Preparation process of peach gum ink

By crushing, soaking and bleaching peach glue, combined with emulsification and grinding technology, the peach glue liquid is fully mixed with carbon black particles, solving the problems of viscosity degradation and gloss of traditional inks, and achieving high viscosity and gloss ink effects.

CN119859435AInactive Publication Date: 2025-04-22屈桂波
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Patent Information

Application Number
CN202510091239.2
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-01-21
Publication Date
2025-04-22
Estimated Expiration
Not applicable · inactive patent

AI Technical Summary

Technical Problem

Traditional ink uses animal gelatin, which leads to viscous degradation, ink particles fall off, lose their luster, and is difficult to completely dissolve, affecting the effect of ink.

Method used

Peach gum is used as a substitute. Through crushing, soaking, decoloring and bleaching, the transparency and viscosity of peach gum liquid are improved, and the carbon black particles are fully mixed with peach gum liquid through emulsification and grinding to ensure adhesion effect.

Benefits of technology

It effectively avoids peach glue affecting the display of ink color, ensures the adhesion between ink particles and between ink particles and paper, and improves the gloss and writing performance of ink.

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Abstract

The invention relates to the technical field of peach gum ink, in particular to a preparation process of peach gum ink, which comprises the following steps: crushing and screening peach gum, treating the peach gum, preparing an ink preparation material, treating the ink preparation material, mixing to prepare ink and preparing the ink. The peach gum is crushed, soaked, decolorized and bleached, the transparency of the peach gum liquid is improved, the viscosity of the peach gum liquid is guaranteed, the situation that traditional peach gum affects the ink color can be effectively avoided, animal gelatin can be effectively replaced, carbon black particles and the peach gum liquid are fully mixed through emulsification and grinding operation, and the color of the peach gum liquid is improved. The carbon black particles are ensured to be adhered, and the adhesion effect between the particles and between the particles and paper is ensured.
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Description

Technical Field

[0001] The invention relates to the technical field of peach gum ink, in particular to a preparation process of peach gum ink. Background Art

[0002] Peach gum is a gelatinous, translucent substance secreted by the trunks of Rosaceae plants such as peach or mountain peach after mechanical injury or disease. The solid substance formed by air drying on the trunk or other dehydration methods is raw peach gum. Raw peach gum is a pink or light yellow translucent solid block with a smooth surface. It can generally only swell and is not easy to completely dissolve. The aqueous solution is viscous and belongs to the polysaccharide substance.

[0003] Traditional ink is prepared by mixing animal gelatin. Animal gelatin is a protein that is easily degraded and loses its viscosity. The ink particles fall off and lose their luster, which is not conducive to ensuring the display of the ink effect.

[0004] The stickiness of peach gum can fully ensure the connectivity of ink particles, which helps to fully ensure the glossiness of ink. However, how to fully utilize the characteristics of peach gum in ink is a difficult problem in this field. Summary of the invention

[0005] The invention aims to solve the shortcomings in the prior art and provides a preparation process of peach gum ink.

[0006] In order to achieve the above object, the present invention adopts the following technical solutions:

[0007] A preparation process of peach gum ink comprises the following steps:

[0008] S1. Peach gum crushing and screening: The surface of the peach gum is cleaned by a cleaning device, and after cleaning, the peach gum is crushed by a cutting device, and the crushed peach gum is collected centrally;

[0009] S2, peach gum processing: the crushed peach gum is introduced into a blender and then purified water is added to obtain a soaking liquid, and the soaking liquid temperature is controlled between 60-70°, and the pH value of the soaking liquid is adjusted and the solution temperature is increased to between 75-80°, and the temperature is maintained until the peach gum is completely dissolved, and the dissolved soaking liquid is processed so that the solution is filtered after standing and settling to obtain peach gum liquid;

[0010] S3, ink material preparation: obtain carbon black, aromatic agent, moisturizer, dispersant, defoamer, preservative and purified water;

[0011] S4, ink material processing: crush the carbon black through a wall-breaking crusher;

[0012] S5, ink mixing: start the emulsifier, pour 1 / 3 of water into the emulsifier and heat it to 75-85°, then pour the peach gum liquid prepared in S2 into the emulsifier, then pour the crushed carbon black into it, and finally pour the fragrance, moisturizer, dispersant, defoamer and preservative in turn, and stir well until the ink paste is formed;

[0013] S6. Prepare ink: grind the ink paste and 1 / 3 of pure water in a grinder, filter through a sieve after grinding, if there is any problem that it does not pass through the sieve, grind it all again until it completely passes through the sieve; after it completely passes through the sieve, transfer the mixed liquid to a blender, pour the remaining 1 / 3 of pure water into the blender and stir and mix for 5-8 minutes, set a filter collector at the discharge end of the blender to filter and collect.

[0014] Compared with the prior art, the present application crushes, soaks, decolorizes and bleaches peach gum, thereby improving the transparency of peach gum liquid while ensuring its viscosity, which can effectively avoid the situation where traditional peach gum affects the ink color, thereby effectively replacing animal gelatin, and through emulsification and grinding operations, the carbon black particles and peach gum liquid are fully mixed to ensure that the carbon black particles are adhered, and the adhesion effect between particles and between particles and paper is guaranteed.

[0015] Preferably, the cleaning equipment in S1 includes a high-pressure bubble cleaning device and a drying machine; the cutting equipment includes a cutter, a vibrating screen and an elevator;

[0016] The peach gum surface cleaning operation comprises the following steps:

[0017] The first step is to put the peach gum into a high-pressure bubble cleaning device, which is distributed in multiple stages to achieve a cycle of soaking, cleaning, and draining.

[0018] In the second step, the drying machine is set at the end of the high-pressure bubble cleaning equipment. After the peach gum is scooped out and drained for the last time, it is transported to the conveyor belt of the drying machine. At the same time, the fan directly above the conveyor belt is operated to make the air flow downward to achieve drying;

[0019] The crushing operation includes the following steps: the dried peach gum is conveyed into the feed hopper of the cutter so as to be conveyed into the cutter for cutting operation; the peach gum cut into pieces is conveyed to the vibrating screen for screening; the qualified peach gum falls down; the unqualified peach gum is conveyed to the feed hopper of the cutter again through the elevator for cutting again.

[0020] Furthermore, through the operation of the above-mentioned cleaning equipment and cutting equipment, the peach gum can be effectively cleaned, its surface attachments can be removed, and the peach gum can be cut into uniform particles, so that it can fully contact with pure water during subsequent soaking, and it is also convenient to contact with corresponding reagents and react evenly, ensuring the consistency of the quality of the soaking liquid everywhere.

[0021] Preferably, adjusting the pH value of the soaking liquid in S2 comprises the following steps:

[0022] The first step is to add any one of N-methyl-2-pyrrolidone and ethylene glycol amine to the soaking solution to make the pH value between 9 and 10;

[0023] The second step is to add hydrogen peroxide solution to adjust the pH value to between 6-7.

[0024] Furthermore, the peach gum can be fully dissolved in pure water.

[0025] Preferably, the processing of the dissolved soaking liquid in S2 comprises the following steps: adding calcium hydroxide to completely dissolve it, adjusting the pH value to between 9 and 10 again, adding hydrogen peroxide solution and stirring.

[0026] Furthermore, the bleaching properties of calcium hydroxide can be used to remove the impurities in the peach gum and improve the transparency of the peach gum liquid.

[0027] Preferably, the fragrance is at least one of camphor oil, borneol powder and camphor powder;

[0028] The moisturizing agent is selected from at least one of Turkish red oil, cottonseed oil, rapeseed oil and glycerin;

[0029] The preservative is selected from at least one of borneol, camphor, chitosan, and plant extract preservatives;

[0030] The dispersant is an acrylic ester polymer dispersant.

[0031] Furthermore, by selecting the above-mentioned agents, it is ensured that the finished ink has a certain fragrance, has long-term fluidity and is easy to store for a long time, and can effectively prevent the colloid and ink particles therein from agglomerating, so as to facilitate better use.

[0032] Preferably, the mesh size of the sieve in S6 is 80-90 meshes, and the mesh size of the filter is 100-120 meshes.

[0033] Furthermore, the fluidity is fully ensured and the presence of large particles that affect the writing effect is avoided.

[0034] Preferably, the grinder in S6 is a ball mill, the rotation speed of the ball mill is 4000-5000 rpm, and the grinding time of the ball mill is 1-2 hours.

[0035] Furthermore, the grinding effect is ensured, and the subsequent mixing effect is ensured.

[0036] Preferably, the mass ratio of peach gum to pure water in S2 is 1:1.8-2.

[0037] Preferably, the mass ratio of the peach gum liquid, carbon black, fragrance, humectant, dispersant, defoamer, preservative and pure water is 1:0.8-1:0.05-0.1:0.05-0.1:0.02-0.05:0.01-0.02:0.01-0.02:5-10.

[0038] The beneficial effects of the present invention are:

[0039] 1. The present application can pre-treat peach gum, thereby improving the transparency of peach gum liquid while ensuring its viscosity, preventing peach gum liquid from affecting the display of ink color, and ensuring the viscosity between ink particles and between magic and paper, so as to effectively write and display;

[0040] 2. By adding corresponding agents, the quality of the finished ink is guaranteed, ensuring its long-term fluidity and long-term storage, and effectively preventing the colloid and ink particles from agglomerating, so as to facilitate better use;

[0041] 3. Through the operation of the above-mentioned cleaning equipment and cutting equipment, the peach gum can be effectively cleaned, its surface attachments can be removed, and the peach gum can be cut into uniform particles so that it can fully contact with pure water during subsequent soaking, and it is also convenient to contact with the corresponding reagents and react evenly, ensuring the consistency of the quality of the soaking liquid everywhere, which helps to improve the quality of the subsequent peach gum liquid. BRIEF DESCRIPTION OF THE DRAWINGS

[0042] Figure 1 The present invention is a flow chart of a preparation process of peach gum ink. DETAILED DESCRIPTION

[0043] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.

[0044] Reference Figure 1 A preparation process of peach gum ink comprises the following steps:

[0045] S1. Peach gum crushing and screening: The surface of peach gum is cleaned by cleaning equipment, and crushed by cutting equipment after cleaning. At the same time, the crushed peach gum is collected centrally to fully ensure the quality of raw materials for preparing peach gum liquid, starting from the source. At the same time, by ensuring the consistency of the particles after the peach gum is crushed, it helps to ensure that the reaction time of the particles is in the same time period, which can make the reaction more uniform and ensure the quality of the peach gum liquid.

[0046] S2. Peach gum processing: introduce the crushed peach gum into the blender and then add pure water to obtain the soaking liquid. The mass ratio of peach gum to pure water is 1:1.8-2, which can effectively and comprehensively soak the peach gum, and control the temperature of the soaking liquid between 60-70°, adjust the pH value of the soaking liquid and increase the solution temperature to between 75-80°, maintain the temperature until the peach gum is completely dissolved, and process the dissolved soaking liquid so that the solution can be filtered after standing and settling to obtain peach gum liquid.

[0047] S3, ink making material preparation: obtain carbon black, fragrance, moisturizing agent, dispersant, defoaming agent, preservative and pure water; the mass ratio of peach gum liquid, carbon black, fragrance, moisturizing agent, dispersant, defoaming agent, preservative and pure water is 1:0.8-1:0.05-0.1:0.05-0.1:0.02-0.05:0.01-0.02:0.01-0.02:5-10; through the precise ratio between the materials, it is used to ensure the glossiness and quality of the finished ink. After the preparation is completed , ensuring that the finished ink has a certain fragrance, can have long-term fluidity and is easy to store for a long time, and can effectively prevent the colloid and ink particles inside it from agglomerating, so that it can be better used; the fragrance agent is selected from at least one of camphor oil, borneol powder, and camphor powder; the moisturizer is selected from at least one of Turkish red oil, cottonseed oil, rapeseed oil and glycerin; the preservative is selected from at least one of borneol, camphor, chitosan, and plant extract preservatives; the dispersant is an acrylic polymer dispersant, and appropriate agents are selected as needed to improve the quality of the final ink.

[0048] S4. Ink-making material processing: The carbon black is crushed by a wall-breaking crusher; the crushing effect of the carbon black is improved so that the carbon black can be crushed into finer particles, which can better mix the carbon black particles with the peach gum liquid and the corresponding agents more evenly, and can ensure the quality of the ink, so that the quality of the ink is consistent everywhere when writing.

[0049] S5, ink mixing: start the emulsifier, pour 1 / 3 of water into the emulsifier and heat it to 75-85°, then pour the peach gum liquid prepared in S2 into the emulsifier, and then pour the crushed carbon black into it, and finally pour the fragrance, moisturizer, dispersant, defoamer and preservative in turn. The emulsifier generates strong shear force, impact force and cavitation effect through the high-speed rotation of built-in stirring paddles, homogenizers and other components, which fully disperse and mix the raw materials such as oil phase, water phase and active ingredients in a short time, and form a uniform and delicate emulsion, and continue stirring until an ink paste is formed.

[0050] S6. Prepare ink: grind the ink paste and 1 / 3 of pure water in a grinder, filter through a sieve after grinding, if there is any problem that it does not pass through the sieve, grind it all again until it completely passes through the sieve; after it completely passes through the sieve, transfer the mixed liquid to a blender, pour the remaining 1 / 3 of pure water into the blender and stir and mix for 5-8 minutes, set a filter collector at the discharge end of the blender to filter and collect.

[0051] In the present invention, the cleaning equipment in S1 includes a high-pressure bubble cleaning device and a drying machine; the cutting equipment includes a cutter, a vibrating screen and an elevator;

[0052] The surface cleaning operation of peach gum includes the following steps:

[0053] The first step is to put the peach gum into the high-pressure bubble cleaning equipment, which is distributed in multiple stages to achieve a cycle of soaking and cleaning - fishing out and draining. It adopts existing technical equipment, and can achieve an effective combination of cleaning and drying through the ingenious cooperation between the equipment. In addition, through the multi-stage distribution mode, it can perform a cycle of cleaning, draining, re-cleaning, and re-draining, which can improve the cleaning quality of the peach gum and ensure that there is no attachment on its surface;

[0054] In the second step, the drying machine is set at the end of the high-pressure bubble cleaning equipment. After the peach gum is taken out and drained for the last time, it is transported to the conveyor belt of the drying machine. At the same time, the fan directly above the conveyor belt is operated to make the air flow downward to achieve drying. It can effectively dry the peach gum. Unlike the traditional drying method that causes the water to evaporate, the drying method can effectively blow away the water attached to the surface, but it does not affect its essence, that is, the internal water content will not be affected;

[0055] The crushing operation includes the following steps: the dried peach gum is conveyed into the feed hopper of the cutter so as to be conveyed into the cutter for cutting operation; the peach gum cut into pieces is conveyed to the vibrating screen for screening; the qualified peach gum falls down; the unqualified peach gum is conveyed to the feed hopper of the cutter again through the elevator for cutting again; the desired cutting parts can be selected according to the needs, and the screening can be fully carried out to ensure the consistency between the final cut particles; through the consistency between the above-mentioned cut particles, the reaction conditions and reaction time of the peach gum particles can be more uniform when they react later.

[0056] In the present invention, adjusting the pH value of the soaking liquid in S2 comprises the following steps:

[0057] The first step is to add any one of N-methyl-2-pyrrolidone and ethylene glycol amine to the soaking solution to make the pH value between 9 and 10;

[0058] The second step is to add hydrogen peroxide solution to adjust the pH value to between 6-7.

[0059] After adjusting the pH value, the dissolved soaking liquid is processed in the following steps: adding calcium hydroxide to completely dissolve it, adjusting the pH value to between 9 and 10 again, adding hydrogen peroxide solution and stirring, which can effectively bleach the peach gum liquid, remove the color in the peach gum liquid, and improve its transparency, so as to effectively display the carbon black particles and improve the color brightness of the ink.

[0060] In the present invention, the mesh number of the screen in S6 is 80-90 meshes, and the mesh number of the filter is 100-120 meshes, which fully ensures the fluidity of the final ink for writing use.

[0061] In the present invention, the grinder in S6 adopts a ball mill, the rotation speed of the ball mill is 4000-5000 rpm, and the grinding time of the ball mill is 1-2 hours, which fully ensures the quality of the ball mill so that the carbon black particles, peach gum particles, and various additives can be evenly mixed, convenient for mutual connection and function.

[0062] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.

Claims

1. A preparation process of peach gum ink, characterized in that: The following steps are involved: S1. Peach gum crushing and screening: The surface of the peach gum is cleaned by a cleaning device, and after cleaning, the peach gum is crushed by a cutting device, and the crushed peach gum is collected centrally; S2, peach gum processing: the crushed peach gum is introduced into a blender and then purified water is added to obtain a soaking liquid, and the soaking liquid temperature is controlled between 60-70°, and the pH value of the soaking liquid is adjusted and the solution temperature is increased to between 75-80°, and the temperature is maintained until the peach gum is completely dissolved, and the dissolved soaking liquid is processed so that the solution is filtered after standing and settling to obtain peach gum liquid; S3, ink material preparation: obtain carbon black, aromatic agent, moisturizer, dispersant, defoamer, preservative and purified water; S4, ink material processing: crush the carbon black through a wall-breaking crusher; S5, ink mixing: start the emulsifier, pour 1 / 3 of water into the emulsifier and heat it to 75-85°, then pour the peach gum liquid prepared in S2 into the emulsifier, then pour the crushed carbon black into it, and finally pour the fragrance, moisturizer, dispersant, defoamer and preservative in turn, and stir well until the ink paste is formed; S6. Prepare ink: grind the ink paste and 1 / 3 of pure water in a grinder, filter through a sieve after grinding, if there is any problem that it does not pass through the sieve, grind it all again until it completely passes through the sieve; after it completely passes through the sieve, transfer the mixed liquid to a blender, pour the remaining 1 / 3 of pure water into the blender and stir and mix for 5-8 minutes, set a filter collector at the discharge end of the blender to filter and collect.

2. The preparation process of peach gum ink according to claim 1, characterized in that: The cleaning equipment in S1 includes a high-pressure bubble cleaning device and a drying machine; the cutting equipment includes a cutter, a vibrating screen and an elevator; The peach gum surface cleaning operation comprises the following steps: The first step is to put the peach gum into a high-pressure bubble cleaning device, which is distributed in multiple stages to achieve a cycle of soaking, cleaning, and draining. In the second step, the drying machine is set at the end of the high-pressure bubble cleaning equipment. After the peach gum is scooped out and drained for the last time, it is transported to the conveyor belt of the drying machine. At the same time, the fan directly above the conveyor belt is operated to make the air flow downward to achieve drying; The crushing operation includes the following steps: the dried peach gum is conveyed into the feed hopper of the cutter so as to be conveyed into the cutter for cutting operation; the peach gum cut into pieces is conveyed to the vibrating screen for screening; the qualified peach gum falls down; the unqualified peach gum is conveyed to the feed hopper of the cutter again through the elevator for cutting again.

3. The preparation process of peach gum ink according to claim 1, characterized in that: The step of adjusting the pH value of the soaking liquid in S2 comprises the following steps: The first step is to add any one of N-methyl-2-pyrrolidone and ethylene glycol amine to the soaking solution to make the pH value between 9 and 10; The second step is to add hydrogen peroxide solution to adjust the pH value to between 6-7.

4. The preparation process of peach gum ink according to claim 1, characterized in that: The processing of the dissolved soaking liquid in S2 includes the following steps: adding calcium hydroxide to completely dissolve it, adjusting the pH value to between 9 and 10 again, adding hydrogen peroxide solution and stirring.

5. The preparation process of peach gum ink according to claim 1, characterized in that: The aromatic agent is at least one of camphor oil, borneol powder and camphor powder; The moisturizing agent is selected from at least one of Turkish red oil, cottonseed oil, rapeseed oil and glycerin; The preservative is selected from at least one of borneol, camphor, chitosan, and plant-extracted preservatives; The dispersant is an acrylic ester polymer dispersant.

6. The preparation process of peach gum ink according to claim 1, characterized in that: The mesh number of the sieve in S6 is 80-90 meshes, and the mesh number of the filter is 100-120 meshes.

7. The preparation process of peach gum ink according to claim 1, characterized in that: The grinder in S6 is a ball mill, the rotation speed of the ball mill is 4000-5000 rpm, and the grinding time of the ball mill is 1-2 hours.

8. The preparation process of peach gum ink according to claim 1, characterized in that: The mass ratio of peach gum to pure water in S2 is 1:1.8-2.

9. The preparation process of peach gum ink according to claim 1, characterized in that: The mass ratio of the peach gum liquid, carbon black, aromatic agent, moisturizing agent, dispersant, defoaming agent, preservative and pure water is 1:0.8-1:0.05-0.1:0.05-0.1:0.02-0.05:0.01-0.02:0.01-0.02:5-10.