A water-based wax crystal inhibiting wax inhibitor, preparation process and reaction tank

Abstract

The invention discloses a water-based wax crystal inhibiting wax inhibitor, a preparation process and a reaction tank, comprising a sulfonate surfactant A, a sulfonate surfactant B, a maleate surfactant C and an ultra-low interfacial tension surfactant D, wherein the weight ratio of the sulfonate surfactant A: the sulfonate surfactant B: the maleate surfactant C: the ultra-low interfacial tension surfactant D is (8-23): (5-10): (3-5): (2-4), and the rest is water. The water-based wax crystal inhibiting wax inhibitor composed of the components can effectively prevent the wax crystals from precipitating and waxing in the wellbore of the oil well and the oil pipeline, and can also reduce the viscosity and pour point of the crude oil, reduce the flow resistance of the crude oil, and reduce the number of wax cleaning operations in the wellbore of the oil well and the oil pipeline; it has no flash point, no oxidant, and is safe in the construction process; it has low corrosiveness and does not produce precipitates.

Description

Technical Field

[0001] The invention relates to the technical field of petroleum extraction, and in particular to a water-based wax crystal inhibition type wax inhibitor, a preparation process and a reaction tank. Background Art

[0002] Most of the crude oil in my country's oil fields has high wax content, high freezing point and high viscosity. Due to the high formation pressure and temperature in the far well area, paraffin is dissolved in the crude oil and the crude oil viscosity is low. When the crude oil flows into the near well area, due to the decrease in pressure and the decrease in the degassing temperature of the crude oil, the heavy components such as paraffin, colloid and asphalt in the crude oil will precipitate and adhere to the pore wall of the crude oil. With the continuous development of oil fields and the continuous exploitation of crude oil, heavy components such as paraffin, colloid and asphalt are constantly precipitated in the wellbore and oil pipeline, causing serious blockage of the wellhead and oil pipeline, seriously affecting the normal production of oil wells.

[0003] Although existing oil-soluble wax removal and prevention agents can quickly remove wax precipitation from wellbores and pipelines, oil-soluble agents are dangerous, such as being flammable and explosive, having a low flash point, involving risks during operation, and being environmentally unfriendly. Therefore, the present application provides a water-based wax crystal inhibition type wax prevention agent, a preparation process, and a reaction tank to meet the needs. Summary of the invention

[0004] The purpose of the present application is to provide a water-based wax crystal inhibiting paraffin inhibitor, a preparation process and a reaction tank, which can effectively prevent the formation of wax precipitation blockages in wellbores and oil pipelines, does not contain organic chlorine and other components prohibited by the oil industry for liquids entering the well, has low corrosiveness, low cost, and is safe and reliable.

[0005] To achieve the above-mentioned purpose, the present application provides the following technical solution: a water-based wax crystal inhibiting wax inhibitor, comprising a sulfonate surfactant A, a sulfonate surfactant B, a maleate surfactant C and an ultra-low interfacial tension surfactant D, wherein the weight ratio of the sulfonate surfactant A: the sulfonate surfactant B: the maleate surfactant C: the ultra-low interfacial tension surfactant D is (8-23): (5-10): (3-5): (2-4), and the rest is water;

[0006] The sulfonate surfactant A is a branched alkyl sulfonic acid fatty amine salt;

[0007] The sulfonate surfactant B is sodium dodecylbenzene sulfonate;

[0008] The maleate surfactant C is isooctyl sulfosuccinate;

[0009] The ultra-low interfacial tension surfactant D is FS-3000 fluorocarbon surfactant.

[0010] As a preferred embodiment of the present application, the weight percentage of the sulfonate surfactant A is 12.5%; the weight percentage of the sulfonate surfactant B is 5%; the weight percentage of the maleate surfactant C is 3%; the weight percentage of the ultra-low interfacial tension surfactant D is 4%; and the rest is water.

[0011] A preparation process of a water-based wax crystal suppression wax inhibitor comprises the following steps:

[0012] S1: At room temperature, inject a formulated amount of water into the reaction tank and turn on the stirrer for pre-stirring;

[0013] S2: Control the temperature at 45 to 50°C, add one third of the formula amount of branched alkyl sulfonic acid fatty amine salt to the reaction tank in S1, and continue stirring until it is completely dissolved;

[0014] S3: Control the temperature at 45 to 50° C., add the formulated amount of isooctyl succinate sulfonate to the reaction tank in S2, and continue stirring until it is completely dissolved;

[0015] S4: Add one third of the formula amount of branched alkyl sulfonic acid fatty amine salt to the reaction tank in S3 at a temperature of 55 to 60° C. and stir until completely dissolved;

[0016] S5: Control the temperature at 55 to 60°C, add the formulated amount of FS-3000 fluorocarbon surfactant to the reaction tank in S4, and continue stirring until it is evenly dispersed;

[0017] S6: The temperature is controlled at 55 to 60°C, and the remaining branched alkylsulfonic acid fatty amine salt and the formulated amount of sodium dodecylbenzene sulfonate are added to the reaction tank in S5 at the same time, and stirring is continued until they are completely dissolved and evenly mixed.

[0018] A reaction tank, comprising a temperature controller, an electric heater and a stirring system, wherein the temperature controller is arranged on the outer wall of the reaction tank and is electrically connected to the electric heater, the electric heater is arranged on the annular inner wall of the reaction tank, the stirring system is installed on the top plate of the reaction tank, the stirring part of the stirring system is located in the inner cavity of the reaction tank, the upper end of the reaction tank is circumferentially provided with four groups of storage bins, which are respectively a first storage bin, a second storage bin, a third storage bin and a fourth storage bin, the bottoms of the storage bins are all arranged as rectangular discharge outlets, and the lower ends of the four rectangular discharge outlets are all installed with a mounting frame, and a quantitative cylinder with a cylindrical structure is rotatably arranged in the inner cavity of the mounting frame, the inner cavity of the quantitative cylinder is provided with a quantitative cavity with a rectangular structure, the upper and lower parts of the mounting frame are both opened, and a driving gear is installed on one end of the quantitative cylinder;

[0019] A mounting ring and a transmission gear are installed on the top of the inner cavity of the reaction tank, a swivel is fixed to the lower end of the mounting ring, and the lower end of the swivel is connected to the gear ring through a plurality of connecting rods, the gear ring is geared with the gear on the output shaft of the driving motor, and the driving motor is connected to the top of the inner cavity of the reaction tank through a mounting plate, a second arc plate is fixed on the outer wall of the gear ring, a first arc plate is installed on the connecting rod, the first arc plate is provided with a group of tooth segments, and two groups of tooth segments are spaced apart on the second arc plate, the tooth segments include a first tooth-connecting portion and a second tooth-connecting portion, a blank section is provided between the first tooth-connecting portion and the second tooth-connecting portion, and the transmission gear is geared with the corresponding driving gear on the first storage bin.

[0020] As a preferred embodiment of the present application, it also includes a feeding unit, one end of which is arranged on the metering cylinder, and the other end extends to the outside of the metering cylinder, which is used to promote the discharge of materials in the first storage bin, the second storage bin and the fourth storage bin into the metering chamber, and at the same time helps to discharge the materials in the metering chamber.

[0021] As a preferred embodiment of the present application, the unloading unit includes a rectangular plate, a receiving groove, a top block, an air outlet pipe, a first L-shaped rotating shaft and a second L-shaped rotating shaft;

[0022] The rectangular plate is sealingly and slidably disposed in the quantitative cavity, and the lower end of the rectangular plate is connected to the inner wall of the bottom of the quantitative cavity via a first pull rope;

[0023] An elastic airbag is arranged in the inner cavity of the containing groove, and the inner cavity of the elastic airbag is communicated with the ventilation flow channel, the ventilation flow channel is connected with the air outlet end and the air inlet end of the air outlet pipe, the air outlet pipe is arranged at the axis center of the mounting shaft of the quantitative cylinder, the air outlet pipe penetrates the mounting frame and passes through the rotary joint and the piston cylinder, a rack is installed on the piston that is sealed and slidably arranged in the inner cavity of the piston cylinder, and the upper end of the rack slides through the top of the inner cavity of the reaction tank;

[0024] The first L-shaped rotating shaft is rotatably arranged on the outer wall of the storage bin, a one-way gear is installed on the first L-shaped rotating shaft, and the one-way gear is gear-connected with the rack;

[0025] The second L-shaped rotating shaft is rotatably arranged at the upper end of the installation frame, a plurality of impact hammers are installed on the second L-shaped rotating shaft, the contact rod of the second L-shaped rotating shaft is located directly below the contact rod of the first L-shaped rotating shaft, and a contact roller is arranged on the end of the contact rod of the first L-shaped rotating shaft.

[0026] As a preferred embodiment of the present application, it also includes an acceleration impact unit, which is arranged in the inner cavity of the metering cylinder and is used to increase the speed when the top block collides with the elastic airbag, thereby causing the impact hammer to form a more intense collision with the storage bin.

[0027] As a preferred embodiment of the present application, the acceleration impact unit includes a trapezoidal movable block, a second pull rope, a return spring, a weight, a second partition plate and a magnetic tube;

[0028] The trapezoidal movable block is sealingly slidably arranged in the inner cavity of the metering cylinder, the two ends of the reset spring are respectively connected to the first partition and the trapezoidal movable block, one end of the second pull rope is connected to the trapezoidal movable block, and the other end of the second pull rope passes through the first partition and the second partition and is connected to the weight.

[0029] As a preferred embodiment of the present application, it also includes an anti-extrusion unit, which is arranged in the inner cavity of the metering cylinder. When the metering cylinder rotates and the feed opening of the metering cavity is blocked by the inner wall of the mounting frame, the anti-extrusion unit prevents the rectangular plate from moving so that the powder material is squeezed into blocks between the inner wall of the mounting frame and the rectangular plate.

[0030] As a preferred implementation in the present application, the anti-extrusion unit includes all structures of the acceleration impact unit, and the anti-extrusion unit also includes a positioning plate with positioning holes.

[0031] In summary, the technical effects and advantages of the present invention are as follows:

[0032] The invention has a reasonable structure. The water-based wax crystal inhibition type paraffin inhibitor composed of the components can effectively prevent the wax crystals from precipitating and waxing in the oil well bore and oil pipeline, and can also reduce the viscosity and pour point of crude oil, reduce the flow resistance of crude oil, and reduce the number of wax removal operations in the oil well bore and oil pipeline; it has no flash point, no oxidant, and a safe construction process; it has low corrosiveness and does not produce precipitates;

[0033] In the present invention, according to the process flow, a water-based wax crystal inhibition type wax inhibitor product with excellent performance, stability and reliability can be obtained;

[0034] In the present invention, the reaction tank used in the process can drive the materials to be discharged in an orderly and quantitative manner by only using one set of motors, and the structure is simple and stable, and the cost is low;

[0035] In the present invention, a material discharge unit is further provided to facilitate the discharge of materials in the first storage bin, the second storage bin and the fourth storage bin into the quantitative cavity, and at the same time facilitate the discharge of materials in the quantitative cavity;

[0036] In the present invention, an accelerating impact unit is also provided to increase the speed of the top block and the elastic airbag when they collide, thereby causing the impact hammer to form a more intense collision with the storage bin, which is beneficial to the unloading of materials from the storage bin;

[0037] In the present invention, an anti-extrusion unit is also provided to prevent the rectangular plate from moving so that the powder material is squeezed into blocks between the inner wall of the installation frame and the rectangular plate. BRIEF DESCRIPTION OF THE DRAWINGS

[0038] In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present application. For those skilled in the art, other drawings can be obtained based on these drawings without paying any creative work.

[0039] Figure 1 It is a schematic diagram of a partial three-dimensional structure of the present invention;

[0040] Figure 2 for Figure 1 Middle partial upward view of the structure;

[0041] Figure 3 for Figure 2 Schematic diagram of the structure of some parts;

[0042] Figure 4 for Figure 3 Schematic diagram of the split structure of the first storage bin;

[0043] Figure 5 for Figure 4 Schematic diagram of the front cross-sectional structure of the middle metering cylinder;

[0044] Figure 6 for Figure 5 A schematic diagram of a partial cross-sectional structure;

[0045] Figure 7 for Figure 3 Schematic diagram of the partially enlarged structure.

[0046] In the figure: 1, reaction tank; 2, stirring system; 3, first storage bin; 4, second storage bin; 5, third storage bin; 6, fourth storage bin; 7, connecting rod; 8, rotating ring; 9, mounting ring; 10, first arc plate; 11, second arc plate; 12, tooth segment; 13, blank segment; 14, mounting plate; 15, driving motor; 16, transmission gear; 17, mounting frame; 18, quantitative cylinder; 19, driving gear; 20, quantitative chamber; 21, rectangular plate; 22, elastic airbag; 23, top block; 24 , the first pull rope; 25, the ventilation channel; 26, the exhaust pipe; 27, the rotary joint; 28, the piston cylinder; 29, the rack; 30, the first L-shaped shaft; 31, the one-way gear; 32, the second L-shaped shaft; 33, the impact hammer; 34, the stopper; 35, the contact roller; 36, the trapezoidal movable block; 37, the return spring; 38, the first partition; 39, the second pull rope; 40, the second partition; 41, the magnetic tube; 42, the weight; 43, the positioning plate; 44, the gear ring; 45, the permanent magnet; 46, the magnetic isolation groove. DETAILED DESCRIPTION

[0047] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0048] A water-based wax crystal inhibiting wax inhibitor, comprising a sulfonate surfactant A, a sulfonate surfactant B, a maleate surfactant C and an ultra-low interfacial tension surfactant D, wherein the weight ratio of the sulfonate surfactant A: the sulfonate surfactant B: the maleate surfactant C: the ultra-low interfacial tension surfactant D is (8-23): (5-10): (3-5): (2-4), and the rest is water;

[0049] The sulfonate surfactant A is a branched alkyl sulfonic acid fatty amine salt;

[0050] The sulfonate surfactant B is sodium dodecylbenzene sulfonate;

[0051] The maleate surfactant C is isooctyl sulfosuccinate;

[0052] The ultra-low interfacial tension surfactant D is FS-3000 fluorocarbon surfactant.

[0053] The water-based wax crystal inhibition type paraffin inhibitor composed of this component can effectively prevent the precipitation and wax formation of wax crystals in oil well bores and oil pipelines, and at the same time can reduce the viscosity and pour point of crude oil, reduce the flow resistance of crude oil, and reduce the number of wax cleaning operations in oil well bores and oil pipelines; it has no flash point, no oxidants, and the construction process is safe; it has low corrosiveness and does not produce any sediment.

[0054] As a preferred embodiment of the present application, the weight percentage of the sulfonate surfactant A is 12.5%; the weight percentage of the sulfonate surfactant B is 5%; the weight percentage of the maleate surfactant C is 3%; the weight percentage of the ultra-low interfacial tension surfactant D is 4%; and the rest is water.

[0055] The overall performance of the wax inhibitor composed of material components under this formula is the best.

[0056] S1: At room temperature, inject a formulated amount of water into the reaction tank and turn on the stirrer for pre-stirring;

[0057] Room temperature adjustment can avoid solvent evaporation. Starting at a lower temperature can reduce water evaporation and ensure that the volume and concentration of the initial solution are stable.

[0058] The benefits of initial stirring: ensuring that the inner wall of the reaction tank and the agitator are fully wetted by water, reducing the possibility of subsequent solute adhesion, while providing a uniform initial environment.

[0059] S2: Control the temperature at 45 to 50°C, add one third of the formula amount of branched alkyl sulfonic acid fatty amine salt to the reaction tank in S1, and continue stirring until it is completely dissolved;

[0060] The benefits of controlling the temperature within 45 to 50°C: Appropriate temperature increase helps to increase the dissolution rate of the solute, ensuring that the branched alkyl sulfonic acid fatty amine salt can be dissolved quickly and evenly. At the same time, the fluidity of the solute is enhanced, reducing the agglomeration phenomenon caused by excessive local concentration, and promoting the performance of the finished wax inhibitor; uniform dissolution helps to form a stable wax inhibitor system, improving its dispersibility and anti-waxing effect in crude oil; when the temperature is lower than 45°C, the solute dissolution rate decreases, which may cause uneven distribution of the solute in the solution, and even the appearance of undissolved solid particles, affecting the subsequent steps and the performance of the final product. When the temperature is higher than 50°C, although high temperature helps the solute dissolve, too high temperature may accelerate the decomposition of the chemical substance or change its chemical properties, thereby affecting the overall effect of the wax inhibitor. In addition, too high temperature will also increase energy consumption and operating costs;

[0061] The batch addition of branched alkyl sulfonic acid fatty amine salt can alleviate the situation where the local concentration of the solution is too high, help the solute to dissolve more evenly, reduce agglomeration, and reduce the resistance during stirring.

[0062] S3: Control the temperature at 45 to 50° C., add the formulated amount of isooctyl succinate sulfonate to the reaction tank in S2, and continue stirring until it is completely dissolved;

[0063] The benefits of controlling the temperature within 45 to 50°C: adding auxiliary solutes at the same temperature can reduce the fluctuation of the solution temperature, which helps to maintain the stability and uniformity of the solution. At this temperature, the auxiliary solutes can better play their synergistic role with the main solute (i.e., branched alkyl sulfonic acid fatty amine salt), improve the overall performance of the wax inhibitor, and promote the performance of the finished wax inhibitor: enhance the surface activity of the wax inhibitor, further improve its permeability and anti-waxing effect in crude oil; when the temperature is lower than 45°C, it may cause uneven mixing with the main solute, affecting the performance of the wax inhibitor; when the temperature is higher than 50°C, although high temperature helps the solute to dissolve, too high temperature may accelerate the decomposition of the chemical substance or change its chemical properties, thereby affecting the overall effect of the wax inhibitor. In addition, too high temperature will also increase energy consumption and operating costs;

[0064] At this point, the solution already has a certain surface activity, and adding auxiliary solutes can further improve the wettability and stability of the solution, laying a good foundation for the subsequent mixing process.

[0065] S4: Add one third of the formula amount of branched alkyl sulfonic acid fatty amine salt to the reaction tank in S3 at a temperature of 55 to 60° C. and stir until completely dissolved;

[0066] The benefits of controlling the temperature within 55 to 60°C: Higher temperatures can further accelerate the dissolution process of the solute, especially when the addition amount is large. At higher temperatures, the convection and diffusion of the solution are enhanced, which helps to evenly distribute the solute in the solution; it promotes the performance of the finished wax inhibitor: it increases the effective concentration of the wax inhibitor in crude oil and improves its stability under low temperature conditions, thereby more effectively reducing the viscosity and freezing point of the crude oil; when the temperature is lower than 55°C, the dissolution rate is further reduced, which may cause the solute to form local high concentration areas in the solution, and even agglomeration, affecting the uniformity and stability of the wax inhibitor; when the temperature is higher than 60°C, the high temperature may accelerate the thermal motion of the solute molecules, resulting in intensified intermolecular collisions in the solution, thereby triggering unnecessary chemical reactions or phase separation, affecting the performance and stability of the wax inhibitor.

[0067] By adding branched alkyl sulfonic acid fatty amine salt in batches, the concentration change of the solution can be better controlled to ensure that the solute added each time can be fully dissolved and fully mixed with the previous solution, thereby improving the overall uniformity.

[0068] S5: Control the temperature at 55 to 60°C, add the formulated amount of FS-3000 fluorocarbon surfactant to the reaction tank in S4, and continue stirring until it is evenly dispersed;

[0069] Benefits of temperature control within 55 to 60°C: FS-3000 fluorocarbon surfactant can fully demonstrate its excellent surface activity at high temperature, which helps to form a stable emulsion or dispersion system; the thermal motion of molecules at high temperature intensifies, which helps to evenly disperse FS-3000 in the solution and improve its interaction ability with crude oil; it promotes the performance of the finished wax inhibitor: it significantly improves the adsorption capacity of the wax inhibitor on the surface of crude oil, forms a dense protective film, and effectively prevents the deposition of wax crystals and the condensation of crude oil; when the temperature is lower than 55°C, the surface activity of FS-3000 fluorocarbon surfactant may not be fully exerted, resulting in reduced dispersibility and stability in the solution, which in turn affects the overall effect of the wax inhibitor; when the temperature is higher than 60°C, the high temperature may cause FS-3000 fluorocarbon surfactant to decompose or react with other chemicals unnecessarily, thereby changing its chemical properties and reducing its surface activity, which in turn affects the wax prevention and viscosity reduction effects of the wax inhibitor;

[0070] FS-3000 fluorocarbon surfactant has special surface activity and wetting properties. Adding it at this time can more effectively improve the surface tension of the solution and promote the dissolution and dispersion of subsequent solutes.

[0071] S6: Control the temperature at 55 to 60° C., add the remaining branched alkylsulfonic acid fatty amine salt and the formulated amount of sodium dodecylbenzenesulfonate to the reaction tank in S5, and continue stirring until completely dissolved and evenly mixed;

[0072] The benefits of controlling the temperature within 55 to 60°C: All solutes are added and mixed at a higher temperature to ensure that all solutes can be fully dissolved and reach the predetermined concentration. Through sufficient mixing and dissolution, a uniform and stable paraffin inhibitor system is formed to maximize its effect of preventing wax deposition, reducing crude oil viscosity and freezing point, and reducing crude oil flow resistance. At the same time, a uniform solution system also helps the uniform distribution and long-lasting effect of the paraffin inhibitor in crude oil;

[0073] In this step, all the remaining solutes are added at once, which can save time and operation steps. Due to the sufficient preparation and dissolution in the previous steps, the solution at this time already has good solubility and dispersion ability, and can quickly accept and dissolve the remaining solutes, thereby ensuring the uniformity and performance of the final product.

[0074] In the above preparation process, the main solute is added in three stages. By first adding one-third of the branched alkyl sulfonic acid fatty amine salt and stirring until it is basically dissolved, the basic system of the wax inhibitor can be initially formed. This step provides a stable solution environment for the subsequent addition of other auxiliary solutes and surfactants; adding again: continuing to add the branched alkyl sulfonic acid fatty amine salt after adding the auxiliary solute can further increase the solute concentration and promote its interaction with the auxiliary solute. This step helps to improve the surface activity and penetration ability of the wax inhibitor; adding finally: adding the remaining branched alkyl sulfonic acid fatty amine salt together with other remaining solutes and mixing evenly to improve work efficiency and ensure that all solutes are fully dissolved and reach a predetermined concentration.

[0075] In summary, the addition of the main solute branched alkyl sulfonic acid fatty amine salt in three steps is based on considerations such as improving dissolution uniformity, promoting mixing effect and optimizing product quality. This step-by-step addition method is helpful to prepare a water-based wax crystal inhibition type wax inhibitor product with excellent performance, stability and reliability. Embodiment 1:

[0076] The dosage of water-based wax crystal inhibition type wax inhibitor is 15 tons, and the dosage concentration is 0.25%.

[0077] The weight percentage composition of the water-based wax crystal inhibitor is as follows: 12.5% ​​sulfonate surfactant A, 5% sulfonate surfactant B, 3% maleate surfactant C, 4% ultra-low interfacial tension surfactant D, and the rest is water. Embodiment 2:

[0078] The dosage of water-based wax crystal inhibition type wax inhibitor is 25 tons, and the dosage concentration is 0.45%.

[0079] The weight percentage composition of the water-based wax crystal inhibition type wax inhibitor is as follows: 10% sulfonate surfactant A, 5% sulfonate surfactant B, 3% maleate surfactant C, 3.5% ultra-low interfacial tension surfactant D, and the rest is water. Embodiment 3:

[0080] The amount of water-based wax crystal inhibition paraffin inhibitor used is 18 tons, and the dosage concentration is 0.3%.

[0081] The weight percentage composition of the water-based wax crystal inhibition type wax inhibitor is as follows: 8% sulfonate surfactant A, 7% sulfonate surfactant B, 4% maleate surfactant C, 3.5% ultra-low interfacial tension surfactant D, and the rest is water.

[0082] The effects of Examples 1 to 3 are shown in the table below.

[0083]

[0084] It can be seen from the above table that after the water-based wax crystal inhibiting paraffin inhibitor was added to the three high-wax oil wells, the viscosity, crude oil pour point and wax deposition amount were significantly reduced, and the paraffin prevention rate could reach more than 70%, which is better than the standard requirement value of the oil-based wax crystal inhibiting paraffin inhibitor of ≥30% in the petroleum and natural gas industry standard "SYT6300-2009 Technical Requirements for Wax Removers and Paraffin Inhibitors for Oil Production", and its viscosity reduction rate is also better than the viscosity reduction rate mentioned in the industry standard.

[0085] like Figure 1-4 As shown, a reaction tank comprises a temperature controller, an electric heater and a stirring system 2, wherein the temperature controller is arranged on the outer wall of the reaction tank 1 and is electrically connected to the electric heater, the electric heater is arranged on the annular inner wall of the reaction tank 1, the stirring system 2 is installed on the top plate of the reaction tank 1, the stirring part of the stirring system 2 is located in the inner cavity of the reaction tank 1, the upper end of the reaction tank 1 is circumferentially provided with four groups of storage bins, which are respectively the first storage bin 3, the second storage bin 4, the third storage bin 5 and the fourth storage bin 6, the bottoms of the storage bins are all arranged as rectangular discharge outlets, and the lower ends of the four rectangular discharge outlets are all installed with a mounting frame 17, and the inner cavity of the mounting frame 17 is rotatably provided with a quantitative cylinder 18 of a cylindrical structure, the inner cavity of the quantitative cylinder 18 is provided with a quantitative cavity 20 of a rectangular structure, the upper and lower parts of the mounting frame 17 are both opened, and a driving gear 19 is installed on one end of the quantitative cylinder 18;

[0086] A mounting ring 9 and a transmission gear 16 are installed on the top of the inner cavity of the reaction tank 1. A swivel ring 8 is fixed to the lower end of the mounting ring 9, and the lower end of the swivel ring 8 is connected to a gear ring 44 through a plurality of connecting rods 7. The gear ring 44 is gear-engaged with the gear on the output shaft of the drive motor 15. The drive motor 15 is connected to the top of the inner cavity of the reaction tank 1 through a mounting plate 14. A second arc plate 11 is fixed on the outer wall of the gear ring 44. A first arc plate 10 is installed on the connecting rod 7. The first arc plate 10 is provided with a group of tooth segments 12. Two groups of tooth segments 12 are arranged at intervals on the second arc plate 11. The tooth segment 12 includes a first tooth connection portion and a second tooth connection portion. A blank section 13 is arranged between the first tooth connection portion and the second tooth connection portion. The transmission gear 16 is gear-engaged with the corresponding drive gear 19 on the first storage bin 3.

[0087] Before use, the first storage bin 3, the second storage bin 4, the third storage bin 5, and the fourth storage bin 6 are respectively filled with branched alkyl sulfonic acid fatty amine salt (powder), succinic acid isooctyl ester sulfonate (powder), FS-3000 fluorocarbon surfactant (liquid) and sodium dodecylbenzene sulfonate (powder). When in use, the drive motor 15 can be controlled to work, and the drive motor 15 can drive the gear ring 44 to rotate clockwise, and the clockwise rotation of the gear ring 44 can drive the first arc plate 10 with the tooth segment 12 and the second arc plate 11 to rotate clockwise. When the second arc plate 11 rotates, it will The driving gear 19 corresponding to the first storage bin 3 is geared and drives the metering cylinder 18 to rotate. In the initial state, the metering cavity 20 of the metering cylinder 18 opens upward and is consistent with the unloading opening of the storage bin. The metering cavity 20 is filled with material. After rotating 180 degrees, the metering cavity 20 opens downward. At this time, the driving gear 19 is geared and separated from the second arc plate 11, and the metering cylinder 18 stops rotating. When all the internal materials fall into the reaction tank 1, as the second arc plate 11 continues to rotate, the second arc plate 11 will be geared with the driving gear 19 again, so that the metering cylinder 18 returns to its original position, that is, the opening of the metering cavity 20 faces upward. State, at this time, the material in the storage bin enters the quantitative chamber 20 by gravity, that is, the loading is automatically completed. After the quantitative cylinder 18 of the first storage bin 3 returns to its original position, the second arc plate 11 and the driving gear 19 are separated, the quantitative cylinder 18 stops rotating, and the driving motor 15 stops working. When adding materials later, the driving motor 15 can be started, the second arc plate 11 is geared with the driving gear 19 of the second storage bin 4, and the material in the corresponding quantitative cylinder 18 is poured into the reaction tank 1. After the quantitative cylinder 18 returns to its original position, the gear ring 44 stops rotating. When the branched alkyl sulfonic acid fatty amine salt needs to be added later, the gear ring 44 stops rotating. The ring 44 continues to rotate, at which time the first arc plate 10 is gear-engaged with the transmission gear 16 and drives the metering cylinder 18 to rotate through the driving gear 19 to deliver the material into the reaction tank 1. Subsequently, as the gear ring 44 continues to rotate, the second arc plate 11 can drive the metering cylinder 18 on the third storage bin 5 to rotate for unloading, and through the cooperation of the first arc plate 10 and the second arc plate 11, the branched alkyl sulfonic acid fatty amine salt and sodium dodecylbenzene sulfonate are unloaded at the same time. The reaction tank 1 only uses one set of motors to drive the materials to be unloaded in an orderly and quantitative manner, and the structure is simple and stable, and the cost is low.

[0088] It should be noted that: 1. The reaction tank 1 is provided with a feed pipe and a discharge pipe, through which water can be added to the reaction tank 1, and the mixed anti-wax agent can be discharged through the discharge pipe; 2. All electrical devices on the reaction tank 1 are electrically connected to the controller; 3. An elastic cushion layer is provided on the outer wall of the metering cylinder 18, which is in close contact with the inner wall of the mounting frame 17 to form a seal, and the tooth-connected and separated metering cylinder 18 can be positioned by the elastic cushion layer; 4. The transmission gear 16 is located above the drive gear 19, and the heights of the drive gears 19 are consistent, so that the second arc plate 11 can be toothed with each drive gear 19, and the first arc plate 10 can be prevented from being toothed with the drive gear 19; 5. The blank section 13 is provided to provide a residence time for the metering cavity 20 with the opening facing downward, which is conducive to the complete discharge of the material in the metering cavity 20; 6. The quantitative cavity 20 of the metering cylinder 18 corresponding to each storage bin has a different capacity, and its capacity is the required addition amount of each material in the above process.

[0089] As a preferred embodiment of the present application, it also includes a feeding unit, one end of which is arranged on the metering cylinder 18, and the other end extends to the outside of the metering cylinder 18, for promoting the discharge of materials in the first storage bin 3, the second storage bin 4 and the fourth storage bin 6 into the metering chamber 20, and at the same time helps to discharge the materials in the metering chamber 20.

[0090] As a preferred implementation in this application, Figure 3 , Figure 5 and Figure 7 As shown, the unloading unit includes a rectangular plate 21, a receiving groove, a top block 23, an air outlet pipe 26, a first L-shaped rotating shaft 30 and a second L-shaped rotating shaft 32;

[0091] The rectangular plate 21 is sealed and slidably disposed in the quantitative chamber 20, and the lower end of the rectangular plate 21 is connected to the inner wall of the bottom of the quantitative chamber 20 via a first pull rope 24;

[0092] An elastic airbag 22 is arranged in the inner cavity of the receiving groove, and the inner cavity of the elastic airbag 22 is communicated with the ventilation flow channel 25, and the ventilation flow channel 25 is connected with the air outlet end and the air inlet end of the air outlet pipe 26, and the air outlet pipe 26 is arranged at the axis center of the mounting shaft of the quantitative cylinder 18, and the air outlet pipe 26 penetrates the mounting frame 17 and passes through the rotary joint 27 and the piston cylinder 28, and a rack 29 is installed on the piston that is sealed and slidably arranged in the inner cavity of the piston cylinder 28, and the upper end of the rack 29 slides through the top of the inner cavity of the reaction tank 1;

[0093] The first L-shaped rotating shaft 30 is rotatably arranged on the outer wall of the storage bin, and a one-way gear 31 is installed on the first L-shaped rotating shaft 30, and the one-way gear 31 is gear-connected with the rack 29;

[0094] The second L-shaped rotating shaft 32 is rotatably set at the upper end of the installation frame 17, and multiple impact hammers 33 are installed on the second L-shaped rotating shaft 32. The contact rod of the second L-shaped rotating shaft 32 is located directly below the contact rod of the first L-shaped rotating shaft 30, and a contact roller 35 is set on the end of the contact rod of the first L-shaped rotating shaft 30.

[0095] When the metering cylinder 18 filled with materials is rotated, the feed opening of the metering chamber 20 is facing upwards at the beginning, and as the metering cylinder 18 rotates, the feed opening of the metering chamber 20 can be set downwards (the metering cylinder 18 needs to stay for a period of time at this time, and this stay time provides enough time for the subsequent pushing movement of the rectangular plate 21). At this time, the rectangular plate 21 moves downwards by gravity, pushing the materials out (because of the gravity of the accumulated materials in the storage bin, the materials in the metering chamber 20 will be squeezed during loading, which may easily cause some materials to clump or form a whole and cannot fall into the reaction tank 1 by their own gravity) and the metering chamber 20 is filled with materials. The material on the inside of the cavity 20 is scraped off and pushed out. When the rectangular plate 21 pushes all the materials out of the quantitative cavity 20, it will not be able to move downward due to the pulling force of the first pull rope 24. At this time, the rectangular plate 21 is still in the inner cavity of the quantitative cavity 20. With the rotation of the quantitative cylinder 18, the rectangular plate 21 will tilt and slowly move downward, and finally the weight of the rectangular plate 21 acts on the elastic airbag 22 through the top block 23. The elastic airbag 22 is squeezed, and the internal gas enters the piston cylinder 28 through the ventilation flow channel 25 and lifts the rack 29. As the rack 29 is lifted, the rack 29 will drive the first L-shaped rotating The shaft 30 rotates counterclockwise, and contacts and squeezes the contact rod on the second L-shaped shaft 32 through the contact roller 35 on the contact rod, so that the impact hammer 33 rotates away from the storage bin. When the contact rod of the first L-shaped shaft 30 and the contact rod of the second L-shaped shaft 32 are vertical, as the first L-shaped shaft 30 rotates, the air pressure will cause the first L-shaped shaft 30 to quickly contact and separate from the second L-shaped shaft 32 and return to its original position. At this time, the impact hammer 33 moves closer to the storage bin through the action of gravity, and finally collides with the outer wall of the storage bin, which is conducive to vibrating the material in the storage bin into the quantitative cavity 20. At the same time, when the impact hammer 33 is hit, it will move a small distance away from the storage bin due to the reaction force, and then collide with the storage bin again. This process is repeated, and multiple impacts can be formed on the storage bin, which is further conducive to vibrating the material in the storage bin into the quantitative chamber 20. After the loading is completed, the quantitative cylinder 18 rotates, the feed opening of the quantitative chamber 20 faces downward and the rectangular plate 21 moves downward, the extrusion force acting on the elastic airbag 22 is released, and the rack 29 moves downward to return to its original position. At the same time, the first L-shaped shaft 30 does not rotate. This unloading unit can automatically promote the unloading of the storage bin and the quantitative cylinder 18.

[0096] It should be noted that, first, a stopper 34 is installed on the rack 29. When the first L-shaped rotating shaft 30 is quickly restored to its original position, the rack 29 is limited by the blocking of the stopper 34 and the top of the reaction tank 1 to prevent it from excessive movement; second, an elastic damping sleeve is provided at the rotation connection between the first L-shaped rotating shaft 30 and the storage bin, and the inner wall of the elastic damping sleeve is in close contact with the outer wall of the first L-shaped rotating shaft 30, which can ensure that the first L-shaped rotating shaft 30 does not rotate in the absence of external force.

[0097] As a preferred embodiment of the present application, it also includes an accelerating impact unit, which is arranged in the inner cavity of the metering cylinder 18, and is used to increase the speed when the top block 23 collides with the elastic airbag 22, thereby causing the impact hammer 33 to form a more violent collision with the storage bin.

[0098] As a preferred implementation in this application, Figure 5 and Figure 6 As shown, the acceleration impact unit includes a trapezoidal movable block 36, a second pull rope 39, a return spring 37, a weight 42, a second partition plate 40 and a magnetic tube 41;

[0099] The trapezoidal movable block 36 is sealingly slidably arranged in the inner cavity of the metering cylinder 18, the two ends of the return spring 37 are respectively connected to the first partition 38 and the trapezoidal movable block 36, one end of the second pull rope 39 is connected to the trapezoidal movable block 36, and the other end of the second pull rope 39 passes through the first partition 38 and the second partition 40 and is connected to the weight 42.

[0100] like Figure 5 At this time, the return spring 37 is in a compressed state, and the second pull rope 39 is in a taut state. When the feed port opening of the quantitative chamber 20 rotates to face downward, during this process, the weight 42 will move closer to the return spring 37 due to gravity (in this process, the iron weight 42 will pass through the magnetic tube 41, and the internal magnetic field will hinder the movement of the weight 42). At this time, the return spring 37 will return to its original position, and the end of the trapezoidal movable block 36 will extend into the quantitative chamber 20. When the rectangular plate 21 moves downward, it will be squeezed with the inclined surface of the trapezoidal movable block 36 and finally move to the bottom of the trapezoidal movable block 36, and the trapezoidal movable block 36 will press the rectangular plate 2 1 forms a blockage, and the metering cylinder 18 continues to rotate. When the metering chamber 20 rotates to the opening facing upward, the weight 42 still moves in the magnetic tube 41 due to gravity. After moving for a period of time, the weight 42 moves out of the magnetic tube 41. At this time, the second pull rope 39 is straightened and pulls the trapezoidal movable block 36 to squeeze the reset spring 37, and finally releases the blockage of the rectangular plate 21. At this time, the rectangular plate 21 accelerates downward under the action of gravity and forms a fierce collision with the elastic airbag 22, which can finally make the second L-shaped shaft 32 subject to a large rotation thrust, so that the impact hammer 33 can rotate at a larger angle, and have a better impact effect on the storage bin.

[0101] It should be noted that: first, a magnetic isolation groove 46 can be set at the bottom of the inner cavity of the quantitative cavity 20, and a permanent magnet 45 can be set in the magnetic isolation groove 46. The magnetic effect of the permanent magnet 45 and the rectangular plate 21 can further accelerate the downward movement of the rectangular plate 21, further increasing the subsequent impact effect on the storage bin. At the same time, the magnetic attraction force generated is smaller than the gravity of the rectangular plate 21, preventing the rectangular plate 21 from being unable to move downward by its own gravity when the feed opening of the quantitative cavity 20 is facing downward; second, when the rectangular plate 21 moves downward, it will be squeezed and contacted with the trapezoidal movable block 36, that is, it will collide with the trapezoidal movable block 36, which is conducive to the falling of dust on the rectangular plate 21; third, the outer surface of the trapezoidal movable block 36 is provided with an elastic sealing layer; fourth, before the rectangular plate 21 collides with the elastic airbag 22, the feed opening of the quantitative cavity 20 of the rectangular plate 21 is aligned with the unloading opening of the storage bin, and after alignment, the impact hammer 33 is used to impact, which is more conducive to the falling of the material in the storage bin and filling the quantitative cavity 20.

[0102] As a preferred embodiment of the present application, it also includes an anti-extrusion unit, which is arranged in the inner cavity of the metering cylinder 18. When the metering cylinder 18 rotates and the feed opening of the metering cavity 20 is blocked by the inner wall of the mounting frame 17, the rectangular plate 21 is prevented from moving so that the powder material is squeezed into blocks between the inner wall of the mounting frame 17 and the rectangular plate 21.

[0103] When the metering cylinder 18 filled with materials rotates, in order to prevent the rectangular plate 21 from moving during the rotation process, the movement of the rectangular plate 21 will cause its weight to act on the material, squeezing the material, and easily squeezing the material into blocks or forming a whole. After the block material falls into the reaction tank 1, the contact area with the solution is reduced and it is easy to form a clumping, which makes it impossible to achieve rapid dissolution of the material, so an anti-extrusion unit is provided.

[0104] As a preferred implementation in this application, Figure 5 and Figure 6 As shown, the anti-extrusion unit includes all structures of the acceleration impact unit, and the anti-extrusion unit also includes a positioning plate 43 with positioning holes.

[0105] like Figure 5As shown, in the anti-extrusion unit (the structures appearing below are all structures in the anti-extrusion unit), when the opening of the quantitative chamber 20 is facing upward, its reset spring 37 is in a natural state, and the end of the trapezoidal movable block 36 is located in the positioning hole of the positioning plate 43, limiting the rectangular plate 21. When the quantitative cylinder 18 is rotated to the point where the feed opening is facing downward, the weight 42 is still moving in the magnetic tube 41 due to gravity. After moving for a period of time, the weight 42 moves out of the magnetic tube 41, and causes the second pull rope 39 to drive the trapezoidal movable block 36 to squeeze the reset spring 37, that is, the trapezoidal movable block 36 moves toward the inner cavity of the quantitative cylinder 18, and finally causes the end of the trapezoidal movable block 36 to move out of the positioning hole. At this time, the rectangular plate 21 moves downward to perform a scraping operation, and continues to rotate to restore the quantitative cylinder 18 to its original position, and finally causes the end of the trapezoidal movable block 36 to be plugged into the positioning hole.

[0106] Finally, it should be noted that the above is only a preferred embodiment of the present invention and is not intended to limit the present invention. Although the present invention has been described in detail with reference to the aforementioned embodiments, it is still possible for those skilled in the art to modify the technical solutions described in the aforementioned embodiments or to make equivalent substitutions for some of the technical features therein. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. A preparation process of a water-based wax crystal suppressant, characterized in that: The following steps are involved: S1: At room temperature, inject a formulated amount of water into the reaction tank and turn on the stirrer for pre-stirring; S2: Control the temperature at 45 to 50°C, add one third of the formula amount of branched alkyl sulfonic acid fatty amine salt to the reaction tank in S1, and continue stirring until it is completely dissolved; S3: Control the temperature at 45 to 50° C., add the formulated amount of isooctyl succinate sulfonate to the reaction tank in S2, and continue stirring until it is completely dissolved; S4: Add one third of the formula amount of branched alkyl sulfonic acid fatty amine salt to the reaction tank in S3 at a temperature of 55 to 60° C. and stir until completely dissolved; S5: Control the temperature at 55 to 60°C, add the formulated amount of FS-3000 fluorocarbon surfactant to the reaction tank in S4, and continue stirring until it is evenly dispersed; S6: Control the temperature at 55 to 60° C., add the remaining branched alkylsulfonic acid fatty amine salt and the formulated amount of sodium dodecylbenzenesulfonate to the reaction tank in S5, and continue stirring until completely dissolved and evenly mixed; The reaction tank comprises a temperature controller, an electric heater and a stirring system (2), wherein the temperature controller is arranged on the outer wall of the reaction tank (1) and is electrically connected to the electric heater, and the electric heater is arranged on the annular inner wall of the reaction tank (1). The stirring system (2) is installed on the top plate of the reaction tank (1), and the stirring part of the stirring system (2) is located in the inner cavity of the reaction tank (1). The upper end of the reaction tank (1) is provided with four groups of storage bins in a circumferential manner, and they are respectively a first storage bin (3), a second storage bin (4), a third storage bin (5) and a fourth storage bin (6). The bottoms of the storage bins are all provided with rectangular discharge outlets, and the lower ends of the four rectangular discharge outlets are all provided with a mounting frame (17), and a cylindrical quantitative cylinder (18) is rotatably provided in the inner cavity of the mounting frame (17), and a rectangular quantitative cavity (20) is provided in the inner cavity of the quantitative cylinder (18). The mounting frame (17) is provided with openings at the top and bottom, and a driving gear (19) is installed at one end of the quantitative cylinder (18); A mounting ring (9) and a transmission gear (16) are mounted on the top of the inner cavity of the reaction tank (1); a rotating ring (8) is fixed to the lower end of the mounting ring (9); and the lower end of the rotating ring (8) is connected to a gear ring (44) via a plurality of connecting rods (7); the gear ring (44) is engaged with a gear on an output shaft of a drive motor (15); the drive motor (15) is connected to the top of the inner cavity of the reaction tank (1) via a mounting plate (14); and a second arc is fixed to the outer wall of the gear ring (44). A first curved plate (10) is mounted on the connecting rod (7), the first curved plate (10) is provided with a group of tooth segments (12), the second curved plate (11) is provided with two groups of tooth segments (12) at intervals, the tooth segments (12) include a first tooth connection portion and a second tooth connection portion, a blank section (13) is provided between the first tooth connection portion and the second tooth connection portion, and the transmission gear (16) is tooth-connected with the corresponding driving gear (19) on the first storage bin (3); Before use, the first storage bin (3), the second storage bin (4), the third storage bin (5), and the fourth storage bin (6) are respectively filled with powdered branched alkyl sulfonic acid fatty amine salt, powdered isooctyl succinate sulfonate, liquid FS-3000 fluorocarbon surfactant, and powdered sodium dodecylbenzene sulfonate. When in use, the drive motor (15) can be controlled to work, and the drive motor (15) can drive the gear ring (44) to rotate clockwise. The clockwise rotation of the gear ring (44) can drive the first arc plate (10) with the tooth segment (12) and the second arc plate (11) to rotate clockwise. When the second arc plate (11) rotates When the first material storage bin (3) is rotated, the driving gear (19) will be gear-engaged with the driving gear (19) corresponding to the first material storage bin (3) and drive the metering cylinder (18) to rotate. In the initial state, the metering cavity (20) of the metering cylinder (18) opens upward and coincides with the material discharge opening of the material storage bin. The metering cavity (20) is filled with material. After rotating (180) degrees, the metering cavity (20) opens downward. At this time, the driving gear (19) and the second arc plate (11) are gear-engaged and separated, and the metering cylinder (18) stops rotating. When all the material inside falls into the reaction tank (1), as the second arc plate (11) continues to rotate, the second arc plate (11) will be gear-engaged with the driving gear (19) again, so that the metering cylinder (18) is (18) returns to its original position, i.e. the metering chamber (20) opens upwards. At this time, the material in the storage bin enters the metering chamber (20) by gravity, i.e. the loading is automatically completed. After the metering cylinder (18) of the first storage bin (3) returns to its original position, the second arc plate (11) and the driving gear (19) are gear-engaged and separated, the metering cylinder (18) stops rotating, and the driving motor (15) stops working. When adding materials subsequently, the driving motor (15) can be started, the second arc plate (11) is gear-engaged with the driving gear (19) of the second storage bin (4), and the material in the corresponding metering cylinder (18) is poured into the reaction tank (1). After the metering cylinder (18) returns to its original position, the second arc plate (11) and the driving gear (19) of the second storage bin (4) are gear-engaged, and the material in the corresponding metering cylinder (18) is poured into the reaction tank (1). After the toothed ring (44) is in position, the rotation of the toothed ring (44) stops. When the branched alkyl sulfonic acid fatty amine salt needs to be added later, the toothed ring (44) continues to rotate. At this time, the first arc plate (10) is gear-engaged with the transmission gear (16) and drives the metering cylinder (18) to rotate through the driving gear (19) to deliver the material into the reaction tank (1). Subsequently, as the toothed ring (44) continues to rotate, the second arc plate (11) can sequentially drive the metering cylinder (18) on the third storage bin (5) to rotate to discharge the material. The first arc plate (10) and the second arc plate (11) cooperate to simultaneously discharge the branched alkyl sulfonic acid fatty amine salt and sodium dodecylbenzene sulfonate.

2. The preparation process of a water-based wax crystal suppression wax inhibitor according to claim 1, characterized in that: It also includes a material discharge unit, one end of which is arranged on the quantitative cylinder (18) and the other end of which extends to the outside of the quantitative cylinder (18), and is used to promote the discharge of materials in the first storage bin (3), the second storage bin (4) and the fourth storage bin (6) into the quantitative chamber (20), and at the same time helps to discharge all the materials in the quantitative chamber (20); The material unloading unit comprises a rectangular plate (21), a containing groove, a top block (23), an air outlet pipe (26), a first L-shaped rotating shaft (30) and a second L-shaped rotating shaft (32); The rectangular plate (21) is sealingly and slidably disposed in the quantitative chamber (20), and the lower end of the rectangular plate (21) is connected to the bottom inner wall of the quantitative chamber (20) via a first pull rope (24); An elastic airbag (22) is arranged in the inner cavity of the containing groove, and the inner cavity of the elastic airbag (22) is communicated with a ventilation channel (25), the ventilation channel (25) and the air outlet end are connected with the air inlet end of the air outlet pipe (26), the air outlet pipe (26) is arranged at the axis center of the mounting shaft of the quantitative cylinder (18), the air outlet pipe (26) passes through the mounting frame (17) and is connected to the piston cylinder (28) through a rotary joint (27), a rack (29) is installed on the piston which is sealingly and slidably arranged in the inner cavity of the piston cylinder (28), and the upper end of the rack (29) slides through the top of the inner cavity of the reaction tank (1); The first L-shaped rotating shaft (30) is rotatably disposed on the outer wall of the storage bin, a one-way gear (31) is mounted on the first L-shaped rotating shaft (30), and the one-way gear (31) is gear-connected with the rack (29); The second L-shaped rotating shaft (32) is rotatably arranged at the upper end of the mounting frame (17), a plurality of impact hammers (33) are mounted on the second L-shaped rotating shaft (32), a contact rod of the second L-shaped rotating shaft (32) is located directly below the contact rod of the first L-shaped rotating shaft (30), and a contact roller (35) is arranged on the end of the contact rod of the first L-shaped rotating shaft (30).

3. The preparation process of a water-based wax crystal suppressant according to claim 2, characterized in that: It also includes an accelerating impact unit, which is arranged in the inner cavity of the metering cylinder (18) and is used to increase the speed of the top block (23) when colliding with the elastic airbag (22), thereby causing the impact hammer (33) to form a more intense collision with the storage bin; The acceleration impact unit comprises a trapezoidal movable block (36), a second pull rope (39), a return spring (37), a weight (42), a second partition plate (40) and a magnetic tube (41); The trapezoidal movable block (36) is sealingly slidably disposed in the inner cavity of the metering cylinder (18), the two ends of the return spring (37) are respectively connected to the first partition (38) and the trapezoidal movable block (36), one end of the second pull rope (39) is connected to the trapezoidal movable block (36), and the other end of the second pull rope (39) passes through the first partition (38) and the second partition (40) and is connected to the weight (42).

4. The preparation process of a water-based wax crystal suppression wax inhibitor according to claim 3, characterized in that: It also includes an anti-extrusion unit, which is arranged in the inner cavity of the metering cylinder (18) and prevents the rectangular plate (21) from moving when the metering cylinder (18) rotates and the feed opening of the metering cavity (20) is blocked by the inner wall of the mounting frame (17), so that the powder material is squeezed into blocks between the inner wall of the mounting frame (17) and the rectangular plate (21); The anti-extrusion unit includes all the structures of the acceleration impact unit, and the anti-extrusion unit also includes a positioning plate (43) with a positioning hole.

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