Static three-phase separator for mixed gas

By designing an electrostatic three-phase separator, the electrostatic field and adsorption materials are used to separate the oil, gas and water produced during the thermal cracking of organic materials. This solves the problem of low oil purity in the existing technology and achieves the separation of high-purity oil. and increase in economic value.

CN119346291APending Publication Date: 2025-01-24CHINA COAL ZHANGJIAKOU COAL MINING MACHINERY
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Patent Information

Application Number
CN202411277596.X
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-09-12
Publication Date
2025-01-24

AI Technical Summary

Technical Problem

The existing mixed gas three-phase separators cannot effectively separate high-purity oil during the thermal cracking of organic materials. The oil often contains impurities such as moisture and carbon black, which affects the use value of the oil.

Method used

A mixed gas electrostatic three-phase separator is designed, which uses a water collecting tray, an insulating ring, an electrode cylinder, an adsorbent material, an electrode diversion column, a condensation coil, an oil collecting cover, an air guide cover, an insulating orifice plate, a tank, etc. Components that use electrostatic fields and adsorption materials to separate oil, gas and water to achieve high-purity separation of oil.

Benefits of technology

The high -purity oil and non -condensed gas are directly separated from the thermal cracking mixture, which improves the economic value of oil.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention relates to an electrostatic three-phase separator for mixed gas, which is mainly used for three-phase separation of oil, gas and water mixed gas generated by thermal cracking of organic materials, and particularly can realize high-purity separation of oil. The device is composed of a water collecting disc, an insulating ring, an electrode cylinder, an adsorption material, an electrode flow guide column, a condensing coil, an oil collecting cover, a gas guide cover, an insulating pore plate and a tank body. Mixed gas generated by thermal cracking enters the tank body from the gas inlet and enters the electrode cylinder from the variable-diameter opening of the electrode cylinder, and gas flow is reduced in flow velocity due to diameter diffusion, passes through an electrostatic field constructed by the electrode flow guide column and the electrode cylinder when moving upwards in the electrode cylinder, and is separated from the electrode cylinder. Water molecules, carbon black and other polar molecule impurities in the mixed gas transversely move under the action of an electrostatic field and are adsorbed on the surfaces of the electrode cylinder, the adsorption material and the electrode flow guide column, and oil molecules are non-polar molecules, are not attracted by the electrostatic field, are accelerated to impact on the oil collecting cover through a shrinkage cavity of the gas guide cover, and are condensed and collected, so that high-purity oil is separated out.
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Description

Technical Field

[0001] The invention relates to a mixed gas electrostatic three-phase separator, which is mainly used for three-phase separation of oil, gas and water mixed gas produced by thermal cracking of organic materials, and can especially realize high-purity separation of oil. Background Art

[0002] The three-phase separator of mixed gas currently used in the thermal cracking of organic materials is found in the process of use that the separated oil is not of high purity and contains a certain amount of impurities such as water and carbon black, which seriously affects the direct use value of the oil. The invention relates to a mixed gas electrostatic three-phase separator which can directly separate pure oil from the mixed gas of the thermal cracking of organic materials and improve its economic value. Summary of the invention

[0003] In order to achieve three-phase separation of oil, gas and water mixed gas produced by thermal cracking of organic materials, especially to achieve high-purity separation of oil, the present invention provides a three-phase electrostatic separator for mixed gas.

[0004] The solution adopted by the present invention to solve the technical problem is: it is composed of a water collecting tray 1, an insulating ring 2, an electrode cylinder 3, an adsorption material 4, an electrode flow guide column 5, a condensing coil 6, an oil collecting cover 7, an air guide cover 8, an insulating orifice plate 9, and a tank body 10. The electrode cylinder 3 is fixed in the tank body 10 through the insulating orifice plate 9 and the insulating ring 2 to maintain insulation from the tank body 10. The insulating orifice plate 9 has a plurality of through holes. The electrode flow guide column 5 is fixed in the middle of the electrode cylinder 3 through the insulating orifice plate 9. Multiple layers of adsorption materials 4 are fixed between the electrode cylinder 3 and the electrode flow guide column 5, and they are kept in a non-contact state with the electrode cylinder 3 and the electrode flow guide column 5. The multiple layers of adsorption materials 4 are also kept in a non-contact state, and the interlayer space is connected to the through hole of the insulating orifice plate 9. The air guide cover 8 is installed in the tank body 10 and is located above the insulating orifice plate 9 and below the oil outlet C. The oil collecting hood 7 is fixed on the air guide hood 8 through multiple columns, the condensing coil 6 is coiled on the oil collecting hood 7, and the exhaust port D is located at the uppermost end of the tank body 10. The water collecting tray 1 is fixed below the air inlet A in the tank body 10, and the drain port B is located at the lowermost end of the tank body 10. The electrode cylinder 3 and the electrode guide column 5 are respectively connected to the two stages of the electrostatic generator through wires, and the wires are insulated from the tank body 10 and the air guide hood 8. The condensing coil 6 can be connected to the circulating water through the water inlet M and the water outlet N, and can also be connected to the radiator to cool the oil collecting hood 7. The mixed gas produced by thermal cracking enters the tank body 10 from the air inlet A. At this time, the valves on the oil drain port C, the drain port B, and the slag discharge port P are all closed, and the mixed gas can only be discharged from the exhaust port D. The mixed gas first enters the electrode tube 3 from the reducing port of the electrode tube 3. At this time, the airflow velocity is reduced due to the diffusion of the port. When it moves upward inside the electrode tube 3, the water molecules and polar molecular impurities such as carbon black in the mixed gas are moved laterally by the electrostatic field constructed by the electrode guide column 5 and the electrode tube 3, and are adsorbed on the surface of the electrode tube 3, the adsorption material 4, and the electrode guide column 5. Since the oil molecules are non-polar molecules, they are not attracted by the electrostatic field and are directly discharged from the holes of the insulating orifice plate 9. When the water molecules adsorbed on the surface of the electrode tube 3, the adsorption material 4, and the electrode guide column 5 are gathered sufficiently, they will drip onto the water collecting tray 1 under the action of gravity, carrying with them polar molecular impurities such as carbon black, and gather at the bottom of the tank body 10. When the liquid level accumulates to the entrance of the drain port B, the valve on it can be opened. At this time, due to the water seal effect, the mixed gas will not be discharged from the drain port B. After the water level gradually rises to the height of the drain port B, the water will automatically be discharged from the drain port B and the water level will remain unchanged. The oil and gas with impurities such as water molecules and carbon black adsorbed are discharged from the multiple through holes of the insulating orifice plate 9 and accelerated to hit the oil collecting hood 7 through the shrinkage holes of the air guide hood 8. The oil vapor condenses into oil droplets and drips outside the air guide hood 8. The condensing coil 6 cools the oil collecting hood 7 by connecting to the circulating water or radiator, further improving the condensation effect of the oil vapor. The remaining non-condensable gas bypasses the oil collecting hood 7 and is discharged through the exhaust port D.When the oil level on the air guide cover 8 is below the entrance of the oil discharge port C, the valve on it is opened, and the non-condensable gas will not be discharged from the oil discharge port C. When the oil level is higher than the oil discharge port C, the oil is automatically discharged from the oil discharge port C. The gate on the slag discharge port P is opened from time to time to discharge the slag slurry accumulated in the tank body 10.

[0005] The beneficial effect of the present invention is that the present invention can directly separate high-purity oil and non-condensable gas from the thermal cracking mixed gas. BRIEF DESCRIPTION OF THE DRAWINGS

[0006] The present invention is further described below in conjunction with the accompanying drawings and embodiments.

[0007] Figure 1 It is a cross-sectional view of the overall structure of the present invention.

[0008] In the figure, 1. water collecting tray, 2. insulating ring, 3. electrode tube, 4. adsorption material, 5. electrode guide column, 6. condensing coil, 7. oil collecting cover, 8. air guide cover, 9. insulating orifice plate, and 10. tank body. DETAILED DESCRIPTION

[0009] exist Figure 1In the embodiment, the invention comprises a water collecting plate 1, an insulating ring 2, an electrode cylinder 3, an adsorbent material 4, an electrode flow guide column 5, a condensing coil 6, an oil collecting hood 7, an air guide hood 8, an insulating orifice plate 9, and a tank body 10. The electrode cylinder 3 is fixed in the tank body 10 through the insulating orifice plate 9 and the insulating ring 2 to maintain insulation from the tank body 10. The insulating orifice plate 9 has a plurality of through holes. The electrode flow guide column 5 is fixed in the middle of the electrode cylinder 3 through the insulating orifice plate 9. A plurality of adsorbent materials 4 are fixed between the electrode cylinder 3 and the electrode flow guide column 5 to maintain a non-contact state with the electrode cylinder 3 and the electrode flow guide column 5. The plurality of adsorbent materials 4 also maintain a non-contact state and the interlayer space is connected to the through holes of the insulating orifice plate 9. The air guide hood 8 is installed in the tank body 10 and is located above the insulating orifice plate 9 and below the oil outlet C. The oil collecting hood 7 is fixed on the air guide hood 8 through a plurality of columns. The condensing coil 6 is wound on the oil collecting hood 7. The exhaust port D is located at the uppermost end of the tank body 10. The water collecting pan 1 is fixed below the air inlet A in the tank body 10, and the drain port B is located at the bottom of the tank body 10. The electrode cylinder 3 and the electrode guide column 5 are respectively connected to the two stages of the electrostatic generator through wires, and the wires are insulated from the tank body 10 and the air guide cover 8. The condensing coil 6 can be connected to the circulating water through the water inlet M and the water outlet N, and can also be connected to the radiator to cool the oil collecting cover 7. The mixed gas generated by thermal cracking enters the tank body from the air inlet A. At this time, the valves on the oil outlet C, the drain port B, and the slag outlet P are all closed, and the mixed gas can only be discharged from the exhaust port D. The mixed gas first enters the electrode tube 3 from the reducing port of the electrode tube 3. At this time, the airflow velocity is reduced due to the diffusion of the port. When it moves upward inside the electrode tube 3, the water molecules and polar molecular impurities such as carbon black in the mixed gas are moved laterally by the electrostatic field constructed by the electrode guide column 5 and the electrode tube 3, and are adsorbed on the surface of the electrode tube 3, the adsorption material 4, and the electrode guide column 5. Since the oil is a non-polar molecule, it is not attracted by the electrostatic field and is directly discharged from the holes of the insulating orifice plate 9. When the water molecules adsorbed on the surface of the electrode tube 3, the adsorption material 4, and the electrode guide column 5 are gathered sufficiently, they will drip onto the water collection tray 1 under the action of gravity, carrying polar molecular impurities such as carbon black, and gather at the bottom of the tank body 10. When the liquid level accumulates to the entrance of the drain port B, the valve on it can be opened. At this time, due to the water seal effect, the mixed gas will not be discharged from the drain port B. After the water level gradually rises to the height of the drain port B, the water will automatically be discharged from the drain port B and the water level will remain unchanged. The oil and gas with impurities such as water molecules and carbon black adsorbed are discharged from the multiple through holes of the insulating orifice plate 9 and accelerated to hit the oil collecting hood 7 through the shrinkage holes of the air guide hood 8. The oil vapor condenses into oil droplets and gathers and drips outside the air guide hood 8. The condensing coil 6 cools the oil collecting hood 7 by connecting to the circulating water or radiator, further improving the condensation effect of the oil vapor. The remaining non-condensable gas bypasses the oil collecting hood 7 and is discharged through the exhaust port D. When the oil level on the air guide hood 8 is above the entrance of the oil drain port C, the valve on it is opened. At this time, the non-condensable gas will not be discharged from the oil drain port C. When the oil level is higher than the oil drain port C, the oil will automatically be discharged from the oil drain port C.The gate on the slag discharge port P is opened from time to time to discharge the slag slurry accumulated in the tank body 10.

Claims

1. A mixed gas electrostatic three-phase separator, characterized by: The invention comprises a water collecting pan (1), an insulating ring (2), an electrode cylinder (3), an adsorbent material (4), an electrode guide column (5), a condensing coil (6), an oil collecting cover (7), an air guide cover (8), an insulating orifice plate (9), and a tank body (10); the electrode cylinder (3) and the electrode guide column (5) are installed in the tank body (10), the two are insulated, and the two poles of the electrostatic generator are connected respectively; an oil air guide cover (8) is installed above the electrode cylinder (3), an oil collecting cover (7) is installed above the air guide cover (8), and a water collecting pan (1) is installed below the electrode cylinder (3).

2. The mixed gas electrostatic three-phase separator according to claim 1, characterized in that: The bottom of the electrode cylinder (3) has a smaller diameter, so that the mixed gas diffuses and the flow rate slows down after passing through.

3. The mixed gas electrostatic three-phase separator according to claim 1, characterized in that: The diameter of the bottom of the electrode guide column (5) gradually decreases to form an inverted cone, so that the collected water is easier to drip.

4. The mixed gas electrostatic three-phase separator according to claim 1, characterized in that: The air guide cover (8) is in the shape of a cone, and has a through hole on the top, so that the oil and gas passing through are accelerated to collide with the oil collecting cover (7) above, making it easier to condense and collect oil droplets.