A natural gas triethylene glycol dehydration device and its use method
By using filter separation components and electrode shunt components in the natural gas triethylene glycol dehydration device, the problems of low gas separation efficiency and corrosion during liquid-rich reactions are solved, and the effect of efficient purification and extending the life of the device is achieved.
Patent Information
- Application Number
- CN202411289004.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-14
- Publication Date
- 2024-12-17
- Estimated Expiration
- 2044-09-14
AI Technical Summary
The existing natural gas triglycol dehydration device is constant during the liquid-rich reaction, resulting in limited separation of carbon dioxide, which cannot completely remove internal gas, and reduces the efficiency of reusing water absorption; the triglycol rich liquid is viscous, which is easy to cause corrosion and flow in the tower. The rich liquid that has slowed down speed and is not fully purified cannot be processed, which will affect the life of the device and the effectiveness of use.
A natural gas triethylene glycol dehydration device is designed, including a filter separation assembly, a decompression discharge assembly and an electrode shunt assembly. The three shunt assembly is realized through a combination of a flow tube, a roller, a heating ring, a scraper, a vibrating plate and an electrode shunt assembly. Efficient filtration and purification of alcohol-rich liquids, remove carbon dioxide and sulfides, prevent corrosion, and reprocess them through reflow tubes.
It improves the purification effect of the three glycemic and alcohol-rich liquid, extends the service life of the device, improves the natural gas dehydration efficiency, reduces energy consumption and costs, and enhances the pipeline conveying capacity.
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Figure CN118807319B_ABST
Abstract
Description
Technical Field
[0001] The present invention relates to the technical field of natural gas processing, and in particular to a natural gas triethylene glycol dehydration device and a use method thereof. Background Art
[0002] The natural gas triethylene glycol dehydration process is one of the most commonly used methods in the natural gas industry. It belongs to the solvent absorption method. This process uses glycol substances as absorbents to fully contact with natural gas, so that water is transferred to the solvent to achieve the purpose of dehydration. Triethylene glycol has strong hydrophilicity and non-conductive properties. It can form hydrogen bonds with water in natural gas, thereby achieving efficient dehydration. The core equipment of this process is the absorption tower, in which the natural gas dehydration process is completed in the absorption tower, and the triethylene glycol rich liquid is heated in the regeneration tower to separate the water under low pressure and high temperature, completing the regeneration process and realizing recycling.
[0003] The existing Chinese patent publication number CN117643744A discloses that the speed of gas generation by triethylene glycol rich liquid is accelerated by heating and stirring to achieve the effect of removing carbon dioxide gas. However, when the triethylene glycol rich liquid reacts, the heating temperature is constant, which only leads to limited separation of carbon dioxide and fails to completely treat the internal gas, making it difficult to achieve a rapid and thorough removal effect, thereby reducing the efficiency of repeated use of water absorption.
[0004] Secondly, the triethylene glycol rich liquid is a viscous liquid. When the temperature is continuously increased, it will produce carbon dioxide and sulfides. In addition, the characteristics of the viscous liquid will cause the triethylene glycol rich liquid and sulfides to adhere to the inner wall of the tower body, slowing down the flow rate and easily causing corrosion in the tower. At the same time, the incompletely purified triethylene glycol rich liquid cannot be reprocessed, which greatly reduces the subsequent use of triethylene glycol, affects the service life of the device, and reduces the transportation of pipelines. Therefore, the present application provides a natural gas triethylene glycol dehydration device and a method for using the same to meet the needs. Summary of the invention
[0005] The technical problem to be solved by the present invention is to provide a natural gas triethylene glycol dehydration device and a method for using the same, so as to solve the problem that during the existing triethylene glycol rich liquid reaction, the heating temperature is constant, which only leads to limited separation of carbon dioxide, and the internal gas cannot be completely processed, making it difficult to achieve a rapid and thorough removal effect, thereby reducing the efficiency of repeated use of water absorption. Secondly, the triethylene glycol rich liquid is a viscous liquid, which will produce carbon dioxide and sulfide when continuously heated, and the characteristics of the viscous liquid will make the triethylene glycol rich liquid and sulfide adhere to the inner wall of the tower body, slowing down the flow rate and easily causing corrosion in the tower. At the same time, the incompletely purified triethylene glycol rich liquid cannot be reprocessed, resulting in a significant reduction in the subsequent use of the triethylene glycol, affecting the service life of the device, and reducing the problem of pipeline transportation.
[0006] In order to solve the above technical problems, the present invention provides the following technical solutions:
[0007] A natural gas triethylene glycol dehydration device comprises a tower body, an artificial ladder platform is installed on the outer surface of the tower body, a box-type motor is installed at one end of the tower body, a servo motor is installed on the top of the tower body, a fan blade tube is installed on the output end of the servo motor, a delivery pipe is installed on one end of the top of the tower body, and an exhaust pipe is installed on the other end of the top of the tower body; it also includes a filtering and separating component, a filtering and separating component is installed at the bottom of the delivery pipe, and the filtering and separating component is used to filter impurities and sulfides contained in triethylene glycol; an impurity removal and emission component, a impurity removal and emission component is installed at the bottom of the filtering and separation component, and the impurity removal and emission component is used to collect triethylene glycol and remove internal sulfides and carbon dioxide again; an electrode shunt component, an electrode shunt component is installed at the bottom of the impurity removal and emission component, and the electrode shunt component is used for a repeated process of discharging or refluxing triethylene glycol.
[0008] Optionally, a pressure relief valve is installed on the top of the tower body, the output end of the box motor is an arc-shaped gear tooth, the output end of the servo motor is provided with a pipe, a plurality of groups of fan blades are arranged inside the pipe, and the delivery pipe is a three-way through pipe.
[0009] Optionally, the filtering and separation assembly includes a guide pipe, which is installed at the bottom of the delivery pipe, with a filter installed at one end of the guide pipe, a sleeve pipe installed at one end of the guide pipe, a hole is opened inside the sleeve pipe, a roller is rotatably connected inside the sleeve pipe, the inner wall of the roller and the inner wall of the hole are in contact with each other, the installation angle of the roller is set to an oblique 15 degree, a heating ring is installed on the surface of the roller, a fixed rotating shaft seat is installed at one end of the roller, and an air supply pipe is installed on the top of one end of the fixed rotating shaft seat.
[0010] Optionally, an extension seat is installed at one end of the fixed rotating shaft seat, a scraper is installed at one end of the extension seat, a vibration plate is hinged at the bottom of the scraper, a connecting block is installed at one end of the vibration plate, the bottom of the connecting block is rotatably connected to a support plate, a positioning rod is installed at one end of the support plate, an elastic frame is installed at the bottom of one end of the support plate, a rotating lever is installed on the inner wall of the drum, and the position of the rotating lever is set on the rotation path of the support plate.
[0011] Optionally, the impurity removal and discharge assembly includes an infusion tube valve, which is installed at one end of the guide tube, a liquid collecting bin is installed at one end of the infusion tube valve, a trigger rod is provided at the top of the infusion tube valve, a feedback button is installed at the top of the trigger rod, a trigger block is installed at one end of the feedback button, an exhaust disk is installed at the top of the liquid collecting bin, and an oil cylinder is installed at the bottom of the exhaust disk.
[0012] Optionally, a conical tube is installed at the bottom of the liquid collecting bin, a molecular sieve is installed at the top of the conical tube, a spring seat is installed on the inner wall of the liquid collecting bin, the spring seat is arranged on the top of the molecular sieve, a pressure plate is installed on the top of the spring seat, a magnet is arranged inside the pressure plate, and the magnet is arranged below the trigger block.
[0013] Optionally, the electrode shunt assembly includes a tee, which is installed at the bottom of the conical tube, a conductive paddle is installed at one end of the tee, the conductive paddle extends to the interior of the tee, an insulating bin is installed at one end of the conductive paddle, a conductive rod is installed inside the insulating bin, a spring is provided on the top of the conductive rod and connected to the bottom of the conductive paddle, and a power box is installed at one end of the insulating bin.
[0014] Optionally, the bottom of the conductive rod is rotatably connected to a connecting rod, one end of the connecting rod is rotatably connected to a main gear, one end of the main gear is meshingly connected to a slave gear, one end of the main gear is installed with a limit frame, both ends of the limit frame are installed at one end of the slave gear, one end of the slave gear is meshingly connected to a rack, one end of the rack is installed with a baffle, and the size of the baffle is the same as the internal diameter of the tee.
[0015] Optionally, a bayonet slot is installed inside the three-way pipe, an extension frame is installed at one end of the bayonet slot, the top of the extension frame is connected to the bottom of the baffle, a discharge port is provided at one end of the three-way pipe, a return pipe is installed at the other end of the three-way pipe, and the other end of the return pipe is provided at one end of the delivery pipe.
[0016] The present application also provides another technical solution: a method for using a natural gas triethylene glycol dehydration device, comprising the following steps:
[0017] S1: Connect the liquid discharge port of the absorption tower to the delivery pipe on the top of the tower body, so that the triethylene glycol rich liquid from the absorption tower is injected into the interior of the tower body;
[0018] S2: The triethylene glycol rich liquid injected into the tower body flows into the two channels through the guide pipe for filtration, and then is discharged to the drum through the guide pipe;
[0019] S3: When TEG is discharged into the drum, the box motor rotates to drive the drum to rotate. At the same time, the heating ring continuously heats the TEG rich liquid inside the drum, increasing the TEG rich liquid on the heating surface and quickly generating gas and sulfide.
[0020] S4: The scraper inside the drum scrapes off the TEG rich liquid and derivatives on the inner wall of the drum to prevent residue. The two layers of drums with different temperatures accelerate the speed at which TEG rich liquid produces gas and sulfide inside. The gas is discharged from the tower through the gas pipe and the fan pipe.
[0021] S5: After the reaction in the drum, the TEG rich liquid carries the reacted derivatives and sulfides and flows to the liquid collecting bin for collection. When the pressing plate contacts the trigger block, the liquid infusion is stopped, and the output end of the oil cylinder squeezes the pressing plate to make the TEG rich liquid pass through the molecular sieve, separating the internal sulfides and water from the TEG rich liquid.
[0022] S6: When the conical tube inputs the re-separated triethylene glycol rich liquid into the electrode diversion assembly, the triethylene glycol rich liquid flows in through the top of the tee. When the triethylene glycol rich liquid contains water, the carbon dioxide gas and sulfide are not completely separated. The conductive rod drives the connecting rod to move, and drives the baffle to descend to the inside of the tee to block the discharge port. At this time, the triethylene glycol rich liquid that has not been purified and separated completely will be transported to the delivery pipe through the reflux pipe for reprocessing, and the triethylene glycol rich liquid that has not been purified and separated completely will be continuously purified.
[0023] Compared with the prior art, the present invention has at least the following beneficial effects:
[0024] In the above scheme, by setting up a filtering and separation component, utilizing the cooperation between the guide pipe, filter, drum, heating ring, air pipe, scraper, vibration plate and elastic frame, the triethylene glycol rich liquid is filtered through a layer and then flows into the drum. The internal triethylene glycol rich liquid is heated by the heating ring to produce carbon dioxide and sulfide. The air pipe transports the carbon dioxide gas. The sulfide follows the triethylene glycol rich liquid and flows into the next layer of the drum for heating treatment at different temperatures, so that it can be removed more efficiently. At the same time, the scraper scrapes the liquid on the inner wall of the drum, and removes the liquid through the vibration plate to prevent the residue and accumulation of liquid and sulfide, which will corrode the inner wall of the drum.
[0025] By setting up impurity removal and discharge components, using a liquid infusion pipe valve, a trigger rod, a liquid collecting bin, a cylinder, a trigger block pressure plate and a molecular sieve, when the triethylene glycol rich liquid removes the internal gas by heating, the triethylene glycol rich liquid carries the sulfide flow into the liquid collecting bin for accumulation. When the accumulation height continues to rise and pushes the pressure plate to touch the trigger block, the liquid infusion pipe valve is closed to stop the infusion, the output end of the cylinder is squeezed toward the pressure plate, and the triethylene glycol rich liquid flows into the conical tube through the molecular sieve. The molecular sieve simultaneously separates the sulfide and water substances in the triethylene glycol rich liquid, thereby improving the purity of the triethylene glycol rich liquid, reducing the energy consumption of the triethylene glycol rich liquid, improving the durability of the circulating use of the triethylene glycol rich liquid, reducing the cost of using the device, and improving the filtering effect of the molecular sieve.
[0026] At the same time, in conjunction with the electrode shunt assembly, using a three-way pipe, a conductive paddle, a conductive rod, a connecting rod, a main gear, a rack, a baffle, a bayonet slot, a discharge port and a reflux pipe, after the triethylene glycol rich liquid is separated from the sulfide and the gas, it flows into the three-way pipe through the tapered pipe and contacts the conductive paddle. At this time, the paddle is not charged to detect the inside of the triethylene glycol rich liquid. When the triethylene glycol rich liquid contains impurities and water components, the conductive paddle conducts electricity and generates attraction with the conductive rod. The two are connected in series, and the conductive rod moves to drive the main gear to rotate, thereby controlling the baffle at the reflux pipe. The baffle plate of the discharge port is closed, and the triethylene glycol rich liquid containing impurities and water passes through the reflux pipe for reprocessing. The triethylene glycol rich liquid that has not been completely purified and separated will be transported to the delivery pipe through the reflux pipe for reprocessing. The triethylene glycol rich liquid that has not been completely purified and separated is continuously purified. When the triethylene glycol rich liquid does not contain impurities and water, the discharge port is continuously opened to transport the triethylene glycol to the front end for recycling in natural gas dehydration, thereby improving the use effect of triethylene glycol, extending the service life of the device, increasing the transportation capacity of the pipeline, and improving the efficiency of dehydration. BRIEF DESCRIPTION OF THE DRAWINGS
[0027] The accompanying drawings, which are incorporated herein and constitute a part of the specification, illustrate embodiments of the invention and, together with the description, further serve to explain the principles of the invention and to enable those skilled in the relevant art to make and use the invention.
[0028] Figure 1 It is a schematic diagram of the main three-dimensional structure of the dehydration device;
[0029] Figure 2 It is a three-dimensional structural schematic diagram of the dehydration device from another perspective;
[0030] Figure 3 It is a three-dimensional structural diagram of the internal structure of the dehydration device;
[0031] Figure 4 It is a schematic diagram of the cross-sectional plan structure of the dehydration device;
[0032] Figure 5 It is a three-dimensional structural schematic diagram of the position relationship between the delivery pipe and the guide pipe;
[0033] Figure 6 It is a schematic diagram of the internal three-dimensional structure of the drum;
[0034] Figure 7 It is a schematic diagram of the three-dimensional structure of the scraper;
[0035] Figure 8 It is a three-dimensional structural schematic diagram of the position relationship between the guide pipe and the impurity removal and discharge component;
[0036] Fig. 9 It is a schematic diagram of the internal three-dimensional structure of the liquid collecting bin;
[0037] Fig.10 Schematic diagram of the three-dimensional structure of molecular sieve;
[0038] Fig.11 It is a schematic diagram of the three-dimensional structure of the tapered tube and the three-way tube;
[0039] Fig.12 It is a schematic diagram of the three-dimensional structure of the electrode shunt component;
[0040] Fig.13 This is a schematic diagram of the three-dimensional structure inside the insulation compartment.
[0041] Reference numerals:
[0042] 1. Tower body; 2. Manual ladder platform; 3. Box motor; 4. Servo motor; 5. Delivery pipe; 6. Filter separation assembly; 61. Guide pipe; 62. Filter; 63. Ring pipe; 64. Roller; 65. Heating ring; 66. Fixed shaft seat; 67. Air pipe; 68. Scraper; 69. Vibrating plate; 610. Connecting block; 611. Support plate; 612. Positioning rod; 613. Extension seat; 614. Elastic frame; 615. Rotating lever; 7. De-impurity discharge assembly; 71. Infusion pipe valve; 72. Trigger rod; 73. Feedback button; 74. Collector Liquid tank; 75, exhaust plate; 76, oil cylinder; 77, trigger block; 78, magnet; 79, pressure plate; 710, spring seat; 711, molecular sieve; 712, conical tube; 8, electrode shunt assembly; 81, three-way pipe; 82, conductive paddle; 83, insulating bin; 84, conductive rod; 85, power box; 86, connecting rod; 87, main gear; 88, slave gear; 89, rack; 810, baffle; 811, bayonet slot; 812, discharge port; 813, reflux pipe; 814, extension frame; 815, limit frame; 9, exhaust pipe; 10, fan blade pipe.
[0043] As shown in the figure, in order to clearly implement the structure of the embodiment of the present invention, specific structures and devices are marked in the figure, but this is only for illustrative purposes and is not intended to limit the present invention to the specific structure, device and environment. According to specific needs, ordinary technicians in this field can adjust or modify these devices and environments. DETAILED DESCRIPTION
[0044] The following is a detailed description of a natural gas triethylene glycol dehydration device and a method for using the device provided by the present invention in conjunction with the accompanying drawings and specific embodiments. At the same time, it is explained here that in order to make the embodiments more detailed, the following embodiments are the best and preferred embodiments, and those skilled in the art may also adopt other alternative methods to implement some known technologies; and the accompanying drawings are only for a more specific description of the embodiments, and are not intended to specifically limit the present invention.
[0045] In general, a term can be understood, at least in part, from its use in context. For example, depending, at least in part, on the context, the term "one or more" as used herein can be used to describe any feature, structure, or characteristic in the singular sense, or can be used to describe a combination of features, structures, or characteristics in the plural sense. Additionally, the term "based on" can be understood as not necessarily intended to convey an exclusive set of factors, but can instead, depending, at least in part, on the context, allow for the presence of other factors that are not necessarily explicitly described.
[0046] It will be understood that the meanings of “on,” “over,” and “above” in the present invention should be interpreted in the broadest manner, so that “on” not only means “directly on” something, but also includes the meaning of being “on” something with intervening features or layers therebetween, and “on” or “over” not only means “on” or “above” something, but also includes the meaning of being “on” or “above” something with no intervening features or layers therebetween.
[0047] Additionally, spatially relative terms such as "under," "beneath," "lower," "above," "upper," and the like may be used herein for descriptive convenience to describe the relationship of one element or feature to another element or features, as shown in the accompanying drawings. Spatially relative terms are intended to encompass different orientations of the device in use or operation in addition to the orientation depicted in the accompanying drawings. The device may be oriented in other ways, and the spatially relative descriptors used herein may be similarly interpreted accordingly.
[0048] like Figures 1 to 13 As shown, an embodiment of the present invention provides a natural gas triethylene glycol dehydration device, including a tower body 1, an artificial ladder platform 2 is installed on the outer surface of the tower body 1, a box motor 3 is installed at one end of the tower body 1, a servo motor 4 is installed on the top of the tower body 1, a fan blade tube 10 is installed at the output end of the servo motor 4, a delivery pipe 5 is installed at one end of the top of the tower body 1, and an exhaust pipe 9 is installed at the other end of the top of the tower body 1; it also includes a filtering and separating component 6, a filtering and separating component 6 is installed at the bottom of the delivery pipe 5, and the filtering and separating component 6 is used to filter impurities and sulfides contained in triethylene glycol; an impurity removal and emission component 7, a impurity removal and emission component 7 is installed at the bottom of the filtering and separation component 6, and the impurity removal and emission component 7 is used to collect triethylene glycol and remove internal sulfides and carbon dioxide again; an electrode shunt component 8, an electrode shunt component 8 is installed at the bottom of the impurity removal and emission component 7, and the electrode shunt component 8 is used for a repeated process of discharging or refluxing triethylene glycol.
[0049] As an implementation method in this embodiment, Figures 5 to 8As shown, a pressure relief valve is installed on the top of the tower body 1, the output end of the box motor 3 is an arc-shaped gear, the output end of the servo motor 4 is provided with a pipeline, a plurality of fan blades are arranged inside the pipeline, the delivery pipe 5 is a three-way through pipe, and the filtering and separating component 6 includes a guide pipe 61, which is installed at the bottom of the delivery pipe 5, a filter 62 is installed at one end of the guide pipe 61, a sleeve pipe 63 is installed at one end of the guide pipe 61, a hole is opened inside the sleeve pipe 63, a roller 64 is rotatably connected inside the sleeve pipe 63, the inner wall of the roller 64 and the inner wall of the hole are fitted together, the installation angle of the roller 64 is set to be inclined at 15 degrees, a heating ring 65 is installed on the surface of the roller 64, a fixed shaft seat 66 is installed at one end of the roller 64, and the top of one end of the fixed shaft seat 66 An air delivery pipe 67 is installed, an extension seat 613 is installed at one end of the fixed rotating shaft seat 66, a scraper 68 is installed at one end of the extension seat 613, a vibration plate 69 is hinged at the bottom of the scraper 68, a connecting block 610 is installed at one end of the vibration plate 69, a support plate 611 is rotatably connected to the bottom of the connecting block 610, a positioning rod 612 is installed at one end of the support plate 611, an elastic frame 614 is installed at the bottom of one end of the support plate 611, a rotating lever 615 is installed on the inner wall of the drum 64, and the position of the rotating lever 615 is set on the rotation path of the support plate 611. When the triethylene glycol rich liquid enters the tower body 1 through the delivery pipe 5, the guide pipe 61 first guides the triethylene glycol rich liquid to the filter 62, and after a layer of filtration, it flows to the next through the bottom guide pipe 61. At the filter 62, the triethylene glycol rich liquid after double-layer filtration flows to the collar pipe 63 through the guide pipe 61, and the box motor 3 is started. The arc gear at the output end of the box motor 3 meshes with the gear at one end of the roller 64 inclined at 15 degrees and rotates synchronously. The collar pipe 63 is arranged at the bottom of the filter 62 and does not rotate. Since the collar pipe 63 and the roller 64 are rotatably installed through a sealed bearing and are partially inside the roller 64, when one end of the roller 64 rotates, the triethylene glycol rich liquid flows into the inside of the roller 64 through the collar pipe 63. At this time, the heating ring 65 continues to heat up before, and continuously heats the triethylene glycol rich liquid inside the roller 64. During the rolling process of the roller 64, the triethylene glycol rich liquid is driven to roll inside, thereby increasing the heating surface. Rapid temperature rise generates gas and sulfide. The air pipe 67 on the fixed rotating shaft seat 66 at one end of the drum 64 is affected by the rotation of the fan blades inside the fan blade tube 10, generating negative pressure to quickly absorb the gas generated inside the drum 64 from the inside of the drum 64 to the air pipe 67, and transport it to the exhaust pipe 9 for gas treatment. When the drum 64 rotates, the scraper 68 scrapes off the triethylene glycol rich liquid and sulfide residues on the inner wall of the drum 64 to prevent them from remaining on the inner wall of the drum 64. The extension seat 613 at one end is fixed to one end of the fixed rotating shaft seat 66, and is fixed by the spring of the extension seat 613 itself and the rotation seat to continuously support the inner wall of the drum 64. At the same time, the rotating lever 615 rotates with the inner wall of the drum 64, and collides with the support plate 611 at the bottom every time it rotates one circle.The support plate 611 is fanned at the front end of the positioning rod 612, and the elastic frames 614 installed at the upper and lower ends of the support plate 611 enable the support plate 611 to perform short-term reciprocating fanning to provide short-term movement. The fanning of the support plate 611 causes the rotationally connected connecting block 610 to move. When the connecting block 610 moves, the vibration plate 69 at one end is fanned, and the force generated by the fanning is transmitted to the scraper 68, thereby preventing the liquid from remaining on the surface and accelerating the flow of the liquid.
[0050] As an implementation method in this embodiment, Figures 8 to 11 As shown, the impurity removal and discharge component 7 includes a liquid infusion pipe valve 71, which is installed at one end of the guide pipe 61, and a liquid collecting bin 74 is installed at one end of the liquid infusion pipe valve 71. A trigger rod 72 is arranged on the top of the liquid infusion pipe valve 71, and a feedback button 73 is arranged on the top of the trigger rod 72. A trigger block 77 is arranged on one end of the feedback button 73. An exhaust disk 75 is installed on the top of the liquid collecting bin 74, and an oil cylinder 76 is installed on the bottom of the exhaust disk 75. A conical tube 712 is installed on the bottom of the liquid collecting bin 74, and a molecular sieve 711 is installed on the top of the conical tube 712. A spring seat 710 is installed on the inner wall of the liquid collecting bin 74, and the spring seat 710 is arranged on the top of the molecular sieve 711. A pressure plate 79 is installed on the top of the spring seat 710, and a magnet 78 is arranged inside the pressure plate 79. The magnet 78 is arranged below the trigger block 77. When the triethylene glycol rich liquid flows to the The infusion pipe valve 71 flows into the interior of the liquid collecting bin 74 at one end through the infusion pipe valve 71. At this time, the triethylene glycol rich liquid accumulates in the liquid collecting bin 74, and lifts up the pressure plate 79. When the pressure plate 79 moves upward, the magnet 78 produces a certain amount of lifting effect on the pressure plate 79. When the pressure plate 79 contacts the trigger block 77, the feedback button 73 presses downward and contacts the trigger rod 72. The trigger rod 72 locks the inside of the infusion pipe valve 71 to close the infusion. The exhaust plate 75 transports the produced carbon dioxide gas and rises to the top of the tower body 1. At this time, the oil cylinder 76 outputs to squeeze the pressure plate 79 downward. When the pressure plate 79 is squeezed downward, the pressure plate 79 squeezes the spring seat 710 downward, and the triethylene glycol rich liquid is separated again through the molecular sieve 711. The triethylene glycol rich liquid after diversion flows into the next component through the tapered tube 712 for diversion treatment.
[0051] As an implementation method in this embodiment, Figures 11 to 13As shown, the electrode shunt assembly 8 includes a three-way pipe 81, which is installed at the bottom of the tapered tube 712, and a conductive paddle 82 is installed at one end of the three-way pipe 81. The conductive paddle 82 extends to the inside of the three-way pipe 81, and an insulating bin 83 is installed at one end of the conductive paddle 82. A conductive rod 84 is installed inside the insulating bin 83, and a spring is provided on the top of the conductive rod 84 to connect with the bottom of the conductive paddle 82. A power box 85 is installed at one end of the insulating bin 83, and a connecting rod 86 is rotatably connected to the bottom of the conductive paddle 82. One end of the connecting rod 86 is rotatably connected to a main gear 87, and one end of the main gear 87 is meshed and connected to a slave gear 88. A limiting frame 81 is installed at one end of the main gear 87 5. Both ends of the limit frame 815 are installed at one end of the slave gear 88. One end of the slave gear 88 is meshed with a rack 89. One end of the rack 89 is installed with a baffle 810. The size of the baffle 810 is the same as the inner diameter of the tee 81. The inside of the tee 81 is installed with a bayonet slot 811. One end of the bayonet slot 811 is installed with an extension frame 814. The top of the extension frame 814 is connected to the bottom of the baffle 810. One end of the tee 81 is provided with a discharge port 812. The other end of the tee 81 is provided with a reflux pipe 813. The other end of the reflux pipe 813 is provided at one end of the delivery pipe 5. When the conical pipe 712 inputs the triethylene glycol rich solution separated again into the electrode shunt assembly At 8, the triethylene glycol rich liquid flows in through the top of the three-way pipe 81, covering the conductive pick 82. At this time, the conductive pick 82 is not charged. Affected by the continuous power transmission of the power box 85 on one side of the insulating chamber 83, the conductive rod 84 is charged, and the triethylene glycol liquid itself is not conductive. When the conductive rod 84 is connected to the conductive pick 82, it means that when the triethylene glycol rich liquid is conductive, the triethylene glycol rich liquid contains water at this time, and the carbon dioxide gas and the sulfide are not completely separated. The conductive rod 84 drives the connecting rod 86 to move. When the connecting rod 86 moves, it drives the main gear 87 to rotate. When the main gear 87 rotates, the slave gear 88 at one end of the reflux pipe 813 rotates. When the slave gear 88 rotates, the one end The meshingly connected rack 89 moves upward and rises. When the rack 89 rises, the baffle 810 at one end rises inside the bayonet slot 811. When the baffle 810 rises, it drives the extension frame 814 to move with it, ensuring the airtightness of one side of the bayonet slot 811. Due to the action of the limiting frame 815, when the main gear 87 rotates, the slave gear 88 of the discharge port 812 at the other end rotates to drive the rack 89 to descend. At the same time, the baffle 810 descends to the inside of the three-way pipe 81 to block the discharge port 812. At this time, the triethylene glycol rich liquid that has not been completely purified and separated will be transported to the delivery pipe 5 through the reflux pipe 813 for further processing, and the triethylene glycol rich liquid that has not been completely purified and separated will be continuously purified.
[0052] The working principle of the technical solution provided by the present invention is as follows:
[0053] First, the drainage pipe of the absorption tower is connected to the delivery pipe 5 on the top of the tower body 1 through the artificial ladder platform 2, so that the triethylene glycol rich liquid in the absorption tower is continuously injected into the tower body 1, and the servo motor 4 is started to make the fan pipe 10 at the output end of the servo motor 4 start to work, so as to generate a negative pressure air duct, which is used to transport the gas generated inside the tower body 1 to the exhaust pipe 9 through the air duct to treat the gas. At the same time, when the triethylene glycol rich liquid enters the tower body 1 through the delivery pipe 5, the filtering and separation component 6 starts to treat the triethylene glycol rich liquid, and the guide pipe 61 first guides the triethylene glycol rich liquid to the filter 62, and after a layer of filtration, it flows to the next filter 62 through the bottom guide pipe 61. The triethylene glycol rich liquid after double-layer filtration flows to the collar pipe 63 through the guide pipe 61, and the box motor 3 is started, and the arc gear at the output end of the box motor 3 , meshing with the gear at one end of the 15-degree inclined roller 64, and rotating synchronously, the sleeve tube 63 is arranged at the bottom of the filter 62 and does not rotate. Since the sleeve tube 63 and the roller 64 are rotatably installed through a sealed bearing and are partially inside the roller 64, when the roller 64 at one end rotates, the triethylene glycol rich liquid flows into the inside of the roller 64 through the sleeve tube 63. At this time, the heating ring 65 continues to heat up before, and continuously heats the triethylene glycol rich liquid inside the roller 64. During the rolling of the roller 64, the triethylene glycol rich liquid is driven to roll inside to increase the heating surface. The triethylene glycol rich liquid quickly heats up inside the roller 64 to produce gas and sulfide. The air delivery pipe 67 on the fixed rotating shaft seat 66 at one end of the roller 64 is affected by the rotation of the fan blades inside the fan blade tube 10, and a negative pressure is generated to quickly absorb the gas generated inside the roller 64 from the inside of the roller 64 to the air delivery pipe 67, and transport it to the exhaust pipe 9 for gas treatment.
[0054] When the drum 64 rotates, the scraper 68 scrapes off the triethylene glycol rich liquid and sulfide residue on the inner wall of the drum 64 to prevent them from remaining on the inner wall of the drum 64, and the extension seat 613 at one end is fixed to one end of the fixed rotating shaft seat 66, and the extension seat 613 itself The spring and the fixing of the rotating seat continue to support the inner wall of the drum 64. At the same time, the rotating lever 615 rotates along with the inner wall of the drum 64. Every time it rotates one circle, it collides with the support plate 611 at the bottom. The support plate 611 is fanned at the front end of the positioning rod 612, and the elastic frames 614 installed at the upper and lower ends of the support plate 611 enable the support plate 611 to perform a short-term reciprocating fanning to provide a short-term power. Under the fanning of the support plate 611, the rotatably connected connecting block 610 moves. When the connecting block 610 moves, the vibrating plate 69 at one end fans, and the force generated by the fanning is transmitted to the scraper 68, thereby preventing the liquid from remaining on the surface and accelerating the flow of the liquid.
[0055] After the separation treatment by the two-layer roller 64, it flows to the impurity removal discharge component 7, and the triethylene glycol rich liquid flows to the infusion pipe valve 71 through the guide pipe 61, and flows into the interior of the liquid collecting bin 74 at one end through the infusion pipe valve 71. At this time, the triethylene glycol rich liquid is accumulated in the liquid collecting bin 74, and the pressure plate 79 is lifted up. When the pressure plate 79 moves upward, the magnet 78 produces a certain amount of lifting effect on the pressure plate 79. When the pressure plate 79 contacts the trigger block 77, the feedback button 73 presses downward and contacts The trigger rod 72 locks the inside of the infusion tube valve 71, closes the infusion, and the exhaust plate 75 delivers the produced carbon dioxide gas and rises to the top of the tower body 1. At this time, the oil cylinder 76 outputs and squeezes the pressure plate 79 downward. When the pressure plate 79 squeezes downward, the pressure plate 79 squeezes the spring seat 710 downward, and the triethylene glycol rich liquid is separated again through the molecular sieve 711. The triethylene glycol rich liquid after diversion flows into the next component through the tapered tube 712 for diversion treatment.
[0056] When the conical tube 712 inputs the separated triethylene glycol rich liquid into the electrode shunt assembly 8, the triethylene glycol rich liquid flows in through the top of the three-way tube 81 and covers the conductive paddle 82. At this time, the conductive paddle 82 is not charged. Affected by the continuous power transmission of the power box 85 on one side of the insulating compartment 83, the conductive rod 84 is charged, and the triethylene glycol liquid itself is not conductive. When the conductive rod 84 is connected to the conductive paddle 82, it means that when the triethylene glycol rich liquid is conductive, the triethylene glycol rich liquid contains water at this time, and the carbon dioxide gas and the sulfide are not completely separated. The conductive rod 84 drives the connecting rod 86 to move. When the connecting rod 86 moves, it drives the main gear 87 to rotate. When the main gear 87 rotates, the slave gear 88 at one end of the reflux pipe 813 rotates. When the slave gear 88 rotates, the rack 89 meshing at one end moves upward and rises. When the rack 89 rises, the baffle 810 at one end rises inside the bayonet slot 811. When the baffle 810 rises, it drives the extension frame 814 to move with it to ensure the airtightness of one side of the bayonet slot 811. With the effect of the limiting frame 815, when the main gear 87 rotates, the slave gear 88 of the discharge port 812 at the other end rotates to drive the rack 89 to descend. At the same time, the baffle 810 descends to the inside of the three-way pipe 81 to block the discharge port 812. At this time, the triethylene glycol rich liquid that has not been completely purified and separated will be transported to the delivery pipe 5 through the reflux pipe 813 for further processing, and the triethylene glycol rich liquid that has not been completely purified and separated will be continuously purified.
[0057] The present application also provides another technical solution: a method for using a natural gas triethylene glycol dehydration device, comprising the following steps:
[0058] S1: Connect the liquid discharge port of the absorption tower to the delivery pipe 5 at the top of the tower body 1, so that the triethylene glycol rich liquid from the absorption tower is injected into the interior of the tower body 1;
[0059] S2: The triethylene glycol rich liquid injected into the tower body 1 flows through the guide pipe 61 into the two-channel filter 62, and then is discharged to the drum 64 through the guide pipe 61;
[0060] S3: When the triethylene glycol is discharged into the drum 64, the box motor 3 rotates to drive the drum 64 to rotate, and at the same time, the heating ring 65 continuously heats the triethylene glycol rich liquid inside the drum 64, increasing the triethylene glycol rich liquid on the heating surface, and quickly generating gas and sulfide;
[0061] S4: The scraper 68 inside the drum 64 scrapes off the TEG rich liquid and derivatives on the inner wall of the drum 64 to prevent residues. The two layers of the drum 64 with different temperatures accelerate the speed at which the TEG rich liquid generates gas and sulfide inside. The gas is discharged from the tower body 1 through the gas pipe 67 and the fan pipe 10.
[0062] S5: The TEG rich liquid after the reaction in the drum 64 carries the reacted derivatives and sulfides and flows to the liquid collecting bin 74 for collection. When the pressing plate 79 contacts the trigger block 77, the liquid infusion is stopped, and the output end of the oil cylinder 76 squeezes the pressing plate 79 to make the TEG rich liquid pass through the molecular sieve 711, and the internal sulfides and water are separated from the TEG rich liquid.
[0063] S6: When the conical tube 712 inputs the re-separated triethylene glycol rich liquid into the electrode diversion assembly 8, the triethylene glycol rich liquid flows in through the top of the tee 81. When the triethylene glycol rich liquid contains water, the carbon dioxide gas and the sulfide are not completely separated. The conductive rod 84 drives the connecting rod 86 to move and transmits, driving the baffle 810 to descend to the inside of the tee 81 to block the discharge port 812. At this time, the triethylene glycol rich liquid that has not been purified and separated completely will be transported to the delivery pipe 5 through the reflux pipe 813 for reprocessing, and the triethylene glycol rich liquid that has not been purified and separated completely will be continuously purified.
[0064] The present invention covers any substitution, modification, equivalent method and scheme made on the essence and scope of the present invention. In order to make the public have a thorough understanding of the present invention, specific details are described in detail in the following preferred embodiments of the present invention, but those skilled in the art can fully understand the present invention without the description of these details. In addition, in order to avoid unnecessary confusion about the essence of the present invention, well-known methods, processes, procedures, components and circuits are not described in detail.
[0065] The above is only a preferred embodiment of the present invention. It should be pointed out that for ordinary technicians in this technical field, several improvements and modifications can be made without departing from the principle of the present invention. These improvements and modifications should also be regarded as the scope of protection of the present invention.
Claims
1. A natural gas triethylene glycol dehydration device, characterized in that: It comprises a tower body, the outer surface of which is provided with a manual ladder platform, one end of which is provided with a box-type motor, the top of which is provided with a servo motor, the output end of which is provided with a fan blade tube, one end of which is provided with a delivery tube, and the other end of which is provided with an exhaust pipe; It also includes a filtering and separating component, which is installed at the bottom of the delivery pipe and is used to filter impurities and sulfides contained in triethylene glycol; An impurity removal and discharge component is installed at the bottom of the filtering and separating component, and the impurity removal and discharge component is used to collect triethylene glycol and remove internal sulfide and carbon dioxide again; An electrode shunt assembly is installed at the bottom of the impurity removal and discharge assembly, and the electrode shunt assembly is used for a repeated process of discharging or refluxing triethylene glycol; A pressure relief valve is installed on the top of the tower body, the output end of the box-type motor is an arc-shaped gear, the output end of the servo motor is provided with a pipeline, a plurality of groups of fan blades are arranged inside the pipeline, and the delivery pipe is a three-way through pipe; The filtering and separation assembly comprises a guide pipe, the guide pipe is installed at the bottom of the delivery pipe, a filter is installed at one end of the guide pipe, a sleeve pipe is installed at one end of the guide pipe, a hole is opened inside the sleeve pipe, a roller is rotatably connected inside the sleeve pipe, the inner wall of the roller and the inner wall of the hole are in contact with each other, the installation angle of the roller is set to an inclination, a heating ring is installed on the surface of the roller, a fixed rotating shaft seat is installed at one end of the roller, and an air supply pipe is installed at the top of one end of the fixed rotating shaft seat; An extension seat is installed at one end of the fixed rotating shaft seat, a scraper is installed at one end of the extension seat, a vibration plate is hinged at the bottom of the scraper, a connecting block is installed at one end of the vibration plate, a support plate is rotatably connected at the bottom of the connecting block, a positioning rod is installed at one end of the support plate, an elastic frame is installed at the bottom of one end of the support plate, a rotating lever is installed on the inner wall of the drum, and the position of the rotating lever is set on the rotation path of the support plate; The impurity removal and discharge assembly includes a liquid infusion pipe valve, which is installed at one end of the guide pipe, a liquid collecting bin is installed at one end of the liquid infusion pipe valve, a trigger rod is provided on the top of the liquid infusion pipe valve, a feedback button is installed on the top of the trigger rod, a trigger block is installed on one end of the feedback button, an exhaust disk is installed on the top of the liquid collecting bin, and an oil cylinder is installed at the bottom of the exhaust disk; A conical tube is installed at the bottom of the liquid collecting bin, a molecular sieve is installed at the top of the conical tube, a spring seat is installed on the inner wall of the liquid collecting bin, the spring seat is arranged on the top of the molecular sieve, a pressure plate is installed on the top of the spring seat, a magnet is arranged inside the pressure plate, and the magnet is arranged below the trigger block; The electrode shunt assembly includes a three-way pipe, the three-way pipe is installed at the bottom of the tapered pipe, a conductive paddle is installed at one end of the three-way pipe, the conductive paddle extends to the inside of the three-way pipe, an insulating bin is installed at one end of the conductive paddle, a conductive rod is installed inside the insulating bin, a spring is provided on the top of the conductive rod and connected to the bottom of the conductive paddle, and a power supply box is installed at one end of the insulating bin; The bottom of the conductive rod is rotatably connected to a connecting rod, one end of the connecting rod is rotatably connected to a main gear, one end of the main gear is meshedly connected to a slave gear, one end of the main gear is installed with a limit frame, both ends of the limit frame are installed at one end of the slave gear, one end of the slave gear is meshedly connected to a rack, one end of the rack is installed with a baffle, and the size of the baffle is the same as the inner diameter of the tee pipe; A bayonet slot is installed inside the three-way pipe, an extension frame is installed at one end of the bayonet slot, the top of the extension frame is connected to the bottom of the baffle, a discharge port is provided at one end of the three-way pipe, a return pipe is installed at the other end of the three-way pipe, and the other end of the return pipe is provided at one end of the delivery pipe.
2. The method for using the natural gas triethylene glycol dehydration device according to claim 1, characterized in that: The method comprises the following steps: S1: Connect the liquid discharge port of the absorption tower to the delivery pipe on the top of the tower body, so that the triethylene glycol rich liquid from the absorption tower is injected into the interior of the tower body; S2: The triethylene glycol rich liquid injected into the tower body flows into the two channels through the guide pipe for filtration, and then is discharged to the drum through the guide pipe; S3: When TEG is discharged into the drum, the box motor rotates to drive the drum to rotate. At the same time, the heating ring continuously heats the TEG rich liquid inside the drum, increasing the TEG rich liquid on the heating surface and generating gas and sulfide. S4: The scraper inside the drum scrapes off the TEG rich liquid and derivatives on the inner wall of the drum to prevent residue. The two layers of drums with different temperatures accelerate the speed at which TEG rich liquid produces gas and sulfide inside. The gas is discharged from the tower through the gas pipe and the fan pipe. S5: After the reaction in the drum, the TEG rich liquid carries the reacted derivatives and sulfides and flows to the liquid collecting bin for collection. When the pressing plate contacts the trigger block, the liquid infusion is stopped, and the output end of the oil cylinder squeezes the pressing plate to make the TEG rich liquid pass through the molecular sieve, separating the internal sulfides and water from the TEG rich liquid. S6: When the conical tube inputs the re-separated triethylene glycol rich liquid into the electrode diversion assembly, the triethylene glycol rich liquid flows in through the top of the tee. When the triethylene glycol rich liquid contains water, the carbon dioxide gas and sulfide are not completely separated. The conductive rod drives the connecting rod to move, and drives the baffle to descend to the inside of the tee to block the discharge port. At this time, the triethylene glycol rich liquid that has not been purified and separated completely will be transported to the delivery pipe through the reflux pipe for reprocessing, and the triethylene glycol rich liquid that has not been purified and separated completely will be continuously purified.
Citation Information
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