Finished product detection equipment for terpilenol preparation

Abstract

The invention relates to the technical field of detection setting, in particular to finished product detection equipment for terpilenol preparation. According to the technical scheme, the device comprises a distillation assembly, a condensation assembly, a gas chromatography system and a data acquisition system, the distillation assembly comprises a distillation box, the condensation assembly comprises a condensation box connected with one end of a steam collecting pipe, and a supercharger is arranged at the end, away from the condensation box, of a liquid pouring hopper. The device is simple in overall structure and convenient to operate, manual intervention can be greatly reduced through mutual cooperation of the distillation assembly, the condensation assembly, the gas chromatography system and the data acquisition system through a filter and a supercharger, so that the detection accuracy of a terpilenol preparation sample is further improved, meanwhile, overall automatic detection is achieved, and the detection efficiency is improved. And the accuracy of a detection result is ensured.

Description

Technical Field

[0001] The invention relates to the technical field of detection equipment, and in particular to a finished product detection equipment for preparing terpineol. Background Art

[0002] Terpineol is an important spice widely used in the preparation of daily and edible flavors. It is a colorless viscous liquid with the scent of lilac flowers, and a bangzi fragrance after dilution. The preparation methods of terpineol mainly include chemical synthesis and direct extraction from plant essential oils. Although there is no economic value in extracting terpineol directly from plant essential oils, turpentine is usually used as a raw material in industry to produce terpineol, which is a mixture mainly composed of α-terpineol. The preparation process of terpineol includes extraction from turpentine or pinene through hydration and dehydration reactions. Terpineol exists in many plant essential oils in nature, such as cypress, cardamom, star anise, orange blossom, lavender, melaleuca, white lemon, cinnamon leaves, etc., among which α-terpineol is the most common. In addition, terpineol has three isomers: α-, β-, and γ-, as well as three optical isomers: left-handed, right-handed and racemic. These isomers and optical isomers exist in different plant essential oils.

[0003] When testing the preparation of pinene alcohol in production, operators are mostly required to perform multiple convenient operations, and manual operations often produce large detection errors, resulting in inaccurate detection results, which leads to unqualified quality of the same batch of pinene alcohol preparation and excessive waste of resources. For this reason, we specially propose a finished product detection equipment for pinene alcohol preparation. Summary of the invention

[0004] The purpose of the present invention is to provide a finished product detection device for terpineol preparation in view of the problems existing in the background technology.

[0005] The technical solution of the present invention is as follows: a finished product detection device for preparing pine oil, comprising a distillation component, a condensation component, a gas chromatography system and a data acquisition system, wherein the distillation component comprises a distillation box, a box cover is arranged above the distillation box, a hinged seat is arranged on one side of the distillation box and the box cover, a cylinder is arranged on one side of the distillation box, a dryer is arranged above the hinged seat, the output end of the dryer passes through the box cover and extends into the distillation box, a placing table is arranged in the distillation box, a thermal conductivity meter is arranged on one side of the distillation component, a filter is arranged between the distillation component and the condensation component, steam collecting pipes are arranged at both ends of the filter, the condensation component comprises a condensation box connected to one end of the steam collecting pipe, a condensation pipe is arranged in the inner cavity of the condensation box, a liquid collecting pipe is arranged in the condensation box, a liquid pouring hopper is arranged below the condensation box, a supercharger is arranged on the end of the liquid pouring hopper away from the condensation box, and the gas chromatography system comprises a detection chassis arranged at one end of the supercharger, and a central control panel is arranged on one side of the detection chassis.

[0006] Preferably, the bottom of the box cover is installed corresponding to the top of the distillation box, the mounting end of the hinged seat is installed corresponding to one side of the distillation box, and the other mounting end of the hinged seat is installed corresponding to one side of the box cover.

[0007] Preferably, the mounting end of the cylinder is mounted correspondingly to the lower side of the distillation box, and the output end of the cylinder is mounted correspondingly to the connecting end of the hinged seat.

[0008] Preferably, the mounting end of the dryer is installed corresponding to the mounting end of the hinged seat, an operating hole is opened on the top of the box cover, the output end of the dryer is installed corresponding to the operating hole, the mounting end of the placement table is installed corresponding to the bottom of the inner cavity of the distillation box, and the mounting end of the thermal conductivity meter is installed corresponding to one side of the distillation box.

[0009] Preferably, the two groups of steam collecting pipes are respectively installed corresponding to the two ends of the filter, a pipe hole one is opened on the box cover, and one end of one group of steam collecting pipes is installed corresponding to the pipe hole one, a pipe hole two is opened on one side of the condensing box, and one end of the other group of steam collecting pipes is installed corresponding to the pipe hole two.

[0010] Preferably, the condensing pipe is evenly laid around the inner cavity of the condensing box, one end of the liquid collecting pipe is installed corresponding to the steam collecting pipe on one side of the second tube hole, a mounting groove is opened at the bottom of the condensing box, and the mounting end of the liquid pouring bucket is installed corresponding to the mounting groove.

[0011] Preferably, both ends of the booster are provided with liquid guide tubes, one end of one group of the liquid guide tubes is installed corresponding to the liquid outlet end of the pouring bucket, and the other end of the other group of the liquid guide tubes is installed corresponding to the detection port of the detection chassis.

[0012] Preferably, the mounting end of the central control panel is mounted corresponding to one side of the detection chassis, and the detection chassis and the central control panel are both electrically connected to the data acquisition system.

[0013] Compared with the prior art, the present invention has the following beneficial technical effects:

[0014] The overall structure of the present invention is simple and easy to operate. The distillation component, the condensation component, the gas chromatography system and the data acquisition system are arranged to cooperate with each other through the filter and the supercharger, which can greatly reduce manual intervention, thereby further improving the detection accuracy of the pinene alcohol preparation sample. At the same time, the overall automated detection ensures the accuracy of the detection result. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] Figure 1 It is a schematic diagram of the overall structure of the present invention;

[0016] Figure 2 It is a cross-sectional view of a part of the present invention;

[0017] Figure 3 It is a schematic diagram of the modules of the present invention.

[0018] Figure numerals: 1. Distillation assembly; 11. Distillation box; 12. Box cover; 13. Articulated seat; 14. Cylinder; 15. Dryer; 16. Placement table; 17. Thermal conductivity meter; 2. Condensation assembly; 21. Condensation box; 22. Condenser; 23. Liquid collecting pipe; 24. Liquid pouring bucket; 3. Gas chromatography system; 31. Detection chassis; 32. Central control panel; 4. Filter; 5. Steam collecting pipe; 6. Supercharger; 7. Liquid guide pipe. DETAILED DESCRIPTION

[0019] The technical solution of the present invention is further described below in conjunction with the accompanying drawings and specific embodiments.

[0020] Example

[0021] like Figure 1-3As shown, a finished product detection device for preparing pine oil alcohol proposed by the present invention comprises a distillation component 1, a condensation component 2, a gas chromatography system 3 and a data acquisition system, wherein the distillation component 1 comprises a distillation box 11, a box cover 12 is arranged above the distillation box 11, the lower part of the box cover 12 is installed corresponding to the upper part of the distillation box 11, when the box cover 12 and the distillation box 11 are in an installed state, the inner cavity of the distillation box 11 is in a sealed state, a hinge seat 13 is arranged on one side of the distillation box 11 and the box cover 12, the installation end of the hinge seat 13 is installed corresponding to one side of the distillation box 11, the installation end of the hinge seat 13 is fixedly connected to one side of the distillation box 11, and the installation end on the other side of the hinge seat 13 is connected to the One side of the box cover 12 is installed accordingly, and the mounting end of the other side of the hinged seat 13 is fixedly connected to the one side of the box cover 12. A cylinder 14 is provided on one side of the distillation box 11, and the mounting end of the cylinder 14 is installed correspondingly to the lower side of the distillation box 11. The mounting end of the cylinder 14 is fixedly connected to the lower side of the distillation box 11. The output end of the cylinder 14 is installed correspondingly to the connecting end of the hinged seat 13. The output end of the cylinder 14 is fixedly connected to the connecting end of the hinged seat 13. The connecting end of the hinged seat 13 is rotatably arranged. A dryer 15 is provided above the hinged seat 13. The mounting end of the dryer 15 is installed correspondingly to the mounting end of the hinged seat 13. The mounting end of the dryer 15 is connected to the hinged seat 13. The top of the box cover 12 is fixedly connected to one side of the seat 13, an operation hole is opened on the top of the box cover 12, the output end of the dryer 15 is installed corresponding to the operation hole, the output end of the dryer 15 is tightly fitted with the inner wall of the operation hole, the output end of the dryer 15 passes through the box cover 12 and extends into the distillation box 11, the setting of the dryer 15 can heat the distillation box 11, and a placement table 16 is provided in the distillation box 11, the installation end of the placement table 16 is installed corresponding to the bottom of the inner cavity of the distillation box 11, the installation end of the placement table 16 is fixedly connected to the inner cavity of the distillation box 11, and the setting of the placement table 16 can enable the operator to stably place the pine oil alcohol preparation sample to be distilled, and one side of the distillation component 1 A thermal conductivity meter 17 is provided, and the mounting end of the thermal conductivity meter 17 is installed corresponding to one side of the distillation box 11, and the mounting end of the thermal conductivity meter 17 is fixedly connected to one side of the distillation box 11. The setting of the thermal conductivity meter 17 can detect the thermal conductivity of the sample placed on the placement table 16, so that the moisture content of the pine ethanol prepared sample can be more accurately calculated. Through the setting of the distillation component 1, the pine ethanol prepared sample in the distillation box 11 can be heated to 80-100°C at a low temperature until all moisture is lost, and its quality remains unchanged. The whole process is carried out at a low temperature to avoid the sample from burning at a high temperature, thereby stably completing the distillation operation of the pine ethanol prepared sample;

[0022] A filter 4 is arranged between the distillation component 1 and the condensation component 2, and steam collecting pipes 5 are arranged at both ends of the filter 4, two groups of steam collecting pipes 5 are respectively installed corresponding to the two ends of the filter 4, and one end of the two groups of steam collecting pipes 5 are respectively fixedly connected to the two ends of the filter 4, a pipe hole 1 is opened on the box cover 12, one end of one group of steam collecting pipes 5 is installed corresponding to the pipe hole 1, and one group of steam collecting pipes 5 is fixedly connected to the pipe hole 1, and the condensation component 2 includes a condensation box 21 connected to one end of the steam collecting pipe 5, a pipe hole 2 is opened on one side of the condensation box 21, one end of another group of steam collecting pipes 5 is installed corresponding to the pipe hole 2, and the other group of steam collecting pipes 5 is fixedly connected to the pipe hole 2. The arrangement of the steam collecting pipes 5 can make the distillation component 1 and the condensation component 2 work better together through the filter 4, so that the water vapor distilled in the distillation component 1 can be transported to the condensation component 2;

[0023] The inner cavity of the condensing box 21 is provided with a condensing pipe 22, which is evenly laid around the inner cavity of the condensing box 21. The installation end of the condensing pipe 22 is fixedly connected to the inner cavity of the condensing box 21. The setting of the condensing pipe 22 can cooperate with the condensing box 21 to cool and condense the water vapor flowing in the steam collecting pipe 5. The condensing box 21 is provided with a liquid collecting pipe 23, one end of the liquid collecting pipe 23 is installed corresponding to the steam collecting pipe 5 on one side of the pipe hole 2, and one end of the liquid collecting pipe 23 is fixedly connected to one end of the steam collecting pipe 5. The liquid collecting pipe 23 The setting can gather the condensed distilled water, a pouring bucket 24 is arranged below the condensation box 21, a mounting groove is provided below the condensation box 21, the mounting end of the pouring bucket 24 is installed corresponding to the mounting groove, the mounting end of the pouring bucket 24 is fixedly connected to the mounting groove, the setting of the pouring bucket 24 can collect and guide the condensed distilled water, the setting of the condensation component 2 can condense the water vapor after distillation by the distillation component 1, so as to better detect the water content of the pine oil prepared sample;

[0024] A booster 6 is provided at one end of the liquid pouring bucket 24 away from the condensation tank 21, and liquid guide tubes 7 are provided at both ends of the booster 6. One end of a group of liquid guide tubes 7 is installed corresponding to the liquid outlet end of the liquid pouring bucket 24, and one end of the liquid guide tubes 7 is fixedly connected to the liquid outlet end of the liquid pouring bucket 24. The gas chromatography system 3 includes a detection chassis 31 arranged at one end of the booster 6, and the other end of another group of liquid guide tubes 7 is installed corresponding to the detection port of the detection chassis 31. The other end of the other group of liquid guide tubes 7 is fixedly connected to the detection port of the detection chassis 31. The setting of the booster 6 can pressurize the collected distilled water so that the distilled water is drained into the detection chassis 31 for detection by an electron capture detector. A central control panel 32 is provided on one side of the detection chassis 31, and the installation end of the central control panel 32 is installed corresponding to one side of the detection chassis 31. The mounting end of the plate 32 is fixedly connected to the detection chassis 31, and the central control panel 32 is electrically connected to the detection chassis 31. The setting of the central control panel 32 can facilitate the operator to operate and observe the detection chassis 31, so that the water content of the sample can be detected more accurately. The detection chassis 31 and the central control panel 32 are both electrically connected to the data acquisition system. The setting of the data acquisition system can cooperate with the gas chromatography system 3, so that the records can be analyzed to ensure the accuracy of the detection. The distillation component 1, the condensation component 2, the gas chromatography system 3 and the data acquisition system are mutually coordinated through the filter 4 and the booster 6, which can greatly reduce manual intervention, thereby further improving the detection accuracy of the pine oil alcohol preparation sample. At the same time, the overall automated detection ensures the accuracy of the detection results.

[0025] In this embodiment, when the operator needs to test the pine oil preparation, the operator first accurately weighs the pine oil preparation sample, and then the operator energizes and starts the cylinder 14, so that the cylinder 14 drives the box cover 12 to move through the hinge seat 13, so that the box cover 12 is separated from the sealed state with the distillation box 11, and then the operator puts the sample to be tested on the placement table 16 in the distillation box 11, and then the operator restores the box cover 12 to the initial state through the cylinder 14, so that the distillation box 11 and the box cover 12 are in a sealed state, and then the operator completely seals the distillation box 11 and the box cover 12 through the airtight component on the box cover 12, and the operator energizes and starts the dryer 15, and the dryer 15 heats the space in the distillation box 11 Distillation is performed until the sample on the placement table 16 completely loses its moisture. At the same time, the thermal conductivity meter 17 operates to monitor the sample on the placement table 16 in real time. The water vapor distilled in the distillation component 1 is guided into the condensation box 21 through the filter 4 and the steam collecting pipe 5. Then the condensation pipe 22 operates to cool and condense the distilled water vapor in the liquid collecting pipe 23, so that the water vapor forms water droplets. Then, the water vapor is concentrated and guided through the pouring bucket 24. Then, the water vapor is guided into the detection box 31 under the action of the supercharger 6 and the liquid guiding pipe 7. Then, the operator detects the distilled water in the detection box 31 through the central control panel 32, and compares the detection results through the data acquisition system, thereby completing the detection operation of the pine oil alcohol preparation sample.

[0026] The above specific embodiment is only a preferred embodiment of the present invention. Based on the technical solution of the present invention and the relevant inspiration of the above embodiment, those skilled in the art can make various alternative improvements and combinations to the above specific embodiment.

Claims

1. A finished product testing device for preparing terpineol, comprising a distillation component (1), a condensation component (2), a gas chromatography system (3) and a data acquisition system, characterized in that: The distillation assembly (1) comprises a distillation box (11), a box cover (12) is arranged above the distillation box (11), a hinged seat (13) is arranged on one side of the distillation box (11) and the box cover (12), a cylinder (14) is arranged on one side of the distillation box (11), a dryer (15) is arranged above the hinged seat (13), the output end of the dryer (15) passes through the box cover (12) and extends into the distillation box (11), a placement table (16) is arranged in the distillation box (11), a thermal conductivity meter (17) is arranged on one side of the distillation assembly (1), and a filter is arranged between the distillation assembly (1) and the condensation assembly (2). (4), both ends of the filter (4) are provided with steam collecting pipes (5), the condensation assembly (2) comprises a condensation box (21) connected to one end of the steam collecting pipe (5), the inner cavity of the condensation box (21) is provided with a condensation pipe (22), a liquid collecting pipe (23) is provided in the condensation box (21), a liquid pouring hopper (24) is provided below the condensation box (21), a supercharger (6) is provided on the end of the liquid pouring hopper (24) away from the condensation box (21), the gas chromatography system (3) comprises a detection box (31) arranged at one end of the supercharger (6), and a central control panel (32) is provided on one side of the detection box (31).

2. The finished product detection equipment for preparing terpineol according to claim 1, characterized in that: The bottom of the box cover (12) is installed corresponding to the top of the distillation box (11), the installation end of the hinged seat (13) is installed corresponding to one side of the distillation box (11), and the other side installation end of the hinged seat (13) is installed corresponding to one side of the box cover (12).

3. The finished product detection equipment for preparing terpineol according to claim 1, characterized in that: The mounting end of the cylinder (14) is mounted correspondingly to the lower side of the distillation box (11), and the output end of the cylinder (14) is mounted correspondingly to the connection end of the hinge seat (13).

4. The finished product detection equipment for preparing terpineol according to claim 1, characterized in that: The mounting end of the dryer (15) is mounted correspondingly to the mounting end of the hinged seat (13); an operation hole is provided on the top of the box cover (12); the output end of the dryer (15) is mounted correspondingly to the operation hole; the mounting end of the placement table (16) is mounted correspondingly to the bottom of the inner cavity of the distillation box (11); and the mounting end of the thermal conductivity meter (17) is mounted correspondingly to one side of the distillation box (11).

5. The finished product detection equipment for terpineol preparation according to claim 1, characterized in that: The two groups of steam collecting pipes (5) are respectively installed corresponding to the two ends of the filter (4); a pipe hole 1 is opened on the box cover (12); one end of one group of steam collecting pipes (5) is installed corresponding to the pipe hole 1; a pipe hole 2 is opened on one side of the condensing box (21); one end of the other group of steam collecting pipes (5) is installed corresponding to the pipe hole 2.

6. The finished product detection equipment for terpineol preparation according to claim 1, characterized in that: The condensing pipe (22) is evenly laid around the inner cavity of the condensing box (21), one end of the liquid collecting pipe (23) is installed corresponding to the steam collecting pipe (5) on one side of the pipe hole 2, and a mounting groove is opened at the bottom of the condensing box (21), and the mounting end of the liquid pouring bucket (24) is installed corresponding to the mounting groove.

7. The finished product detection equipment for preparing terpineol according to claim 1, characterized in that: Both ends of the booster (6) are provided with liquid guide tubes (7), one end of one group of the liquid guide tubes (7) is installed corresponding to the liquid outlet end of the liquid pouring bucket (24), and the other end of the other group of the liquid guide tubes (7) is installed corresponding to the detection port of the detection box (31).

8. The finished product detection equipment for terpineol preparation according to claim 1, characterized in that: The installation end of the central control panel (32) is installed corresponding to one side of the detection chassis (31), and the detection chassis (31) and the central control panel (32) are both electrically connected to the data acquisition system.

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