Intelligent temperature control anhydrous hydrogen fluoride reaction kettle

Abstract

The invention discloses an intelligent temperature control anhydrous hydrogen fluoride reaction kettle, and relates to the technical field of reaction kettles. The reaction kettle comprises a reaction kettle body, the top end of the reaction kettle body is communicated with feeding guide pipes which are matched for use, and the feeding guide pipes are symmetrically distributed; through the arrangement and use of the supporting mechanism, the first motor can be driven after the reaction kettle body is installed and fixed, so that the first motor rotates forwards or backwards correspondingly, and a driving side gear can be driven to rotate forwards or backwards correspondingly; furthermore, three adjusting screw rods can be driven to synchronously and correspondingly rotate forwards or backwards through a driven bevel gear, a driven rotating rod, a first bevel gear and a second bevel gear, and three supporting inclined frames can be further driven to synchronously move upwards or downwards, so that the reaction kettle body can be driven to move upwards or downwards through three fixed side lugs; the use height of the reaction kettle body can be adjusted in real time according to use requirements, so that the practicability of the equipment is effectively improved.

Description

Technical Field

[0001] The invention relates to the technical field of reactors, in particular to an intelligent temperature-controlled anhydrous hydrogen fluoride reactor. Background Art

[0002] Reactors are widely used in the fields of petroleum, chemical industry, rubber, pesticide, dye, medicine and food. Anhydrous hydrofluoric acid, also known as anhydrous hydrogen fluoride, is a widely used chemical product. Its processing requires the use of an intelligent temperature-controlled anhydrous hydrogen fluoride reactor.

[0003] However, the existing intelligent temperature-controlled anhydrous hydrogen fluoride reactor cannot adjust the use height in real time according to the use requirements after being installed and fixed, and its practicality is poor. In addition, the existing intelligent temperature-controlled anhydrous hydrogen fluoride reactor cannot quickly and fully mix the anhydrous hydrogen fluoride processing raw materials, and the mixing efficiency and mixing adequacy of the materials are poor. In addition, the existing intelligent temperature-controlled anhydrous hydrogen fluoride reactor cannot perform multi-point sampling on the materials being mixed, which is not convenient for users to monitor and grasp the real-time situation of the materials being mixed.

[0004] In view of the above problems, the inventors proposed an intelligent temperature-controlled anhydrous hydrogen fluoride reactor to solve the above problems. Summary of the invention

[0005] In order to solve the problems that the existing intelligent temperature-controlled anhydrous hydrogen fluoride reactor cannot adjust the use height in real time according to the use requirements after being installed and fixed, cannot quickly and fully mix the anhydrous hydrogen fluoride processing raw materials, and cannot perform multi-point sampling on the mixed materials; the purpose of the present invention is to provide an intelligent temperature-controlled anhydrous hydrogen fluoride reactor.

[0006] In order to solve the above technical problems, the present invention adopts the following technical scheme: an intelligent temperature-controlled anhydrous hydrogen fluoride reactor, comprising a reactor body, the top of the reactor body is connected to a feed conduit for use, and the feed conduits are symmetrically distributed, the middle of the bottom end of the reactor body is connected to a discharge conduit for use, and a control valve is fixedly installed on the discharge conduit, the bottom end of the reactor body is provided with a supporting mechanism for use, and the top of the reactor body is provided with a mixing mechanism for use, and the inner cavity of the reactor body is provided with a sampling mechanism for use with the mixing mechanism, the setting and use of the supporting mechanism can adjust its use height in real time according to the use requirements after the reactor body is installed and fixed, the setting and use of the mixing mechanism can quickly and fully mix the anhydrous hydrogen fluoride processing raw materials, and the setting and use of the sampling mechanism can sample the materials in the mixture at multiple points.

[0007] Preferably, the supporting mechanism includes a supporting base and fixed side ears, the supporting base is a Y-shaped structure, and a first motor is fixedly installed in the middle of the top end of the supporting base, the output end of the first motor rotates through the supporting base and a driving side gear is fixedly sleeved at its end, the lower end of the supporting base is rotatably plugged with an array-distributed driven rotating rod, and the end of the driven rotating rod close to the first motor is fixedly sleeved with a driven bevel gear, the driven bevel gear is meshed with the driving side gear, and the end of the driven rotating rod away from the driven bevel gear is fixedly sleeved with the first bevel gear, and the end of the supporting base away from the first motor is rotatably plugged with three adjusting screws The bottom end of the adjusting screw rod is fixedly sleeved with a second bevel gear, the second bevel gear is meshed with the first bevel gear, the fixed side ear is fixedly installed on the outer lower end of the reactor body, and the fixed side ears are distributed in an array, the bottom end of the fixed side ear is fixedly installed with a supporting inclined frame, the supporting inclined frame is slidably connected to the supporting base frame, and the supporting inclined frame is threadedly sleeved on the adjusting screw rod, the end of the supporting base frame is fixedly inserted with a symmetrically arranged guide vertical rod, and the bottom end of the supporting inclined frame is slidably sleeved on the adjacent guide vertical rod, the top end of the supporting base frame is penetrated by symmetrically distributed mounting through holes, and the guide vertical rods are fixedly inserted in the mounting through holes.

[0008] Preferably, the mixing mechanism comprises a mounting top frame, which is fixedly mounted on the top of the reactor body, and a second motor is fixedly mounted on one side of the top of the mounting top frame, a mixing rotating rod is fixedly connected to the end of the output end of the second motor, and the mixing rotating rod is rotatably inserted on the mounting top frame, a driven rotating plate is fixedly sleeved on one end of the mixing rotating rod close to the second motor, and a third motor is fixedly mounted on one side of the top of the driven rotating plate, the output end of the third motor rotates through the driven rotating plate and a driving gear is fixedly sleeved on its end, an adjusting screw barrel is rotatably inserted at the middle part of the top of the reactor body, and the adjusting screw barrel is rotatably sleeved on the mixing rotating rod, and the top of the adjusting screw barrel is fixedly sleeved on the The fixed sleeve is provided with a driven gear, and the driven gear is meshed with the driving gear. The lower end of the adjusting screw barrel is threadedly sleeved with a lifting bracket, and both ends of the lifting bracket are rotatably plugged with a first rotating shaft, both ends of the first rotating shaft are rotatably sleeved with a first T-shaped mixing plate, and the end of the adjacent first T-shaped mixing plate away from the lifting bracket is rotatably plugged with a second rotating shaft, the middle part of the second rotating shaft is rotatably sleeved with a second T-shaped mixing plate, the bottom end of the mixing rotating rod is fixedly sleeved with an H-shaped rotating frame, and both ends of the H-shaped rotating frame are rotatably plugged with a third rotating shaft, the bottom end of the second T-shaped mixing plate is rotatably sleeved on the third rotating shaft, and the end of the second T-shaped mixing plate is rotatably clamped in the H-shaped rotating frame.

[0009] Preferably, the sampling mechanism includes a sampling pump body and a mounting side ear, the sampling pump body is fixedly mounted on one side of the top of the mounting top frame, and the bottom end of the sampling pump body is provided with an L-shaped material delivery pipe and a Z-shaped material guide pipe for use in conjunction with each other, the Z-shaped material guide pipe is fixedly inserted on the mounting top frame and the reactor body, and the end of the Z-shaped material guide pipe is connected to a material collection sleeve, a first plug hole is opened through the top of the reactor body, a second plug hole is opened through the mounting top frame, and the Z-shaped material guide pipe is fixedly inserted in the first plug hole and the second plug hole, and the material collection sleeve is fixedly installed on the reactor body The top of the inner cavity, and the material collecting sleeve is movably sleeved on the outside of the adjusting screw barrel, the inner diameter of the material collecting sleeve is larger than the outer diameter of the adjusting screw barrel, the bottom of the inner cavity of the material collecting sleeve is rotatably installed with an internal turntable, and the internal turntable is connected to a symmetrically distributed material conveying conduit, the bottom of the material conveying conduit is connected to a sleeved outer tube, and a symmetrically arranged mixing rotating plate is fixedly installed on the outer wall of the sleeved outer tube, the mounting side ears are fixedly installed on the lifting bracket, and the mounting side ears are symmetrically structured, an L-shaped sampling tube is fixedly inserted in the mounting side ears, and the L-shaped sampling tube is slidably inserted in the sleeved outer tube.

[0010] Compared with the prior art, the present invention has the following beneficial effects:

[0011] 1. Through the setting and use of the supporting mechanism, after the reactor body is installed and fixed, the first motor can be driven to rotate forward or reverse accordingly, thereby driving the driving side gear to rotate forward or reverse accordingly, and then driving the three adjusting screws to rotate forward or reverse synchronously through the driven bevel gear, the driven rotating rod, the first bevel gear and the second bevel gear, and further driving the three supporting inclined frames to move up or down synchronously, thereby driving the reactor body to move up or down through the three fixed side ears, and then the use height of the reactor body can be adjusted in real time according to the use requirements, thereby effectively improving the practicality of the equipment;

[0012] 2. Through the setting and use of the mixing mechanism, the driving gear can be driven to rotate while driving the first T-shaped mixing plate and the second T-shaped mixing plate to revolve, thereby driving the driven gear to rotate, and then driving the adjusting screw to rotate, thereby driving the lifting bracket to move up or down, and then the adjacent first T-shaped mixing plate and the second T-shaped mixing plate can be driven to rotate relative to each other by coordinating with the use of the first rotating shaft, the second rotating shaft and the third rotating shaft, and further the angle between the adjacent first T-shaped mixing plate and the second T-shaped mixing plate can be adjusted, so that the relative position and relative combination shape of the first T-shaped mixing plate and the second T-shaped mixing plate can be changed at any time, so that the anhydrous hydrogen fluoride processing raw materials can be quickly and fully mixed, thereby improving the material mixing efficiency and mixing adequacy;

[0013] 3. Through the setting and use of the sampling mechanism, the lifting bracket can drive the installation side ears to rotate and lift synchronously, thereby driving the two L-shaped sampling tubes to rotate and lift synchronously, and then the L-shaped sampling tube can slide along the inner wall of the corresponding sleeve outer tube and drive the corresponding sleeve outer tube to rotate, and further drive the mixing turntable, the feed pipe and the inner turntable to rotate synchronously, so that the anhydrous hydrogen fluoride processing raw materials can be further mixed and stirred. In addition, the mixed materials at different depths and different positions can be drawn into the sleeve outer tube through the L-shaped sampling tube, and then the mixed materials will be introduced into the collection sleeve through the feed pipe for concentration and introduced into the L-shaped feed pipe by the Z-shaped feed pipe, and then the mixed materials will be exported by the L-shaped feed pipe, thereby realizing multi-point sampling of the mixed materials, and thus providing convenience for monitoring and mastering the real-time situation of the mixed materials. BRIEF DESCRIPTION OF THE DRAWINGS

[0014] In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative work.

[0015] Figure 1 It is a schematic diagram of the structure of the present invention.

[0016] Figure 2 It is a schematic diagram of the installation of the sampling mechanism in the present invention.

[0017] Figure 3 For the present invention Figure 2 A schematic diagram of the enlarged structure in the middle.

[0018] Figure 4 For the present invention Figure 2 Enlarged schematic diagram of the structure at point B in the middle.

[0019] Figure 5 For the present invention Figure 2 Enlarged schematic diagram of the structure at point C in the middle.

[0020] Figure 6 For the present invention Figure 2 Enlarged schematic diagram of the structure at point D in the middle.

[0021] Figure 7 For the present invention Figure 2 Enlarged schematic diagram of the structure at point E in the middle.

[0022] Figure 8 For the present invention Figure 2 Enlarged schematic diagram of the structure at F in the middle.

[0023] Fig. 9 For the present invention Figure 2 Enlarged schematic diagram of the structure at G in the middle.

[0024] In the figure: 1, reactor body; 11, first jack; 12, feed conduit; 13, discharge conduit; 14, control valve; 2, support mechanism; 21, support base; 22, fixed side ear; 23, first motor; 24, drive side gear; 25, driven rotating rod; 26, driven bevel gear; 27, first bevel gear; 28, adjustment screw; 29, second bevel gear; 210, support oblique frame; 211, guide vertical rod; 212, installation through hole; 3, mixing mechanism; 31, installation top frame; 32, second motor; 33, mixing rotating rod; 34, driven rotating plate; 35, first Three motors; 36, driving gear; 37, adjusting screw; 38, driven gear; 39, lifting bracket; 310, first rotating shaft; 311, first T-type mixing plate; 312, second rotating shaft; 313, second T-type mixing plate; 314, H-type rotating frame; 315, third rotating shaft; 316, second jack; 4, sampling mechanism; 41, sampling pump body; 42, mounting side ears; 43, L-type feed pipe; 44, Z-type guide pipe; 45, collecting sleeve; 46, internal turntable; 47, feed conduit; 48, sleeve outer pipe; 49, mixing rotating plate; 410, L-type sampling tube. DETAILED DESCRIPTION

[0025] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0026] Example: Figure 1-Figure 9As shown, the present invention provides an intelligent temperature-controlled anhydrous hydrogen fluoride reactor, including a reactor body 1, the reactor body 1 has an intelligent temperature control function, which is a prior art and will not be described in detail here. The top of the reactor body 1 is connected to a feed conduit 12 for use, and the feed conduits 12 are symmetrically distributed, and the middle of the bottom end of the reactor body 1 is connected to a discharge conduit 13 for use, and a control valve 14 is fixedly installed on the discharge conduit 13. The feed conduit 12, the discharge conduit 13 and the control valve 14 are used in conjunction with each other to guide the raw materials in the reactor body 1. The reactor body 1 is provided with a supporting mechanism 2 for use in combination with the reactor body 1, and a mixing mechanism 3 for use in combination with the reactor body 1 is provided at the top of the reactor body 1. A sampling mechanism 4 for use in combination with the mixing mechanism 3 is provided in the inner cavity of the reactor body 1. The supporting mechanism 2 can adjust its use height in real time according to use requirements after the reactor body 1 is installed and fixed. The mixing mechanism 3 can quickly and fully mix the anhydrous hydrogen fluoride processing raw materials. The sampling mechanism 4 can sample the mixed materials at multiple points.

[0027] The support mechanism 2 includes a support base 21 and a fixed side ear 22. The support base 21 is a Y-shaped structure. A fixed through hole is provided on the support base 21, so as to facilitate the fixing of the support base 21. This is a prior art and will not be described in detail here. A first motor 23 is fixedly installed in the middle of the top end of the support base 21. The output end of the first motor 23 rotates through the support base 21 and a driving side gear 24 is fixedly sleeved at its end. An array-distributed driven rotating rod 25 is rotatably inserted at the lower end of the support base 21, and a driven bevel gear 26 is fixedly sleeved at one end of the driven rotating rod 25 close to the first motor 23. The driven bevel gear 26 is meshed with the driving side gear 24, and a first bevel gear 27 is fixedly sleeved at one end of the driven rotating rod 25 away from the driven bevel gear 26. Three adjusting screws 28 are rotatably inserted at the end of the support base 21 away from the first motor 23, and the adjusting screws 28 are rotatably inserted at the end of the support base 21. The bottom end of the screw rod 28 is fixedly sleeved with a second bevel gear 29, and the second bevel gear 29 is meshed with the first bevel gear 27. The fixed side ear 22 is fixedly installed on the outer lower end of the reactor body 1, and the fixed side ear 22 is distributed in an array. The bottom end of the fixed side ear 22 is fixedly installed with a supporting inclined frame 210, and the supporting inclined frame 210 is slidably connected to the supporting base frame 21, and the supporting inclined frame 210 is threadedly sleeved on the adjusting screw rod 28. The end of the supporting base frame 21 is fixedly inserted with a symmetrically arranged guide vertical rod 211, and the bottom end of the supporting inclined frame 210 is slidably sleeved on the adjacent guide vertical rod 211. The top end of the supporting base frame 21 is penetrated by symmetrically distributed mounting through holes 212, and the guide vertical rod 211 is fixedly inserted in the mounting through holes 212. The coordinated use of the mounting through holes 212 and the guide vertical rod 211 plays a limiting and guiding role in the movement and adjustment of the supporting inclined frame 210.

[0028] By adopting the above technical solution, when in use, the supporting base frame 21 is fixed, and then the first motor 23 is started, so that the driving side gear 24 can be driven to rotate, and then the three driven bevel gears 26 can be driven to rotate synchronously, and further the three driven rotating rods 25 can be driven to rotate synchronously, so that the three first bevel gears 27 can be driven to rotate synchronously, and then the three adjusting screw rods 28 can be driven to rotate synchronously through the second bevel gear 29, and further the three supporting inclined frames 210 can be driven to move upward synchronously, so that the reactor body 1 can be driven to move upward through the three fixed side ears 22, and the first motor 23 is turned off when the reactor body 1 moves to a suitable height, and then the reactor body 1 can be used to process anhydrous hydrogen fluoride, and during subsequent use, the first motor 23 can be started again according to the use requirements and made to rotate forward or reverse accordingly, so that the reactor body 1 can be driven to move up or down, and then the use height of the reactor body 1 can be adjusted in real time according to the use requirements.

[0029] The mixing mechanism 3 includes a mounting top frame 31, which is fixedly mounted on the top of the reactor body 1, and a second motor 32 is fixedly mounted on one side of the top of the mounting top frame 31, a mixing rotating rod 33 is fixedly connected to the end of the output end of the second motor 32, and the mixing rotating rod 33 is rotatably inserted on the mounting top frame 31, and a driven rotating plate 34 is fixedly sleeved on one end of the mixing rotating rod 33 close to the second motor 32, and a third motor 35 is fixedly mounted on one side of the top of the driven rotating plate 34, the output end of the third motor 35 rotates through the driven rotating plate 34 and a driving gear 36 is fixedly sleeved on its end, an adjusting screw barrel 37 is rotatably inserted in the middle of the top of the reactor body 1, and the adjusting screw barrel 37 is rotatably sleeved on the mixing rotating rod 33, a driven gear 38 is fixedly sleeved on the top of the adjusting screw barrel 37, and the driven gear 38 is meshed with the driving gear 36, and the lower end screw of the adjusting screw barrel 37 is fixedly sleeved. The sleeve is provided with a lifting bracket 39, and the two ends of the lifting bracket 39 are rotatably plugged with a first rotating shaft 310, and the two ends of the first rotating shaft 310 are rotatably sleeved with a first T-shaped mixing plate 311, and the end of the adjacent first T-shaped mixing plate 311 away from the lifting bracket 39 is rotatably plugged with a second rotating shaft 312, and the middle part of the second rotating shaft 312 is rotatably sleeved with a second T-shaped mixing plate 313, and the bottom end of the mixing rotating rod 33 is fixedly sleeved with an H-shaped rotating frame 314, and the two ends of the H-shaped rotating frame 314 are rotatably plugged with a third rotating shaft 315, the bottom end of the second T-shaped mixing plate 313 is rotatably sleeved on the third rotating shaft 315, and the end of the second T-shaped mixing plate 313 is rotatably clamped in the H-shaped rotating frame 314, and the setting and use of the first rotating shaft 310, the second rotating shaft 312 and the third rotating shaft 315 ensure the stable rotation of the first T-shaped mixing plate 311 and the second T-shaped mixing plate 313.

[0030] By adopting the above technical solution, when in use, the second motor 32 will drive the mixing rod 33 to revolve, thereby driving the driven rotating plate 34, the adjusting screw barrel 37 and the H-shaped rotating frame 314 to revolve, and then driving the lifting bracket 39 to revolve, and further driving the first T-shaped mixing plate 311 and the second T-shaped mixing plate 313 to revolve, so that the anhydrous hydrogen fluoride processing raw materials can be mixed and stirred. At the same time, the third motor 35 can drive the driving gear 36 to rotate, and then drive the driven gear 38 to rotate, and further drive the adjusting screw barrel 37 to rotate, so as to drive the lifting bracket 39 moves up or down, and then can cooperate with the use of the first rotating shaft 310, the second rotating shaft 312 and the third rotating shaft 315 to drive the adjacent first T-shaped mixing plate 311 and the second T-shaped mixing plate 313 to perform relative rotation adjustment, and further can adjust the angle between the adjacent first T-shaped mixing plate 311 and the second T-shaped mixing plate 313, so that the relative position and relative combination shape of the first T-shaped mixing plate 311 and the second T-shaped mixing plate 313 can be changed at any time, and then the anhydrous hydrogen fluoride processing raw materials can be quickly and fully mixed, thereby improving the material mixing efficiency and mixing adequacy.

[0031] The sampling mechanism 4 includes a sampling pump body 41 and a mounting side ear 42. The sampling pump body 41 is fixedly mounted on one side of the top of the mounting top frame 31, and the bottom end of the sampling pump body 41 is provided with an L-shaped material delivery pipe 43 and a Z-shaped material guide pipe 44 for use together. The Z-shaped material guide pipe 44 is fixedly inserted on the mounting top frame 31 and the reactor body 1, and the end of the Z-shaped material guide pipe 44 is connected with a material collecting sleeve 45. A first plug hole 11 is opened through the top of the reactor body 1, and a second plug hole 316 is opened through the mounting top frame 31, and the Z-shaped material guide pipe 44 is fixedly inserted in the first plug hole 11 and the second plug hole 316. The setting and use of the first plug hole 11 and the second plug hole 316 provide a guarantee for the stable insertion of the Z-shaped material guide pipe 44, and the material collecting sleeve 45 is fixedly installed It is installed on the top of the inner cavity of the reactor body 1, and the collecting sleeve 45 is movably sleeved on the outside of the adjusting screw barrel 37. The inner diameter of the collecting sleeve 45 is larger than the outer diameter of the adjusting screw barrel 37, thereby ensuring the normal rotation of the adjusting screw barrel 37. An internal turntable 46 is rotatably installed at the bottom of the inner cavity of the collecting sleeve 45, and the internal turntable 46 is connected to a symmetrically distributed material delivery conduit 47, and the bottom end of the material delivery conduit 47 is connected to a sleeve outer tube 48, and a symmetrically arranged mixing rotating plate 49 is fixedly installed on the outer wall of the sleeve outer tube 48. The mounting side ear 42 is fixedly installed on the lifting bracket 39, and the mounting side ear 42 is a symmetrical structure. An L-shaped sampling tube 410 is fixedly inserted in the mounting side ear 42, and the L-shaped sampling tube 410 is slidably inserted in the sleeve outer tube 48.

[0032] By adopting the above technical solution, when in use, the lifting bracket 39 can drive the mounting side ear 42 to rotate and lift synchronously, thereby driving the two L-shaped sampling tubes 410 to rotate and lift synchronously, and then the L-shaped sampling tube 410 can slide along the inner wall of the corresponding sleeve outer tube 48 and drive the corresponding sleeve outer tube 48 to rotate, and further drive the mixing turntable 49, the material delivery conduit 47 and the inner turntable 46 to rotate synchronously, so that the anhydrous hydrogen fluoride processing raw materials can be further mixed and stirred. In addition, the user can start the sampling pump body 41, so that the mixed materials at different depths and different positions can be drawn into the sleeve outer tube 48 through the L-shaped sampling tube 410, and then the mixed materials will be introduced into the collection sleeve 45 through the material delivery conduit 47 for concentration and introduced into the L-shaped material delivery pipe 43 by the Z-shaped material guide pipe 44, and then the mixed materials will be exported from the L-shaped material delivery pipe 43, and then the user can detect the exported samples.

[0033] Working principle: when in use, the support base 21 is fixed, and then the first motor 23 is started, so that the driving side gear 24 can be driven to rotate, and then the three driven bevel gears 26 can be driven to rotate synchronously, and further the three driven rotating rods 25 can be driven to rotate synchronously, so that the three first bevel gears 27 can be driven to rotate synchronously, and then the three adjusting screw rods 28 can be driven to rotate synchronously through the second bevel gear 29, and further the three supporting inclined frames 210 can be driven to move upward synchronously, so that the reactor body 1 can be driven to move upward through the three fixed side ears 22, and the first motor 23 is turned off when the reactor body 1 moves to a suitable height, and then the reactor body 1 can be used to process anhydrous hydrogen fluoride, and during subsequent use, the first motor 23 can be started again according to the use requirements and made to rotate forward or reverse accordingly, so that the reactor body 1 can be driven to move up or down, and then the use height of the reactor body 1 can be adjusted in real time according to the use requirements;

[0034] During the processing of anhydrous hydrogen fluoride, the second motor 32 will drive the mixing rod 33 to revolve, thereby driving the driven rotating plate 34, the adjusting screw 37 and the H-shaped rotating frame 314 to revolve, and then driving the lifting bracket 39 to revolve, and further driving the first T-shaped mixing plate 311 and the second T-shaped mixing plate 313 to revolve, so that the anhydrous hydrogen fluoride processing raw materials can be mixed and stirred. At the same time, the third motor 35 can drive the driving gear 36 to rotate, and then drive the driven gear 38 to rotate, and further drive the adjusting screw 37 to rotate, so as to drive the lifting bracket 39. Move up or down, and then cooperate with the use of the first rotating shaft 310, the second rotating shaft 312 and the third rotating shaft 315 to drive the adjacent first T-shaped mixing plate 311 and the second T-shaped mixing plate 313 to perform relative rotation adjustment, and further adjust the angle between the adjacent first T-shaped mixing plate 311 and the second T-shaped mixing plate 313, so that the relative position and relative combination shape of the first T-shaped mixing plate 311 and the second T-shaped mixing plate 313 can be changed at any time, and then the anhydrous hydrogen fluoride processing raw materials can be quickly and fully mixed, thereby improving the material mixing efficiency and mixing adequacy;

[0035] During this period, the lifting bracket 39 can drive the mounting side ear 42 to rotate and lift synchronously, thereby driving the two L-shaped sampling tubes 410 to rotate and lift synchronously, and then the L-shaped sampling tube 410 can slide along the inner wall of the corresponding sleeve outer tube 48 and drive the corresponding sleeve outer tube 48 to rotate, and further drive the mixing turntable 49, the feed conduit 47 and the inner turntable 46 to rotate synchronously, so that the anhydrous hydrogen fluoride processing raw materials can be further mixed and stirred. In addition, the user can start the sampling pump body 41, so that the mixed materials at different depths and different positions can be drawn into the sleeve outer tube 48 through the L-shaped sampling tube 410, and then the mixed materials will be introduced into the collection sleeve 45 through the feed conduit 47 for concentration and introduced into the L-shaped feed pipe 43 by the Z-shaped feed guide pipe 44, and then the mixed materials will be exported from the L-shaped feed pipe 43, and then the user can detect the exported samples.

[0036] Obviously, those skilled in the art can make various changes and modifications to the present invention without departing from the spirit and scope of the present invention. Thus, if these modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include these modifications and variations.

Claims

1. An intelligent temperature-controlled anhydrous hydrogen fluoride reactor, comprising a reactor body (1), characterized in that: The bottom end of the reactor body (1) is provided with a supporting mechanism (2) for use in conjunction with it, and the top end of the reactor body (1) is provided with a mixing mechanism (3) for use in conjunction with it. The inner cavity of the reactor body (1) is provided with a sampling mechanism (4) for use in conjunction with the mixing mechanism (3). The support mechanism (2) is arranged and used so that its use height can be adjusted in real time according to use requirements after the reactor body (1) is installed and fixed. The mixing mechanism (3) is arranged and used so that the anhydrous hydrogen fluoride processing raw materials can be quickly and fully mixed. The sampling mechanism (4) is arranged and used so that multi-point sampling of the materials being mixed can be performed.

2. The intelligent temperature-controlled anhydrous hydrogen fluoride reactor according to claim 1, characterized in that: The support mechanism (2) comprises a support base (21) and a fixed side ear (22); the support base (21) is a Y-shaped structure, and a first motor (23) is fixedly installed at the middle of the top end of the support base (21); the output end of the first motor (23) rotates through the support base (21) and a driving side gear (24) is fixedly sleeved at its end; a driven rotating rod (25) distributed in an array is rotatably inserted at the lower end of the support base (21), and a driven bevel gear (26) is fixedly sleeved at one end of the driven rotating rod (25) close to the first motor (23); the driven bevel gear (26) is meshed with the driving side gear (24), and the driven rotating rod (25) is away from the driven bevel gear (26). ) is fixedly sleeved with a first bevel gear (27) at one end, three adjusting screw rods (28) are rotatably inserted at the end of the supporting base frame (21) away from the first motor (23), and a second bevel gear (29) is fixedly sleeved at the bottom end of the adjusting screw rod (28), and the second bevel gear (29) is meshed with the first bevel gear (27), the fixed side ears (22) are fixedly installed at the outer lower end of the reactor body (1), and the fixed side ears (22) are distributed in an array, and a supporting inclined frame (210) is fixedly installed at the bottom end of the fixed side ears (22), the supporting inclined frame (210) is slidably connected to the supporting base frame (21), and the supporting inclined frame (210) is threadedly sleeved on the adjusting screw rod (28).

3. The intelligent temperature-controlled anhydrous hydrogen fluoride reactor according to claim 2, characterized in that: The end of the supporting bottom frame (21) is fixedly plugged with a symmetrically arranged guide vertical rod (211), and the bottom end of the supporting oblique frame (210) is slidably sleeved on an adjacent guide vertical rod (211).

4. The intelligent temperature-controlled anhydrous hydrogen fluoride reactor according to claim 3, characterized in that: The top end of the supporting base frame (21) is penetrated by symmetrically distributed mounting through holes (212), and the guide vertical rods (211) are fixedly inserted in the mounting through holes (212).

5. The intelligent temperature-controlled anhydrous hydrogen fluoride reactor according to claim 1, characterized in that: The mixing mechanism (3) comprises a mounting top frame (31), the mounting top frame (31) is fixedly mounted on the top of the reactor body (1), and a second motor (32) is fixedly mounted on one side of the top of the mounting top frame (31), a mixing rotating rod (33) is fixedly connected to the end of the output end of the second motor (32), and the mixing rotating rod (33) is rotatably inserted on the mounting top frame (31), a driven rotating plate (34) is fixedly sleeved on one end of the mixing rotating rod (33) close to the second motor (32), and a third motor (35) is fixedly mounted on one side of the top of the driven rotating plate (34), the output end of the third motor (35) rotates through the driven rotating plate (34) and a driving gear (36) is fixedly sleeved on the end thereof, an adjusting screw barrel (37) is rotatably inserted in the middle of the top of the reactor body (1), and the adjusting screw barrel (37) is rotatably sleeved on the mixing rotating rod (33), and the top of the adjusting screw barrel (37) is fixedly sleeved with a driven gear The adjusting screw barrel (37) is provided with a lifting bracket (39) on the lower end thereof, and the lifting bracket (39) is rotatably connected with a first rotating shaft (310) at both ends thereof, and the first rotating shaft (310) is rotatably connected with a first T-shaped mixing plate (311) at both ends thereof, and the end of the adjacent first T-shaped mixing plate (311) away from the lifting bracket (39) is rotatably connected with a second rotating shaft (311). 2), a second T-shaped mixing plate (313) is rotatably sleeved at the middle of the second rotating shaft (312), an H-shaped rotating frame (314) is fixedly sleeved at the bottom end of the mixing rotating rod (33), and a third rotating shaft (315) is rotatably inserted at both ends of the H-shaped rotating frame (314), the bottom end of the second T-shaped mixing plate (313) is rotatably sleeved on the third rotating shaft (315), and the end of the second T-shaped mixing plate (313) is rotatably clamped in the H-shaped rotating frame (314).

6. The intelligent temperature-controlled anhydrous hydrogen fluoride reactor according to claim 5, characterized in that: The sampling mechanism (4) comprises a sampling pump body (41) and a mounting side ear (42); the sampling pump body (41) is fixedly mounted on one side of the top of the mounting top frame (31); and the bottom end of the sampling pump body (41) is provided with an L-shaped material delivery pipe (43) and a Z-shaped material guide pipe (44) for use in conjunction with each other; the Z-shaped material guide pipe (44) is fixedly inserted on the mounting top frame (31) and the reactor body (1); and the end of the Z-shaped material guide pipe (44) is connected to a material collection sleeve (45); the material collection sleeve (45) is fixedly mounted on the top of the inner cavity of the reactor body (1); and the material collection sleeve (45) is movably sleeved on the outside of the adjusting screw barrel (37). On the side, an inner turntable (46) is rotatably mounted at the bottom of the inner cavity of the collecting sleeve (45), and a symmetrically distributed material conveying conduit (47) is connected to the inner turntable (46), and a sleeve outer tube (48) is connected to the bottom end of the material conveying conduit (47), and a symmetrically arranged mixing rotating plate (49) is fixedly mounted on the outer wall of the sleeve outer tube (48), and the mounting side ear (42) is fixedly mounted on the lifting bracket (39), and the mounting side ear (42) is a symmetrical structure, and an L-shaped sampling tube (410) is fixedly inserted in the mounting side ear (42), and the L-shaped sampling tube (410) is slidably inserted in the sleeve outer tube (48).

7. The intelligent temperature-controlled anhydrous hydrogen fluoride reactor according to claim 6, characterized in that: A first insertion hole (11) is formed through the top of the reactor body (1), a second insertion hole (316) is formed through the mounting top frame (31), and a Z-shaped material guide tube (44) is fixedly inserted in the first insertion hole (11) and the second insertion hole (316).

8. The intelligent temperature-controlled anhydrous hydrogen fluoride reactor according to claim 6, characterized in that: The inner diameter of the material collecting sleeve (45) is greater than the outer diameter of the adjusting screw barrel (37).

9. The intelligent temperature-controlled anhydrous hydrogen fluoride reactor according to claim 1, characterized in that: The top end of the reactor body (1) is connected to a feed conduit (12) for use with the reactor body, and the feed conduits (12) are symmetrically distributed.

10. The intelligent temperature-controlled anhydrous hydrogen fluoride reactor according to claim 1, characterized in that: A discharge conduit (13) for use with the reactor body (1) is provided in the middle of the bottom end thereof, and a control valve (14) is fixedly mounted on the discharge conduit (13).

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