the push frame 11 is fixedly connected to a guide rod 12. The inner wall of the limit ring 10 is located on the outer surface of the guide rod 12 and is fixedly connected to a fixing ring 13.

[0036] The guide rod 12 is arranged in an arc shape, and the guide rod 12 passes through the fixed ring 13. The outer surface of the guide rod 12 is located between the fixed ring 13 and the pushing frame 11 and is sleeved with a reset spring 14. The reset spring 14 is arranged to facilitate the reset of the adjusting wheel 8 when the top block 7 is separated from the pushing groove 9. The inner wall of the collecting pipe 3 is located on the outer surface of the moving rod 6 and is fixedly connected to the limiting frame 15. The top of the collecting pipe 3 is located on the outer surface of the moving rod 6 and is rotatably connected to the connecting pipe 16. The outer wall of the top of the moving rod 6 is slidably connected to the inner wall of the limiting frame 15. The connecting pipe 16 is connected to the external pumping mechanism. The rear end of the connecting pipe 16 The outer wall is provided with a fixing frame fixedly connected to the top wall of the reactor body 1, the top of the movable rod 6 is located at the top of the connecting tube 16 and is fixedly connected to the contact rod 17, the outer wall of the connecting tube 16 is located at the rear end of the contact rod 17 and is fixedly connected to a supporting frame 18, the front end of the top of the supporting frame 18 is rotatably connected to a rotating wheel 19 close to the outer wall of the contact rod 17, the contact rod 17 is composed of a plurality of discs, the outer walls of the discs are provided with teeth meshing with the rotating wheel 19, the top of the supporting frame 18 is provided with a supporting ring slidably connected to the outer wall of the contact rod 17, and the supporting ring supports and fixes the contact rod 17.

[0037] The right end of the rotating wheel 19 is located at the top of the support frame 18 and is fixedly connected to a servo motor 20. A connecting wheel 21 is meshed on the right side of the driving wheel 4. The connecting wheel 21 is composed of two gears of different sizes. The setting of the connecting wheel 21 makes the rotation speed of the stirring rod 27 greater than the rotation speed of the collecting tube 3. This setting facilitates solvent mixing. The connecting wheel 21 is rotatably connected to the top wall of the reactor body 1. A toothed belt 22 is meshed on the top outer surface of the connecting wheel 21. The inside of the toothed belt 22 is located on the right side of the connecting wheel 21 and is meshed with a driving motor 23. The outer wall of the driving motor 23 is fixedly connected to the top wall of the reactor body 1 by setting a supporting frame 24. An infusion tube 25 is connected through the right side of the reactor body 1. An electromagnetic valve is provided at the connection between the infusion tube 25 and the reactor body 1. The right end of the infusion tube 25 is connected through the solvent tank 26, and a feeding pipe is provided on the top of the solvent tank 26.

[0038] A stirring rod 27 is fixedly connected to the solvent tank 26 below the output end of the driving motor 23. The outer wall of the stirring rod 27 is composed of spiral sheets. The outer wall of the top end of the stirring rod 27 is located on the inner wall of the solvent tank 26 and is fixedly connected to a scraper 28. The scraper 28 forms a sliding connection with the inner wall of the solvent tank 26. A feed pipe 29 is connected to the bottom end of the reactor body 1. The bottom of the feed pipe 29 is connected to an external pumping mechanism. When in use, the external pumping mechanism transports wastewater to the reactor body 1 through the feed pipe 29. The external temperature control mechanism adjusts the temperature of the wastewater through the temperature regulating tube 2. The driving motor 23 drives the toothed belt 22 to rotate. The toothed belt 22 drives the driving wheel 4 to rotate through the connecting wheel 21. The driving wheel 4 drives the collecting pipe 3 to rotate. The collecting pipe 3 drives the guide plate 5 to rotate. The guide plate 5 stirs the wastewater. At the same time, the driving motor 23 drives the stirring rod 27 to rotate, and the stirring rod 27 fully mixes the solvent in the solvent tank 26.

[0039] In this embodiment, the solenoid valve delivers the solvent to the reactor body 1 through the infusion tube 25 until the solvent completely enters the reactor body 1. A baffle 30 is inserted into the feed tube 29, and the front end of the baffle 30 is engaged with the inner wall of the feed tube 29. The driving motor 23 stops rotating and waits for the solid-liquid separation of the wastewater. According to the solid-liquid stratification position of the wastewater, the through hole at the corresponding position of the collecting tube 3 is adjusted to open. The servo motor 20 drives the rotating wheel 19 to rotate, and the rotating wheel 19 drives the contact rod 17 to move a certain distance. The contact rod 17 drives the moving rod 6 to move, and the moving rod 6 drives the top block 7 to move. The top block 7 moves into the pushing groove 9. Under the action of the pushing groove 9, the top block 7 drives the adjusting wheel 8 to rotate counterclockwise by 30 degrees. At this time, the through hole at the corresponding position of the adjusting wheel 8 is opened, and the external pumping mechanism pumps the liquid through the collecting tube 3.

[0040] The rear end of the baffle 30 is internally rotatably connected with an adjusting rod 31, and the bottom wall of the reactor body 1 is rotatably connected with the rear end of the adjusting rod 31 by setting a fixed plate. The outer wall of the adjusting rod 31 is provided with a thread, and the adjusting rod 31 is connected to an external power mechanism. After the pumping is completed, the driving motor 23 runs again, and the guide plate 5 pushes the solids at the bottom of the reactor body 1 to the top of the feed pipe 29. The baffle 30 is separated from the obstruction of the feed pipe 29 again, and the external pumping mechanism pumps the solids through the feed pipe 29 and sends them to the drying device to form solid polyaluminium chloride.

[0041] The implementation principle of the AMS monomer resin production wastewater treatment equipment of the embodiment of the present application is as follows: when in use, the external pumping mechanism conveys the wastewater to the reactor body 1 through the feed pipe 29, the external temperature control mechanism adjusts the temperature of the wastewater through the temperature regulating pipe 2, the external power mechanism drives the adjusting rod 31 to rotate, the adjusting rod 31 drives the baffle 30 to block the feed pipe 29, at this time, the driving motor 23 drives the toothed belt 22 to rotate, the toothed belt 22 drives the driving wheel 4 to rotate through the connecting wheel 21, the driving wheel 4 drives the collecting pipe 3 to rotate, the collecting pipe 3 drives the guide plate 5 to rotate, the guide plate 5 stirs the wastewater, and at the same time, the driving motor 23 drives the stirring rod 27 to rotate, the stirring rod 27 fully mixes the solvent in the solvent tank 26, and the solenoid valve conveys the solvent to the reactor body 1 through the infusion pipe 25 until the solvent completely enters the reactor body. The servo motor 20 drives the rotating wheel 19 to rotate, and the rotating wheel 19 drives the contact rod 17 to move a certain distance. The contact rod 17 drives the moving rod 6 to move, and the moving rod 6 drives the top block 7 to move. The top block 7 moves into the pushing groove 9. The top block 7 drives the adjusting wheel 8 to rotate counterclockwise by 30 degrees under the action of the pushing groove 9. At this time, the through hole at the corresponding position of the adjusting wheel 8 is opened, and the external pumping mechanism pumps the liquid through the collecting pipe 3. After the pumping is completed, the driving motor 23 runs again, and the guide plate 5 pushes the solids at the bottom of the reactor body 1 to the top of the feeding pipe 29. The baffle 30 is separated from the flow resistance of the feeding pipe 29 again, and the external pumping mechanism pumps the solids through the feeding pipe 29.

[0042] The above are all preferred embodiments of the present application, and the protection scope of the present application is not limited thereto. Therefore, any equivalent changes made according to the structure, shape, and principle of the present application should be included in the protection scope of the present application.

Claims

1. AMS monomer resin production wastewater treatment equipment, including a reactor body (1), characterized in that: The reactor body (1) is inlaid with a temperature regulating tube (2), the top of the reactor body (1) is rotatably connected to a collecting tube (3), the inner wall of the reactor body (1) is provided with a bracket at the center of the collecting tube (3), the bottom side wall of the collecting tube (3) is provided with six rows of through holes, the top outer wall of the collecting tube (3) is located above the reactor body (1) and is fixedly connected to a driving wheel (4), the left and right sides of the bottom of the collecting tube (3) are fixedly connected to guide plates (5), the inside of the collecting tube (3) is slidably connected to a moving rod (6), the bottom outer wall of the moving rod (6) is fixedly connected to a top block (7), the bottom of the moving rod (6) is located above the top block (7) and is connected to six adjusting wheels (8) in an array, the outside of the adjusting wheel (8) is composed of six flow blocking blocks, and a flow blocking block is formed between the flow blocking blocks. The drainage channel is provided with a flow block and an inner wall of the collection pipe (3) in sliding connection. The inner wall of the regulating wheel (8) is provided with a push groove (9) in sliding connection with the outer wall of the top block (7). The push groove (9) is arranged above the top block (7). The upper and lower ends of the push groove (9) are composed of vertical grooves. The center position of the push groove (9) is arranged in a "">" shape. The inner wall of the collection pipe (3) is located at the upper and lower ends of the regulating wheel (8) and is fixedly connected to a limit ring (10). The top wall of the regulating wheel (8) is fixedly connected to a push frame (11). The side wall of the push frame (11) is fixedly connected to a guide rod (12). The inner wall of the limit ring (10) is located at the outer surface of the guide rod (12) and is fixedly connected to a fixing ring (13). The outer surface of the guide rod (12) is located between the fixing ring (13) and the push frame (11). A return spring (14) is connected, the inner wall of the collecting tube (3) is located on the outer surface of the moving rod (6) and is fixedly connected to a limiting frame (15), the top of the collecting tube (3) is located on the outer surface of the moving rod (6) and is rotatably connected to a connecting tube (16), the top of the moving rod (6) is located on the top of the connecting tube (16) and is fixedly connected to a contact rod (17), the outer wall of the connecting tube (16) is located at the rear end of the contact rod (17) and is fixedly connected to a support frame (18), the front end of the top of the support frame (18) is close to the outer wall of the contact rod (17) and is rotatably connected to a rotating wheel (19), the right end of the rotating wheel (19) is located on the top of the supporting frame (18) and is fixedly connected to a servo motor (20), the right side of the driving wheel (4) is meshed with a connecting wheel (21), and the outer surface of the top of the connecting wheel (21) is meshed with a toothed belt (22) The toothed belt (22) is internally located on the right side of the connecting wheel (21) and is meshed with a drive motor (23). The outer wall of the drive motor (23) is fixedly connected to the top wall of the reactor body (1) by providing a carrier frame (24). A liquid infusion tube (25) is connected through the right side of the reactor body (1). The right end of the liquid infusion tube (25) is connected through the solvent tank (26). A stirring rod (27) is fixedly connected to the solvent tank (26) below the output end of the drive motor (23). The outer wall of the top end of the stirring rod (27) is located on the inner wall of the solvent tank (26) and is fixedly connected to a scraper (28). A feed pipe (29) is connected through the bottom end of the reactor body (1). A baffle (30) is inserted into the feed pipe (29). An adjusting rod (31) is rotatably connected to the rear end of the baffle (30).The bottom wall of the reactor body (1) is rotatably connected to the rear end of the adjusting rod (31) by means of a fixed plate.

2. The AMS monomer resin production wastewater treatment equipment according to claim 1, characterized in that: The reactor body (1) is provided with an interlayer inside, the temperature regulating tube (2) is arranged in the interlayer, and the liquid inlet and outlet of the temperature regulating tube (2) are respectively arranged on the top side wall of the reactor body (1) and the bottom wall of the reactor body (1).

3. The AMS monomer resin production wastewater treatment equipment according to claim 1, characterized in that: The guide plate (5) extends into the interior of the feed pipe (29) at an inclined angle, the guide plate (5) is slidably connected to the inner wall of the reactor body (1), and a receiving groove is provided at the bottom of the collecting pipe (3) and engages with the bottom end of the moving rod (6).

4. The AMS monomer resin production wastewater treatment equipment according to claim 1, characterized in that: The guide rod (12) is arranged in an arc shape, the guide rod (12) passes through the fixed ring (13), the outer wall of the top end of the movable rod (6) and the inner wall of the limit frame (15) form a sliding connection, the connecting pipe (16) is connected to the external pumping mechanism, and the outer wall of the rear end of the connecting pipe (16) is provided with a fixed frame fixedly connected to the top wall of the reactor body (1).

5. The AMS monomer resin production wastewater treatment equipment according to claim 1, characterized in that: The contact rod (17) is composed of a plurality of discs, the outer walls of the discs are provided with teeth meshing with the rotating wheel (19), the top of the support frame (18) is provided with a support ring which is slidably connected to the outer wall of the contact rod (17), the connecting wheel (21) is composed of two gears of different sizes, and the connecting wheel (21) is rotatably connected to the top wall of the reactor body (1).

6. The AMS monomer resin production wastewater treatment equipment according to claim 1, characterized in that: A solenoid valve is provided at the connection between the liquid delivery pipe (25) and the reactor body (1); a feed pipe is provided at the top of the solvent tank (26); the outer wall of the stirring rod (27) is composed of spiral sheets; the scraper (28) is slidably connected to the inner wall of the solvent tank (26); the front end of the baffle (30) is meshed with the inner wall of the delivery pipe (29); the bottom of the delivery pipe (29) is connected to an external pumping mechanism; the outer wall of the adjustment rod (31) is provided with threads; and the adjustment rod (31) is connected to an external power mechanism.

7. The AMS monomer resin production wastewater treatment process performed by the equipment according to any one of claims 1 to 6 comprises the following steps: S1. Catalyst wastewater is used as a raw material and is transferred into a reactor body (1) by a dosing pump. A driving motor (23) drives a driving wheel (4) to drive a collecting tube (3) to rotate. The collecting tube (3) stirs the raw material through a guide plate (5). At the same time, a temperature control tube (2) adjusts the raw material in the reactor body (1) to a temperature of 150° C. as a process requirement under the action of an external temperature control mechanism, and then the temperature is maintained for 3 hours to obtain a polyaluminum finished product slurry. S2, the driving motor (23) fully stirs the solvent in the solvent tank (26) via the stirring rod (27), and the solenoid valve delivers the solvent in the solvent tank (26) into the reactor body (1); S3, after the wastewater and the solvent in the reactor body (1) are fully mixed, the external pumping mechanism pumps the liquid after solid-liquid separation through the collecting pipe (3); S4. The external power mechanism drives the adjusting rod (31) to rotate, and the adjusting rod (31) drives the baffle plate (30) to disengage from the obstruction to the conveying pipe (29). At the same time, the guide plate (5) completely pushes the sediment on the inner bottom wall of the reactor body (1) to the top of the conveying pipe (29). The external pumping mechanism pumps the solid after the solid-liquid separation through the conveying pipe (29) and sends it to the drying device to form solid polyaluminium chloride.

Citation Information

Patent Citations

  • Catalyst adding device for preparing ultraviolet light absorber

    CN220696670U