Synthesis method and system of copper oxide precursor product

Abstract

The invention discloses a synthesis method and system of a copper oxide precursor product, the change quantity of a PH value is collected, the corresponding maintenance time is defined based on the comparison of the change quantity of the PH value and the preset change quantity, the maintenance time is controlled, the PH value is continuously controlled, and the dynamic accuracy of the PH value is ensured. Further, if the holding time is longer than the preset holding time, extracting a mixed solution formed by the acidic waste etching solution and the sodium carbonate solution; the corresponding synthesis model is matched according to the content, the temperature system and the stirring system of the mixed solution, the overall consideration of the content, the temperature system and the stirring system of the mixed solution is compatible, multi-dimensional control of the content, the temperature system and the stirring system of the mixed solution is achieved, the accuracy of the synthesis model is guaranteed, the synthesis model is introduced, and the synthesis efficiency is improved. The synthesis model autonomously controls the synthesis of the mixed solution, and autonomously forms the copper oxide precursor product, thereby ensuring the autonomous control of the copper oxide precursor product.

Description

Technical Field

[0001] The present invention relates to the technical field of copper oxide precursor products, and in particular to a method and system for synthesizing a copper oxide precursor product. Background Art

[0002] With the development of science and technology, a large amount of strong acids such as hydrochloric acid and sulfuric acid, strong bases such as sodium hydroxide and sodium carbonate, and chemical raw materials such as volatile and irritating ammonia are often used in the production process of copper salts. In the prior art, in the common copper salt production process, steps such as raw material loading, product drying, and wastewater treatment are all assisted by equipment with a high degree of automation, which greatly reduces manual work. Only the reaction control step requires manual on-site intervention and processing, and the copper oxide precursor product cannot be formed. Summary of the invention

[0003] The purpose of the present invention is to overcome the shortcomings of the prior art. The present invention provides a method and system for synthesizing a copper oxide precursor product, wherein the temperature of water is controlled and stirred until the temperature of the water reaches a first preset temperature; a corresponding pH value is defined based on water, acidic etching waste liquid and sodium carbonate solution, and the pH value is between 6 and 6.5; the filling of acidic etching waste liquid and sodium carbonate solution is monitored in real time, the pH value is adjusted to 6.5, and maintained for a preset time; the change in the pH value is collected, and the corresponding maintenance time is defined based on the comparison between the change in the pH value and the preset change, thereby achieving control of the maintenance time, and continuously controlling the pH value to ensure the dynamic accuracy of the pH value.

[0004] Furthermore, if the holding time is greater than the preset holding time, the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution is extracted; the corresponding synthesis model is matched according to the content, temperature system and stirring system of the mixed liquid, which is compatible with the overall consideration of the content, temperature system and stirring system of the mixed liquid, and realizes multi-dimensional control of the content, temperature system and stirring system of the mixed liquid, thereby ensuring the accuracy of the synthesis model, and introducing a synthesis model, which independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product, thereby ensuring the independent control of the copper oxide precursor product.

[0005] The embodiment of the present invention provides a method for synthesizing a copper oxide precursor product, which is applied to the synthesis scenario of a copper oxide precursor product; The method for synthesizing the copper oxide precursor product comprises: Controlling the temperature of the water and stirring the water until the temperature of the water reaches a first preset temperature; Based on the corresponding pH values ​​defined for water, acidic etching waste liquid and sodium carbonate solution, the pH value is between 6 and 6.5; Real-time monitoring of the addition of acidic etching waste liquid and sodium carbonate solution, adjusting the pH value to 6.5 and maintaining it for a preset time; Collecting the change of pH value, and defining the corresponding maintenance time based on the comparison between the change of pH value and the preset change; If the holding time is greater than the preset holding time, the mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution is extracted; The corresponding synthesis model is matched according to the content of the mixed liquid, the temperature system and the stirring system. The synthesis model independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product.

[0006] Optionally, the step of controlling the temperature of the water and stirring the water until the temperature of the water reaches a first preset temperature includes: Collect water content; Match the corresponding control system based on the water content and the spatial volume of the reactor; In this control system, the water is temperature controlled and stirred, dynamically correlating the temperature and stirring rate; The temperature of the water is monitored in real time until the temperature of the water reaches a first preset temperature.

[0007] Optionally, the corresponding pH values ​​defined based on water, acidic etching waste liquid and sodium carbonate solution, the pH value is between 6 and 6.5, including: Freeze the space where the water is; Add acidic etching waste liquid and sodium carbonate solution to the space where the water is located; Dynamically mixing water, acidic etching waste liquid and sodium carbonate solution; The corresponding pH value is defined based on the dynamic mixing of water, acidic etching waste liquid and sodium carbonate solution.

[0008] Optionally, the real-time monitoring of the addition of acidic etching waste liquid and sodium carbonate solution, adjusting the pH value to 6.5, and maintaining it for a preset time, includes: Fixed-frame acid etching waste liquid and sodium carbonate solution filling; Real-time monitoring of the filling of acid etching waste liquid and sodium carbonate solution; With the addition of acidic etching waste liquid and sodium carbonate solution, the pH value was adjusted to 6.5; When the pH value is 6.5, maintain the preset time.

[0009] Optionally, the collecting the change in pH value and defining a corresponding maintenance time based on a comparison between the change in pH value and a preset change in pH value include: Real-time monitoring of pH value; Collect the change of pH value; The change amount of the associated pH value and the preset change amount; Compare the change in pH value with the preset change; The corresponding maintenance time is defined according to the comparison between the change amount of the pH value and the preset change amount.

[0010] Optionally, if the holding time is greater than a preset holding time, extracting a mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution, comprising: Freeze-frame maintenance time; Compare the holding time with the preset holding time; If the holding time is greater than the preset holding time, the pumping signal is collected.

[0011] Optionally, if the holding time is greater than a preset holding time, extracting a mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution, further comprising: Defining the pumping information according to the analysis of the pumping signal; Based on the liquid extraction information, extraction of the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution is triggered.

[0012] Optionally, the synthesis model corresponding to the content, temperature system and stirring system of the mixed solution is matched, and the synthesis model independently controls the synthesis of the mixed solution and independently forms a copper oxide precursor product, including: Real-time monitoring of the mixed solution; Collect the content of the mixed solution; The corresponding temperature system and stirring system are matched based on the components contained in the mixed liquid and the copper oxide precursor product.

[0013] Optionally, the method further includes matching a corresponding synthesis model according to the content, temperature system and stirring system of the mixed solution, wherein the synthesis model autonomously controls the synthesis of the mixed solution and autonomously forms a copper oxide precursor product: The content, temperature system and stirring system of the associated mixed liquid; A synthetic model matching the corresponding content, temperature system and stirring system of the mixed liquid; The synthesis model independently controls the synthesis of the mixed solution and independently forms the copper oxide precursor product.

[0014] In addition, an embodiment of the present invention further provides a synthesis system of a copper oxide precursor product, the synthesis system of the copper oxide precursor product comprising: A first temperature module, used for controlling the temperature of water and stirring the water until the temperature of the water reaches a first preset temperature; PH value module, used to define the corresponding PH value based on water, acidic etching waste liquid and sodium carbonate solution, the PH value is 6-6.5; Filling module, used to monitor the filling of acidic etching waste liquid and sodium carbonate solution in real time, adjust the pH value to 6.5, and maintain it for a preset time; A time module is used to collect the change of the pH value and define the corresponding maintenance time based on the comparison between the change of the pH value and the preset change; A mixing module, used for extracting a mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution if the holding time is greater than a preset holding time; The synthesis module is used to match the corresponding synthesis model according to the content of the mixed liquid, the temperature system and the stirring system. The synthesis model independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product.

[0015] In an embodiment of the present invention, the water is temperature-controlled and stirred by the method in the embodiment of the present invention until the temperature of the water reaches a first preset temperature; the corresponding pH value is defined based on water, acidic etching waste liquid and sodium carbonate solution, and the pH value is between 6 and 6.5; the filling of acidic etching waste liquid and sodium carbonate solution is monitored in real time, the pH value is adjusted to 6.5, and maintained for a preset time; the change in the pH value is collected, and the corresponding maintenance time is defined based on the comparison between the change in the pH value and the preset change, thereby achieving control of the maintenance time, and continuously controlling the pH value to ensure the dynamic accuracy of the pH value.

[0016] Furthermore, if the holding time is greater than the preset holding time, the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution is extracted; the corresponding synthesis model is matched according to the content, temperature system and stirring system of the mixed liquid, which is compatible with the overall consideration of the content, temperature system and stirring system of the mixed liquid, and realizes multi-dimensional control of the content, temperature system and stirring system of the mixed liquid, thereby ensuring the accuracy of the synthesis model, and introducing a synthesis model, which independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product, thereby ensuring the independent control of the copper oxide precursor product. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative work.

[0018] Figure 1 1 is a schematic flow chart of a method for synthesizing a copper oxide precursor product in an embodiment of the present invention; Figure 2 is a schematic flow chart of S11 in the method for synthesizing a copper oxide precursor product in an embodiment of the present invention; Figure 3 is a schematic flow diagram of S12 in the method for synthesizing a copper oxide precursor product in an embodiment of the present invention; Figure 4 is a schematic flow chart of S13 in the method for synthesizing a copper oxide precursor product in an embodiment of the present invention; Figure 5 is a schematic flow chart of S14 in the method for synthesizing a copper oxide precursor product in an embodiment of the present invention; Figure 6 is a schematic flow chart of S15 in the method for synthesizing a copper oxide precursor product in an embodiment of the present invention; Figure 7 is a schematic flow diagram of S16 in the method for synthesizing a copper oxide precursor product in an embodiment of the present invention; Figure 8 Schematic diagram of the structure of the synthesis system of the copper oxide precursor product in the embodiment of the present invention; Fig. 9 The figure is a hardware diagram of an electronic device according to an exemplary embodiment. DETAILED DESCRIPTION

[0019] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0020] See also Figures 1 to 9 , a method for synthesizing a copper oxide precursor product, which is applied to the synthesis scenario of the copper oxide precursor product; the method for synthesizing the copper oxide precursor product includes: Step S11: temperature controlling and stirring the water until the temperature of the water reaches a first preset temperature; Step S12: defining corresponding pH values ​​based on water, acidic etching waste liquid and sodium carbonate solution, wherein the pH value is between 6 and 6.5; Step S13: real-time monitoring of the addition of acidic etching waste liquid and sodium carbonate solution, adjusting the pH value to 6.5, and maintaining it for a preset time; Step S14: collecting the change of the pH value, and defining the corresponding maintenance time based on the comparison between the change of the pH value and the preset change; Step S15: if the holding time is greater than the preset holding time, extracting the mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution; Step S16: A corresponding synthesis model is matched according to the content, temperature system and stirring system of the mixed solution. The synthesis model autonomously controls the synthesis of the mixed solution and autonomously forms a copper oxide precursor product.

[0021] In an embodiment of the present invention, the water is temperature-controlled and stirred by the method in the embodiment of the present invention until the temperature of the water reaches a first preset temperature; the corresponding pH value is defined based on water, acidic etching waste liquid and sodium carbonate solution, and the pH value is between 6 and 6.5; the filling of acidic etching waste liquid and sodium carbonate solution is monitored in real time, the pH value is adjusted to 6.5, and maintained for a preset time; the change in the pH value is collected, and the corresponding maintenance time is defined based on the comparison between the change in the pH value and the preset change, thereby achieving control of the maintenance time, and continuously controlling the pH value to ensure the dynamic accuracy of the pH value.

[0022] Furthermore, if the holding time is greater than the preset holding time, the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution is extracted; the corresponding synthesis model is matched according to the content, temperature system and stirring system of the mixed liquid, which is compatible with the overall consideration of the content, temperature system and stirring system of the mixed liquid, and realizes multi-dimensional control of the content, temperature system and stirring system of the mixed liquid, thereby ensuring the accuracy of the synthesis model, and introducing a synthesis model, which independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product, thereby ensuring the independent control of the copper oxide precursor product.

[0023] refer to Figure 2 , in step S11, the water is temperature controlled and stirred until the temperature of the water reaches a first preset temperature; In the specific implementation process of the present invention, the specific steps may be: S111: Collect water content; S112: Matching a corresponding control system based on the water content and the spatial volume of the reactor; S113: In the control system, the water is temperature controlled and stirred, and the temperature and stirring rate are dynamically correlated; S114: Monitor the temperature of the water in real time until the temperature of the water reaches a first preset temperature.

[0024] In an embodiment of the present application, the water content is collected and controlled, so that a corresponding control system is matched based on the water content and the spatial volume of the reactor, which is compatible with the overall consideration of the water content and the spatial volume of the reactor and achieves the matching accuracy of the control system.

[0025] Therefore, in this management and control system, the water temperature is controlled and stirred, and the temperature and stirring rate are dynamically linked; the water temperature is monitored in real time until the water temperature reaches the first preset temperature, thereby realizing automatic control of the water temperature and being compatible with the temperature and stirring rate, so as to facilitate control under the temperature and stirring system.

[0026] refer to Figure 3 In step S12, the corresponding pH values ​​are defined based on water, acidic etching waste liquid and sodium carbonate solution, and the pH value is between 6 and 6.5; In the specific implementation process of the present invention, the specific steps may be: S121: Freeze the space where the water is located; S122: Adding acidic etching waste liquid and sodium carbonate solution into the space where the water is located; S123: dynamically mixing water, acidic etching waste liquid and sodium carbonate solution; S124: defining a corresponding pH value based on the dynamic mixing of water, acidic etching waste liquid and sodium carbonate solution.

[0027] In an embodiment of the present application, the space where the water is located is frozen and controlled, so that the space where the water is located is filled with acidic etching waste liquid and sodium carbonate solution, and the acidic etching waste liquid and sodium carbonate solution are introduced to realize the interaction of water, acidic etching waste liquid and sodium carbonate solution.

[0028] Therefore, water, acidic etching waste liquid and sodium carbonate solution are dynamically mixed; the corresponding pH value is defined based on the dynamic mixing of water, acidic etching waste liquid and sodium carbonate solution, thereby realizing the dynamic mixing of water, acidic etching waste liquid and sodium carbonate solution, ensuring the dynamic control of pH value, and controlling the dynamic mixing of water, acidic etching waste liquid and sodium carbonate solution.

[0029] refer to Figure 4 , in step S13, the filling of the acidic etching waste liquid and the sodium carbonate solution is monitored in real time, the pH value is adjusted to 6.5, and maintained for a preset time; In the specific implementation process of the present invention, the specific steps may be: S131: Fixed-grid acid etching waste liquid and sodium carbonate solution filling; S132: real-time monitoring of the filling of acidic etching waste liquid and sodium carbonate solution; S133: With the addition of acidic etching waste liquid and sodium carbonate solution, the pH value is adjusted to 6.5; S134: When the pH value is 6.5, maintain the preset time.

[0030] In the embodiments of the present application, the filling of the acidic etching waste liquid and the sodium carbonate solution is fixed, and the filling of the acidic etching waste liquid and the sodium carbonate solution is monitored in real time, thereby ensuring the real-time monitoring of the filling of the acidic etching waste liquid and the sodium carbonate solution.

[0031] Therefore, with the addition of acidic etching waste liquid and sodium carbonate solution, the pH value is adjusted to 6.5; when the pH value is 6.5, it is maintained for the preset time, thereby achieving precise control of the pH value and control of the maintenance time period.

[0032] refer to Figure 5 , S14: collecting the change of the pH value, and defining the corresponding maintenance time based on the comparison between the change of the pH value and the preset change; In the specific implementation process of the present invention, the specific steps may be: S141: real-time monitoring of pH value; S142: Collecting the change of pH value; S143: Correlate the change amount of the pH value with the preset change amount; S144: comparing the change in pH value with a preset change; S145: defining a corresponding maintenance time according to a comparison between the change amount of the pH value and a preset change amount.

[0033] In an embodiment of the present application, the water is temperature-controlled and stirred until the temperature of the water reaches a first preset temperature; corresponding pH values ​​are defined based on water, acidic etching waste liquid and sodium carbonate solution, and the pH value is between 6 and 6.5; the filling of acidic etching waste liquid and sodium carbonate solution is monitored in real time, the pH value is adjusted to 6.5, and maintained for a preset time; the change in the pH value is collected, and the corresponding maintenance time is defined based on the comparison between the change in the pH value and the preset change, thereby achieving control of the maintenance time, and continuously controlling the pH value to ensure the dynamic accuracy of the pH value.

[0034] At this time, the pH value is monitored in real time; the change in the pH value is collected, the change in the pH value is introduced, and the change in the pH value is controlled.

[0035] At the same time, the change in pH value and the preset change are associated; the change in pH value and the preset change are compared; the corresponding maintenance time is defined according to the comparison between the change in pH value and the preset change, thereby achieving control of the maintenance time and continuously controlling the pH value to ensure the dynamic accuracy of the pH value.

[0036] refer to Figure 6 , S15: if the holding time is greater than the preset holding time, extracting the mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution; In the specific implementation process of the present invention, the specific steps may be: S151: freeze frame maintenance time; S152: Compare the maintenance time with the preset maintenance time; S153: If the holding time is greater than the preset holding time, collecting the liquid extraction signal; S154: defining the liquid extraction information according to the analysis of the liquid extraction signal; S155: triggering the extraction of the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution based on the liquid extraction information.

[0037] In the embodiments of the present application, the maintenance time is frozen, the maintenance time is introduced, the maintenance time is controlled, and the maintenance time is compared with the preset maintenance time, thereby realizing the comparison between the maintenance time and the preset maintenance time.

[0038] Therefore, if the holding time is greater than the preset holding time, the liquid extraction signal is collected; the liquid extraction information is defined based on the analysis of the liquid extraction signal; based on the liquid extraction information, the extraction of the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution is triggered, thereby ensuring the extraction of the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution.

[0039] refer to Figure 7 , S16: matching a corresponding synthesis model according to the content, temperature system and stirring system of the mixed solution, the synthesis model autonomously controls the synthesis of the mixed solution and autonomously forms a copper oxide precursor product; In the specific implementation process of the present invention, the specific steps may be: S161: real-time monitoring of the mixed solution; S162: Collect the content of the mixed solution; S163: matching a corresponding temperature system and a stirring system based on the components contained in the mixed solution and the copper oxide precursor product; S164: associating the content, temperature system and stirring system of the mixed liquid; S165: Matching the corresponding synthesis model based on the content of the mixed liquid, the temperature system and the stirring system; S166: This synthesis model autonomously controls the synthesis of the mixed solution and autonomously forms the copper oxide precursor product.

[0040] During the specific implementation of the present invention, if the holding time is greater than the preset holding time, the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution is extracted; the corresponding synthesis model is matched according to the content, temperature system and stirring system of the mixed liquid, which is compatible with the overall consideration of the content, temperature system and stirring system of the mixed liquid, and realizes multi-dimensional control of the content, temperature system and stirring system of the mixed liquid, thereby ensuring the accuracy of the synthesis model, and introducing a synthesis model, which autonomously controls the synthesis of the mixed liquid and autonomously forms a copper oxide precursor product, thereby ensuring autonomous control of the copper oxide precursor product.

[0041] At this time, the mixed liquid is monitored in real time and controlled to collect the content of the mixed liquid; based on the components contained in the mixed liquid and the copper oxide precursor product, the corresponding temperature system and stirring system are matched, which is compatible with the overall consideration of the components contained in the mixed liquid and the copper oxide precursor product, and realizes multi-dimensional control of the components contained in the mixed liquid and the copper oxide precursor product, ensuring the accuracy of the temperature system and the stirring system.

[0042] Therefore, the content, temperature system and stirring system of the mixed liquid are correlated; the corresponding synthesis model is matched based on the content, temperature system and stirring system of the mixed liquid, which is compatible with the overall consideration of the content, temperature system and stirring system of the mixed liquid, realizes the multi-dimensional control of the content, temperature system and stirring system of the mixed liquid, and ensures the accuracy of the synthesis model.

[0043] The synthesis model independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product. A synthesis model is introduced. The synthesis model independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product, ensuring independent control of the copper oxide precursor product.

[0044] Specifically, in the synthesis method of the copper oxide precursor product, copper carbonate is prepared by using acidic etching waste liquid and 30% sodium carbonate solution as raw materials; Step 1: The main control chip sends a command to the pump control module to use the feed pump to deliver water until the low liquid level switch level changes. After receiving the command, the pump control module adds water to the low liquid level switch. The low liquid level switch level changes, and the pump control module stops the feed pump and returns the result of the execution completion command to the main control chip.

[0045] Step 2: After receiving the result of water injection completion, the main control chip sends a command to the heating and stirring module to heat the water at 400 rpm until the water temperature reaches 60°C. After the water temperature reaches 60°C, the stirring does not stop, the heating module stops heating and returns the execution completion command result to the main control chip, and the first reaction step is completed.

[0046] Step 3: After receiving the result returned by the heating chip, the main control chip sends a command to the pump control chip to start the peristaltic pumps for the acidic waste liquid and sodium carbonate solution, maintain the pH value at 6-6.5, and stop after the solution is added to the high liquid level pump. Send a command to the heating and stirring control module to maintain the temperature at 55-65 degrees Celsius. After receiving the command, the pump control chip uses pwm to control the feeding speed of the peristaltic pump. After receiving the command, the heating and stirring control chip uses a relay to control the switch of the heating wire. When the high liquid level switch level changes, the pump control module stops the peristaltic pump from feeding and returns the result of the execution completion command to the main control chip.

[0047] Step 4: The main control chip receives the return result from the pump control module and sends a command to the pump control module to adjust the pH value to 6.5 and maintain it for 20 minutes.

[0048] Step 5: The pump control module controls the peristaltic pump to add material at 0 or 10% of the maximum flow rate, and adjusts the pH value to 6.5. After the pH value stops changing, the chip's built-in clock or external clock module is used to time 15 minutes, and the pH value change does not exceed ±0.1. After exceeding the limit, readjust and re-time. After the pH value is maintained for 15 minutes, the execution instruction completion result is returned to the main control chip.

[0049] Step six, after receiving the result returned by the pump control module, the main control chip sends an instruction to the heating and stirring module to stop stirring and heating. The heating and stirring control module stops stirring and heating after receiving the instruction, and returns the instruction completion result to the main control chip.

[0050] Step 7: The main control chip receives the result returned by the heating and stirring control module, sends a command to the pump control chip, and the discharge pump runs until the discharge is completed. The pump control chip controls the discharge diaphragm pump to run, and starts timing after the low liquid level switch level changes. The timing time is After the timing is completed, the pump control module stops the discharge pump and returns the instruction execution result to the main control chip.

[0051] Step 8: The main control chip receives the completion instruction and the reaction process is completed.

[0052] In an embodiment of the present invention, the water is temperature-controlled and stirred by the method in the embodiment of the present invention until the temperature of the water reaches a first preset temperature; the corresponding pH value is defined based on water, acidic etching waste liquid and sodium carbonate solution, and the pH value is between 6 and 6.5; the filling of acidic etching waste liquid and sodium carbonate solution is monitored in real time, the pH value is adjusted to 6.5, and maintained for a preset time; the change in the pH value is collected, and the corresponding maintenance time is defined based on the comparison between the change in the pH value and the preset change, thereby achieving control of the maintenance time, and continuously controlling the pH value to ensure the dynamic accuracy of the pH value.

[0053] Furthermore, if the holding time is greater than the preset holding time, the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution is extracted; the corresponding synthesis model is matched according to the content, temperature system and stirring system of the mixed liquid, which is compatible with the overall consideration of the content, temperature system and stirring system of the mixed liquid, and realizes multi-dimensional control of the content, temperature system and stirring system of the mixed liquid, thereby ensuring the accuracy of the synthesis model, and introducing a synthesis model, which independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product, thereby ensuring the independent control of the copper oxide precursor product.

[0054] See also Figure 8 , Figure 8 It is a schematic diagram of the structural composition of the synthesis system of the copper oxide precursor product in an embodiment of the present invention.

[0055] like Figure 8 As shown, a synthesis system of a copper oxide precursor product, the synthesis system of the copper oxide precursor product comprises: The first temperature module 21 is used to control the temperature of water and stir it until the temperature of the water reaches a first preset temperature; A pH value module 22 is used to define corresponding pH values ​​based on water, acidic etching waste liquid and sodium carbonate solution, and the pH value is between 6 and 6.5; A filling module 23 is used to monitor the filling of acidic etching waste liquid and sodium carbonate solution in real time, adjust the pH value to 6.5, and maintain it for a preset time; A time module 24 is used to collect the change of the pH value and define a corresponding maintenance time based on the comparison between the change of the pH value and a preset change; A mixing module 25, for extracting a mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution if the holding time is greater than a preset holding time; The synthesis module 26 is used to match the corresponding synthesis model according to the content, temperature system and stirring system of the mixed solution. The synthesis model independently controls the synthesis of the mixed solution and independently forms a copper oxide precursor product.

[0056] See also Fig. 9 , refer to the following Fig. 9 The electronic device 40 according to this embodiment of the present invention will be described. Fig. 9 The electronic device 40 shown is only an example and should not bring any limitation to the functions and scope of use of the embodiments of the present invention.

[0057] like Fig. 9As shown, the electronic device 40 is in the form of a general computing device. The components of the electronic device 40 may include but are not limited to: at least one processing unit 41, at least one storage unit 42, and a bus 43 connecting different system components (including the storage unit 42 and the processing unit 41).

[0058] The storage unit stores program codes, which can be executed by the processing unit 41, so that the processing unit 41 executes the steps according to various exemplary embodiments of the present invention described in the above “Embodiment Method” section of this specification.

[0059] The storage unit 42 may include a readable medium in the form of a volatile storage unit, such as a random access memory unit (RAM) 421 and / or a cache memory unit 422 , and may further include a read-only memory unit (ROM) 423 .

[0060] The storage unit 42 may also include a program / utility 424 having a set (at least one) of program modules 425, such program modules 425 including but not limited to: an operating system, one or more application programs, other program modules, and program data, each of which or some combination may include an implementation of a network environment.

[0061] Bus 43 may represent one or more of several types of bus structures, including a memory unit bus or memory unit controller, a peripheral bus, an accelerated graphics port, a processing unit, or a local bus using any of a variety of bus architectures.

[0062] The electronic device 40 may also communicate with one or more external devices (e.g., keyboards, pointing devices, Bluetooth devices, etc.), one or more devices that enable a user to interact with the electronic device 40, and / or any device that enables the electronic device 40 to communicate with one or more other computing devices (e.g., routers, modems, etc.). Such communication may be performed via an input / output (I / O) interface 44. Furthermore, the electronic device 40 may also communicate with one or more networks (e.g., a local area network (LAN), a wide area network (WAN), and / or a public network, such as the Internet) via a network adapter 45. Fig. 9 As shown, the network adapter 45 communicates with other modules of the electronic device 40 via the bus 43. It should be understood that although Fig. 9 Not shown, other hardware and / or software modules may be used in conjunction with the electronic device 40, including but not limited to: microcode, device drivers, redundant processing units, external disk drive arrays, RAID systems, tape drives, and data backup planning systems.

[0063] Through the description of the above implementation, it is easy for those skilled in the art to understand that the example implementation described here can be implemented by software, or by software combined with necessary hardware. Therefore, the technical solution according to the implementation of the present disclosure can be embodied in the form of a software product, which can be stored in a non-volatile storage medium (which can be a CD-ROM, a USB flash drive, a mobile hard disk, etc.) or on a network, and includes a number of instructions to enable a computing device (which can be a personal computer, a server, a terminal device, or a network device, etc.) to execute the method according to the implementation of the present disclosure.

[0064] Those skilled in the art can understand that all or part of the steps in the various methods of the above embodiments can be completed by instructing related hardware through a program, and the program can be stored in a computer-readable storage medium, and the storage medium can include: a read-only memory (ROM), a random access memory (RAM), a disk or an optical disk, etc. In addition, it stores computer program instructions, and when the computer program instructions are executed by a computer, the computer executes the above method.

[0065] In addition, the above is a detailed introduction to the synthesis method and system of the copper oxide precursor product provided in the embodiment of the present invention. Specific examples are used herein to illustrate the principle and implementation mode of the present invention. The description of the above embodiments is only used to help understand the method of the present invention and its core idea. At the same time, for those skilled in the art, according to the idea of ​​the present invention, there will be changes in the specific implementation mode and application scope. In summary, the content of this specification should not be understood as limiting the present invention.

Claims

1. A method for synthesizing a copper oxide precursor product, characterized in that: Applied to the synthesis scenario of copper oxide precursor products; The method for synthesizing the copper oxide precursor product comprises: Controlling the temperature of the water and stirring the water until the temperature of the water reaches a first preset temperature; Based on the corresponding pH values ​​defined for water, acidic etching waste liquid and sodium carbonate solution, the pH value is between 6 and 6.5; Real-time monitoring of the addition of acidic etching waste liquid and sodium carbonate solution, adjusting the pH value to 6.5 and maintaining it for a preset time; Collecting the change of pH value, and defining the corresponding maintenance time based on the comparison between the change of pH value and the preset change; If the holding time is greater than the preset holding time, the mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution is extracted; The corresponding synthesis model is matched according to the content of the mixed liquid, the temperature system and the stirring system. The synthesis model independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product.

2. The method for synthesizing the copper oxide precursor product according to claim 1, characterized in that: The step of controlling the temperature of the water and stirring the water until the temperature of the water reaches a first preset temperature comprises: Collect water content; Match the corresponding control system based on the water content and the spatial volume of the reactor; In this control system, the water is temperature controlled and stirred, dynamically correlating the temperature and stirring rate; The temperature of the water is monitored in real time until the temperature of the water reaches a first preset temperature.

3. The method for synthesizing the copper oxide precursor product according to claim 1, characterized in that: The pH value corresponding to the pH value defined based on water, acidic etching waste liquid and sodium carbonate solution is 6-6.5, including: Freeze the space where the water is; Add acidic etching waste liquid and sodium carbonate solution to the space where the water is located; Dynamically mixing water, acidic etching waste liquid and sodium carbonate solution; The corresponding pH value is defined based on the dynamic mixing of water, acidic etching waste liquid and sodium carbonate solution.

4. The method for synthesizing the copper oxide precursor product according to claim 3, characterized in that: The method of real-time monitoring the addition of acidic etching waste liquid and sodium carbonate solution, adjusting the pH value to 6.5, and maintaining the pH value for a preset time includes: Fixed-frame acid etching waste liquid and sodium carbonate solution filling; Real-time monitoring of the filling of acid etching waste liquid and sodium carbonate solution; With the addition of acidic etching waste liquid and sodium carbonate solution, the pH value was adjusted to 6.5; When the pH value is 6.5, maintain the preset time.

5. The method for synthesizing the copper oxide precursor product according to claim 4, characterized in that: The collecting the change of the pH value and defining the corresponding maintenance time based on the comparison between the change of the pH value and the preset change include: Real-time monitoring of pH value; Collect the change of pH value; The change amount of the associated pH value and the preset change amount; Compare the change in pH value with the preset change; The corresponding maintenance time is defined according to the comparison between the change amount of the pH value and the preset change amount.

6. The method for synthesizing the copper oxide precursor product according to claim 5, characterized in that: If the holding time is greater than the preset holding time, extracting the mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution, comprising: Freeze hold time; Compare the holding time with the preset holding time; If the holding time is greater than the preset holding time, the pumping signal is collected.

7. The method for synthesizing a copper oxide precursor product according to claim 6, characterized in that: If the holding time is greater than the preset holding time, the mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution is extracted, and the method further comprises: Defining the pumping information according to the analysis of the pumping signal; Based on the liquid extraction information, extraction of the mixed liquid formed by the acidic etching waste liquid and the sodium carbonate solution is triggered.

8. The method for synthesizing a copper oxide precursor product according to claim 7, characterized in that: The synthesis model corresponding to the content, temperature system and stirring system of the mixed solution is matched, and the synthesis model independently controls the synthesis of the mixed solution and independently forms a copper oxide precursor product, including: Real-time monitoring of the mixed solution; Collect the content of the mixed solution; The corresponding temperature system and stirring system are matched based on the components contained in the mixed liquid and the copper oxide precursor product.

9. The method for synthesizing a copper oxide precursor product according to claim 8, characterized in that: The method further includes matching a corresponding synthesis model according to the content, temperature system and stirring system of the mixed solution, wherein the synthesis model autonomously controls the synthesis of the mixed solution and autonomously forms a copper oxide precursor product. The content, temperature system and stirring system of the associated mixed liquid; A synthetic model matching the corresponding content, temperature system and stirring system of the mixed liquid; The synthesis model independently controls the synthesis of the mixed solution and independently forms the copper oxide precursor product.

10. A synthesis system of a copper oxide precursor product, characterized in that: The synthesis system of the copper oxide precursor product is applied to the synthesis method of the copper oxide precursor product as claimed in any one of claims 1 to 9, and the synthesis system of the copper oxide precursor product comprises: A first temperature module, used for controlling the temperature of water and stirring the water until the temperature of the water reaches a first preset temperature; PH value module, used to define the corresponding PH value based on water, acidic etching waste liquid and sodium carbonate solution, the PH value is 6-6.5; Filling module, used to monitor the filling of acidic etching waste liquid and sodium carbonate solution in real time, adjust the pH value to 6.5, and maintain it for a preset time; A time module is used to collect the change of the pH value and define the corresponding maintenance time based on the comparison between the change of the pH value and the preset change; A mixing module, used for extracting a mixed solution formed by the acidic etching waste liquid and the sodium carbonate solution if the holding time is greater than a preset holding time; The synthesis module is used to match the corresponding synthesis model according to the content of the mixed liquid, the temperature system and the stirring system. The synthesis model independently controls the synthesis of the mixed liquid and independently forms a copper oxide precursor product.

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