Production device of cyclopentanone product
By designing multiple reaction zones in the cyclopentanone production device and stirring them separately, the problem of insufficient stirring caused by the accumulation of barium hydroxide in the prior art is solved, and a more efficient reaction effect is achieved.
Patent Information
- Application Number
- CN202411320950.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-23
- Publication Date
- 2025-01-24
- Estimated Expiration
- 2044-09-23
AI Technical Summary
When analyzing adipic acid and barium hydroxide is used in a vertically arranged stirring tank in the prior art, barium hydroxide is prone to accumulate, resulting in insufficient stirring, long reaction time and insufficient reaction.
Design a production device for cyclopentanone products, including a hollow installation cylinder, several partitions, arc-shaped connecting plates and stirring rods, by separating barium hydroxide and adipic acid for mixing reactions in multiple reaction areas, and Stir each reaction area individually to improve the mixing effect and reaction effect.
By "reorganization into zero", mixed reactions and stirring in multiple reaction areas solved the problem of inadequate mixing caused by the accumulation of raw materials in the traditional vertical stirring tank, and improved the reaction efficiency and effect.
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Figure CN119345711A_ABST
Abstract
Description
Technical Field
[0001] The invention belongs to the technical field of cyclopentanone preparation, and in particular relates to a production device for a cyclopentanone product. Background Art
[0002] In the prior art, the preparation of cyclopentanone generally adopts the following steps: adipic acid and barium hydroxide are uniformly mixed, and then heated within a certain temperature range. The temperature is generally between 285-295°C. At this temperature, adipic acid undergoes a decomposition reaction under the catalytic action of barium hydroxide to produce cyclopentanone. Subsequently, a distillation operation is performed to separate the produced cyclopentanone from the reaction mixture.
[0003] When cyclopentanone is prepared by the cyclopentanone preparation steps in the prior art, a vertically arranged stirring tank is usually used to stir and mix adipic acid and barium hydroxide so that the two can react fully. However, the vertically arranged stirring tank has the following problems when it is actually used: when the amount of oxalic acid and barium hydroxide participating in the reaction is large, the barium hydroxide will accumulate layer by layer in the vertically arranged reaction tank, which will make it difficult to stir it fully during stirring, thereby resulting in a long reaction time of barium hydroxide and adipic acid, and the reaction is not sufficient. Summary of the invention
[0004] In view of this, the object of the present invention is to provide a production device for a cyclopentanone product, so as to solve the problem that in the prior art, when preparing cyclopentanone, a vertically arranged stirring tank is used to stir adipic acid and barium hydroxide, and the accumulation of barium hydroxide leads to insufficient stirring and mixing, resulting in a long reaction time of barium hydroxide and adipic acid, and insufficient reaction.
[0005] In order to achieve the above object, the present invention provides the following technical solutions:
[0006] The present invention discloses a production device for a cyclopentanone product, comprising a stirring reaction mechanism, wherein the stirring reaction mechanism comprises a hollow mounting cylinder, one end of the mounting cylinder is closed, a support leg is arranged on the outer surface of the mounting cylinder facing the ground, one end of the support leg is fixed to the outer surface of the mounting cylinder, a plurality of partitions are arranged in the axial direction of the interior of the mounting cylinder, the edges of the partitions are in sliding contact with the inner wall of the mounting cylinder, an arc-shaped connecting plate is arranged between adjacent partitions, the two side surfaces of the arc-shaped connecting plate are respectively fixed to the end surfaces of two adjacently arranged partitions, a notch is arranged between the two ends of the arc-shaped connecting plate, and the notch faces the side of the mounting cylinder away from the ground. The surface of the invention is arranged, and a feeding pipe is provided on the installation cylinder just above the notch of the arc-shaped connecting plate, and the feeding pipe is connected to the notch. A rotating bearing is provided in the middle of several of the partitions, and the outer ring of the rotating bearing is fixed on the partition, and the inner ring of the rotating bearing is provided with a rotating shaft, and the inner ring of the bearing is fixed on the rotating shaft. A stirring rod is provided on the rotating shaft between two adjacent partitions, and one end of the stirring rod is fixed on the rotating shaft. A driving motor is provided on the end of the rotating shaft located outside the installation cylinder, and the output end of the driving motor is fixed on the rotating shaft. A sliding mechanism is provided on the unclosed end of the installation cylinder, and the driving motor is fixed on the sliding mechanism.
[0007] Furthermore, the sliding mechanism includes a symmetrically arranged arc guide rail, one end of the arc guide rail is fixed on the mounting cylinder, the inner wall of the arc guide rail is flush with the inner wall of the mounting cylinder, an installation spacing is provided between the two arc guide rails, a slider is provided on the two arc guide rails, both ends of the slider are respectively slidably connected to the two arc guide rails, a fixed block is provided on the slider, the drive motor is fixed on the fixed block, and the length of the arc guide rail is greater than the length of the mounting cylinder.
[0008] Furthermore, a retaining ring is provided on the arc-shaped guide rail, and the retaining ring is detachably connected to the arc-shaped guide rail, and the retaining ring is used to prevent the sliding of the slider.
[0009] Furthermore, the plurality of partitions located in the middle are each provided with two groups of symmetrically arranged communicating holes, the communicating hole groups include a plurality of vertically arranged communicating holes, and the two groups of communicating holes are located on both sides of the rotating shaft.
[0010] Furthermore, a card plate is provided on the outer side of any group of the connecting hole groups, and the card plate is fixed on the partition and is arranged near the middle of the partition. A plurality of baffles corresponding to the positions of the connecting holes are provided on the card plate, and the baffle is slidably connected to the card plate, and one end of the baffle is arranged toward the connecting hole, and a first magnetic block is provided on the other end of the baffle, and one end of the first magnetic block is fixed to the baffle, and the two first magnetic blocks arranged opposite to each other have different magnetic properties from the end fixed to the baffle, a second magnetic block is provided on the outer side of the first magnetic block, and a mounting rod is provided in the middle of the second magnetic block, and the second magnetic block is rotatably connected to the mounting rod, and both ends of the mounting rod are detachably connected to the partition.
[0011] Furthermore, a sealing piston is provided on the portion of the rotating shaft close to the unclosed end of the mounting cylinder, the middle part of the sealing piston is rotatably connected to the rotating shaft, the edge of the sealing piston is in extrusion contact with the inner wall of the mounting cylinder, the edge of the sealing piston facing the mounting cylinder is conically set, and horizontal marking lines are provided on the sealing piston and the unclosed end of the mounting cylinder.
[0012] Furthermore, a collection box is provided directly below the arc-shaped guide rail.
[0013] Furthermore, it also includes a distillation mechanism, which includes a heat transfer block, the upper surface of which is in arc-shaped contact with the outer surface of the lower middle part of the installation cylinder, and a heating wire is arranged inside the heat transfer block.
[0014] Furthermore, support rods are provided at both ends of the heat transfer block, one end of the support rod is fixed on the heat transfer block, a slide plate is provided on the other end of the support rod, one side of the slide plate is fixed on the support rod, a linear push rod is provided in the middle of the other side of the slide plate, and the output end of the linear push rod is fixed on the slide plate.
[0015] The beneficial effects of the present invention are:
[0016] This technical solution separates a large amount of raw materials into several different reaction areas (composed of adjacent reaction tanks and arc-shaped connecting plates therebetween) by a "break-down" method for mixed reaction, and stirs each reaction area individually, thereby improving the stirring and mixing effect. At the same time, it improves the reaction effect and solves the problem of raw materials being easily accumulated in traditional vertical stirring tanks, resulting in insufficient mixing.
[0017] Other advantages, objectives and features of the present invention will be described in the following description and will be apparent to those skilled in the art to some extent, or those skilled in the art may be taught from the practice of the present invention. The objectives and other advantages of the present invention may be realized and obtained through the following description. BRIEF DESCRIPTION OF THE DRAWINGS
[0018] In order to make the purpose, technical solution and beneficial effects of the present invention clearer, the present invention provides the following drawings for illustration:
[0019] Figure 1 It is a three-dimensional schematic diagram of the production device of the present invention;
[0020] Figure 2 A three-dimensional schematic diagram of the arrangement of several partitions of the present invention;
[0021] Figure 3 It is a schematic diagram of the connection relationship between the arc guide rail and the mounting cylinder of the present invention;
[0022] Figure 4 It is a three-dimensional schematic diagram of the distillation mechanism of the present invention;
[0023] Figure 5 A three-dimensional schematic diagram of a baffle plate provided on the partition of the present invention;
[0024] Figure 6 is a three-dimensional schematic diagram of the arc-shaped connecting plate of the present invention;
[0025] Figure 7-Figure 8 It is a three-dimensional schematic diagram of a connecting hole and a baffle plate provided on the partition of the present invention;
[0026] Fig. 9 It is a schematic diagram of the arrangement of the first magnetic block and the second magnetic block of the present invention.
[0027] The following are marked in the accompanying drawings:
[0028] 1. Install the cylinder; 2. Feeding pipe; 3. Support leg; 4. Drive motor; 5. Rotating shaft; 6. Partition; 7. Rotating bearing; 8. Arc connecting plate; 9. Sealing piston; 10. Stirring rod; 11. Connecting hole; 12. Card plate; 13. Baffle; 14. Arc guide rail; 15. Slider; 16. Fixed block; 17. Heat transfer block; 18. Heating wire; 19. Support rod; 20. Slide plate; 21. Linear push rod; 22. Collecting box; 23. First magnetic block; 24. Second magnetic block; 25. Install rod. DETAILED DESCRIPTION
[0029] like Figures 1 to 9As shown, a production device of a cyclopentanone product of the present invention comprises a stirring reaction mechanism, wherein the stirring reaction mechanism comprises a hollow mounting cylinder 1, one end of the mounting cylinder 1 is closed, a support leg 3 is arranged on the outer surface of the mounting cylinder 1 facing the ground, one end of the support leg 3 is fixed to the outer surface of the mounting cylinder 1, a plurality of partitions 6 are arranged in the axial direction inside the mounting cylinder 1, the edges of the partitions 6 are in sliding contact with the inner wall of the mounting cylinder 1, an arc-shaped connecting plate 8 is arranged between adjacent partitions 6, the two side surfaces of the arc-shaped connecting plate 8 are respectively fixed to the end surfaces of two adjacently arranged partitions 6, a notch is arranged between the two ends of the arc-shaped connecting plate 8, and the notch faces the side of the mounting cylinder 1 away from the ground. The surface is arranged, and a feeding pipe 2 is provided on the installation cylinder 1 just above the notch of the arc-shaped connecting plate 8, and the feeding pipe 2 is connected to the notch. A rotating bearing 7 is provided in the middle of several partitions 6, and the outer ring of the rotating bearing 7 is fixed on the partition 6. The inner ring of the rotating bearing 7 is provided with a rotating shaft 5, and the inner ring of the bearing is fixed on the rotating shaft 5. A stirring rod 10 is provided on the rotating shaft 5 between two adjacent partitions 6, and one end of the stirring rod 10 is fixed on the rotating shaft 5. A driving motor 4 is provided on the end of the rotating shaft 5 located outside the installation cylinder 1, and the output end of the driving motor 4 is fixed on the rotating shaft 5. A sliding mechanism is provided on the unclosed end of the installation cylinder 1, and the driving motor 4 is fixed on the sliding mechanism.
[0030] The working principle of the above technical solution is:
[0031] When preparing cyclopentanone, first add barium hydroxide particles between each adjacent partition 6, and then slide the partition 6 arranged side by side into the interior of the mounting cylinder 1 so that the partition 6 at the end is tightly set against the closed end of the mounting cylinder 1. It should be noted that at this time, the gap between the ends of the arc-shaped connecting plate 8 should be set facing upward, and then a certain amount of adipic acid is added to the position between the two partitions 6 through the feeding pipe 2, and then the driving motor 4 is rotated to drive the stirring rod 10 to rotate, so as to glue the space between the adjacent partitions 6, so that the barium hydroxide and adipic acid in the area can be fully mixed and reacted.
[0032] It is not difficult to understand that this method separates a large amount of raw materials (barium hydroxide) into multiple different reaction areas (composed of adjacent reaction tanks and the arc-shaped connecting plate 8 between the two) for mixed reaction, and stirs each reaction area separately, which can improve the stirring and mixing effect and the reaction effect at the same time; this technical solution separates a large amount of raw materials into small amounts of raw materials in multiple areas in a "breakdown" manner, thereby solving the problem of raw materials being easily accumulated in traditional vertical stirring tanks, resulting in insufficient mixing.
[0033] In one practicable manner, the sliding mechanism includes a symmetrically arranged arc guide rail 14, one end of the arc guide rail 14 is fixed on the mounting cylinder 1, and the inner wall of the arc guide rail 14 is flush with the inner wall of the mounting cylinder 1, that is, it can be understood that the inner ring diameter of the arc guide rail 14 is consistent with the inner ring diameter of the mounting cylinder 1, and an installation spacing is provided between the two arc guide rails 14. A slider 15 is provided on the two arc guide rails 14, and both ends of the slider 15 are respectively slidably connected to the two arc guide rails 14. A fixed block 16 is provided on the slider 15, and the drive motor 4 is fixed on the fixed block 16. The length of the arc guide rail 14 is greater than the length of the mounting cylinder 1.
[0034] With the guidance and support of the arc guide rail 14, when installing or removing several partitions 6 in the installation cylinder 1, it is only necessary to manually pull the slider 15 to pull the partition 6 onto the arc guide rail 14. Since the inner wall of the arc guide rail 14 is flush with the inner wall of the installation cylinder 1, the guidance of the partition 6 is smoother. At the same time, an installation spacing is provided between the two arc guide rails 14. The notch can be aligned with the installation spacing by rotating the partition 6, and the product after the reaction is completed can be poured out.
[0035] In one feasible manner, a retaining ring is provided on the arc guide rail 14, and the retaining ring is detachably connected to the arc guide rail 14, and is used to block the sliding of the slider 15. The function of the retaining ring is to block the movement of the slider 15 when the drive motor 4 is working, so as to prevent the partition 6 from slipping off to the outside of the mounting cylinder 1.
[0036] In one practicable manner, two groups of symmetrically arranged communicating holes 11 are provided on the plurality of partitions 6 located in the middle, and the communicating holes 11 groups include a plurality of vertically arranged communicating holes 11, and the two groups of communicating holes 11 groups are located on both sides of the rotating shaft 5. The arrangement of the communicating holes 11 can play a connecting role, even if the pages of adipic acid in each reaction area are flush, that is, when an equal amount of barium hydroxide is added to each reaction area, when adipic acid is added, there is no need to accurately control the amount of addition to each reaction area separately, so that the amount of adipic acid added to each area can be guaranteed to be consistent. At the same time, it can be understood here that the addition of adipic acid in each area is "rounded off", and only the adipic acid required to meet the total amount of barium hydroxide needs to be added, so as to achieve rapid addition of adipic acid. Of course, the part where the cylinder 1 is installed can be transparent, so as to facilitate observation of the amount of adipic acid added.
[0037] like Figure 7-Figure 9As shown, in an implementable manner, a card plate 12 is provided on the outer side of any group of connecting holes 11, the card plate 12 is fixed on the partition 6 and is arranged near the middle of the partition 6, a plurality of baffles 13 corresponding to the positions of the connecting holes 11 are provided on the card plate 12, the baffle 13 is slidably connected to the card plate 12, and one end of the baffle 13 is arranged toward the connecting holes 11, a first magnetic block 23 is provided on the other end of the baffle 13, one end of the first magnetic block 23 is fixed on the baffle 13, and the two first magnetic blocks 23 arranged opposite to each other have different magnetic properties from the end fixed to the baffle 13, a second magnetic block 24 is provided on the outer side of the first magnetic block 23, a mounting rod 25 is provided in the middle of the second magnetic block 24, the second magnetic block 24 is rotatably connected to the mounting rod 25, and both ends of the mounting rod 25 are detachably connected to the partition 6.
[0038] The baffle 13 is provided to block and close the connecting hole 11, that is, one connecting hole 11 in the group of several vertical connecting holes 11 can be selected according to needs to remain unobstructed (selecting the height of the connecting hole 11 can also be understood as selecting the height of adding adipic acid). The advantage of this is that the connecting holes 11 at a lower position can be closed to prevent the barium hydroxide particles in each reaction area from moving through the connecting holes 11 during stirring, resulting in uneven distribution of barium hydroxide in each reaction area. At the same time, it also prevents the connecting holes 11 at a lower position from being blocked, resulting in a large amount of cleaning work in the later stage (it is not difficult to understand that the unobstructed connecting holes 11 are located above the accumulated barium hydroxide, that is, they will not be blocked during stirring).
[0039] It is not difficult to understand that the two magnetic poles of the second magnetic block 24 can respectively pull the ends of the first magnetic blocks 23 set on both sides, that is, the connecting hole 11 is in an open state at this time, and the baffle 13 at the connecting hole 11 at other positions does not need to be opened. At this time, you only need to rotate the second magnetic block 24 on the mounting rod 25 to swap the magnetic poles of the second magnetic block 24. That is, at this time, the two ends of the second magnetic pole repel the ends of the first magnetic blocks 23 on both sides, that is, push the baffle 13 to move to close the connecting hole. In this way, the position state of the baffle 13 can be guaranteed, and there will be no problem of the baffle 13 slipping on the card plate 12 due to vibration.
[0040] The sealing piston 9 is provided with a sealing piston 9 on the part of the rotating shaft 5 close to the unsealed end of the mounting cylinder 1. The middle part of the sealing piston 9 is rotatably connected to the rotating shaft 5, and the end face is fixed on the partition 6 arranged at one end. The edge of the sealing piston 9 is squeezed and contacted with the inner wall of the mounting cylinder 1 to prevent liquid leakage. The edge of the sealing piston 9 facing the mounting cylinder 1 is conical. The conical setting can guide the sealing piston 9 to enter the mounting cylinder 1 to avoid the problem that it cannot enter the mounting cylinder 1 due to its relatively large diameter. Horizontal marking lines are provided on the unsealed end of the sealing piston 9 and the mounting cylinder 1. The horizontal marking lines are convenient for positioning and adjusting the partition 6 and the arc connecting plate 8 to ensure the position accuracy of the notch. It is not difficult to understand that bolts or the like can be set on the end face of the sealing piston 9 to tighten it against the mounting cylinder 1 to prevent it from rotating due to vibration. Furthermore, the part where the partition 6 and the sealing piston 9 are rotatably connected to the rotating shaft 5 needs to be sealed, such as the shaft seal in the prior art, which will not be described in detail.
[0041] In an practicable manner, a collection box 22 is provided directly below the arc-shaped guide rail 14 , and the collection box 22 can collect the slag after the reaction.
[0042] In one practicable manner, a distillation mechanism is also included, and the distillation mechanism includes a heat transfer block 17, the upper surface of the heat transfer block 17 is in arc-shaped contact with the outer surface of the middle and lower part of the installation cylinder 1, and the interior of the heat transfer block 17 is provided with a heating wire 18, which is a prior art and will not be described in detail here. The heat transfer block 17 is in contact with the installation cylinder 1 to transfer heat, so that the heat transfer is more uniform, that is, the reaction temperature applied to the internal reactants is more uniform. At the same time, a higher temperature can be applied to achieve a distillation operation on the product after the reaction, thereby obtaining cyclopentanone. It is not difficult to find that during the distillation operation, the evaporated cyclopentanone can be discharged through the feed pipe for condensation and collection.
[0043] In one feasible manner, support rods 19 are provided at both ends of the heat transfer block 17, one end of the support rod 19 is fixed on the heat transfer block 17, a slide plate 20 is provided on the other end of the support rod 19, one side of the slide plate 20 is fixed on the support rod 19, a linear push rod 21 is provided in the middle of the other side of the slide plate 20, and the output end of the linear push rod 21 is fixed on the slide plate 20. By changing the distance between the heat transfer block 17 and the mounting cylinder 1, the heat transfer block 17 can perform thermal radiation heating on the mounting cylinder, that is, the reaction temperature can be controlled by controlling the distance between the two. It is not difficult to understand that the distance between the heat transfer block 17 and the mounting cylinder 1 can be controlled by electrically connecting the temperature sensor and the linear push rod 21.
[0044] Finally, it should be noted that the above preferred embodiments are only used to illustrate the technical solutions of the present invention rather than to limit it. Although the present invention has been described in detail through the above preferred embodiments, those skilled in the art should understand that various changes can be made in form and details without departing from the scope defined by the claims of the present invention.
Claims
1. A production device for a cyclopentanone product, characterized in that: The invention comprises a stirring reaction mechanism, wherein the stirring reaction mechanism comprises a hollow mounting cylinder (1), one end of the mounting cylinder (1) is closed, a support leg (3) is provided on the outer surface of the mounting cylinder (1) facing the ground, one end of the support leg (3) is fixed to the outer surface of the mounting cylinder (1), a plurality of partitions (6) are provided in the axial direction inside the mounting cylinder (1), the edges of the partitions (6) are in sliding contact with the inner wall of the mounting cylinder (1), an arc-shaped connecting plate (8) is provided between adjacent partitions (6), the two side surfaces of the arc-shaped connecting plate (8) are respectively fixed to the end surfaces of two adjacent partitions (6), a notch is provided between the two ends of the arc-shaped connecting plate (8), the notch is arranged toward the surface of the mounting cylinder (1) away from the ground, and the notch of the arc-shaped connecting plate (8) A feeding pipe (2) is provided on the installation cylinder (1) directly above, and the feeding pipe (2) is connected to the notch. A rotating bearing (7) is provided in the middle of each of the partitions (6). The outer ring of the rotating bearing (7) is fixed on the partition (6). The inner ring of the rotating bearing (7) is provided with a rotating shaft (5). The inner ring of the bearing is fixed on the rotating shaft (5). A stirring rod (10) is provided on the rotating shaft (5) between two adjacent partitions (6). One end of the stirring rod (10) is fixed on the rotating shaft (5). A driving motor (4) is provided on the end of the rotating shaft (5) located outside the installation cylinder (1). The output end of the driving motor (4) is fixed on the rotating shaft (5). A sliding mechanism is provided on the unsealed end of the installation cylinder (1). The driving motor (4) is fixed on the sliding mechanism.
2. The production device of a cyclopentanone product according to claim 1, characterized in that: The sliding mechanism comprises a symmetrically arranged arc guide rail (14), one end of the arc guide rail (14) is fixed on the mounting cylinder (1), the inner wall of the arc guide rail (14) is arranged flush with the inner wall of the mounting cylinder (1), an installation spacing is arranged between the two arc guide rails (14), a slider (15) is arranged on the two arc guide rails (14), the two ends of the slider (15) are respectively slidably connected to the two arc guide rails (14), a fixing block (16) is arranged on the slider (15), the drive motor (4) is fixed on the fixing block (16), and the length of the arc guide rail (14) is greater than the length of the mounting cylinder (1).
3. A production device for a cyclopentanone product according to claim 2, characterized in that: The arc-shaped guide rail (14) is provided with a retaining ring, which is detachably connected to the arc-shaped guide rail (14) and is used to prevent the sliding of the slider (15).
4. The production device of a cyclopentanone product according to claim 1, characterized in that: Two groups of symmetrically arranged communicating holes (11) are provided on the plurality of partitions (6) located in the middle, the communicating holes (11) groups comprising a plurality of vertically arranged communicating holes (11), and the two groups of communicating holes (11) are located on both sides of the rotating shaft (5).
5. The production device of a cyclopentanone product according to claim 4, characterized in that: A card plate (12) is provided on the outside of any group of the connecting holes (11), the card plate (12) is fixed on the partition (6), and is arranged near the middle of the partition (6). The card plate (12) is provided with a plurality of baffles (13) corresponding to the positions of the connecting holes (11), the baffles (13) are slidably connected to the card plate (12), and one end of the baffle (13) is arranged toward the connecting hole (11), and the other end of the baffle (13) is provided with a first magnetic block (23), one end of the first magnetic block (23) is fixed on the baffle (13), and the two first magnetic blocks (23) arranged opposite to each other have different magnetic properties at one end fixed to the baffle (13). A second magnetic block (24) is arranged on the outer side of the first magnetic block (23), and a mounting rod (25) is arranged in the middle of the second magnetic block (24). The second magnetic block (24) is rotatably connected to the mounting rod (25), and both ends of the mounting rod (25) are detachably connected to the partition (6).
6. The production device of a cyclopentanone product according to claim 1, characterized in that: A sealing piston (9) is provided on a portion of the rotating shaft (5) close to the unsealed end of the mounting cylinder (1); the middle portion of the sealing piston (9) is rotatably connected to the rotating shaft (5); the edge of the sealing piston (9) is in extrusion contact with the inner wall of the mounting cylinder (1); the edge of the sealing piston (9) facing the mounting cylinder (1) is conically arranged; and horizontal marking lines are provided on both the sealing piston (9) and the unsealed end of the mounting cylinder (1).
7. The production device of a cyclopentanone product according to claim 2, characterized in that: A collection box (22) is provided directly below the arc-shaped guide rail (14).
8. The production device of a cyclopentanone product according to claim 1, characterized in that: It also includes a distillation mechanism, which includes a heat transfer block (17). The upper surface of the heat transfer block (17) is in arc-shaped contact with the outer surface of the lower part of the installation cylinder (1), and a heating wire (18) is provided inside the heat transfer block (17).
9. The production device of a cyclopentanone product according to claim 8, characterized in that: Support rods (19) are provided at both ends of the heat transfer block (17), one end of the support rod (19) is fixed to the heat transfer block (17), a slide plate (20) is provided on the other end of the support rod (19), one side of the slide plate (20) is fixed to the support rod (19), a linear push rod (21) is provided in the middle of the other side of the slide plate (20), and an output end of the linear push rod (21) is fixed to the slide plate (20).
Citation Information
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