Device and method for testing and measuring reaction rate of copper oxide

By designing a device for copper oxide reaction rate detection and determination, the heating rod is automatically removed and cleaned by driving components, the temperature control difficulties and scale accumulation problems caused by heating rod fixation in the prior art are solved, and more efficient heating and more precise temperature control are achieved.

CN119827696AActive Publication Date: 2025-04-15JIANGSU TEHO METAL IND
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Patent Information

Application Number
CN202510295907.3
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-03-13
Publication Date
2025-04-15
Estimated Expiration
2045-03-13

AI Technical Summary

Technical Problem

In the existing glass reactor water bath heating method, the heating rod is fixed inside the container, making it difficult to accurately control the temperature and the heating rod cannot be moved out. After long-term use, scale will accumulate, hinder heat conduction and reduce heating efficiency.

Method used

A device for copper oxide reaction rate testing and determination is designed, including a glass reactor, a water bath ring and a collection ring. The heating rod is driven to move from the water bath ring and enter the collection ring through the driving assembly, scraping off the scale from the outer wall of the heating rod, achieving automated cleaning and precise temperature control.

Benefits of technology

Accurate control of the reaction temperature is achieved, temperature fluctuations caused by the residual heat of the heating rod are avoided, heating efficiency is improved, equipment service life is extended, and manual operation risks are reduced.

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Abstract

The invention discloses a device and method for testing and measuring the reaction rate of copper oxide, and relates to the technical field of oxidation cylinder experiments.The device comprises a glass reaction kettle, a water bath ring and a collection ring, the structure for conducting water bath heating on the glass reaction kettle is the water bath ring, the outer wall of the water bath ring is sleeved with the collection ring, and a driving assembly is arranged below the water bath ring; the driving assembly can drive the heating rod to move out of the water bath ring after the heating rod is powered off, the influence of waste heat on the water bath temperature can be rapidly reduced by moving the heating rod out of the water bath ring after the heating rod is powered off, the situation that the water bath container is continuously heated by the waste heat of the heating rod is avoided, temperature fluctuation caused by the waste heat of the heating rod is avoided, and therefore more accurate temperature control is achieved. The temperature stability in the reaction process is ensured, when the heating rod is moved out of the water bath ring, potential safety hazards caused by overheating and too high temperature can be effectively prevented, and particularly, after the reaction is finished, unnecessary heat accumulation can be rapidly prevented through an automatic rod moving system.
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Description

Technical Field

[0001] The invention relates to the technical field of oxidation cylinder experiments, and in particular to a device and a method for testing and measuring the reaction rate of copper oxidation. Background Art

[0002] Testing the reaction rate of copper oxide solution helps to understand the kinetic characteristics of the reaction and evaluate the effects of different temperatures, concentrations and reaction conditions on the reaction rate. By real-time monitoring of the reaction rate, the reaction conditions can be optimized, production efficiency can be improved, and the safety and stability of the reaction process can be ensured to avoid adverse results caused by too fast or too slow reactions. For glass reactors, water bath heating is a common temperature control method. By uniformly heating the reactor, the stability of the reaction temperature is ensured, local overheating or cooling is prevented, thereby improving the uniformity and controllability of the reaction. In addition, water bath heating can also avoid excessive temperatures or glass reactor breakage caused by direct heating.

[0003] In the prior art, some glass reactor water bath heating methods are to fix multiple heating rods to the inside of a container in contact with the glass reactor, and the heating rods heat the water stored in the container. However, the method of fixing the heating rods inside the container has many disadvantages. First, even if the heating rods are powered off, the residual heat of the heating rods causes the water bath temperature to continue to rise, resulting in difficulty in accurately controlling the temperature. Especially when the temperature needs to be strictly controlled during the reaction process, the residual heat may cause the temperature to exceed the standard, thereby affecting the stability of the reaction and the quality of the product. In addition, the heating rods cannot be removed from the water bath container, and scale will accumulate after long-term use. The scale forms an insulating layer on the surface of the heating rods, which hinders heat conduction, resulting in a decrease in heating efficiency and a longer time to reach the required temperature. Summary of the invention

[0004] The purpose of the present invention is to solve the problem that some glass reactors in the prior art are heated in a water bath by fixing multiple heating rods to the inside of a container in contact with the glass reactor, and the heating rods heat the water source stored in the container. However, the method of fixing the heating rods in the container has many disadvantages. On the one hand, even if the heating rods are powered off, the residual heat of the heating rods causes the water bath temperature to continue to rise, resulting in difficulty in accurately controlling the temperature. Especially when the temperature needs to be strictly controlled during the reaction process, the residual heat may cause the temperature to exceed the standard, thereby affecting the stability of the reaction and the quality of the product. In addition, the heating rods cannot be removed from the water bath container, and scale will accumulate after long-term use. The scale forms an insulating layer on the surface of the heating rods, which hinders heat conduction, resulting in a decrease in heating efficiency and a longer time to reach the required temperature. The present invention proposes a device and method for testing and measuring the reaction rate of copper oxide.

[0005] In order to achieve the above object, the present invention adopts the following technical solutions: A device for testing and measuring the reaction rate of copper oxide comprises a glass reactor, a water bath ring and a collecting ring. The bottom of the glass reactor is fixedly connected to the top of a support plate, a side of the support plate is provided with an avoidance groove, the four corners of the support plate are fixedly connected to support columns, an outer protective tube is fixedly arranged on the top of the outer wall of the glass reactor, a water bath ring is movably sleeved on the bottom of the outer wall of the glass reactor, a mounting tube is arranged on the other side of the injection pipe at the top of the glass reactor, a pH sensor and a conductivity sensor are movably inserted into the mounting tube in sequence along the vertical direction, a top ring is fixedly arranged on the top of the support column, and a circular array of the top rings has a function of heating the glass reactor with a water bath. A hot heating component, the heating component includes a heating rod and a vertical folding rod. The top of the heating rod is fixedly provided with a vertical folding rod, the heating rod extends into the water bath ring, and the support plate is provided with a driving component below the water bath ring. The driving component can drive the heating rod to move out of the water bath ring and enter the collecting ring, so as to scrape off the scale that may be attached to the outer wall of the heating rod. The driving component includes a vertical cylinder, a horizontal U rod and an expansion support component that drives multiple heating components to move horizontally above the collecting ring. The inner wall of the horizontal U rod is provided with a reversing component that drives the collecting ring to move up and connect with the heating rod when the horizontal U rod moves down. The reversing component includes an active gear rod, a switching gear, and a driven gear rod.

[0006] Optionally, a leveling foot is screwed into the bottom thread of the support column, and the leveling foot includes a vertical section and a frustum section. The vertical section of the leveling foot is provided with a bolt, and the material of the frustum section of the leveling foot is set to be rubber material.

[0007] Optionally, a discharge pipe is fixedly connected to the bottom of the glass reactor, a release valve is arranged on the side of the discharge pipe, an injection pipe is fixedly connected to one side of the top of the glass reactor, a closing cover is threaded into the top of the injection pipe, a stirring motor is fixedly arranged in the middle position of the top of the glass reactor, a vertical axis is fixedly arranged at the output end of the stirring motor, stirring blades are equidistantly arranged along the vertical direction of the vertical axis, and the front cross-sectional shape of the stirring blades is U-shaped.

[0008] Optionally, a vertical cylinder is symmetrically fixedly arranged at the bottom of the support plate, a horizontal U-rod is fixedly arranged at the output end of the vertical cylinder after passing through the support plate, the bottom of the side of the horizontal U-rod is fixedly connected to the side of the water bath ring, the expansion assembly includes an expansion tube, a horizontal column, and a connecting spring, the top of the vertical folding rod is fixedly connected to the horizontal column in the horizontal direction, and a vertical ring is slidably arranged on the outer wall of the horizontal column.

[0009] Optionally, the outer wall of the vertical ring is fixedly connected to one end of the connecting spring, the other end of the connecting spring is fixedly connected to the side of the vertical folding rod, the end of the horizontal column is arranged to be hemispherical, the top of the top ring is a circular array and a horizontal column is movably inserted therein, and the horizontal column is movably inserted into the side of the top ring away from one end of the vertical ring.

[0010] Optionally, the collecting ring is sleeved on the outer wall of the water bath ring, and a driven gear rod is symmetrically fixedly arranged on the outer wall of the collecting ring. The side surface of the driven gear rod is stably meshed with the switching gear, and the other side surface of the switching gear is stably meshed with an active gear rod, and the active gear rod is fixedly connected to the side surface of the horizontal U rod, and the switching gear is rotatably connected to the side surface of the support seat, and the bottom of the support seat is fixedly connected to the top of the support plate with bolts.

[0011] Optionally, a scraper ring is movably inserted into the collecting ring along the vertical direction, a circular array of scraper holes is provided on the top of the scraper ring, an inverted U rod is symmetrically fixedly connected to the bottom of the scraper ring, and the bottom of the inverted U rod overlaps the inner cavity of the collecting ring.

[0012] Optionally, the interior of the expansion tube is hollow, a closed ring is fixedly connected to the top of the expansion tube, the outer wall of the expansion tube is provided with a wide vertical surface, an inclined surface and a narrow vertical surface in sequence along the vertical direction, the top side of the horizontal U-rod is fixedly connected to the side of the wide vertical surface, and one end of the horizontal column is set to be hemispherical and contacts the wide vertical surface, the inclined surface or the narrow vertical surface of the outer wall of the expansion tube.

[0013] Optionally, the outer protective tube is made of transparent acrylic plate material, a controller is fixedly arranged on the side of the outer protective tube, an inverted U groove is symmetrically opened at the bottom of the side of the outer protective tube, and both ends of the water bath ring are fixedly connected with an AC pipe, and the AC pipe extends from the inverted U groove.

[0014] A method for testing the reaction rate of copper oxide comprises the following steps: S1: Conduct a copper oxide reaction experiment. At this time, the heating rod is inserted into the water bath ring to heat the external water source connected to the water bath ring. The water bath ring heats the glass reactor in a water bath. The copper oxide reaction reagent is introduced into the glass reactor through the injection tube. The stirring motor stirs the copper oxide reaction reagent through the stirring blades. At the same time, the pH sensor and conductivity sensor installed on the top of the glass reactor obtain the copper oxide reaction rate.

[0015] S2: After the oxidation cylinder reaction experiment is completed, the controller controls the driving assembly, which drives the water bath ring to move downward, and at the same time drives multiple heating rods to move to the top of the collecting ring through the expansion assembly. At the same time, the horizontal U-rod in the expansion assembly drives the collecting ring to move upward through the reversing assembly. The scraper ring on the collecting ring passes through the heating rod, and the scale attached to the surface of the heating rod is scraped off and collected inside the collecting ring.

[0016] Compared with the prior art, the present invention has the following advantages: 1. The structure of the present invention for water-bath heating of a glass reactor is a water-bath ring, a collecting ring is sleeved on the outer wall of the water-bath ring, and a driving assembly is arranged under the water-bath ring. The driving assembly can drive the heating rod to move out of the water-bath ring after the heating rod is powered off. When the heating rod is powered off, moving out of the water-bath ring can quickly reduce the influence of residual heat on the water-bath temperature, avoid the residual heat of the heating rod to continue to heat the water-bath container, avoid temperature fluctuations caused by the residual heat of the heating rod, thereby achieving more precise temperature control and ensuring temperature stability during the reaction. When the heating rod is moved out of the water-bath ring, overheating can be effectively prevented, and the potential safety hazard caused by excessive temperature can be reduced. In particular, after the reaction is completed, unnecessary heat accumulation can be quickly prevented through the automatic rod moving system.

[0017] 2. One of the core components of the driving assembly of the present invention is the expansion support assembly. Since the collecting ring is debugged on the outer wall of the water bath ring, when the driving assembly drives the heating rod to move out from the inside of the water bath ring, a plurality of heating rods are driven to move to the top of the collecting ring by a purely mechanical structure, waiting for the scraping assembly inside the collecting ring to scrape the scale on the outer wall of the heating rod. On the one hand, the collecting ring can automatically scrape and collect the scale. The combination of the collecting ring and the scraping assembly makes the scale removal process automatic. The relative movement of the heating rod and the scraping assembly is driven by the mechanical structure to avoid manual operation, greatly improve the cleaning efficiency and accuracy, and reduce manual intervention and operation risks. On the other hand, the scale is scraped off in a timely and automatic manner to avoid the long-term accumulation of scale on the surface of the heating rod. This not only improves the heating efficiency, but also prevents the damage of scale to the heating rod, effectively extending the service life of the equipment. The scraping of scale ensures the direct contact between the surface of the heating rod and the water source of the water bath, and maintains the heating efficiency. Without the interference of scale, the heating rod can transfer heat more efficiently and improve the overall heating performance of the system.

[0018] 3. One of the core components of the driving assembly of the present invention is the expansion assembly, and a reversing assembly is arranged under the expansion assembly. When the driving assembly drives the heating rod to move relatively out of the water bath ring, the collecting ring will be driven upward through the reversing assembly to connect with multiple heating rods. There is no need for multiple heating rods to be displaced in the vertical direction, thereby reducing the layout and guiding pressure of the power lines of multiple heating rods on the entire device. In general, the driving assembly is designed with a linkage of the expansion assembly, the reversing assembly and the collecting ring. The whole process only requires the program to control one vertical cylinder, which reduces the complexity of the program and the difficulty of equipment maintenance. Through automation and precise control, not only the cleaning efficiency and heat utilization efficiency of the heating rod are improved, but also the manual operation is reduced, thereby improving the overall safety, stability and economy of the equipment. BRIEF DESCRIPTION OF THE DRAWINGS

[0019] Figure 1 It is a schematic diagram of the overall structure of the present invention.

[0020] Figure 2 for Figure 1Schematic diagram of the structure after removing the outer casing.

[0021] Figure 3 for Figure 2 Another perspective structural diagram of .

[0022] Figure 4 for Figure 3 Schematic diagram of the structure for dismantling the glass reactor.

[0023] Figure 5 It is a schematic diagram of the structure of the glass reactor.

[0024] Figure 6 for Figure 5 Schematic diagram of the half-section structure.

[0025] Figure 7 It is a structural schematic diagram of the horizontal U rod and its connecting parts.

[0026] Figure 8 It is a schematic diagram of the structure of the expansion support tube and its connecting parts.

[0027] Fig. 9 It is a schematic diagram of the structure of the collecting ring and its connecting parts.

[0028] Fig.10 for Fig. 9 Schematic diagram of the local enlarged structure at A.

[0029] Fig.11 It is a schematic diagram of the structure of the heating rod and its connecting parts.

[0030] Fig.12 Schematic diagram of the structure of the internal components of the collecting ring.

[0031] Fig.13 for Fig.12 Schematic diagram of the local enlarged structure at point B.

[0032] In the figure: 1, outer casing; 2, controller; 201, inverted U groove; 3, support plate; 4, support column; 5, leveling foot; 6, avoidance groove; 7, top ring; 8, stirring motor; 9, closing cover; 10, injection pipe; 11, glass reactor; 12, discharge pipe; 121, release valve; 13, installation cylinder; 131, PH sensor; 132, conductivity sensor; 14, vertical axis; 141, stirring blade; 15, expansion cylinder; 151, Wide vertical surface; 152, inclined surface; 153, narrow vertical surface; 16, water bath ring; 161, AC pipe; 17, closed ring; 18, horizontal U rod; 19, vertical cylinder; 20, collecting ring; 21, active gear rod; 22, switching gear; 23, supporting seat; 24, driven gear rod; 25, connecting spring; 26, vertical ring; 27, horizontal column; 28, vertical folding rod; 29, heating rod; 30, scraper ring; 31, scraper hole; 32, inverted U rod. DETAILED DESCRIPTION

[0033] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.

[0034] In the description of the present invention, it is necessary to understand that the terms "upper", "lower", "front", "back", "left", "right", "top", "bottom", "inside", "outside", etc., indicating the orientation or position relationship are based on the orientation or position relationship shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention.

[0035] Reference Figure 1-13 A device for testing and measuring the reaction rate of copper oxide comprises a glass reactor 11, a water bath ring 16, and a collecting ring 20. The bottom of the glass reactor 11 is fixedly connected to the top of a support plate 3. A side of the support plate 3 is provided with an avoidance groove 6. The four corners of the support plate 3 are fixedly connected with support columns 4. The bottom of the support column 4 is threaded with a leveling foot 5. The leveling foot 5 comprises a vertical section and a truncated cone section. The vertical section of the leveling foot 5 is provided with a bolt. The material of the truncated cone section of the leveling foot 5 is set to rubber material. Multiple leveling feet 5 are used to level the entire device. The bottom of the glass reactor 11 is fixedly connected with a discharge pipe 12. A release valve 121 is provided on the side of the discharge pipe 12 to control the glass reactor 11 to discharge the reaction material.

[0036] An outer casing 1 is fixedly installed on the top of the outer wall of the glass reactor 11 to protect the components arranged outside the glass reactor 11, and the outer casing 1 is made of a transparent acrylic plate material, which is convenient for experimenters to observe the chemical reaction inside the glass reactor 11 with the naked eye. A controller 2 is fixedly installed on the side of the outer casing 1. The controller 2 is a PLC controller commonly used in the prior art, and is used to control the following PH sensor 131 and conductivity sensor 132, vertical cylinder 19 and heating rod 29.

[0037] An inverted U-groove 201 is symmetrically provided at the bottom of the side of the outer casing 1. AC pipes 161 are fixedly connected to both ends of the water bath ring 16. The AC pipe 161 extends out of the inverted U-groove 201. The inverted U-groove 201 is used to make way for the AC pipe 161 when it is displaced in the vertical direction. The AC pipe 161 requires an external water source. A water bath ring 16 is movably sleeved at the bottom of the outer wall of the glass reactor 11. The water bath ring 16 is made of heat-conducting material, which is convenient for transferring heat to the glass reactor 11 when the water source inside the water bath ring 16 is heated.

[0038] A mounting tube 13 is provided at the top of the glass reactor 11 on the other side of the injection tube 10. The mounting tube 13 is movably inserted with a PH sensor 131 and a conductivity sensor 132 in sequence along the vertical direction. A top ring 7 is fixedly provided on the top of the support column 4. The top ring 7 has a circular array with a heating component for water bath heating of the glass reactor 11. The heating component includes a heating rod 29 and a vertical folding rod 28. A vertical folding rod 28 is fixedly provided on the top of the heating rod 29. The heating rod 29 extends into the water bath ring 16. A driving component is provided on the support plate 3 below the water bath ring 16.

[0039] The driving assembly can drive the heating rod 29 to move out of the water bath ring 16 and into the collecting ring 20, so as to scrape off the scale that may be attached to the outer wall of the heating rod 29. The driving assembly includes a vertical cylinder 19, a horizontal U rod 18 and an expansion assembly that drives multiple heating assemblies to move horizontally above the collecting ring 20. The expansion assembly includes an expansion tube 15, a horizontal column 27, and a connecting spring 25. The top of the vertical folding rod 28 is fixedly connected to the horizontal column 27 in the horizontal direction. The outer wall of the horizontal column 27 is slidably provided with a vertical ring 26. The outer wall of the vertical ring 26 is fixedly connected to one end of the connecting spring 25, and the other end of the connecting spring 25 is fixedly connected to the side of the vertical folding rod 28. The end of the horizontal column 27 is arranged in a hemispherical shape. The top of the top ring 7 is circularly arrayed and movably inserted with the horizontal column 27. The horizontal column 27 is movably inserted into the side of the top ring 7 away from the end of the vertical ring 26.

[0040] The inner wall of the horizontal U-rod 18 is provided with a reversing assembly which drives the collecting ring 20 to move up and connect with the heating rod 29 when the horizontal U-rod 18 moves down. The reversing assembly includes an active gear rod 21, a switching gear 22, and a driven gear rod 24. An injection pipe 10 is fixedly connected to one side of the top of the glass reactor 11. A closing cover 9 is screwed into the top of the injection pipe 10. A stirring motor 8 is fixedly provided at the middle position of the top of the glass reactor 11. A vertical shaft 14 is fixedly provided at the output end of the stirring motor 8. Stirring blades 141 are equidistantly provided along the vertical direction of the vertical shaft 14. The front cross-sectional shape of the stirring blade 141 is U-shaped, which assists in stirring the reaction material in the inner cavity of the glass reactor 11.

[0041] A vertical cylinder 19 is symmetrically fixedly arranged at the bottom of the support plate 3, and a horizontal U-rod 18 is fixedly arranged at the output end of the vertical cylinder 19 after passing through the support plate 3. The bottom of the side of the horizontal U-rod 18 is fixedly connected to the side of the water bath ring 16. The collecting ring 20 is sleeved on the outer wall of the water bath ring 16, and a driven gear rod 24 is symmetrically fixedly arranged on the outer wall of the collecting ring 20. The side of the driven gear rod 24 is stably meshed with the switching gear 22, and the other side of the switching gear 22 is stably meshed with an active gear rod 21, which is fixedly connected to the side of the horizontal U-rod 18. The switching gear 22 is rotatably connected to the side of the support seat 23. The bottom of the support seat 23 is fixedly connected to the top of the support plate 3 by bolts. A scraper ring 30 is movably inserted into the collecting ring 20 in the vertical direction. The top of the scraper ring 30 has a circular array of scraper holes 31. The bottom of the scraper ring 30 is symmetrically fixedly connected with an inverted U rod 32, which is used to support the scraper ring 30 inside the collecting ring 20. The diameter of the scraper hole 31 is the same as the diameter of the heating rod 29.

[0042] The bottom of the inverted U-rod 32 is overlapped with the inner cavity of the collecting ring 20, the interior of the expansion tube 15 is hollow, and a closed ring 17 is fixedly connected to the top of the expansion tube 15. The outer wall of the expansion tube 15 is provided with a wide vertical surface 151, an inclined surface 152 and a narrow vertical surface 153 in sequence along the vertical direction. The top side of the horizontal U-rod 18 is fixedly connected to the side of the wide vertical surface 151, and the horizontal column 27 is set to have one end of a hemisphere that contacts the wide vertical surface 151, the inclined surface 152 or the narrow vertical surface 153 of the outer wall of the expansion tube 15.

[0043] The specific implementation steps and principles of the present invention are as follows: In the initial state, the heating rod 29 extends into the water bath ring 16, the collecting ring 20 is flush with the top of the water bath ring 16, one end of the horizontal column 27 contacts the side wall of the narrow vertical surface 153, and the active gear rod 21 is above the switching gear 22 and does not contact the switching gear 22. When the copper oxide reaction experiment is carried out, the external water source connected to the water bath ring 16 is heated, and the water bath ring 16 heats the glass reactor 11 in a water bath. The copper oxide reaction reagent is introduced into the glass reactor 11 through the injection tube 10, and the stirring motor 8 stirs the copper oxide reaction reagent through the stirring blade 141. At the same time, the pH sensor 131 and the conductivity sensor 132 arranged on the top of the glass reactor 11 obtain the copper oxide reaction rate.

[0044] After the oxidation tube reaction experiment is over, the controller 2 controls the vertical cylinder 19 to retract, and the vertical cylinder 19 drives the water bath ring 16 to move downward, and at the same time drives the expansion tube 15 to move downward through the horizontal U rod 18. During this process, the water bath ring 16 moves downward, and when the horizontal column 27 reaches the top of the narrow vertical surface 153, the heating rod 29 moves out of the water bath ring 16, and one end of the horizontal column 27 moves along the inclined surface 152. Multiple heating rods 29 move to the top of the collecting ring 20. When the horizontal column 27 reaches the top of the inclined surface 152 and begins to contact the wide vertical surface 151, multiple heating rods 29 stop moving away from each other, and the active gear rod 21 is above the switching gear 22 and contacts the switching gear 22. The collecting ring 20 is driven to move upward by the driven gear rod 24. The scraper ring 30 arranged inside the collecting ring 20 passes through multiple heating rods 29, and the scale that may exist on the outside of the heating rod 29 is scraped off by the scraper hole 31.

[0045] When multiple heating rods 29 are driven to expand and move to just above the collecting ring 20, the horizontal U-rod 18 in the expansion assembly drives the collecting ring 20 to move upward through the reversing assembly, and the scraper ring 30 on the collecting ring 20 passes through the heating rods 29, and the scale attached to the surface of the heating rods 29 is scraped off and collected inside the collecting ring 20.

[0046] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.

Claims

1. A device for testing and measuring the reaction rate of copper oxide, comprising a glass reaction kettle (11), a water bath ring (16), and a collecting ring (20), characterized in that: The bottom of the glass reactor (11) is fixedly connected to the top of the support plate (3), the side of the support plate (3) is provided with an avoidance groove (6), the four corners of the support plate (3) are fixedly connected to support columns (4), the top of the outer wall of the glass reactor (11) is fixedly provided with an outer protective tube (1), the bottom of the outer wall of the glass reactor (11) is movably sleeved with a water bath ring (16), the top of the glass reactor (11) is provided with a mounting tube (13) on the other side of the injection pipe (10), the mounting tube (13) is movably inserted with a pH sensor (131) and a conductivity sensor (132) in sequence in the vertical direction, the top of the support column (4) is fixedly provided with a top ring (7), the top ring (7) has a circular array of heating components for heating the glass reactor (11) in a water bath, the heating components comprising a heating rod (29), a vertical A folding rod (28), a vertical folding rod (28) is fixedly arranged on the top of the heating rod (29), the heating rod (29) extends into the water bath ring (16), the support plate (3) is provided with a driving assembly below the water bath ring (16), the driving assembly can drive the heating rod (29) to move out of the water bath ring (16) and into the collecting ring (20), so as to scrape off scale that may be attached to the outer wall of the heating rod (29), the driving assembly comprises a vertical cylinder (19), a horizontal U rod (18), and an expansion support assembly that drives multiple heating assemblies to move horizontally to the top of the collecting ring (20), the inner wall of the horizontal U rod (18) is provided with a reversing assembly that drives the collecting ring (20) to move upward to connect with the heating rod (29) when the horizontal U rod (18) moves downward, and the reversing assembly comprises an active gear rod (21), a switching gear (22), and a driven gear rod (24).

2. A copper oxide reaction rate testing and measuring device according to claim 1, characterized in that: A leveling foot (5) is screwed into a thread at the bottom of the support column (4), the leveling foot (5) comprising a vertical section and a truncated cone section, the vertical section of the leveling foot (5) being provided with a bolt, and the material of the truncated cone section of the leveling foot (5) being set to be a rubber material.

3. A copper oxide reaction rate testing and measuring device according to claim 1, characterized in that: The bottom of the glass reactor (11) is fixedly connected to a discharge pipe (12), a release valve (121) is arranged on the side of the discharge pipe (12), one side of the top of the glass reactor (11) is fixedly connected to an injection pipe (10), a sealing cap (9) is screwed into the top of the injection pipe (10), a stirring motor (8) is fixedly arranged at the middle position of the top of the glass reactor (11), a vertical shaft (14) is fixedly arranged at the output end of the stirring motor (8), stirring blades (141) are arranged equidistantly along the vertical direction on the vertical shaft (14), and the front view cross-section of the stirring blades (141) is U-shaped.

4. A copper oxide reaction rate testing and measuring device according to claim 1, characterized in that: A vertical cylinder (19) is symmetrically fixedly arranged at the bottom of the support plate (3); a horizontal U-rod (18) is fixedly arranged at the output end of the vertical cylinder (19) after passing through the support plate (3); the bottom of the side of the horizontal U-rod (18) is fixedly connected to the side of the water bath ring (16); the expansion component comprises an expansion cylinder (15), a horizontal column (27), and a connecting spring (25); the top of the vertical folding rod (28) is fixedly connected to the horizontal column (27) in the horizontal direction; and a vertical ring (26) is slidably arranged on the outer wall of the horizontal column (27).

5. A copper oxide reaction rate testing and measuring device according to claim 4, characterized in that: The outer wall of the vertical ring (26) is fixedly connected to one end of the connecting spring (25), the other end of the connecting spring (25) is fixedly connected to the side of the vertical folding rod (28), the end of the horizontal column (27) is arranged in a hemispherical shape, the top of the top ring (7) is a circular array and the horizontal column (27) is movably inserted, and the horizontal column (27) is movably inserted into the side of the top ring (7) away from one end of the vertical ring (26).

6. A copper oxide reaction rate testing and measuring device according to claim 1, characterized in that: The collecting ring (20) is sleeved on the outer wall of the water bath ring (16), and a driven gear rod (24) is symmetrically fixedly arranged on the outer wall of the collecting ring (20). The side of the driven gear rod (24) is stably meshed with the switching gear (22), and the other side of the switching gear (22) is stably meshed with an active gear rod (21), and the active gear rod (21) is fixedly connected to the side of the horizontal U rod (18). The switching gear (22) is rotatably connected to the side of the support seat (23), and the bottom of the support seat (23) is fixedly connected to the top of the support plate (3) by bolts.

7. A copper oxide reaction rate testing and measuring device according to claim 1, characterized in that: The collecting ring (20) is movably inserted with a scraping ring (30) in the vertical direction; the scraping ring (30) has a circular array of scraping holes (31) on the top; an inverted U-rod (32) is symmetrically fixedly connected to the bottom of the scraping ring (30); the bottom of the inverted U-rod (32) overlaps the inner cavity of the collecting ring (20).

8. A copper oxide reaction rate testing and measuring device according to claim 5, characterized in that: The expansion tube (15) is hollow inside, a closed ring (17) is fixedly connected to the top of the expansion tube (15), a wide vertical surface (151), an inclined surface (152) and a narrow vertical surface (153) are sequentially provided on the outer wall of the expansion tube (15) along the vertical direction, the top side surface of the horizontal U rod (18) is fixedly connected to the side surface of the wide vertical surface (151), and one end of the horizontal column (27) which is arranged in a hemispherical shape contacts the wide vertical surface (151), the inclined surface (152) or the narrow vertical surface (153) of the outer wall of the expansion tube (15).

9. A copper oxide reaction rate testing and measuring device according to claim 1, characterized in that: The outer protective tube (1) is made of a transparent acrylic plate material. A controller (2) is fixedly arranged on the side of the outer protective tube (1). An inverted U-groove (201) is symmetrically provided on the bottom of the side of the outer protective tube (1). Both ends of the water bath ring (16) are fixedly connected with an AC pipe (161), and the AC pipe (161) extends out of the inverted U-groove (201).

10. A method for testing the reaction rate of copper oxide, used in a device for testing the reaction rate of copper oxide as claimed in any one of claims 1 to 9, characterized in that: The following steps are involved: S1: Conducting a copper oxide reaction experiment, at which time the heating rod (29) extends into the water bath ring (16) to heat the external water source connected to the water bath ring (16), the water bath ring (16) performs water bath heating on the glass reactor (11), and the copper oxide reaction reagent is introduced into the glass reactor (11) through the injection tube (10), the stirring motor (8) stirs the copper oxide reaction reagent through the stirring blade (141), and at the same time, the pH sensor (131) and the conductivity sensor (132) arranged on the top of the glass reactor (11) obtain the copper oxide reaction rate; S2: After the oxidation tube reaction experiment is finished, the controller (2) controls the driving assembly, and the driving assembly drives the water bath ring (16) to move downward, and at the same time drives the plurality of heating rods (29) to expand and move to the top of the collecting ring (20) through the expansion assembly. At the same time, the horizontal U rod (18) in the expansion assembly drives the collecting ring (20) to move upward through the reversing assembly, and the scraping ring (30) on the collecting ring (20) passes through the heating rod (29), and the scale attached to the surface of the heating rod (29) is scraped off, and the scale is collected inside the collecting ring (20).

Citation Information

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