Oil-controlling and antipruritic composition containing natural active ingredients, preparation method and application thereof

By using oil-control and anti-it-it-up compositions prepared with traditional Chinese medicine raw materials such as Kuiyi leaves, the residual and irritating problems of existing shampoos are solved, and gentle and effective oil-control and anti-it-it-up effect is achieved, and scalp health is enhanced.

CN118948704BActive Publication Date: 2025-03-18ZHAOQING KAIJOE TECH CO LTD
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Patent Information

Application Number
CN202411083286.4
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-08-08
Publication Date
2025-03-18
Estimated Expiration
2044-08-08

AI Technical Summary

Technical Problem

Existing shampoos are residual and irritating in oil control and anti-itchiness, which may cause new hair health problems.

Method used

The oil-controlled and anti-it-it-composition made of traditional Chinese medicine raw materials such as kui'an leaves, nettles, chicken blood vines, stinky peony roots, bay leaf geraniums, peach branches, licorice and saccharin, was used to obtain a concentrated solution with a solid content of 10%-15% for preparation of washing and care products.

Benefits of technology

It achieves a gentle and non-irritating oil-control and anti-it-it-resistance effect, enhances scalp immunity, reduces scalp oil secretion and relieves itching, and has a significant inhibitory effect on Malassezia and 5-α reductase.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention discloses an oil-control and antipruritic composition containing natural active ingredients, a preparation method and an application thereof, wherein the composition is prepared from the following Chinese medicinal raw materials in parts by weight: 1 to 20 parts of Artemisia argyi leaf, 1 to 15 parts of nettle, 1 to 10 parts of Millettia spatholobi, 1 to 10 parts of stinking peony root, 1 to 10 parts of geranium, 1 to 10 parts of peach branch, 1 to 5 parts of licorice, and 1 to 5 parts of polygonatum. The invention utilizes the theory of monarch, minister, assistant and envoy of traditional Chinese medicine, and prepares the oil-control and antipruritic composition by compounding Artemisia argyi leaf, nettle, Millettia spatholobi, stinking peony root, geranium, peach branch, licorice and polygonatum, and extracts by controlling the temperature of ethanol and water respectively, so as to effectively extract the volatile or water-insoluble active ingredients of the Chinese medicinal raw materials, so as to make the active ingredients synergistic and enhance the efficacy.
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Description

Technical Field

[0001] The invention relates to the technical field of daily chemicals, and in particular to an oil-controlling and itching-relieving shampoo containing natural active ingredients, and a preparation method and application thereof. Background Art

[0002] At present, most shampoos use chemical drugs such as selenium disulfide, piroctone ethanol ammonium salt, climbazole, salicylic acid, pyrithione zinc, ketoconazole, etc. to kill microorganisms, improve dandruff problems, and achieve oil control and itching relief functions, but they are residual and irritating, and easily cause new hair health problems. Therefore, it is necessary to develop a shampoo that takes into account oil control and itching relief, is mild and non-irritating, and will not damage the scalp barrier and cause new hair health problems after long-term use. Summary of the invention

[0003] The invention provides an oil-controlling and antipruritic composition containing natural active ingredients, a preparation method and application thereof, so as to solve the technical problem that current shampoo easily causes new hair health problems.

[0004] In order to solve the above technical problems, in the first aspect, the present invention provides an oil-control and antipruritic composition containing natural active ingredients, which is prepared from the following Chinese medicinal raw materials in parts by weight: 1 to 20 parts of Artemisia selengensis leaves, 1 to 15 parts of nettles, 1 to 10 parts of Millettia reticulata, 1 to 10 parts of stinking peony roots, 1 to 10 parts of geranium, 1 to 10 parts of peach branches, 1 to 5 parts of licorice, and 1 to 5 parts of Polygonatum odoratum;

[0005] The preparation method of the oil-controlling and antipruritic composition comprises the following steps:

[0006] Step 1, weighing the Chinese medicinal raw materials by mass, and mixing and crushing the Chinese medicinal raw materials to 20-60 mesh, adding 60%-90% ethanol to submerge the Chinese medicinal raw materials, and ultrasonically treating at a temperature of 40° C. to 60° C. for 25 min to 60 min at an ultrasonic frequency of 15 kHz to 60 kHz, and filtering out the first filtrate and the filter residue;

[0007] Step 2: Add 5 to 15 times the weight of water to the filter residue, soak for 1 to 3 hours, then heat to 90°C to 100°C, keep warm and stir for 30 to 50 minutes, and filter out the second filtrate;

[0008] Step 3, mixing the first filtrate and the second filtrate and concentrating them by evaporation to obtain a concentrated solution with a solid content of 10% to 15%;

[0009] Step 4: After the concentrated liquid is cooled, centrifugation, filtration and sterilization are performed to obtain an oil-controlling and antipruritic composition.

[0010] The Artemisia quercetinus leaf involved in the present invention belongs to the perennial herbaceous plant of the genus Artemisia of the Asteraceae family. According to the "Chinese Materia Medica", the Artemisia quercetinus leaf contains 0.45% to 1.00% of volatile oil, 60 components such as 2-methylbutanol and 2-vinylaldehyde, as well as flavonoids, eucalyptanes, triterpenes and other components. Flavonoids have certain antibacterial and antipruritic effects on the scalp.

[0011] The nettle involved in the present invention is a perennial herbaceous plant of the Urticaceae family and the genus Urtica. Modern research shows that the main active ingredients of nettle are flavonoids, lignin, organic acids, terpenes, steroids, coumarins, volatile oils and polysaccharides, etc., and it has the effects of clearing away heat and detoxification, anti-inflammatory and analgesic, antibacterial and antiviral.

[0012] The Millettia spatholobi involved in the present invention is the dried stem of the leguminous plant Beans densiflora. Millettia spatholobi contains isoflavones, flavonoids, flavanols, terpenes, and steroids such as beta-sitosterol and Millettia spatholobiol, and has the effects of promoting blood circulation, replenishing blood, and relaxing meridians and activating collaterals.

[0013] The stinking peony root involved in the present invention is the root of the dicotyledonous plant Verbenaceae plant stinking peony, also known as stinking maple root. The stinking peony root contains succinic acid, anisic acid, vanillic acid, magnesium lactate and maltol, etc., and has the effects of clearing away heat and detoxification, anti-inflammatory and sterilization, and promoting blood circulation.

[0014] The geranium involved in the present invention is a perennial herbaceous plant of the Geranium family and the genus Pelargonium. The main components of geranium are geraniol, citronellol and linalool, which have the effects of antibacterial and sterilization, promoting blood circulation, relieving stress and the like.

[0015] The licorice involved in the present invention is a perennial herbaceous plant of the genus Glycyrrhiza of the Leguminosae family. Licorice contains licorice flavonoids, coumarins, triterpenoid saponins and triterpenoid aglycone compounds, and has the effects of clearing away heat and detoxifying, anti-inflammatory and anti-allergic reactions.

[0016] The peach branch involved in the present invention is a dried paper strip of peach of the Rosaceae plant. The peach branch contains naringenin and its glucoside, kaempferol and its glucoside, dihydrokaempferol, kaempferol glucoside, hesperidin glucoside, quercetin glucoside, dextrorotatory catechin, beta-sitosterol glucoside, prunin (i.e. naringenin-7-O-glucoside), hesperidin-5-O-glucoside and other ingredients, and has the effects of promoting blood circulation, unblocking meridians, detoxifying and killing insects.

[0017] The present invention relates to a perennial herbaceous plant of the Asparagaceae family and the genus Polygonatum, which contains flavonoids, saponins, polysaccharides, volatile oils and other components, and has the effects of nourishing yin and moistening dryness, promoting body fluid and quenching thirst, and enhancing body resistance.

[0018] In some preferred embodiments, it is made from the following Chinese medicine raw materials in parts by weight:

[0019] 8 to 12 parts of Artemisia quercetin leaves, 5 to 7 parts of nettles, 2 to 5 parts of Millettia reticulata, 2 to 5 parts of stinking peony roots, 2 to 5 parts of geranium, 2 to 5 parts of peach branches, 1 to 3 parts of liquorice, and 1 to 3 parts of polygonatum.

[0020] In some preferred embodiments, the ethanol concentration in step 1 is 80%.

[0021] In some preferred embodiments, the temperature in step 1 is 45° C., the ultrasonic time is 45 min, and the ultrasonic frequency is 30 kHz.

[0022] In some preferred embodiments, the mass fraction of water in step 2 is 12 times that of the filter residue, and the infiltration time is 2.5 hours.

[0023] In some preferred embodiments, the step 2 is heating to 95° C. and stirring for 35 minutes.

[0024] In some preferred embodiments, the solid content of the concentrated solution in step three is 12%.

[0025] In a second aspect, the present invention provides an application of the oil-control and antipruritic composition containing natural active ingredients as described in the first aspect in a hair care product, wherein the hair care product includes shampoo, conditioner, hair mask, scalp essence or scalp massage cream.

[0026] In some preferred embodiments, the amount of the oil-controlling and antipruritic composition added to the cleaning products is 3% to 8%.

[0027] Compared with the prior art, the present invention has at least the following beneficial effects:

[0028] The present invention utilizes the theory of monarch, minister, assistant and envoy of traditional Chinese medicine, and prepares an oil-controlling and antipruritic composition by compounding Artemisia selengensis leaf, nettle, Millettia spatholobi, stinking peony root, geranium, peach branch, licorice and Polygonatum odoratum through the above preparation method. Artemisia selengensis leaf and nettle are used as monarch drugs to ensure a strong oil-controlling and antipruritic effect, enhance scalp immunity, reduce scalp oil secretion and relieve itching; Millettia spatholobi and stinking peony root are used as minister drugs to improve the heat-clearing and detoxifying and active blood-stasis-removing abilities of the composition, assist the monarch drug in resisting damp-heat and inflammation, and enhance The invention has the effects of oil control and antipruritic; using geranium and peach branch as adjuvants to soothe and relax the scalp and improve the blood circulation between the scalp muscles, and assist the main medicine in improving the health of the scalp; using licorice and polygonatum as guiding medicines to moisturize the scalp, harmonize the medicinal properties of the group of medicines, and enhance the overall efficacy of the group of medicines; through temperature-controlled extraction by ethanol and water respectively, the volatile or water-insoluble active ingredients of the Chinese medicine raw materials can be effectively extracted, so that the active ingredients can be synergistically enhanced; at the same time, the preparation method is simple, does not require special equipment, and is suitable for industrial production. DETAILED DESCRIPTION

[0029] In order to make the above-mentioned purpose, features and advantages of the present invention more obvious and easy to understand, the specific embodiments of the present invention are described in detail below. In the following description, many specific details are set forth to facilitate a full understanding of the present invention. However, the present invention can be implemented in many other ways different from those described herein, and those skilled in the art can make similar improvements without violating the connotation of the present invention, so the present invention is not limited by the specific embodiments disclosed below.

[0030] As used herein, the term "prepared from" is synonymous with "comprising." As used herein, the terms "comprising," "including," "having," "containing," or any other variation thereof, are intended to cover a non-exclusive inclusion. For example, a composition, process, method, article, or apparatus that comprises the listed elements is not necessarily limited to only those elements but may include other elements not expressly listed or inherent to such composition, process, method, article, or apparatus.

[0031] When amount, concentration or other value or parameter is expressed as range, preferred range or a series of upper preferred value and lower preferred value limit range, this should be understood as specifically disclosing all ranges formed by any pairing of any range upper limit or preferred value and any range lower limit or preferred value, regardless of whether the range is disclosed separately. For example, when disclosing range "1 to 5", described range should be interpreted as including range "1 to 4", "1 to 3", "1 to 2", "1 to 2 and 4 to 5", "1 to 3 and 5" etc. When numerical range is described in this article, unless otherwise stated, the range is intended to include its end value and all integers and fractions within the range.

[0032] In addition, the indefinite articles "a" and "an" before the elements or components of the present invention have no restrictions on the quantity requirements (i.e. the number of occurrences) of the elements or components. Therefore, "a" or "an" should be interpreted as including one or at least one, and the elements or components in the singular form also include the plural form, unless the number is obviously intended to be in the singular form.

[0033] Unless otherwise defined, all technical and scientific terms used herein have the same meaning as those commonly understood by those skilled in the art of the present invention. The terms used herein in the specification of the present invention are only for the purpose of describing specific embodiments and are not intended to limit the present invention. The term "and / or" used herein includes any and all combinations of one or more related listed items.

[0034] Example 1

[0035] An oil-control and antipruritic composition containing natural active ingredients is prepared from the following Chinese medicinal raw materials in parts by weight: 1 part of Artemisia argyi leaf, 1 part of nettle, 1 part of Millettia spatholobi, 1 part of stinking peony root, 1 part of geranium, 1 part of peach branch, 1 part of liquorice, and 1 part of polygonatum odoratum;

[0036] The preparation method of the oil-controlling and antipruritic composition comprises the following steps:

[0037] Step 1, weighing the Chinese medicinal materials by mass, and mixing and crushing the Chinese medicinal materials to 20 meshes, adding 60% ethanol to submerge the Chinese medicinal materials, and ultrasonically treating at a temperature of 40° C. for 25 minutes at an ultrasonic frequency of 60 kHz, and filtering out the first filtrate and the filter residue;

[0038] Step 2: add 5 times the weight of water to the filter residue, soak for 1 hour, then heat to 90°C, keep warm and stir for 50 minutes, and filter out the second filtrate;

[0039] Step 3, mixing the first filtrate and the second filtrate and concentrating them by evaporation to obtain a concentrated solution with a solid content of 10%;

[0040] Step 4: After the concentrated liquid is cooled, centrifugation, filtration and sterilization are performed to obtain an oil-controlling and antipruritic composition.

[0041] Example 2

[0042] An oil-control and antipruritic composition containing natural active ingredients is prepared from the following Chinese medicinal raw materials in parts by weight: 8 parts of Artemisia argyi leaves, 5 parts of nettles, 2 parts of Millettia spatholobi, 2 parts of stinking peony roots, 2 parts of geranium, 2 parts of peach branches, 1 part of liquorice, and 1 part of polygonatum odoratum;

[0043] The preparation method of the oil-controlling and antipruritic composition comprises the following steps:

[0044] Step 1, weighing the Chinese medicinal materials by mass, and mixing and crushing the Chinese medicinal materials to 45 meshes, adding 80% ethanol to submerge the Chinese medicinal materials, and ultrasonically treating at a temperature of 45° C. for 45 minutes at an ultrasonic frequency of 30 kHz, and filtering out the first filtrate and the filter residue;

[0045] Step 2: add 12 times the weight of water to the filter residue, soak for 2.5 hours, then heat to 95°C, keep warm and stir for 35 minutes, and filter out the second filtrate;

[0046] Step 3, mixing the first filtrate and the second filtrate and concentrating them by evaporation to obtain a concentrated solution with a solid content of 12%;

[0047] Step 4: After the concentrated liquid is cooled, centrifugation, filtration and sterilization are performed to obtain an oil-controlling and antipruritic composition.

[0048] Example 3

[0049] An oil-control and antipruritic composition containing natural active ingredients is prepared from the following Chinese medicinal raw materials in parts by weight: 12 parts of Artemisia argyi leaves, 7 parts of nettles, 5 parts of Millettia spatholobi, 5 parts of stinking peony roots, 5 parts of geraniums, 5 parts of peach branches, 3 parts of liquorice, and 3 parts of polygonatum odoratum; the preparation method of the oil-control and antipruritic composition is the same as that of Example 2.

[0050] Example 4

[0051] An oil-control and antipruritic composition containing natural active ingredients is prepared from the following Chinese medicinal raw materials in parts by weight: 20 parts of Artemisia argyi leaves, 15 parts of nettles, 10 parts of Millettia spatholobi, 10 parts of stinking peony roots, 10 parts of geranium, 10 parts of peach branches, 5 parts of liquorice, and 5 parts of polygonatum odoratum;

[0052] The preparation method of the oil-controlling and antipruritic composition comprises the following steps:

[0053] Step 1, weighing the Chinese medicinal materials by mass, and mixing and crushing the Chinese medicinal materials to 60 meshes, adding 90% ethanol to submerge the Chinese medicinal materials, and ultrasonically treating at a temperature of 60° C. for 60 minutes at an ultrasonic frequency of 15 kHz, and filtering out the first filtrate and the filter residue;

[0054] Step 2: add 15 times the weight of water to the filter residue, soak for 3 hours, then heat to 100°C, keep warm and stir for 50 minutes, and filter out the second filtrate;

[0055] Step 3, mixing the first filtrate and the second filtrate and concentrating them by evaporation to obtain a concentrated solution with a solid content of 15%;

[0056] Step 4: After the concentrated liquid is cooled, centrifugation, filtration and sterilization are performed to obtain an oil-controlling and antipruritic composition.

[0057] Comparative Example 1

[0058] The difference from Example 3 is that Comparative Example 1 does not contain Artemisia quercetinus leaves and nettles, and the rest is the same as Example 3.

[0059] Comparative Example 2

[0060] The difference from Example 3 is that Comparative Example 2 does not contain Millettia spatholobi and Clematis spatholobi root, and the rest is the same as Example 3.

[0061] Comparative Example 3

[0062] The difference from Example 3 is that Comparative Example 3 does not contain geranium and liquorice, and the rest is the same as Example 3.

[0063] Comparative Example 4

[0064] The difference from Example 3 is that Comparative Example 4 does not contain peach branches and polygonatum odoratum, and the rest is the same as Example 3.

[0065] 1. Malassezia inhibition ring test:

[0066] Test principle: Malassezia is one of the main pathogens that cause dandruff and itching.

[0067] The Malassezia inhibition ring was tested to determine whether the compositions of Examples 1 to 4 and Comparative Examples 1 to 4 had an antipruritic effect.

[0068] Test method: The ambient temperature is 18℃~25℃, and the ambient humidity is 30%~70%. The sterile filter paper with the test sample is placed on the stained Malassezia plate and cultured in an incubator at 30℃ for 3-7 days; the diameter of the Malassezia inhibition ring is measured with a ruler. If the diameter of the inhibition ring is greater than 7mm, it can be considered that the test sample has a certain antipruritic effect. The results of the Malassezia inhibition ring test are shown in Table 1.

[0069] Table 1 Malassezia inhibition ring test results

[0070] sample Diameter of antibacterial ring / mm Antipruritic effectiveness Example 1 10.3 efficient Example 2 13.9 efficient Example 3 15.2 efficient Example 4 11.5 efficient Comparative Example 1 <7.0 invalid Comparative Example 2 <7.0 invalid Comparative Example 3 7.6 efficient Comparative Example 4 7.8 efficient

[0071] Examples 1 to 4 have a good inhibitory effect on Malassezia, and the diameter of the antibacterial ring is all above 10 mm, among which Example 3 has the best antibacterial effect; Comparative Example 1 does not contain a monarch drug, and has no inhibitory effect on Malassezia; Comparative Example 2 does not contain a ministerial drug, and has no inhibitory effect on Malassezia; Comparative Example 3 does not contain an adjuvant drug, and has an inhibitory effect on Malassezia, but its antibacterial ring is far different from that of Example 3; Comparative Example 4 does not contain a messenger drug, and has an inhibitory effect on Malassezia, but its antibacterial ring is also far different from that of Example 3. It can be seen that compared with Comparative Examples 1 to 4, Example 3 uses the traditional Chinese medicine theory of monarch, minister, assistant and messenger, and the oil-control and antipruritic composition prepared with Artemisia quercetinus leaves, nettles, Millettia spatholobi, stinking peony root, geranium, peach twig, licorice, and Polygonatum odoratum can play a synergistic effect.

[0072] 2.5α-reductase inhibition test

[0073] Test principle: 5α-reductase can convert testosterone into dihydrotestosterone (androgen), which will affect the excessive secretion of oil by the sebaceous glands. The oil control effect of the compositions of Examples 1 to 4 and Comparative Examples 1 to 4 is determined by detecting the inhibition rate of 5α-reductase.

[0074] Test method: Add a blank control solution (100 μL of 0.5 mg / ml testosterone, 200 μL of phosphate buffer, 15 μL of 1 mg / ml reduced coenzyme II tetrasodium salt solution) to the reaction tube, then add 15 μL of 150 mg / ml 5α-reductase, mix and incubate at 37°C, and measure the A340nm value after 60 minutes (blank control sample A1).

[0075] A blank control solution and 50 μL of 0.1% finasteride solution were added to the reaction tube, and finally 15 μL of 150 mg / ml 5α-reductase was added, mixed and incubated at 37° C. for 60 min, and then the A340nm value was measured (finasteride control sample A2).

[0076] A blank control solution and 50 μL of the composition of Examples 1 to 4 or Comparative Examples 1 to 4 were added to the reaction tube, and then 15 μL of 150 mg / ml 5α-reductase was added, mixed and incubated at 37° C. for 60 min, and then the A340nm value was measured (test sample A2).

[0077] The calculation formula of 5α-reductase inhibition rate is: A1: absorbance of blank control sample; A2: absorbance of sample. The test results of 5α-reductase inhibition rate are shown in Table 2.

[0078] Table 2 5α-reductase inhibition test results

[0079]

[0080]

[0081] Examples 1 to 4 have a good inhibitory effect on 5α-reductase, with an inhibition rate higher than 39.87%, which is almost more obvious than the inhibitory effect of finasteride on 5α-reductase. Compared with comparative examples 1 to 4, the oil-controlling and antipruritic composition of Example 3, which is compounded with Artemisia argyi leaves, nettles, Millettia spatholobi, Cryophyllum scabra, Pelargonium graveolens, peach branches, licorice, and Polygonatum odoratum, has a significantly improved inhibitory effect on 5α-reductase, and can play a synergistic role.

[0082] 3. User Testing

[0083] Test sample: The compositions of Examples 1 to 4 and Comparative Examples 1 to 4 were prepared into shampoos at an addition amount of 5%.

[0084] Test subjects: 40 volunteers aged 18 to 50 years old with itchy scalp and greasy hair problems, 5 people for each embodiment and comparative example.

[0085] Test steps: Volunteers used shampoo to wash their hair every day in the same process and method, with the amount used each time being 5g to 10g. After 28 days of use, the volunteers were subjected to sensory evaluation and the average score of each item was calculated. The sensory evaluation results are shown in Table 3.

[0086] Oil control effect evaluation criteria: 1 point - very greasy, 2 points - very greasy, 3 points - relatively greasy, 4 - slightly greasy, 5 points - not greasy.

[0087] Evaluation criteria for antipruritic effect: 1 point - frequent severe itching, 2 points - frequent itching, 3 points - occasional itching, 4 points - mild itching, 5 points - no itching.

[0088] Irritation evaluation criteria: 1 point - severe irritation, 2 points - moderate irritation, 3 points - mild to moderate irritation, 4 points - mild irritation, 5 points - no irritation.

[0089] The evaluation criteria for preference are: 1 point - very disgusted, 2 points - relatively disgusted, 3 points - neither disgusted nor liked, 4 points - relatively liked, 5 points - very much liked.

[0090] Table 3 Sensory evaluation results

[0091]

[0092]

[0093] Examples 1 to 4 are significantly better than Comparative Examples 1 to 4 in terms of oil control effect, antipruritic effect and likability, indicating that the shampoos prepared from the oil control and antipruritic compositions of Examples 1 to 4 better meet the user's shampooing needs and are more popular with users.

[0094] The present invention utilizes the theory of monarch, minister, assistant and envoy of traditional Chinese medicine, and prepares the oil-controlling and antipruritic composition by compounding Artemisia quercetinii leaves, nettles, Millettia spatholobi, stinking peony root, geranium, peach twig, licorice and Polygonatum odoratum through the above preparation method, wherein Artemisia quercetinii leaves and nettles are used as monarch drugs to ensure a strong oil-controlling and antipruritic effect, enhance scalp immunity, reduce scalp oil secretion and relieve itching; Millettia spatholobi and stinking peony root are used as assistant drugs to improve the heat-clearing and detoxifying and active blood-stasis-removing abilities of the composition, assist the monarch drug in resisting damp-heat and inflammation, and enhance the oil-controlling and antipruritic effects; and Geranium and peach twigs are used as adjuvants to soothe and relax the scalp and improve the blood circulation between the scalp muscles, thereby assisting the main medicine in improving the health of the scalp; licorice and polygonatum are used as guiding medicines to moisturize the scalp, harmonize the medicinal properties of the group of medicines, enhance the overall efficacy of the group of medicines, and have a significant inhibitory effect on Malassezia and 5-α reductase; ethanol and water are used for temperature-controlled extraction respectively to effectively extract the volatile or water-insoluble active ingredients of the Chinese medicine raw materials, so that the active ingredients are synergistically enhanced; at the same time, the preparation method is simple, does not require special equipment, and is suitable for industrial production.

[0095] The technical features of the above-described embodiments may be arbitrarily combined. To make the description concise, not all possible combinations of the technical features in the above-described embodiments are described. However, as long as there is no contradiction in the combination of these technical features, they should be considered to be within the scope of this specification.

[0096] The specific embodiments described above further illustrate the purpose, technical solutions and beneficial effects of the present invention. It should be understood that the above description is only a specific embodiment of the present invention and is not intended to limit the scope of protection of the present invention. It is particularly pointed out that for those skilled in the art, any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention should be included in the scope of protection of the present invention.

Claims

1. An oil-controlling and antipruritic composition containing natural active ingredients, characterized in that: The method is prepared from the following Chinese medicinal raw materials in parts by weight: 1 to 20 parts of Artemisia selengensis leaves, 1 to 15 parts of nettles, 1 to 10 parts of Millettia reticulata, 1 to 10 parts of stinking peony roots, 1 to 10 parts of geraniums, 1 to 10 parts of peach branches, 1 to 5 parts of liquorice, and 1 to 5 parts of polygonatum odoratum; The preparation method of the oil-controlling and antipruritic composition comprises the following steps: Step 1, weighing the Chinese medicinal raw materials by mass, and mixing and crushing the Chinese medicinal raw materials to 20-60 mesh, adding 60%-90% ethanol to submerge the Chinese medicinal raw materials, and ultrasonically treating at a temperature of 40° C. to 60° C. for 25 min to 60 min at an ultrasonic frequency of 15 kHz to 60 kHz, and filtering out the first filtrate and the filter residue; Step 2: Add 5 to 15 times the weight of water to the filter residue, soak for 1 to 3 hours, then heat to 90°C to 100°C, keep warm and stir for 30 to 50 minutes, and filter out the second filtrate; Step 3, mixing the first filtrate and the second filtrate and concentrating them by evaporation to obtain a concentrated solution with a solid content of 10% to 15%; Step 4: After the concentrated liquid is cooled, centrifugation, filtration and sterilization are performed to obtain an oil-controlling and antipruritic composition.

2. The oil-control and antipruritic composition containing natural active ingredients according to claim 1, characterized in that: Made from the following Chinese medicinal materials in parts by weight: 8 to 12 parts of Artemisia quercetin leaves, 5 to 7 parts of nettles, 2 to 5 parts of Millettia reticulata, 2 to 5 parts of stinking peony roots, 2 to 5 parts of geranium, 2 to 5 parts of peach branches, 1 to 3 parts of liquorice, and 1 to 3 parts of polygonatum.

3. The oil-controlling and antipruritic composition containing natural active ingredients according to claim 1, characterized in that: The ethanol concentration in step 1 is 80%.

4. The oil-controlling and antipruritic composition containing natural active ingredients according to claim 1, characterized in that: The temperature in step 1 is 45° C., the ultrasonic time is 45 min, and the ultrasonic frequency is 30 kHz.

5. The oil-controlling and antipruritic composition containing natural active ingredients according to claim 1, characterized in that: In the step 2, the mass fraction of water is 12 times that of the filter residue, and the soaking time is 2.5 hours.

6. The oil-controlling and antipruritic composition containing natural active ingredients according to claim 1, characterized in that: In step 2, the mixture was heated to 95° C. and stirred for 35 minutes.

7. The oil-controlling and antipruritic composition containing natural active ingredients according to claim 1, characterized in that: The solid content of the concentrated liquid in step 3 is 12%.

8. Use of the oil-controlling and antipruritic composition containing natural active ingredients as claimed in any one of claims 1 to 7 in the preparation of cleaning products, characterized in that: The cleaning and care products include shampoo, hair conditioner, hair mask, scalp essence or scalp massage cream.

9. Use of the oil-controlling and antipruritic composition containing natural active ingredients as claimed in claim 8 in the preparation of cleaning products, characterized in that: The oil-controlling and antipruritic composition is added in a washing and care product in an amount of 3% to 8%.

Citation Information

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