A monitoring device for the production process of organosilicon surfactants
By designing a sampling, air extraction, air supply and stirring system inside the tank, the hydrogen content in the production process of silicone surfactants can be monitored in real time, solving the problem of cumbersome operation and large errors in determining hydrogen content in the existing technology, and achieving optimization of the production process and efficiency improvement.
Patent Information
- Application Number
- CN202510013878.7
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2025-01-06
- Publication Date
- 2025-09-19
- Estimated Expiration
- 2045-01-06
AI Technical Summary
The existing methods for determining the hydrogen content in the production process of organosilicon surfactants are cumbersome and have large errors, which affects production efficiency.
A monitoring device is designed, which includes a tank body, a monitoring component, an FTIR detection device and a processing component. The hydrogen content is monitored in real time through the sampling, pumping and gas delivery systems in the tank body. The linear relationship is used to regulate the production process, and the mixing efficiency is improved in combination with the stirring system.
It realizes real-time monitoring of hydrogen content during the production of silicone surfactants, optimizes the production process, improves production efficiency, avoids material adhesion, and improves mixing efficiency.
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Figure CN119643497B_ABST
Abstract
Description
Technical Field
[0001] The present invention relates to the technical field of active agent monitoring, in particular to a monitoring device for the production process of an organosilicon surfactant. Background Art
[0002] With the rise of new organosilicon materials, organosilicon surfactants have become a research hotspot in recent years. Because their structure contains both organic groups and silicon-oxygen bonds (Si-O-Si), organosilicon surfactants not only possess the high surface activity of general hydrocarbon surfactants, but also possess the excellent properties of inorganic silica, such as high and low temperature resistance, weathering resistance, non-toxicity, non-corrosiveness, and physiological inertness. They are suitable for use in textiles, pesticides, daily chemical products, and more.
[0003] During the production of organosilicon surfactants, hydrogen content directly impacts their performance. Effectively controlling and accurately measuring hydrogen content during the production process is of significant theoretical and practical significance for efficient product preparation. Current methods for determining hydrogen content include infrared, chemical, and gas flow methods. Chemical methods are more mature, but they are cumbersome and inefficient. Gas flow methods require simple equipment, but hydrogen's volume fluctuates significantly with temperature, and manual manipulation can significantly influence the test results, leading to significant errors.
[0004] Therefore, in view of this, the existing structure and defects are studied and improved, and a monitoring device for the production process of silicone surfactants is proposed. Summary of the Invention
[0005] The object of the present invention is to provide a monitoring device for the production process of an organosilicon surfactant to solve the problems raised in the above background technology.
[0006] To achieve the above-mentioned objectives, the present invention provides the following technical solutions: a monitoring device for the production process of an organosilicon surfactant, comprising a tank body and a monitoring component, wherein a monitoring component is provided on one side of the tank body, and the monitoring component comprises a sampling tube, a control valve, a sampling pump, an FTIR detection device and a reflux pipe, a sampling tube is connected to one side of the tank body, and a control valve is connected to the middle of the sampling tube, a sampling pump is connected to the other end of the sampling tube, and a FTIR detection device is connected to one side of the sampling pump through a pipeline, and a reflux pipe is provided on the other side of the FTIR detection device.
[0007] Furthermore, the FTIR detection device is an infrared detection device, and the reflux pipe is connected to the interior of the tank.
[0008] Furthermore, a feed hopper is provided on the upper side of the tank body, a discharge port is provided on the lower side of the tank body, and a processing component is provided on the upper part of the tank body.
[0009] Furthermore, the processing component includes an exhaust port, an exhaust pipe, an exhaust pump and a ventilation pipe. An exhaust port is provided on one side of the upper wall of the tank body, and an exhaust pipe is provided in the exhaust port. An exhaust pump is provided on one side of the exhaust pipe, and a ventilation pipe is connected to one side of the exhaust pump.
[0010] Furthermore, the processing component also includes an air box, an air pump and an air pipe. One side of the ventilation pipe is connected to the air box, and one side of the air box is connected to the air pump through a pipeline, and one side of the air pump is connected to the air pipe.
[0011] Furthermore, a separation membrane is provided in the air box, the ventilation pipe is connected to the air supply pipe, and electromagnetic valves are provided at the connection points between the ventilation pipe, the air box and the air supply pipe.
[0012] Furthermore, a driving motor is provided on one side above the tank body, and a driving wheel is connected to one side of the driving motor, and a mixing assembly is provided in the tank body.
[0013] Furthermore, the mixing assembly includes a stirring shaft, a transmission wheel and a ventilation chamber. The stirring shaft is rotatably connected in the tank body, and the top of the stirring shaft is connected to the transmission wheel. A ventilation chamber is provided in the center of the stirring shaft and the transmission wheel, and the ventilation pipe is connected to the ventilation chamber, and the drive wheel is engaged with the transmission wheel.
[0014] Furthermore, the mixing assembly also includes a stirring rod, a center wheel and a planetary wheel. The stirring rod is symmetrically connected to the stirring shaft, and a center wheel is provided on one side of the stirring shaft. Planetary wheels are symmetrically provided around the center wheel. The stirring rod is a hollow tube, and a one-way valve is provided at the end of the stirring rod.
[0015] Furthermore, the mixing assembly also includes a support plate, an annular groove, a swivel, an annular plate and a scraper. A support plate is provided below the center wheel, and an annular groove is provided on the side where the support plate and the tank body are close to each other. A swivel is engaged in the annular groove, and an annular plate is connected between the swivels. Scrapers are symmetrically connected around the annular plate, and the center wheel, planetary gear and annular plate are meshed with each other.
[0016] The present invention provides a monitoring device for the production process of an organosilicon surfactant, which has the following beneficial effects: when in use, the hydrogen content of a sample in the production process can be determined using a linear relationship established in the laboratory, thereby monitoring and observing the progress of the reaction in real time during the production process, and regulating the device based on the detection results, thereby optimizing the production process and improving production efficiency. During the regulation, the integration of hydrogen can be accelerated and the material can be prevented from adhering to the inner wall of the device.
[0017] 1. Before use, the present invention first draws a standard curve (linear relationship) in the laboratory. After the linear relationship is established, the material can be put into the tank from the feed port for stirring and processing. During the production process, the control valve is opened regularly, and the sampling pump can draw the reaction product in the tank through the sampling tube into the FTIR detection device for detection, thereby utilizing the established linear relationship to determine the hydrogen content of the sample in the production process. The reaction product after the detection is completed can leave the FTIR detection device through the reflux pipe and flow back into the tank to continue to participate in production. At the same time, the operation of the processing component is controlled according to the detection result of the FTIR detection device, thereby regulating the production process. In summary, when in use, the linear relationship established in the laboratory can be used to determine the hydrogen content of the sample in the production process, thereby monitoring and observing the progress of the reaction in real time during the production process.
[0018] When the air in the tank is exhausted, the exhaust gas will be sucked out of the tank, and the exhaust gas in the tank will be sucked out of the tank, so that the exhaust gas in the tank can be sucked out of the tank, and the exhaust gas in the tank can be sucked out of the tank, so that the exhaust gas in the tank can be sucked out of the tank, and the exhaust gas in the tank can be sucked out of the tank, so that the exhaust gas in the tank can be sucked out of the tank, and the exhaust gas in the tank can be sucked out of the tank, and the exhaust gas in the tank can be sucked out of the tank, so that the exhaust gas in the tank can be sucked out of the tank, and the exhaust gas in the tank can be sucked out of the tank,
[0019] 3. In the present invention, after the material enters the tank body, the driving motor is started, and the driving wheel can be driven to rotate by the driving wheel, thereby driving the stirring rod to rotate in the tank body through the stirring shaft to mix and stir the material. The one-way valve at the end of the stirring rod can prevent the material from entering the stirring rod, and when the stirring shaft rotates, it can drive the center wheel to rotate synchronously, and drive the ring plate to rotate through the planetary gear. The support plate and the tank body can limit the ring plate through the ring groove and the rotating ring to prevent the ring plate from deflecting during rotation. The support plate can shield the gap between the ring plate, the planetary gear and the center wheel through the ring groove and the rotating ring to prevent the material from splashing into the ring plate, the planetary gear and the center wheel during stirring. The ring plate can drive the scraper to move synchronously in the tank body when it rotates, and the movement direction of the scraper is opposite to that of the stirring rod, thereby improving the mixing efficiency of the material and cleaning the inner wall of the tank body to avoid the material from adhering to the inner wall of the tank body and being difficult to clean. When the air supply pipe supplies air to the tank body, the gas enters the ventilation cavity from the air supply pipe and can enter the tank body through the stirring rod. As the stirring rod moves, it is directly mixed with the material to accelerate the integration and reaction of the gas. In summary, when in use, the mixing efficiency of the material can be improved, the integration and reaction of hydrogen can be accelerated, and the material can be prevented from adhering to the inner wall of the device. BRIEF DESCRIPTION OF THE DRAWINGS
[0020] Figure 1 This is a schematic diagram of the overall three-dimensional structure of a monitoring device for the production process of an organosilicon surfactant according to the present invention;
[0021] Figure 2 This is a schematic diagram of the overall main structure of a monitoring device for the production process of an organosilicon surfactant according to the present invention;
[0022] Figure 3 This is a schematic diagram of a half-cutaway exploded structure of a tank body of a monitoring device for a production process of an organosilicon surfactant according to the present invention;
[0023] Figure 4 This is a schematic diagram of a half-cutaway three-dimensional structure of a monitoring device for a production process of an organosilicon surfactant according to the present invention;
[0024] Figure 5 This is a schematic diagram of the cross-sectional front view of a monitoring device for a production process of an organosilicon surfactant according to the present invention;
[0025] Figure 6 This is a schematic diagram of the half-cutaway exploded structure of a stirring shaft of a monitoring device for the production process of an organosilicon surfactant according to the present invention.
[0026] In the figure: 1. Tank body; 2. Monitoring component; 201. Sampling tube; 202. Control valve; 203. Sampling pump; 204. FTIR detection device; 205. Reflux pipe; 3. Feed hopper; 4. Discharge port; 5. Processing component; 501. Exhaust port; 502. Exhaust pipe; 503. Exhaust pump; 504. Ventilation pipe; 505. Air box; 506. Air pump; 507. Air supply pipe; 6. Driving motor; 7. Driving wheel; 8. Mixing component; 801. Stirring shaft; 802. Transmission wheel; 803. Ventilation chamber; 804. Stirring rod; 805. Center wheel; 806. Planetary gear; 807. Support plate; 808. Ring groove; 809. Rotating ring; 810. Ring plate; 811. Scraper. DETAILED DESCRIPTION
[0027] See also Figures 1 to 6 The present invention provides a technical solution: a monitoring device for the production process of an organosilicon surfactant, comprising a tank body 1 and a monitoring component 2. The monitoring component 2 is provided on one side of the tank body 1, and the monitoring component 2 includes a sampling tube 201, a control valve 202, a sampling pump 203, an FTIR detection device 204 and a reflux pipe 205. The sampling tube 201 is connected to one side of the tank body 1, and the control valve 202 is connected to the middle of the sampling tube 201. The other end of the sampling tube 201 is connected to the sampling pump 203, and one side of the sampling pump 203 is connected to the FTIR detection device 204 through a pipeline, and the other side of the FTIR detection device 204 is provided with a reflux pipe 205.
[0028] See also Figures 1 to 5 The FTIR detection device 204 is an infrared detection device. The reflux pipe 205 is connected to the interior of the tank body 1. A feed hopper 3 is provided on the upper side of the tank body 1, and a discharge port 4 is provided on the lower side of the tank body 1. A processing component 5 is provided on the upper part of the tank body 1. The processing component 5 includes an exhaust port 501, an exhaust pipe 502, an exhaust pump 503 and a vent pipe 504. An exhaust port 501 is provided on one side of the upper wall of the tank body 1, and an exhaust pipe 502 is provided in the exhaust port 501. An exhaust pump 503 is provided on one side of the exhaust pipe 502. One side of the air pump 503 is connected to a vent pipe 504. The processing assembly 5 also includes an air box 505, an air supply pump 506 and an air supply pipe 507. One side of the vent pipe 504 is connected to the air box 505, and one side of the air box 505 is connected to the air supply pump 506 through a pipeline. One side of the air supply pump 506 is connected to the air supply pipe 507. A separation membrane is provided in the air box 505. The vent pipe 504 is in communication with the air supply pipe 507, and electromagnetic valves are provided at the connections between the vent pipe 504, the air box 505 and the air supply pipe 507.
[0029] The specific operation is as follows. Before use, a standard curve linear relationship is first drawn in the laboratory. After the linear relationship is established, the material can be put into the tank body 1 from the feed port for stirring and processing. During the production process, the control valve 202 is opened regularly, and the sampling pump 203 can draw the reaction product in the tank body 1 through the sampling tube 201 into the FTIR detection device 204 for detection, so as to use the established linear relationship to determine the hydrogen content of the sample in the production process. After the detection is completed, the reaction product can leave the FTIR detection device 204 through the reflux pipe 205 and flow back into the tank body 1 to continue to participate in production. At the same time, the operation of the processing component 5 is controlled according to the detection result of the FTIR detection device 204, so as to regulate the production process. In summary, when in use, the linear relationship established in the laboratory can be used to determine the hydrogen content of the sample in the production process, so as to monitor and observe the progress of the reaction in real time during the production process. During the production process, the air pump 503 can pump the air in the tank body 1 through the exhaust pipe 205. The air inlet 501 is drawn from the air extraction pipe 502 into the vent pipe 504 and is sent back to the tank body 1 through the air supply pipe 507. While ensuring the stability of the air pressure in the tank body 1, the gas in the upper part of the tank body 1 can fully participate in the reaction. When it is detected that the hydrogen content is too high, the air extraction pump 503 will send the air in the upper part of the tank body 1 into the air box 505 through the vent pipe 504, and the hydrogen will be separated by the separation membrane in the air box 505 and stored in the upper part of the air box 505. When it is detected that the hydrogen content is too low, the air supply pump 506 can be used to The hydrogen on the upper part of the gas box 505 is extracted and sent into the tank body 1 through the air supply pipe 507, so as to regulate the reaction process of the material, thereby optimizing the production process and improving production efficiency. During the extraction and supply of gas, the solenoid valve provided at the connection between the vent pipe 504 and the gas box 505 and the air supply pipe 507 can adjust the air flow path according to the detection results to ensure the smooth progress of the regulation process. In summary, when in use, the device can be regulated according to the detection results, thereby optimizing the production process and improving production efficiency.
[0030] See also Figures 4 to 6, a driving motor 6 is provided on one side above the tank body 1, and a driving wheel 7 is connected to one side of the driving motor 6. A mixing assembly 8 is provided in the tank body 1, and the mixing assembly 8 includes a stirring shaft 801, a transmission wheel 802 and a ventilation cavity 803. The stirring shaft 801 is rotatably connected in the tank body 1, and the top of the stirring shaft 801 is connected to the transmission wheel 802. A ventilation cavity 803 is provided in the center of the stirring shaft 801 and the transmission wheel 802, and the ventilation pipe 504 is connected to the ventilation cavity 803. The driving wheel 7 is meshed with the transmission wheel 802. The mixing assembly 8 also includes a stirring rod 804, a center wheel 805 and a planetary wheel 806. The stirring shaft 801 is symmetrically connected to the stirring rod 804 around, and the stirring shaft 8 01 is provided with a central wheel 805 on one side, and planetary wheels 806 are symmetrically provided around the central wheel 805. The stirring rod 804 is a hollow tube, and a one-way valve is provided at the end of the stirring rod 804. The mixing assembly 8 also includes a supporting plate 807, an annular groove 808, a rotating ring 809, an annular plate 810 and a scraper 811. A supporting plate 807 is provided below the central wheel 805, and an annular groove 808 is provided on the side where the supporting plate 807 and the tank body 1 are close. A rotating ring 809 is engaged and connected in the annular groove 808, and an annular plate 810 is connected between the rotating rings 809. Scrapers 811 are symmetrically connected around the annular plate 810, and the central wheel 805, the planetary wheels 806 and the annular plate 810 are meshed with each other;
[0031] The specific operation is as follows: after the material enters the tank body 1, the driving motor 6 is started, and the transmission wheel 802 can be driven to rotate through the driving wheel 7, thereby driving the stirring rod 804 to rotate in the tank body 1 through the stirring shaft 801 to mix and stir the material. The one-way valve at the end of the stirring rod 804 can prevent the material from entering the stirring rod 804, and when the stirring shaft 801 rotates, it can drive the center wheel 805 to rotate synchronously, and drive the ring plate 810 to rotate through the planetary gear 806. The support plate 807 and the tank body 1 can limit the ring plate 810 through the ring groove 808 and the rotating ring 809 to prevent the ring plate 810 from deflecting during rotation, and the support plate 807 can shield the gap between the ring plate 810, the planetary gear 806 and the center wheel 805 through the ring groove 808 and the rotating ring 809 to prevent the material from splashing during stirring. Entering between the ring plate 810, the planetary gear 806 and the center wheel 805, affecting the normal transmission, when the ring plate 810 rotates, it can drive the scraper 811 to move synchronously in the tank body 1, and the movement direction of the scraper 811 is opposite to the movement direction of the stirring rod 804, thereby improving the mixing efficiency of the material, and at the same time, the inner wall of the tank body 1 can be cleaned to avoid the material adhering to the inner wall of the tank body 1 and being difficult to clean. When the air supply pipe 507 supplies air to the tank body 1, after the gas enters the ventilation cavity 803 from the air supply pipe 507, it can enter the tank body 1 through the stirring rod 804, and directly mix with the material as the stirring rod 804 moves, accelerating the integration of the gas and the reaction. In summary, when in use, the mixing efficiency of the material can be improved, the integration and reaction of hydrogen can be accelerated, and the material can be prevented from adhering to the inner wall of the device.
[0032] In summary, when using this monitoring device for the production process of an organosilicon surfactant, first, a standard curve linear relationship is plotted in the laboratory. To plot the standard curve, accurately weigh 9.766g of hydrogen-containing silicone oil with a hydrogen content of 1.024% into a 100ml dry beaker, dilute with carbon tetrachloride, quantitatively transfer to a 100ml volumetric flask, dilute to the mark with carbon tetrachloride, and shake well to obtain a 1.000mgH / ml standard solution. Pipette 0.50, 1.00, 1.50, 2.00, 2.50, 3.00, 3.50, 4.00, and 4.50ml of the above standard solution into nine 10ml volumetric flasks, dilute to the mark with carbon tetrachloride, and shake well. The prepared standard solutions are transferred to a fixed sealed liquid pool in sequence with a micro syringe, and carbon tetrachloride blank is used as a reference. Scanning is performed in the range of 2500~2000cm-1, and infrared spectra are recorded. The absorbance is measured and a standard curve is drawn. After the linear relationship is established, the material can be put into the tank body 1 from the feed port for stirring and processing. After the material enters the tank body 1, the drive motor 6 is started, and the drive wheel 7 drives the transmission wheel 802 to rotate, thereby driving the stirring rod 804 to rotate in the tank body 1 through the stirring shaft 801 to mix and stir the material. The one-way valve at the end of the mixing rod 804 can prevent the material from entering the mixing rod 804, and when the mixing shaft 801 rotates, it can drive the center wheel 805 to rotate synchronously, and drive the ring plate 810 to rotate through the planetary gear 806. The support plate 807 and the tank body 1 can limit the ring plate 810 through the ring groove 808 and the rotating ring 809 to prevent the ring plate 810 from deflecting during rotation, and the support plate 807 can shield the gap between the ring plate 810, the planetary gear 806 and the center wheel 805 through the ring groove 808 and the rotating ring 809 to prevent the material from splashing into the ring plate 810 during stirring. 10. Between the planetary gear 806 and the center wheel 805, the normal transmission is affected. When the ring plate 810 rotates, it can drive the scraper 811 to move synchronously in the tank body 1, and the movement direction of the scraper 811 is opposite to the movement direction of the stirring rod 804, thereby improving the mixing efficiency of the materials. At the same time, the inner wall of the tank body 1 can be cleaned to prevent the material from adhering to the inner wall of the tank body 1 and being difficult to clean. During the production process, the control valve 202 is opened regularly, and the sampling pump 203 can pump the reaction product in the tank body 1 into the FTIR detection device 2 through the sampling tube 201. 04 for detection, thereby using the established linear relationship to determine the hydrogen content of the sample during the production process, and the reaction product after the detection can leave the FTIR detection device 204 through the reflux pipe 205 and flow back into the tank body 1 to continue participating in the production. At the same time, the operation of the processing component 5 is controlled according to the detection result of the FTIR detection device 204, thereby regulating the production process. During the production process, the air pump 503 can extract the air in the tank body 1 from the air extraction pipe 502 through the air extraction port 501 to the ventilation pipe 504, and send it back to the tank body 1 through the air supply pipe 507.While ensuring the stability of the air pressure in the tank body 1, the gas in the upper part of the tank body 1 can fully participate in the reaction. When it is detected that the hydrogen content is too high, the air pump 503 will send the air in the upper part of the tank body 1 into the air box 505 through the vent pipe 504, and separate the hydrogen through the separation membrane in the air box 505 and store it in the upper part of the air box 505. When it is detected that the hydrogen content is too low, the air pump 506 can extract the hydrogen in the upper part of the air box 505 and send it into the tank body 1 through the air pipe 507, thereby adjusting the reaction process of the material. Control, thereby optimizing the production process and improving production efficiency. During air extraction and delivery, the solenoid valve installed at the connection between the ventilation pipe 504, the air box 505, and the air supply pipe 507 can adjust the airflow path according to the detection results to ensure the smooth progress of the control process. When the air supply pipe 507 delivers air to the tank body 1, the gas enters the ventilation cavity 803 through the air supply pipe 507, then enters the tank body 1 through the stirring rod 804. As the stirring rod 804 moves, it directly mixes with the material, accelerating the gas integration and reaction.
[0033] The embodiments of the present invention are presented for purposes of illustration and description and are not intended to be exhaustive or to limit the invention to the disclosed forms. Many modifications and variations will be apparent to those skilled in the art. The embodiments are chosen and described in order to better illustrate the principles of the invention and its practical application and to enable those skilled in the art to understand the invention and design various embodiments with various modifications as suited for specific applications.
Claims
1. A monitoring device for the production process of an organosilicon surfactant, characterized in that: The invention comprises a tank body (1) and a monitoring assembly (2), wherein the monitoring assembly (2) is provided on one side of the tank body (1), and the monitoring assembly (2) comprises a sampling tube (201), wherein the sampling tube (201) is connected to one side of the tank body (1), and a control valve (202) is connected to the middle of the sampling tube (201), and the other end of the sampling tube (201) is connected to a sampling pump (203), and one side of the sampling pump (203) is connected to an FTIR detection device (204) through a pipeline, and the other side of the FTIR detection device (204) is provided with a reflux valve. The tank body (1) is provided with a feeding hopper (3) on the upper side, and a discharge port (4) on the lower side, and a processing assembly (5) is provided on the upper part of the tank body (1). The processing assembly (5) includes an air extraction port (501). An air extraction port (501) is provided on one side of the upper wall of the tank body (1), and an air extraction pipe (502) is provided in the air extraction port (501). An air extraction pump (503) is provided on one side of the air extraction pipe (502), and a ventilation pipe (504) is connected to one side of the air extraction pump (503). The processing The component (5) further comprises an air box (505), one side of the ventilation pipe (504) is connected to the air box (505), and one side of the air box (505) is connected to an air pump (506) through a pipeline, and one side of the air pump (506) is connected to an air supply pipe (507), a separation membrane is provided in the air box (505), the ventilation pipe (504) is in communication with the air supply pipe (507), and electromagnetic valves are provided at the connection between the ventilation pipe (504), the air box (505), and the air supply pipe (507), and the control valve (202) is opened regularly to adopt The sample pump (203) draws the reaction product in the tank body (1) through the sampling tube (201) into the FTIR detection device (204) for detection. The hydrogen content of the sample in the production process is determined by using the established linear relationship. After the detection is completed, the reaction product can leave the FTIR detection device (204) through the reflux tube (205) and flow back into the tank body (1) to continue participating in the production. The operation of the processing component (5) is controlled according to the detection result of the FTIR detection device (204) to regulate the production process.
2. The monitoring device for the production process of an organosilicon surfactant according to claim 1, characterized in that: The FTIR detection device (204) is an infrared detection device, and the reflux pipe (205) is connected to the interior of the tank body (1).
3. The monitoring device for the production process of an organosilicon surfactant according to claim 1, characterized in that: A driving motor (6) is provided on one side above the tank body (1), and a driving wheel (7) is connected to one side of the driving motor (6). A mixing assembly (8) is provided inside the tank body (1).
4. The monitoring device for the production process of an organosilicon surfactant according to claim 3, characterized in that: The mixing assembly (8) comprises a stirring shaft (801), a transmission wheel (802) and a ventilation cavity (803); the stirring shaft (801) is rotatably connected in the tank body (1), and the top end of the stirring shaft (801) is connected to the transmission wheel (802); a ventilation cavity (803) is provided in the center of the stirring shaft (801) and the transmission wheel (802), and a ventilation pipe (504) is connected to the ventilation cavity (803); the driving wheel (7) is meshed with the transmission wheel (802).
5. The monitoring device for the production process of an organosilicon surfactant according to claim 4, characterized in that: The mixing assembly (8) further comprises a stirring rod (804), a center wheel (805) and a planetary wheel (806), wherein the stirring shaft (801) is symmetrically connected to the stirring rod (804), and a center wheel (805) is provided on one side of the stirring shaft (801), and planetary wheels (806) are symmetrically provided on the center wheel (805), wherein the stirring rod (804) is a hollow tube, and a one-way valve is provided at the end of the stirring rod (804), and the mixing assembly (8) further comprises a support plate (807), an annular groove (808), a rotating ring ( 809), annular plates (810) and scrapers (811), a supporting plate (807) is provided below the center wheel (805), and annular grooves (808) are provided on the sides of the supporting plate (807) and the tank body (1) where they are close to each other, a rotating ring (809) is engaged and connected in the annular groove (808), and annular plates (810) are connected between the rotating rings (809), and scrapers (811) are symmetrically connected around the annular plates (810), and the center wheel (805), the planetary wheels (806) and the annular plates (810) are meshed with each other.
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