Ultrahigh-temperature rapid heating stage and using method thereof

Abstract

The invention belongs to the technical field of high-temperature heating, and particularly relates to an ultrahigh-temperature rapid heating stage and a using method thereof.The ultrahigh-temperature rapid heating stage comprises a heating stage furnace body, a heating stage top cover, a high-temperature-resistant base, a B-type thermocouple heating stage, a lamplight temperature compensation window, a vacuum and atmosphere control assembly and an outer controller; the use method comprises the following specific steps: S1, fixing the B-type thermocouple heating stage on the high-temperature-resistant base; s2, the sample is placed on a B-type thermocouple heating stage, corresponding gas is supplied based on a vacuum and atmosphere control assembly, and the atmosphere environment in a furnace body of the heating stage is adjusted; and S3, setting the temperature required by the experiment and a temperature rise curve through the external controller, heating the B-type thermocouple heating stage, and raising the temperature to the target temperature. The device is suitable for experiments such as high-temperature material performance testing and microstructure analysis, and an ideal experimental platform is provided for research in the fields of material science, high-temperature physics, micro-nano technology and the like. The innovative heating technology can obviously promote research and development in related fields.

Description

Technical Field

[0001] The present invention relates to the technical field of high temperature heating, in particular to an ultra-high temperature rapid heating stage and a method for using the same. Background Art

[0002] With the rapid development of materials science, energy technology and aerospace, the performance testing and behavior characterization of high-temperature materials have played an increasingly important role in scientific research and industry. Under high temperature conditions, the mechanical properties, thermal stability, phase change behavior and microstructural evolution of materials are directly related to their reliability and durability in practical applications. Therefore, researchers have an increasing demand for experiments in ultra-high temperature environments (>1500℃), especially in-situ observation and real-time performance evaluation of materials under dynamic conditions, which has become one of the core directions of materials research.

[0003] However, existing high-temperature hot stages generally have problems such as low temperature (<1500℃) and slow heating rate. For example, Linkam's TS1500 high-temperature hot stage has a temperature range of room temperature to 1500℃ and a heating rate of up to 200℃ / minute; INSTEC's HP1500G high-temperature hot stage has a temperature range of 30-1500℃ and a heating rate of up to 20℃ / minute when the temperature is greater than 800℃. In addition, the heating element and the temperature measuring element are separated in the traditional device, the system is complex and fragile, and it is difficult to achieve real-time temperature control and efficient heating. There are great limitations for the dynamic characterization of materials in ultra-high temperature environments and special atmosphere experiments.

[0004] Therefore, in order to solve the above-mentioned problems of low heating temperature and slow heating rate, the present invention discloses an ultra-high temperature rapid heating hot stage for high-temperature in-situ analysis of materials and interface behavior research, which can achieve a heating temperature of 1800°C and a heating rate of 900°C / min, and can also perform in-situ contact angle testing. Summary of the invention

[0005] The purpose of the present invention is to provide an ultra-high temperature rapid heating hot stage and a method of using the same, so as to solve the problems of low heating temperature and slow heating speed of current heating experimental equipment mentioned in the above background technology.

[0006] To achieve the above object, the present invention provides the following technical solution: an ultra-high temperature rapid heating hot stage, comprising:

[0007] Hot stage furnace body, hot stage top cover, high temperature resistant base, B-type thermocouple hot stage, light temperature compensation window, vacuum and atmosphere control components and external controller;

[0008] The heating platform furnace body is hollow and has an upper opening, the heating platform top cover is detachably connected to the upper opening of the heating platform furnace body, the high temperature resistant base is arranged on the left side of the interior of the heating platform furnace body, the B-type thermocouple heating platform is connected to the high temperature resistant base, the vacuum and atmosphere control components are arranged in the inner cavity of the heating platform furnace body, the B-type thermocouple heating platform is located in the middle of the heating platform furnace body, a light temperature compensation window corresponding to the position of the B-type thermocouple heating platform is arranged in the middle of the lower surface of the inner cavity of the heating platform furnace body, the external controller is located on the outer side of the heating platform furnace body, and the external controller is electrically connected to the B-type thermocouple heating platform and the light temperature compensation window.

[0009] Preferably, the four corners of the heating platform furnace body and the heating platform top cover are provided with connecting holes, the connecting holes of the heating platform furnace body are provided with internal threads, and the connecting holes of the heating platform top cover are threadedly connected to the connecting holes of the heating platform furnace body through bolts.

[0010] Preferably, a sealing embedding groove is provided at the edge of the upper surface of the heating platform furnace body, and an embedding ring is provided on the lower surface of the heating platform top cover, and the embedding ring corresponds to the sealing embedding groove in position and has a matching size.

[0011] Preferably, two vacuum and atmosphere control components are provided, and the two vacuum and atmosphere control components are respectively located at the opposite side walls of the inner cavity of the hot table furnace body. The vacuum and atmosphere control component is hollow and has an air nozzle at one end and an interface at the other end. The interface of the vacuum and atmosphere control component is connected to an air pipe, and the side wall of the hot table furnace body is hollow and sandwich-shaped, and the connecting air pipe is led out from the hollow sandwich of the side wall of the hot table furnace body.

[0012] Preferably, a side observation window is provided on the right side wall of the heating platform furnace body, and a front observation window is provided in the middle of the heating platform top cover.

[0013] Preferably, a through hole is provided on the left side wall of the heating platform furnace body, and the wiring between the external controller and the B-type thermocouple heating platform and the light temperature compensation window all passes through the through hole.

[0014] Preferably, the high temperature resistant base comprises an upper seat plate and a lower seat plate, and the right sides of the mutually facing side walls of the upper seat plate and the lower seat plate are provided with a wire pressing groove, and the wires of the B-type thermocouple hot stage are pressed and plugged in the wire pressing groove, and the middle parts of the mutually facing side walls of the upper seat plate and the lower seat plate are provided with a receiving groove, and the receiving groove is used to receive the control circuit of the B-type thermocouple hot stage.

[0015] Preferably, a high temperature resistant clamping plate is arranged on the left side of the inner cavity of the hot table furnace body, a groove is opened on the right side of the lower surface of the high temperature resistant clamping plate, the left side of the high temperature resistant base is inserted into the groove, and the high temperature resistant clamping plate is connected to the high temperature resistant base by screws.

[0016] Preferably, the wire of the B-type thermocouple hot stage includes a heating circuit and a temperature measurement circuit. The B-type thermocouple hot stage includes a positive electrode and a negative electrode. The two parts are respectively made of 70% platinum, 30% rhodium and 94% platinum, 6% rhodium alloy. The welding point part is pressed into a thin sheet for placing the sample. The thin sheet can realize heating and temperature measurement at the same time. The heating circuit and the temperature measurement circuit are connected to the thin sheet at the same time.

[0017] The method of using the ultra-high temperature rapid heating hot plate is as follows:

[0018] S1: Fix the B-type thermocouple heating platform to the high temperature resistant base;

[0019] S2: Place the sample on a B-type thermocouple hot stage, and supply corresponding gas based on the vacuum and atmosphere control components to adjust the atmosphere in the hot stage furnace;

[0020] S3: Set the temperature and heating curve required for the experiment through the external controller, heat the B-type thermocouple hot plate, and heat it to the target temperature;

[0021] S4: Observation of the behavior of samples in the hot stage furnace under high temperature environment;

[0022] S5: After the experiment is completed, turn off the power supply and take out the sample after it cools down to a safe range.

[0023] Compared with the prior art, the present invention has the following beneficial effects:

[0024] Heating principle selection: The heating and temperature measuring elements of this hot stage are B-type platinum-rhodium thermocouples (Pt-Rh thermocouples), which have an operating temperature range of 0°C to 1800°C, making the maximum operating temperature of the chip up to 1800°C. The heating method uses the same B-type thermocouple hot stage, which can realize heating and temperature measurement functions at the same time.

[0025] Rapid heating capability: The heating chip design includes efficient heating elements (B-type thermocouple hot stage) to achieve rapid heating (maximum heating rate greater than 900°C / minute), meeting the requirements for temperature change rate under different experimental conditions.

[0026] High-temperature interface behavior analysis capability: The side of the hot stage furnace is equipped with an observation window to facilitate obtaining the contact angle between the sample and the hot stage during the experiment.

[0027] Stability and reliability at high temperatures: The structure and material selection of the furnace are optimized to withstand temperatures up to 1800°C.

[0028] Wide applicability: The ultra-high temperature rapid heating stage of the present invention is suitable for experiments such as high temperature material performance testing and microstructure analysis, and provides an ideal experimental platform for research in the fields of materials science, high temperature physics, micro-nano technology, etc. This innovative heating technology will significantly promote the research and development of related fields. BRIEF DESCRIPTION OF THE DRAWINGS

[0029] Figure 1 It is a schematic diagram of the structure of the present invention;

[0030] Figure 2 It is a schematic diagram of the lower surface structure of the heating platform top cover of the present invention;

[0031] Figure 3 It is a schematic diagram of the internal structure of the hot stage furnace body of the present invention;

[0032] Figure 4 It is a structural schematic diagram of the high temperature resistant pressing plate and the trough body of the present invention;

[0033] Figure 5 It is a structural schematic diagram of the present invention when the upper seat plate and the lower seat plate are separated;

[0034] Figure 6 It is a structural schematic diagram of the vacuum and atmosphere control components, gas nozzles, and connecting gas pipes of the present invention;

[0035] Figure 7 This is a contact angle test diagram of an ultra-high temperature rapid heating hot stage for high-temperature in-situ analysis of materials and research on interface behavior provided by an embodiment of the present invention.

[0036] In the figure: 1. hot plate furnace body; 2. hot plate top cover; 3. front observation window; 4. side observation window; 5. embedding ring; 6. sealing embedding groove; 7. high temperature resistant pressing plate; 8. groove body; 9. upper seat plate; 10. lower seat plate; 11. wire pressing groove; 12. receiving groove; 13. B-type thermocouple hot plate; 14. light temperature compensation window; 15. vacuum and atmosphere control component; 16. air nozzle; 17. connecting air pipe; 18. through hole; 19. external controller. DETAILED DESCRIPTION

[0037] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0038] In the description of the present invention, it is necessary to understand that the terms "upper", "lower", "front", "back", "left", "right", "top", "bottom", "inside", "outside", etc., indicating the orientation or position relationship are based on the orientation or position relationship shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention.

[0039] Embodiment 1:

[0040] See also Figure 1-6 , the present invention provides a technical solution: an ultra-high temperature rapid heating hot stage, comprising: a hot stage furnace body 1, a hot stage top cover 2, a high temperature resistant base, a B-type thermocouple hot stage 13, a light temperature compensation window 14, a vacuum and atmosphere control component 15 and an external controller 19;

[0041] The heating platform furnace body 1 is hollow and has an upper opening, the heating platform top cover 2 is detachably connected to the upper opening of the heating platform furnace body 1, the high temperature resistant base is arranged on the left side of the interior of the heating platform furnace body 1, the B-type thermocouple heating platform 13 is connected to the high temperature resistant base, the vacuum and atmosphere control component 15 is arranged in the inner cavity of the heating platform furnace body 1, the B-type thermocouple heating platform 13 is located in the middle of the heating platform furnace body 1, and a light temperature compensation window 14 corresponding to the position of the B-type thermocouple heating platform 13 is arranged in the middle of the lower surface of the inner cavity of the heating platform furnace body 1, the external controller 19 is located on the outer side of the heating platform furnace body 1, and the external controller 19 is electrically connected to the B-type thermocouple heating platform 13 and the light temperature compensation window 14.

[0042] Analysis of the above content: For specific practical methods, refer to Example 10.

[0043] The welding point of the B-type thermocouple hot stage 13 is pressed into a thin sheet for placing samples, which can achieve heating and temperature measurement; the external controller 19 is connected to the B-type thermocouple hot stage 13, and adjusts the current by real-time monitoring of the temperature signal to achieve precise temperature control. The two ends of the B-type thermocouple hot stage 13 are fixed to a high-temperature resistant base, which contains a heating circuit and a temperature measurement circuit for heating the hot stage and collecting temperature signals.

[0044] Embodiment 2:

[0045] See also Figure 1-6 The present invention provides a technical solution based on the first embodiment: the four corners of the hot plate furnace body 1 and the hot plate top cover 2 are provided with connecting holes, the connecting holes of the hot plate furnace body 1 are provided with internal threads, and the connecting holes of the hot plate top cover 2 are threadedly connected to the connecting holes of the hot plate furnace body 1 through bolts.

[0046] Analysis of the above content: The bolt connection method is adopted to facilitate the connection and disassembly between the heating table furnace body 1 and the heating table top cover 2, and the positions between the heating table furnace body 1 and the heating table top cover 2 can be guaranteed to be directly opposite, thereby closing the upper opening of the heating table furnace body 1.

[0047] Embodiment three:

[0048] See also Figure 1-6 The present invention provides a technical solution based on the first embodiment: a sealing embedding groove 6 is provided at the edge of the upper surface of the heating platform furnace body 1, and an embedding ring 5 is provided on the lower surface of the heating platform top cover 2. The embedding ring 5 corresponds to the sealing embedding groove 6 in position and has a matching size.

[0049] Analysis of the above content: Through the plug-in cooperation of the sealing embedding groove 6 and the embedding ring 5, the hot plate furnace body 1 and the hot plate top cover 2 are closely matched, and the sealing effect of the upper opening of the hot plate furnace body 1 is improved.

[0050] Embodiment 4:

[0051] See also Figure 1-6 The present invention provides a technical solution based on the first embodiment: two vacuum and atmosphere control components 15 are provided, and the two vacuum and atmosphere control components 15 are respectively located at the two opposite side walls of the inner cavity of the hot plate furnace body 1. The vacuum and atmosphere control component 15 is hollow and has a gas nozzle 16 at one end and an interface at the other end. The interface of the vacuum and atmosphere control component 15 is connected to an air pipe 17. The side wall of the hot plate furnace body 1 is a hollow sandwich shape, and the connecting air pipe 17 is led out from the hollow sandwich of the side wall of the hot plate furnace body 1.

[0052] Analysis of the above content: According to the needs of use, the corresponding gas can be provided to the inside of the hot plate furnace body 1 based on the vacuum and atmosphere control component 15, the gas nozzle 16, and the connecting gas pipe 17 to form a corresponding atmosphere in the hot plate furnace body 1, and an external vacuum pump can also be connected to evacuate the inside of the hot plate furnace body 1.

[0053] Embodiment five:

[0054] See also Figure 1-6 The present invention provides a technical solution based on the first embodiment: a side observation window 4 is provided on the right side wall of the heating platform furnace body 1, and a front observation window 3 is provided in the middle of the heating platform top cover 2.

[0055] Analysis of the above contents: the side observation window 4 and the front observation window 3 are used to observe the state of the material sample inside the hot stage furnace body 1.

[0056] Embodiment six:

[0057] See also Figure 1-6The present invention provides a technical solution based on the first embodiment: a through hole 18 is opened on the left wall of the heating platform furnace body 1, and the wiring between the external controller 19 and the B-type thermocouple heating platform 13 and the light temperature compensation window 14 all passes through the through hole 18.

[0058] Embodiment seven:

[0059] See also Figure 1-6 The present invention provides a technical solution based on the first embodiment: the high temperature resistant base includes an upper seat plate 9 and a lower seat plate 10, and the right sides of the upper seat plate 9 and the lower seat plate 10 are provided with a wire pressing groove 11, and the wires of the B-type thermocouple hot stage 13 are pressed and plugged in the wire pressing groove 11, and the middle parts of the upper seat plate 9 and the lower seat plate 10 are provided with a receiving groove 12, and the receiving groove 12 is used to accommodate the control circuit of the B-type thermocouple hot stage 13.

[0060] Analysis of the above content: The high temperature resistant base is made of ceramic materials and metal materials, including platinum-rhodium alloy, copper, alumina, zirconium oxide and aluminum nitride and other materials (using the existing raw material ratio, here is the market purchasing agency in actual use).

[0061] Embodiment eight:

[0062] See also Figure 1-6 The present invention provides a technical solution based on Example 7: a high temperature resistant clamping plate 7 is arranged on the left side of the inner cavity of the hot plate furnace body 1, a groove 8 is opened on the right side of the lower surface of the high temperature resistant clamping plate 7, the left side of the high temperature resistant base is inserted into the groove 8, and the high temperature resistant clamping plate 7 is connected to the high temperature resistant base by screws.

[0063] Analysis of the above content: The high temperature resistant pressing plate 7 presses and fixes the high temperature resistant base as a whole through the groove body 8.

[0064] Embodiment nine:

[0065] See also Figure 1-6 The present invention provides a technical solution based on the seventh embodiment: the wire of the B-type thermocouple hot stage 13 includes a heating circuit and a temperature measuring circuit, and the B-type thermocouple hot stage 13 includes a positive electrode and a negative electrode. The two parts are respectively made of 70% platinum, 30% rhodium and 94% platinum, 6% rhodium alloy. The welding point part is pressed into a thin sheet for placing the sample. The thin sheet can realize heating and temperature measurement at the same time, and the heating circuit and the temperature measuring circuit are connected to the thin sheet at the same time.

[0066] Embodiment ten:

[0067] See also Figure 1-6 The present invention provides a technical solution based on any one of the first to ninth embodiments: a method for using an ultra-high temperature rapid heating hot plate, the specific steps of the method are as follows:

[0068] S1: Fix the B-type thermocouple heating platform 13 to the high temperature resistant base;

[0069] S2: placing the sample on the B-type thermocouple hot stage 13, and supplying corresponding gas based on the vacuum and atmosphere control component 15 to adjust the atmosphere in the hot stage furnace body 1;

[0070] S3: The temperature and heating curve required for the experiment are set by the external controller 19, and the B-type thermocouple heating table 13 is heated to the target temperature. The light temperature compensation window 14 is used to assist in increasing the heating temperature. The light temperature compensation window 14 uses the current electric heating lamp, which is the existing technology and will not be described in detail here;

[0071] S4: Observe the behavior of the sample in the hot stage furnace body 1 under high temperature environment.

[0072] S5: After the experiment is completed, turn off the power supply and take out the sample after it cools down to a safe range.

[0073] The hot stage of this solution can not only achieve extreme heating up to 1800℃, but also the heating rate can reach 900℃ / minute. And through the side observation window 4 of the hot stage furnace body 1, the contact angle test between the material and the platinum-rhodium alloy and other materials can be realized. The development of this innovative ultra-high temperature fast heating hot stage is expected to provide better experimental conditions for material performance testing and structural observation under ultra-high temperature conditions.

[0074] The high temperature resistant base can be made of aluminum nitride, which has a high melting point and excellent insulation properties to ensure the test stability under high temperature conditions of 1800°C. The size of the wire pressing groove 11 on the high temperature resistant base is precisely matched with the B-type thermocouple hot stage 13 to ensure its stable installation and excellent electrical and thermal conductivity.

[0075] The two ends of the B-type thermocouple hot stage 13 are connected to the external controller 19 through a platinum-rhodium wire and a copper wire respectively. The platinum-rhodium wire is used to transmit the temperature signal of the hot stage, and the copper wire is used to provide the heating current; the external controller 19 accurately adjusts the input current by real-time monitoring of the temperature signal of the thermocouple to achieve a temperature control accuracy higher than ±0.1°C.

[0076] For example: high temperature in-situ analysis of materials and interface behavior research using ultra-high temperature rapid heating hot stage contact angle test for 5SiO 2 -2CaO-2Na 2 O-Al 2 O 3The contact angle test of the quaternary system sample is carried out to study its high-temperature interface behavior. The high-temperature resistant base of the hot stage can be made of alumina and zirconia to ensure the structural stability at a high temperature of 1800°C. The B-type thermocouple hot stage 13 is embedded in the wire pressing groove 11 of the high-temperature resistant base, and its welding end is pressed into a thin sheet for placing the sample and realizing the heating and temperature measurement functions. The sample is prepared into a small disc with a diameter of 2mm and a height of 2mm by a powder pressing method and then placed in the middle of the B-type thermocouple hot stage 13. The experimental environment is adjusted to an argon atmosphere by the vacuum and atmosphere control component 15.

[0077] During the experiment, the external controller 19 sets the heating rate to 600°C / min and the target temperature to 1650°C. Through the side observation window 4, the sample melting and contact angle changes are monitored in real time using a high-resolution camera. As the temperature rises, the sample begins to soften and gradually melts at 1400°C. When it is completely melted at 1650°C, its contact angle with the hot plate is stabilized at 54° ( Figure 7 The temperature control accuracy is ±0.1℃, ensuring the reliability of experimental conditions and data accuracy. The experimental results show that the system exhibits strong wettability in the molten state.

[0078] The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention. For those skilled in the art, it is obvious that the present invention is not limited to the details of the above exemplary embodiments, and the present invention can be implemented in other specific forms without departing from the spirit or basic features of the present invention; therefore, no matter from which point of view, the embodiments should be regarded as exemplary and non-restrictive. The scope of the present invention is limited by the attached claims rather than the above description. Therefore, it is intended to include all changes within the meaning and scope of the equivalent elements of the claims in the present invention, and any figure marks in the claims should not be regarded as limiting the claims involved.

[0079] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. Ultra-high temperature rapid heating hot stage, characterized by: include: A heating platform furnace body (1), a heating platform top cover (2), a high temperature resistant base, a B-type thermocouple heating platform (13), a light temperature compensation window (14), a vacuum and atmosphere control component (15) and an external controller (19); The heating platform furnace body (1) is hollow and has an upper opening, the heating platform top cover (2) is detachably connected to the upper opening of the heating platform furnace body (1), the high temperature resistant base is arranged on the left side of the interior of the heating platform furnace body (1), the B-type thermocouple heating platform (13) is connected to the high temperature resistant base, the vacuum and atmosphere control component (15) is arranged in the inner cavity of the heating platform furnace body (1), the B-type thermocouple heating platform (13) is located in the middle of the heating platform furnace body (1), and a light temperature compensation window (14) corresponding to the position of the B-type thermocouple heating platform (13) is provided in the middle of the lower surface of the inner cavity of the heating platform furnace body (1), the external controller (19) is located on the outside of the heating platform furnace body (1), and the external controller (19) is electrically connected to the B-type thermocouple heating platform (13) and the light temperature compensation window (14).

2. The ultra-high temperature rapid heating stage according to claim 1, characterized in that: The four corners of the heating platform furnace body (1) and the heating platform top cover (2) are provided with connection holes, the connection holes of the heating platform furnace body (1) are provided with internal threads, and the connection holes of the heating platform top cover (2) are threadedly connected to the connection holes of the heating platform furnace body (1) via bolts.

3. The ultra-high temperature rapid heating stage according to claim 1, characterized in that: A sealing embedding groove (6) is provided at the edge of the upper surface of the heating platform furnace body (1), and an embedding ring (5) is provided on the lower surface of the heating platform top cover (2). The embedding ring (5) corresponds to the sealing embedding groove (6) in position and has a matching size.

4. The ultra-high temperature rapid heating stage according to claim 1, characterized in that: Two vacuum and atmosphere control components (15) are provided. The two vacuum and atmosphere control components (15) are respectively located on the two opposite side walls of the inner cavity of the hot plate furnace body (1). The vacuum and atmosphere control component (15) is hollow and has a gas nozzle (16) at one end and an interface at the other end. The interface of the vacuum and atmosphere control component (15) is connected to an air pipe (17). The side wall of the hot plate furnace body (1) is in a hollow sandwich shape, and the connecting air pipe (17) is led out from the hollow sandwich of the side wall of the hot plate furnace body (1).

5. The ultra-high temperature rapid heating stage according to claim 1, characterized in that: A side observation window (4) is provided on the right side wall of the heating platform furnace body (1), and a front observation window (3) is provided in the middle of the heating platform top cover (2).

6. The ultra-high temperature rapid heating stage according to claim 1, characterized in that: A through hole (18) is provided on the left side wall of the heating platform furnace body (1), and the wiring between the external controller (19), the B-type thermocouple heating platform (13) and the light temperature compensation window (14) all pass through the through hole (18).

7. The ultra-high temperature rapid heating stage according to claim 1, characterized in that: The high-temperature resistant base comprises an upper base plate (9) and a lower base plate (10); the right sides of the mutually facing side walls of the upper base plate (9) and the lower base plate (10) are provided with a wire pressing groove (11); the wires of the B-type thermocouple hot table (13) are pressed and plugged into the wire pressing groove (11); the middle parts of the mutually facing side walls of the upper base plate (9) and the lower base plate (10) are provided with a receiving groove (12); the receiving groove (12) is used to receive the control circuit of the B-type thermocouple hot table (13).

8. The ultra-high temperature rapid heating stage according to claim 7, characterized in that: A high-temperature resistant pressing plate (7) is provided on the left side of the inner cavity of the hot plate furnace body (1), a groove (8) is provided on the right side of the lower surface of the high-temperature resistant pressing plate (7), the left side of the high-temperature resistant base is inserted into the groove (8), and the high-temperature resistant pressing plate (7) is connected to the high-temperature resistant base by screws.

9. The ultra-high temperature rapid heating stage according to claim 7, characterized in that: The wire of the B-type thermocouple hot stage (13) includes a heating circuit and a temperature measurement circuit. The B-type thermocouple hot stage (13) includes two parts, a positive electrode and a negative electrode. The two parts are respectively made of 70% platinum, 30% rhodium and 94% platinum, 6% rhodium alloys. The welding point part is pressed into a thin sheet for placing a sample. The thin sheet can realize heating and temperature measurement at the same time. The heating circuit and the temperature measurement circuit are connected to the thin sheet at the same time.

10. The method for using the ultra-high temperature rapid heating hot stage according to any one of claims 1 to 9, characterized in that: The specific steps of this method are as follows: S1: Fixing the B-type thermocouple heating platform (13) to a high temperature resistant base; S2: placing the sample on a B-type thermocouple hot stage (13), and supplying corresponding gases based on the vacuum and atmosphere control component (15) to adjust the atmosphere in the hot stage furnace (1); S3: Setting the required temperature and heating curve for the experiment through the external controller (19), heating the B-type thermocouple hot stage (13) to the target temperature; S4: Observation of the behavior of the sample in the hot stage furnace (1) under high temperature environment; S5: After the experiment is completed, turn off the power and take out the sample after it cools down to a safe range.

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