Monitoring and sampling device for lithium hexafluorophosphate

By configuring a sampling mechanism and a common conveying mechanism on each reaction tank, synchronous automated sampling of lithium hexafluorophosphate sampling device is achieved, and the problem of difficulty in sampling multiple reaction tanks is solved, which improves work efficiency and safety and reduces equipment costs.

CN120254316AActive Publication Date: 2025-07-04DUOFU DUOYANGFU NEW MATERIAL CO LTD
View PDF 10 Cites 0 Cited by

Patent Information

Application Number
CN202510717325.X
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-05-30
Publication Date
2025-07-04
Estimated Expiration
2045-05-30

AI Technical Summary

Technical Problem

The existing lithium hexafluorophosphate sampling equipment cannot achieve synchronous sampling of multiple reaction tanks, resulting in large manual burdens, high sample loss and high risk of personnel injury, and is not suitable for small workshop configurations.

Method used

A sampling mechanism is arranged on each reaction tank, and a common conveying mechanism and sample temporary storage assembly are set below the multiple sampling mechanisms. The driving mechanism realizes automatic switching of sample vials and the opening and operation of the sampling mechanism, so as to realize the synchronization of multiple reaction tanks and automatic material sampling.

Benefits of technology

Reduce labor burden, improve work efficiency, ensure personnel safety, ensure the authenticity and accuracy of samples, reduce equipment costs, and facilitate the promotion and application of small workshops.

✦ Generated by Eureka AI based on patent content.

Smart Images

  • Figure CN120254316A_ABST
    Figure CN120254316A_ABST
Patent Text Reader

Abstract

The invention discloses a monitoring and sampling device for lithium hexafluorophosphate, and belongs to the technical field of lithium hexafluorophosphate sampling. Aiming at the problem that a plurality of reaction tanks are difficult to sample synchronously in the existing product, the invention provides the following technical scheme: the device comprises a plurality of reaction parts which are distributed linearly, each reaction part comprises a reaction tank and a stirring mechanism, and each reaction tank is provided with a sampling mechanism for sampling materials. According to the invention, each reaction tank is provided with a sampling mechanism, a common conveying mechanism is arranged below the plurality of sampling mechanisms, and corresponding sample temporary storage assemblies are arranged, so that each corresponding sample temporary storage assembly can be progressively conveyed through the conveying mechanism under the action of the driving mechanism, and the sample temporary storage assemblies can be continuously conveyed through the conveying mechanism. The sampling mechanism is started to operate on one side, so that synchronous and automatic material sampling is performed on a plurality of reaction tanks, the working efficiency is improved, each sample temporary storage assembly and each sampling mechanism can be independently and manually operated, and single sampling inspection is facilitated.
Need to check novelty before this filing date? Find Prior Art

Description

Technical Field

[0001] The present invention relates to the technical field of lithium hexafluorophosphate sampling, and specifically to a monitoring and sampling device for lithium hexafluorophosphate. Background Art

[0002] Lithium hexafluorophosphate is an inorganic compound, which is a white crystalline powder, soluble in water, and soluble in organic solvents such as low-concentration methanol, ethanol, acetone, and carbonate esters. It is mainly used as an electrolyte material for lithium-ion batteries. During the production process of lithium hexafluorophosphate, it is necessary to monitor and sample its reaction process and purification process.

[0003] Currently, the existing sampling methods include manual sampling and intelligent sampling. Among them, the equipment cost of intelligent sampling and the requirements for control programs are relatively high, which is not suitable for the configuration of small workshops. Manual sampling places a heavy burden on workers, and since lithium hexafluorophosphate is easily decomposed when in contact with air during the sampling process, the sampling operation is rather troublesome. For example: A Chinese patent with the authorization announcement number CN216847033U discloses a lithium hexafluorophosphate detection and sampling device, which includes a packaging barrel and a sampling tube connected to the bottom thereof. A sampling bottle is arranged below the sampling tube. A stirring shaft is rotatably arranged vertically in the packaging barrel, and stirring plates are arranged circumferentially at the bottom of the stirring shaft. A transfer box is hermetically sleeved on the lower part of the sampling tube, and sampling bottles can be detachably arranged on both sides of the bottom of the transfer box. A sealing plug is hermetically slidably connected in the sampling tube.

[0004] Although the technical solution in the above patent document simplifies the sampling steps, it can only sample the materials in a single reaction tank. When facing the sampling operations of multiple reaction tanks in a workshop, it is impossible to quickly sample multiple reaction tanks simultaneously, making it difficult to ensure that each sample truly reflects the real situation of the materials in the corresponding reaction tank under the same period conditions. Moreover, the sampling operations of multiple reaction tanks place a heavy burden on workers, and frequent sampling operations are extremely likely to result in sampling failures, causing losses of samples and injuries to personnel. Summary of the Invention

[0005] In order to overcome the above-mentioned defects of the prior art, the present invention provides a monitoring and sampling device for lithium hexafluorophosphate. By configuring a sampling mechanism on each reaction tank, then arranging a shared conveying mechanism below multiple sampling mechanisms, and configuring a corresponding sample temporary storage component, under the action of a driving mechanism, the sample temporary storage components can be progressively conveyed through the conveying mechanism while the sampling mechanisms are opened and operated, so as to automatically switch the sample bottles, and at the same time, the sampling mechanisms are opened and operated, thereby realizing synchronous and automated material sampling of multiple reaction tanks, reducing the manual burden, improving work efficiency, ensuring personnel safety, and each sample temporary storage component and sampling mechanism can be individually manually operated, thus facilitating individual inspections to solve the problems raised in the above background art.

[0006] To achieve the above object, the present invention provides the following technical solutions: A monitoring and sampling device for lithium hexafluorophosphate includes a plurality of linearly distributed reaction components. The reaction components include reaction tanks and stirring mechanisms. A sampling mechanism for material sampling is installed on each reaction tank. A sample temporary storage component for temporarily storing samples is provided below the sampling mechanism. A conveying mechanism for transporting the sample temporary storage component is jointly provided below the plurality of sampling mechanisms. An inflation mechanism for gas filling and a liquid pumping mechanism for liquid suction are also installed on the conveying component; The conveying mechanism includes a conveying component and a driving mechanism. Among them, the conveying component includes a frame serving as a bearing structure. A conveying member for transporting the sample temporary storage component and a pushing member for adjusting the sampling mechanism are installed on the frame. The driving mechanism includes a motor provided on the conveying component. A half gear is installed at the output end of the motor. A driven gear for driving the conveying member is provided on the front side of the half gear. A transmission gear is installed on the rear side of the half gear through a transmission shaft. A disc is provided at the right end of the transmission shaft. A moving plate is movably connected to the right side of the disc. A fixed rod is installed on the side wall of the moving plate. A driving wedge block for driving the pushing member is fixedly connected to the rear end of the fixed rod; The sampling mechanism includes a shunt member provided on the reaction tank. A vertical component is installed on the shunt member. An adjusting component is movably sleeved on the vertical component. An air inlet pipe is provided on the adjusting component. A gas check valve and a liquid suction pipe located on the vertical component are provided above the adjusting component.

[0007] As a further aspect of the present invention, the reaction tank includes a tank body for material reaction. A tank cover is installed at the top of the tank body through bolts. The stirring mechanism includes a stirring motor fixedly connected to the tank cover through bolts. A stirring shaft extending into the tank body is installed at the output end of the stirring motor. A hole for installing the sampling mechanism is provided on the peripheral wall of the tank body.

[0008] As a further aspect of the present invention, the shunt member includes a shunt pipe provided in the hole. An end cover is threadedly connected to the top of the shunt pipe. A round hole is provided at the center of the end cover. An adjusting rod is movably connected in the round hole. The bottom end of the adjusting rod is located inside the shunt pipe and is provided with a plug for blocking. The top end of the adjusting rod is located outside the shunt pipe and is provided with a movable member through bolts. A return spring located on the adjusting rod is sleeved between the plug and the end cover; The vertical component includes a slot formed in the shunt pipe. The vertical component includes a first vertical pipe disposed in the slot. A second vertical pipe is provided directly below the first vertical pipe. Among them, the first vertical pipe and the second vertical pipe are connected by an arc-shaped plate group. A base ring is integrally provided on the outer circumference of the bottom end of the second vertical pipe. A moving ring located on the second vertical pipe is sleeved above the base ring. Two pressing rods are installed at the bottom of the moving ring. A through hole located on the base ring is formed below each pressing rod. The bottom ends of the plurality of pressing rods respectively penetrate through the corresponding through holes and are installed with a traction member. Among them, an extrusion spring is sleeved on each pressing rod. The top of the extrusion spring is disposed on the bottom shell wall of the moving ring, and the bottom of the extrusion spring is disposed on the top shell wall of the base ring; The traction member includes a steering wheel and a lifting member. Among them, the steering wheel is disposed on the bottom shell wall of the base ring through a straight plate group. The lifting member is slidably connected to the bottom shell wall of the base ring. A traction belt is wound around the steering wheel. One end of the traction belt is bound to the lifting member, and the other end of the traction belt is disposed on the corresponding pressing rod; A connection hole and an installation hole located on the first vertical pipe are formed above the adjustment component. The gas check valve is disposed in the installation hole. The liquid extraction pipe is disposed in the connection hole, and a control valve is further provided on the liquid extraction pipe.

[0009] As a further solution of the present invention, the adjustment component includes a pipe body sleeved on the first vertical pipe. A fixed ring for pressing the moving ring is integrally provided on the outer circumference of the bottom end of the pipe body. A vertical plate is provided above the fixed ring on the outer shell wall of the pipe body. An inclined slot is formed in the vertical plate. A push-pull member is slidably connected in the inclined slot. A guiding member is slidably connected to the push-pull member. The bottom of the guiding member is fixedly connected to the conveying component. The push-pull member and the movable member are also slidably connected; An air inlet pipe is installed in a notch formed in the peripheral wall of the pipe body. Sealing rings for improving the sealing performance are provided on the inner circles of the top and bottom of the pipe body.

[0010] As a further solution of the present invention, the frame includes a bottom plate. Side plates are welded to the front and rear sides of the bottom plate. A cross plate located between the two side plates is provided above the bottom plate. The cross plate is used to carry the sample temporary storage component, and a rectangular through slot is formed in the cross plate; The conveying member is located between the bottom plate and the cross plate. The conveying member includes two movable rollers and a conveyor belt. Among them, the two movable rollers are respectively disposed on the inner walls of the corresponding side plates through carrier frames. The two movable rollers are connected by the conveyor belt. A plurality of bases are equidistantly arranged on the outer surface of the conveyor belt. A push top plate is movably connected to each base through a pin shaft. Among them, a torsion spring for resetting and adjusting the push top plate is also sleeved on the pin shaft. A groove is formed in each side plate.

[0011] As a further aspect of the present invention, the pushing member includes a sliding plate slidably connected to the groove. A contact rod for pushing the sampling mechanism is arranged between the two sliding plates. Bent rods are installed on the outer walls of each sliding plate. The two bent rods are connected by a driven wedge block. The driven wedge block is slidably connected to the top shell wall of the bottom plate, and the inclined surface of the driven wedge block is in sliding contact with the inclined surface of the active wedge block.

[0012] As a further aspect of the present invention, the sample temporary storage assembly includes a carrier plate placed on the cross plate. A convex block is integrally arranged at the center of the bottom of the carrier plate. The bottom of the convex block penetrates through the rectangular through groove and contacts the corresponding push top plate. A plurality of placement frames are linearly distributed on the top of the carrier plate, and sample bottles for temporarily storing samples are placed in the placement frames; The sample bottle includes a bottle body placed in the placement frame. A sealing member is installed at the bottle mouth of the bottle body. The sealing member includes a sealing cover box threadedly connected to the bottle mouth of the bottle body. An accommodation chamber is opened inside the sealing cover box. Cavities are opened on the inner walls on both sides of the accommodation chamber. Round rods are arranged in the cavities. Sealing baffles for plugging are symmetrically arranged left and right in the accommodation chamber. Sliders movably connected to the corresponding round rods are installed on the front and rear sides of each sealing baffle. Return springs located on the corresponding round rods are sleeved on the side walls of each slider; One side of the two sealing baffles away from each other respectively penetrates through the corresponding side wall of the accommodation chamber and is provided with a U-shaped groove for the assembly of the lifting member.

[0013] As a further aspect of the present invention, a placement plate is integrally arranged on the side wall of the bottom plate. The motor is arranged on the top shell wall of the placement plate through a cushion seat. The left end of the transmission shaft is installed with an L-shaped plate through a bearing. The bottom of the L-shaped plate is fixedly connected to the top of the placement plate by bolts. The driven gear is arranged at the left end of the front side active roller. The driven gear meshes with the half gear, and the half gear also meshes with the transmission gear; A convex rod is installed on the right side shell wall of the disc. A vertical groove is opened on the moving plate. The convex rod is movably connected in the vertical groove, and the bottom of the moving plate is slidably connected to the bottom plate.

[0014] As a further aspect of the present invention, the inflation mechanism includes an inflation pump main body arranged on the bottom plate. An inflation main pipe is arranged at the air outlet port of the inflation pump main body. A plurality of branch pipes are linearly distributed on the inflation main pipe. The plurality of inlet pipes and the corresponding branch pipes are connected by hoses; The liquid pumping mechanism includes a liquid pumping pump main body arranged on the bottom plate. A liquid pumping main pipe is arranged at the feed port of the liquid pumping pump main body. One ends of the plurality of liquid pumping pipes away from the corresponding vertical components are all arranged on the liquid pumping main pipe.

[0015] Compared with the prior art, the beneficial effects of the present invention are: 1. By configuring a sampling mechanism on each reaction tank, then setting a shared conveying mechanism below multiple sampling mechanisms, and configuring corresponding sample temporary storage components, under the action of the driving mechanism, the conveying mechanism can be used to progressively convey the corresponding sample temporary storage components, thereby realizing the automatic switching of sample bottles. At the same time, the sampling mechanism can be opened and operated to synchronously and automatically sample the materials of multiple reaction tanks, reducing the manual burden, improving work efficiency, and ensuring personnel safety; 2. The synchronous sampling of multiple reaction tanks can ensure that multiple samples are the materials in the same period state of the materials in each reaction tank, which is beneficial to the authenticity and accuracy of data during sample detection, and further facilitates the management of each reaction tank; 3. The automatic operation of the conveying mechanism and the sampling mechanism is realized through a single set driving mechanism, reducing the configuration of the driving structure, further reducing the manufacturing cost of the equipment, and facilitating its popularization and application in small workshops; 4. The sampling mechanism on each reaction tank and the corresponding sample temporary storage components can be manually operated and adjusted, which is convenient for the staff to freely spot-check the materials in each reaction tank; 5. By setting a liquid pumping mechanism, the vertical components in each sampling mechanism can be pumped first, which can not only extract the residual materials in the vertical components and make the inside of the vertical components in a negative pressure state, but also realize the rapid filling of inert gas into the vertical components under the action of the gas filling mechanism and the gas one-way valve, further improving the replacement effect of the air in the vertical components and ensuring the purity of the samples taken and the accuracy of sample detection. Description of the Drawings

[0016] Figure 1 Schematic diagram of the three-dimensional structure of a monitoring and sampling device for lithium hexafluorophosphate Figure 1 ; Figure 2 Schematic diagram of the three-dimensional structure of a monitoring and sampling device for lithium hexafluorophosphate Figure 2 ; Figure 3 For Figure 1 Schematic diagram of the structure of the conveying mechanism; Figure 4 For Figure 2 Schematic diagram of the structure of the conveying mechanism; Figure 5 For Figure 4 Enlarged schematic diagram of the partial structure at A; Figure 6 For Figure 4 Schematic diagram of the bottom view structure; Figure 7 For Figure 1 Schematic diagram of the structure of the reaction component and the sampling mechanism; Figure 8 is Figure 7 the isometric view structural schematic diagram of Figure 9 is Figure 7 the structural schematic diagram of the sampling mechanism of Figure 10 is Figure 8 the enlarged partial structure schematic diagram at position B of Figure 11 is Figure 9 the enlarged partial structure schematic diagram at position C of Figure 12 is Figure 9 the bottom view structural schematic diagram of Figure 13 is Figure 12 the enlarged partial structure schematic diagram at position D of Figure 14 is Figure 9 the structural schematic diagram of the sampling bottle of Figure 15 is Figure 14 the enlarged partial structure schematic diagram at position E of Figure 16 is Figure 3 the structural schematic diagram of the conveying member of

[0017] In the figure: 1, reaction tank; 11, tank body; 12, tank cover; 2, stirring mechanism; 21, stirring motor; 22, stirring shaft; 3, sampling mechanism; 31, shunt member; 311, shunt pipe; 312, end cover; 313, adjusting rod; 314, sealing plug; 315, movable member; 32, vertical assembly; 321, vertical pipe one; 322, vertical pipe two; 323, base ring; 324, moving ring; 325, pressing rod; 326, traction member; 3261, steering wheel; 3262, lifting member; 33, adjusting assembly; 331, pipe body; 332, fixed ring; 333, vertical plate; 334, pushing and pulling member; 335, guiding member; 34, gas one-way valve; 35, liquid extraction pipe; 36, intake pipe; 4, conveying assembly; 41, frame; 411, bottom plate; 412, side plate; 413, cross plate; 42, conveying member; 43, pushing member; 431, sliding plate; 432, contact rod; 433, bent rod; 434, driven wedge block; 5, sample temporary storage assembly; 51, loading plate; 52, convex block; 53, placing frame; 54, sample bottle; 541, bottle body; 542, sealing member; 5421, sealing cover box; 5422, sealing baffle; 5423, round rod; 6, driving mechanism; 61, motor; 62, semi-gear; 63, driven gear; 64, transmission gear; 65, disc; 66, moving plate; 67, fixed rod; 68, driving wedge block; 7, inflation mechanism; 71, inflation pump body; 72, inflation main pipe; 8, liquid extraction mechanism; 81, liquid extraction pump body; 82, liquid extraction main pipe. Specific embodiments

[0018] Please refer to Figures 1 - 2 In an embodiment of the present invention, a monitoring and sampling device for lithium hexafluorophosphate includes a plurality of linearly distributed reaction components. The reaction components include a reaction tank 1 and a stirring mechanism 2. The arrangement of the stirring mechanism 2 on the reaction tank 1 can improve the efficiency of material processing inside it and prevent phenomena such as crystallization and precipitation of materials inside the reaction tank 1.

[0019] A sampling mechanism 3 for material sampling is installed on each reaction tank 1. A sample temporary storage component 5 for temporarily storing samples is provided below the sampling mechanism 3. A conveying mechanism for transporting the sample temporary storage component 5 is jointly provided below the plurality of sampling mechanisms 3. An inflation mechanism 7 for gas filling and a liquid pumping mechanism 8 for liquid suction are also installed on the conveying component 4. The arrangement of the conveying mechanism can perform synchronous displacement adjustment on the plurality of sample temporary storage components 5, and thus, in cooperation with the corresponding sampling mechanisms 3, synchronous sampling of materials in the plurality of reaction tanks 1 can be achieved.

[0020] Please refer to Figures 3 - 4 In an embodiment of the present invention, the conveying mechanism includes a conveying component 4 and a driving mechanism 6. Among them, the conveying component 4 includes a frame 41 serving as a bearing structure. A conveying member 42 for transporting the sample temporary storage component 5 and a pushing member 43 for adjusting the sampling mechanism 3 are installed on the frame 41. The arrangement of the conveying member 42 realizes the transportation of the sample temporary storage component 5 placed on the frame 41.

[0021] Please refer to Figures 4 - 6 In an embodiment of the present invention, the driving mechanism 6 includes a motor 61 provided on the conveying component 4. A half gear 62 is installed at the output end of the motor 61. A driven gear 63 for driving the conveying member 42 is provided on the front side of the half gear 62. A transmission gear 64 is installed on the rear side of the half gear 62 through a transmission shaft. The half gear 62 and the driven gear 63 are meshed and driven, and the half gear 62 and the transmission gear 64 are also meshed and driven. Among them, the number of teeth of the half gear 62 is half of that of the driven gear 63, and the number of teeth of the transmission gear 64 is greater than that of the driven gear 63. Thus, when the half gear 62 rotates half a circle, it can drive the driven gear 63 to move 180 degrees, but it cannot drive the transmission gear 64 to move 180 degrees.

[0022] A disc 65 is provided at the right end of the transmission shaft. A moving plate 66 is movably connected to the right side of the disc 65. A fixed rod 67 is installed on the side wall of the moving plate 66. A driving wedge block 68 for driving the pushing member 43 is fixedly connected to the rear end of the fixed rod 67. The half gear 62 drives the transmission gear 64 to move, and then drives the disc 65 to rotate and move through the transmission shaft, causing the moving plate 66 to linearly displace, and driving the driving wedge block 68 to move through the fixed rod 67.

[0023] Please refer toFigures 7 - 10 , in the embodiment of the present invention, the sampling mechanism 3 includes a shunt member 31 disposed on the reaction tank 1, and a vertical component 32 is installed on the shunt member 31. An adjustment component 33 is movably sleeved on the vertical component 32, and an intake pipe 36 is provided on the adjustment component 33. Above the adjustment component 33, there are a gas check valve 34 and a liquid suction pipe 35 located on the vertical component 32. The shunt member 31 seals and diverts the material in the reaction tank 1, and then realizes the sampling of the material through the movement of the shunt member 31 in cooperation with the vertical component 32 and the adjustment component 33.

[0024] Please refer to Figures 7 - 8 , in the embodiment of the present invention, the reaction tank 1 includes a tank body 11 for material reaction, and a tank cover 12 is installed on the top end of the tank body 11 by bolts. The stirring mechanism 2 includes a stirring motor 21 fixedly connected to the tank cover 12 by bolts. The output end of the stirring motor 21 is provided with a stirring shaft 22 extending into the interior of the tank body 11, and a hole for installing the sampling mechanism 3 is opened on the peripheral wall of the tank body 11. The hole is designed to be inclined on the tank body 11, so that the sampling mechanism 3 is also in an inclined state when installed.

[0025] Please refer to Figure 9 , in the embodiment of the present invention, the shunt member 31 includes a shunt pipe 311 disposed in the hole, and an end cover 312 is threadedly connected to the top end of the shunt pipe 311. The threaded connection between the end cover 312 and the shunt pipe 311 enables the disassembly and cleaning of the shunt member 31.

[0026] A round hole is opened at the center of the end cover 312, and an adjusting rod 313 is movably connected in the round hole. The bottom end of the adjusting rod 313 is located inside the shunt pipe 311, and a sealing plug 314 for blocking is installed. The sealing plug 314 is provided to prevent the material in the reaction tank 1 from leaking and for sampling adjustment.

[0027] The top end of the adjusting rod 313 is located outside the shunt pipe 311, and a movable member 315 is installed by bolts. The movable member 315 is composed of an end plate and a support rod. Among them, the end plate is fixedly connected to the top end of the adjusting rod 313 by bolts, and the support rod is fixedly connected to the bottom of the end plate. A return spring is sleeved on the adjusting rod 313 between the sealing plug 314 and the end cover 312. The setting of the return spring can ensure the reset adjustment of the adjusting rod 313 without external force.

[0028] Please refer to Figures 9 - 13, in the embodiments of the present invention, the vertical component 32 includes a slot formed in the shunt pipe 311, and the vertical component 32 includes a first vertical pipe 321 disposed in the slot. A second vertical pipe 322 is provided directly below the first vertical pipe 321. The first vertical pipe 321 and the second vertical pipe 322 have the same diameter, which is convenient for carrying and sampling the material. When the plug 314 cancels the blockage of the slot during movement, the blocking effect is not completely cancelled, and due to the inclined design of the end face of the plug 314, the material will not contact the gas check valve 34 during sampling.

[0029] Wherein, the first vertical pipe 321 and the second vertical pipe 322 are connected by an arc plate group. The arc plate group is composed of three arc plates, which are arranged circumferentially between the first vertical pipe 321 and the second vertical pipe 322 for splicing the first vertical pipe 321 and the second vertical pipe 322. The gaps between the arc plates are for facilitating the passage of inert gas into it.

[0030] An integral base ring 323 is provided on the outer periphery of the bottom end of the second vertical pipe 322, and a movable ring 324 located on the second vertical pipe 322 is sleeved above the base ring 323. Two pressing rods 325 are installed at the bottom of the movable ring 324. The two pressing rods 325 are fixed to the movable ring 324 by bolts, and the two pressing rods 325 are symmetrically distributed.

[0031] A through hole located on the base ring 323 is formed below each pressing rod 325, and the bottom ends of the plurality of pressing rods 325 respectively penetrate through the corresponding through holes and are provided with a traction member 326. The movable ring 324 drives the pressing rod 325 to move, thereby causing the traction member 326 to move.

[0032] Wherein, an extrusion spring is sleeved on each pressing rod 325. The top of the extrusion spring is disposed on the bottom shell wall of the movable ring 324, and the bottom of the extrusion spring is disposed on the top shell wall of the base ring 323. The extrusion spring is provided to facilitate the reset adjustment of the movable ring 324 and ensure that the movable ring 324 is at a high position without external force.

[0033] The traction member 326 includes a steering wheel 3261 and a lifting member 3262. Among them, the steering wheel 3261 is disposed on the bottom shell wall of the base ring 323 through a straight plate group. The lifting member 3262 is slidably connected to the bottom shell wall of the base ring 323. A traction belt is wound around the steering wheel 3261. One end of the traction belt is bound to the lifting member 3262, and the other end of the traction belt is disposed on the corresponding pressing rod 325. The lifting member 3262 includes an integrated plate slidably connected to the bottom shell wall of the base ring 323, and a plurality of insertion rods are linearly arranged at the bottom of the integrated plate.

[0034] Above the adjustment component 33, a connection hole and a mounting hole located on the first vertical pipe 321 are provided. The gas check valve 34 is arranged in the mounting hole, the liquid extraction pipe 35 is arranged in the connection hole, and a control valve is also arranged on the liquid extraction pipe 35. The liquid extraction pipe 35 adopts a bent pipe structure, and the bottom end of the pipe located in the vertical component 32 is in the same plane as the bottom end of the second vertical pipe 322, so as to facilitate the suction of the material remaining in the vertical component 32.

[0035] The adjustment component 33 includes a pipe body 331 sleeved on the first vertical pipe 321. An integral fixed ring 332 for pressing the moving ring 324 is provided on the outer circle of the bottom end of the pipe body 331. Above the fixed ring 332, a vertical plate 333 is provided on the outer wall of the outer circle of the pipe body 331. An inclined slot is provided on the vertical plate 333, and a push-pull member 334 is slidably connected in the inclined slot. The push-pull member 334 includes a rod body movably connected in the inclined slot, and strip-shaped plates are installed at both the front and rear ends of the rod body. A restraint ring is jointly installed at the right ends of the two strip-shaped plates.

[0036] A guide member 335 is slidably connected to the push-pull member 334, and the bottom of the guide member 335 is fixedly connected to the conveying component 4. The guide member 335 includes a sliding seat slidably connected to the two strip-shaped plates, and a support rod is fixedly connected to the bottom of the sliding seat. The bottom end of the support rod is fixedly connected to the conveying component 4.

[0037] The push-pull member 334 is also slidably connected to the movable member 315. The restraint ring in the push-pull member 334 is movably sleeved on the strut of the movable member 315.

[0038] An air inlet pipe 36 is installed in the notch provided on the peripheral wall of the pipe body 331. Sealing rings for improving the sealing performance are provided on both the inner circles of the top and bottom of the pipe body 331.

[0039] Please refer to Figures 3 - 6 and Figure 16 , in the embodiment of the present invention, the frame 41 includes a bottom plate 411, and side plates 412 are welded to both the front and rear sides of the bottom plate 411. Above the bottom plate 411, a cross plate 413 located between the two side plates 412 is provided. The cross plate 413 is used to carry the sample temporary storage component 5, and a rectangular through slot is provided on the cross plate 413.

[0040] The conveying member 42 is located between the bottom plate 411 and the cross plate 413. The conveying member 42 includes two movable rollers and a conveyor belt. Among them, the two movable rollers are respectively arranged on the inner walls of the corresponding side plates 412 through carrier frames. The two movable rollers are connected by a conveyor belt, and a plurality of bases are equidistantly arranged on the outer surface of the conveyor belt. A push top plate is movably connected to each base through a pin shaft. Among them, a torsion spring for reset adjustment of the push top plate is also sleeved on the pin shaft. The arrangement of the push top plate and the base through the cooperation of the pin shaft and the torsion spring can not only enable the conveying member 42 to drive the plurality of sample temporary storage assemblies 5 to displace synchronously, but also realize the manual displacement adjustment of a single sample temporary storage assembly 5 on the frame 41.

[0041] A groove is formed in each side plate 412. The pushing member 43 includes a sliding plate 431 slidably connected to the groove. A contact rod 432 for pushing the sampling mechanism 3 is arranged between the two sliding plates 431.

[0042] A bent rod 433 is installed on the outer wall of each sliding plate 431, and the two bent rods 433 are connected by a driven wedge block 434. The driven wedge block 434 is slidably connected to the top shell wall of the bottom plate 411, so as to ensure the stability of the force movement of the driven wedge block 434. The inclined surface of the driven wedge block 434 is in sliding contact with the inclined surface of the active wedge block 68. Furthermore, when the active wedge block 68 moves, the driven wedge block 434 is extruded and forced, so that the bent rod 433 drives each sliding plate 431 to move, and then drives the contact rod 432 to displace and adjust.

[0043] Please refer to Figure 1 、 Figure 3 and Figures 7 - 12 In the embodiment of the present invention, the sample temporary storage assembly 5 includes a carrier plate 51 placed on the cross plate 413. A convex block 52 is integrally arranged at the center of the bottom of the carrier plate 51. The bottom of the convex block 52 penetrates through the rectangular through groove and contacts the corresponding push top plate. Furthermore, when the conveying member 42 operates, the push top plate pushes the convex block 52 to realize the displacement adjustment of the sample temporary storage assembly 5. A plurality of placement frames 53 are linearly distributed on the top of the carrier plate 51, and sample bottles 54 for temporarily storing samples are placed in the placement frames 53.

[0044] Please refer to Figures 14 - 15, in the embodiment of the present invention, the sample bottle 54 includes a bottle body 541 placed in a placement frame 53. A seal 542 is installed at the mouth of the bottle body 541. The seal 542 includes a capping box 5421 threadedly connected to the mouth of the bottle body 541. A rectangular groove is formed at the top of the capping box 5421. Thus, when the sample bottle 54 is displaced below the sampling mechanism 3, the edge of the top of the capping box 5421 contacts the sampling mechanism 3, realizing the sealing contact between the sample bottle 54 and the sampling mechanism 3. An accommodation chamber is formed inside the capping box 5421. Cavities are formed on the inner walls on both sides of the accommodation chamber, and round rods 5423 are arranged in the cavities. A material passing hole is formed at the center of the capping box 5421, and the material passing hole and the port of the bottle body 541 are on the same axis line. Sealing baffles 5422 for blocking are symmetrically arranged on the left and right in the accommodation chamber, and the mutual approach of the two sealing baffles 5422 realizes the blocking of the material passing hole. Sliders movably connected to the corresponding round rods 5423 are installed on the front and rear sides of each sealing baffle 5422. A return spring sleeved on the corresponding round rod 5423 is arranged on the side wall of each slider. The arrangement of the return spring enables the sealing baffle 5422 to reset without external force, thereby realizing the blocking of the material passing hole and ensuring the stable reset of the traction member 326 in the vertical component 32.

[0045] On the mutually remote sides of the two sealing baffles 5422, they respectively penetrate through the corresponding side walls of the accommodation chamber, and U-shaped grooves for the assembly of the lifting member 3262 are formed.

[0046] Please refer to Figures 1 - 5 , in the embodiment of the present invention, a placement plate is integrally arranged on the side wall of the bottom plate 411. The motor 61 is arranged on the top shell wall of the placement plate through a cushion seat. The left end of the transmission shaft is installed with an L-shaped plate through a bearing. The bottom of the L-shaped plate is fixedly connected to the top of the placement plate through bolts. The driven gear 63 is arranged at the left end of the front side movable roller.

[0047] A convex rod is installed on the right shell wall of the disc 65, and a vertical groove is formed on the moving plate 66. The convex rod is movably connected in the vertical groove, and the bottom of the moving plate 66 is slidably connected to the bottom plate 411.

[0048] Please refer to Figure 1 , Figure 2 , Figure 8 , Figure 9 , Figure 10 and Figure 11 , in the embodiment of the present invention, the inflation mechanism 7 includes an inflation pump main body 71 arranged on the bottom plate 411. An inflation main pipe 72 is arranged at the air outlet port of the inflation pump main body 71. The air inlet port of the inflation pump main body 71 is connected to an external air source through a pipeline, and the air source adopts an inert gas, such as nitrogen, etc. A plurality of branch pipes are linearly distributed on the inflation main pipe 72, and a plurality of intake pipes 36 and the corresponding branch pipes are connected through hoses.

[0049] The liquid extraction mechanism 8 includes a liquid extraction pump main body 81 disposed on the bottom plate 411, and a liquid extraction main pipe 82 is provided on the feed port of the liquid extraction pump main body 81. The discharge port of the liquid extraction pump main body 81 is connected to an external collection tank through a pipeline, and is used for cleaning the residual materials after sampling. One ends of a plurality of liquid extraction pipes 35 far away from the corresponding vertical components 32 are all disposed on the liquid extraction main pipe 82.

[0050] The working principle of the present invention is as follows: when the materials are being processed in the reaction tank 1, the stirring motor 21 in the stirring mechanism 2 moves under the control of an external controller main body, drives the corresponding stirring shaft 22 to move, and realizes stirring of the materials in the corresponding reaction tank 1.

[0051] When sampling operations need to be performed on a plurality of reaction tanks 1, the external controller main body first turns on the air inflation pump main body 71 in the air inflation mechanism 7 and the liquid extraction pump main body 81 in the liquid extraction mechanism 8. Then, the control valves on each liquid extraction pipe 35 are started, so that each liquid extraction pipe 35 is communicated with the vertical pipe one 321 in the corresponding vertical component 32. At this time, the liquid extraction main pipe 82 in the liquid extraction mechanism 8 extracts the liquid and gas in the vertical component 32 under the action of the operation of the liquid extraction pump main body 81, so that a negative pressure state is formed inside the vertical component 32. The time for the external controller main body to turn on the control valve can be preset, and the control valve will close automatically after being turned on for a period of time.

[0052] Next, the external controller main body controls the motor 61 in the driving mechanism 6 to run counterclockwise, and the motor 61 drives the half gear 62 to rotate. The first half of the movement of the half gear 62 is in meshing transmission with the driven gear 63, and then drives the conveying member 42 in the conveying assembly 4 to move. Since the motor 61 takes half a turn of movement as one mileage, the motor 61 will pause for a period of time after rotating half a turn, and then start running the remaining half turn again. During one mileage of the movement of the half gear 62, its meshing transmission with the driven gear 63 realizes the movement of the conveying member 42 for one mileage. Furthermore, the conveying member 42 drives a plurality of sample temporary storage components 5 located on the conveying assembly 4 to synchronously displace for one mileage, realizing the displacement switching of a plurality of sample bottles 54 linearly placed in the sample temporary storage components 5.

[0053] After each sample temporary storage component 5 completes the displacement switching, the new unused sample bottle 54 moves to directly below the corresponding sampling mechanism 3 and plugs the bottom end of the vertical pipe two 322 in the sampling mechanism 3. And when the sample bottle 54 moves below the sampling mechanism 3, the U-shaped grooves on each sealing plate 5422 of the seal 542 in the sample bottle 54 are respectively slidably inserted into the lifting members 3262 of the traction members 326 of the vertical component 32 in the sampling mechanism 3.

[0054] Finally, the external controller body starts the motor 61 in the driving mechanism 6 again. At this time, the half gear 62 disengages from the driven gear 63 and thus will not drive the conveying member 42 to move. However, the half gear 62 meshes with the transmission gear 64 at this time, and drives the disc 65 to rotate through the transmission shaft. During the rotation of the disc 65, it drives the moving plate 66 to linearly slide, and synchronously drives the active wedge block 68 to displace and adjust through the fixed rod 67. During the movement of the active wedge block 68, it contacts the driven wedge block 434 of the pusher 43 in the conveying assembly 4 and applies an extrusion force to it. After the driven wedge block 434 is stressed, it drives the corresponding slide plate 431 to displace through the bent rod 433, and thus the contact rod 432 moves. During the displacement of the contact rod 432, it contacts the movable member 315 of the shunt member 31 in each sampling mechanism 3 and pushes against it. After the movable member 315 is stressed, it moves in the movement direction of the contact rod 432, stretching the adjusting rod 313 and the push-pull member 334 in the adjusting assembly 33. After the adjusting rod 313 is pulled, it compresses the return spring and drives the plug 314 to displace.

[0055] When the push-pull member 334 moves with the movement of the movable member 315, due to the constraint of the guiding member 335, the vertical plate 333 drives the pipe body 331 to move downward during the movement of the movable member 315.

[0056] When the air inlet pipe 36 on the pipe body 331 leaves the vertical pipe one 321 in the vertical component 32, under the action of the operation of the air inflation pump body 71 in the air inflation mechanism 7, the main air inflation pipe 72 and each corresponding hose input the inert gas from the air inlet pipe 36 into each corresponding vertical component 32. The filling of the inert gas into the vertical component 32 enables the air remaining in the vertical component 32 to be discharged through the gas one-way valve 34, realizing the filling of the inert gas in the vertical component 32.

[0057] During the continuous downward movement of the pipe body 331, when the air inlet pipe 36 on the pipe body 331 contacts the vertical pipe two 322, the air inlet pipe 36 is blocked. At this time, the plug 314 still realizes the blocking of the slot hole. During the continuous downward movement of the pipe body 331, the plug 314 cancels the blocking of the slot hole, and thus the material in the reaction tank 1 directly enters the vertical component 32 from the reaction tank 1 through the shunt pipe 311 in the shunt member 31 under the action of gravity.

[0058] At this time, the fixed ring 332 in the adjusting assembly 33 contacts the moving ring 324 and performs a pressing operation on it. After the moving ring 324 is stressed and moves downward, it drives the corresponding pressing rod 325 to move synchronously. During the downward movement of the pressing rod 325, it adjusts the traction belt in the corresponding traction member 326, enabling the traction belt to move on the corresponding steering wheel 3261 and pulling the corresponding lifting member 3262 to displace.

[0059] Thereby, the baffle plate 5422 of the seal 542 in the corresponding sample bottle 54 is opened, so that the material in the vertical component 32 directly flows into the corresponding bottle body 541, thus realizing the sampling operation of the material.

[0060] Under the action of gravity, the material flows following the displacement of the sealing plug 314. When the sealing plug 314 cancels the blockage of the slot hole, the material then enters the vertical component 32. Furthermore, when the baffle plate 5422 of the seal 542 in the sample bottle 54 is opened, the material also enters the bottle body 541, and there is no need to pause the equipment waiting for the material to fall.

[0061] After the motor 61 drives the half gear 62 to rotate the remaining half circle, each sampling mechanism 3 and the corresponding sample temporary storage component 5 complete the synchronous sampling of the material in the corresponding reaction tank 1.

[0062] After the half gear 62 completes the movement of the remaining half circle, the half gear 62 disengages from the transmission gear 64. As a result, the active wedge 68 lacks the force applied to the driven wedge 434. The return springs of the shunt member 31 in each sampling mechanism 3, the compression spring on the pressing rod 325 in the vertical component 32, and the return spring in the seal 542 of the corresponding sample bottle 54 perform return movements, respectively causing the shunt member 31, the traction member 326 in the vertical component 32, and the baffle plate 5422 in the seal 542 to return.

[0063] When the shunt member 31 returns, the pusher 43 automatically returns. Then, the driven wedge 434 squeezes and adjusts the active wedge 68, causing the fixed rod 67 and the moving plate 66 to perform a return movement, thereby driving the reverse movement of the disc 65.

[0064] Since the number of teeth of the transmission gear 64 is more than that of the driven gear 63, the half gear 62 rotating half a circle can drive the driven gear 63 to rotate synchronously half a circle, but the transmission gear 64 cannot rotate a half - circle path, which provides favorable conditions for the active wedge 68 to drive the return of the moving plate 66.

[0065] The return of the shunt member 31 realizes the blockage of the material inside the reaction tank 1, and the return of the baffle plate 5422 realizes the reset blockage of the seal 542 in the sample bottle 54, avoiding the sample in the sample bottle 54 from contacting the air.

[0066] After sampling is completed, the external controller main body opens the control valves on each liquid extraction pipe 35 again, realizing the re - extraction of the liquid and gas in the vertical component 32 of each sampling mechanism 3, avoiding the material in the vertical component 32 from being discharged and contacting the air when the sample temporary storage component 5 is switched.

[0067] In a cycle, the synchronous sampling of the materials in multiple reaction tanks 1 is thus realized.

[0068] When randomly selecting any one of the reaction vessels 1 for spot-checking the materials in a single reaction vessel 1, after selecting a reaction vessel 1, the sample temporary storage assembly 5 used in this reaction vessel 1 is integrally moved a certain distance on the cross plate 413, so that the new sample bottle 54 of the sample temporary storage assembly 5 moves to directly below the sampling mechanism 3.

[0069] When the sample temporary storage assembly 5 is manually pushed on the cross plate 413, since the push top plate on the conveyor belt in the conveyor 42 and the base are arranged through the cooperation of a pin shaft and a torsion spring, when the sample temporary storage assembly 5 moves forward actively, the push top plate will not hinder the sample temporary storage assembly 5, which is convenient for the displacement adjustment of the sample temporary storage assembly 5. After the position adjustment of the sample temporary storage assembly 5 is completed, the inflation mechanism 7 and the liquid pumping mechanism 8 are started through an external controller main body to realize the negative pressure adjustment of the vertical component 32 in the sampling mechanism 3. Then, the movable part 315 of the shunt part 31 in the sampling mechanism 3 is manually pulled, so as to realize the sampling operation of the sampling mechanism 3 on the materials in the corresponding reaction vessel 1.

[0070] The above is only the preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any person skilled in the art within the technical scope disclosed by the present invention, according to the technical solution of the present invention and its inventive concept, makes equivalent replacements or changes, and should be covered within the protection scope of the present invention.

Claims

1. A monitoring and sampling device for lithium hexafluorophosphate, comprising a plurality of linearly distributed reaction components, the reaction components including a reaction tank (1) and a stirring mechanism (2), characterized in that: A sampling mechanism (3) for material sampling is installed on each of the reaction vessels (1). A sample temporary storage assembly (5) for temporarily storing samples is provided below the sampling mechanism (3). A conveying mechanism for conveying the sample temporary storage assembly (5) is jointly provided below multiple sampling mechanisms (3). An inflation mechanism (7) for gas filling and a liquid pumping mechanism (8) for liquid suction are also installed on the conveying assembly (4). The conveying mechanism includes a conveying assembly (4) and a driving mechanism (6). Among them, the conveying assembly (4) includes a frame (41) serving as a bearing structure. A conveying member (42) for conveying the sample temporary storage assembly (5) and a pushing member (43) for adjusting the sampling mechanism (3) are installed on the frame (41). The driving mechanism (6) includes a motor (61) arranged on the conveying assembly (4). A half gear (62) is installed at the output end of the motor (61). A driven gear (63) for driving the conveying member (42) is provided on the front side of the half gear (62). A transmission gear (64) is installed on the rear side of the half gear (62) through a transmission shaft. A disc (65) is provided at the right end of the transmission shaft. A moving plate (66) is movably connected to the right side of the disc (65). A fixed rod (67) is installed on the side wall of the moving plate (66). A driving wedge block (68) for driving the pushing member (43) is fixedly connected to the rear end of the fixed rod (67). The sampling mechanism (3) includes a flow splitting member (31) arranged on the reaction vessel (1). A vertical component (32) is installed on the flow splitting member (31). An adjusting component (33) is movably sleeved on the vertical component (32). An air inlet pipe (36) is provided on the adjusting component (33). A gas one-way valve (34) and a liquid suction pipe (35) located on the vertical component (32) are provided above the adjusting component (33).

2. The monitoring and sampling device for lithium hexafluorophosphate according to claim 1, wherein The reaction vessel (1) includes a tank body (11) for material reaction. A tank cover (12) is installed at the top end of the tank body (11) through bolts. The stirring mechanism (2) includes a stirring motor (21) fixedly connected to the tank cover (12) through bolts. A stirring shaft (22) extending into the interior of the tank body (11) is installed at the output end of the stirring motor (21). A hole for installing the sampling mechanism (3) is formed in the peripheral wall of the tank body (11).

3. The monitoring and sampling device for lithium hexafluorophosphate according to claim 2, characterized in that, The flow splitting member (31) includes a flow splitting pipe (311) arranged in the hole. An end cover (312) is threadedly connected to the top end of the flow splitting pipe (311). A round hole is formed at the center of the end cover (312). An adjusting rod (313) is movably connected in the round hole. The bottom end of the adjusting rod (313) is located inside the flow splitting pipe (311) and is provided with a plug (314) for blocking. The top end of the adjusting rod (313) is located outside the flow splitting pipe (311) and is provided with a movable member (315) through bolts. A return spring sleeved on the adjusting rod (313) is arranged between the plug (314) and the end cover (312). The vertical component (32) includes a slot formed in the shunt pipe (311). The vertical component (32) includes a first vertical pipe (321) disposed in the slot. A second vertical pipe (322) is provided directly below the first vertical pipe (321). Among them, the first vertical pipe (321) and the second vertical pipe (322) are connected by an arc plate group. A base ring (323) is integrally provided on the outer circumference of the bottom end of the second vertical pipe (322). A moving ring (324) located on the second vertical pipe (322) is sleeved above the base ring (323). Two pressing rods (325) are installed at the bottom of the moving ring (324). A through hole located on the base ring (323) is formed below each pressing rod (325). The bottom ends of the plurality of pressing rods (325) respectively penetrate through the corresponding through holes and are installed with a traction member (326). Among them, an extrusion spring is sleeved on each pressing rod (325). The top of the extrusion spring is disposed on the bottom shell wall of the moving ring (324), and the bottom of the extrusion spring is disposed on the top shell wall of the base ring (323); The traction member (326) includes a steering wheel (3261) and a lifting member (3262). Among them, the steering wheel (3261) is disposed on the bottom shell wall of the base ring (323) through a straight plate group. The lifting member (3262) is slidably connected to the bottom shell wall of the base ring (323). A traction belt is wound around the steering wheel (3261). One end of the traction belt is bound to the lifting member (3262), and the other end of the traction belt is disposed on the corresponding pressing rod (325); Above the adjustment component (33), a connection hole and an installation hole located on the first vertical pipe (321) are formed. The gas one-way valve (34) is disposed in the installation hole. The liquid extraction pipe (35) is disposed in the connection hole, and a control valve is further provided on the liquid extraction pipe (35).

4. The monitoring and sampling device for lithium hexafluorophosphate according to claim 3, characterized in that, The adjustment component (33) includes a pipe body (331) sleeved on the first vertical pipe (321). A fixed ring (332) for pressing the moving ring (324) is integrally provided on the outer circumference of the bottom end of the pipe body (331). A vertical plate (333) is provided above the fixed ring (332) on the outer shell wall of the pipe body (331). An inclined slot is formed in the vertical plate (333). A push-pull member (334) is slidably connected in the inclined slot. A guiding member (335) is slidably connected to the push-pull member (334). The bottom of the guiding member (335) is fixedly connected to the conveying component (4). The push-pull member (334) is also slidably connected to the movable member (315); A notch is formed on the peripheral wall of the pipe body (331), and an air inlet pipe (36) is installed in the notch. Sealing rings for improving the sealing performance are provided on the inner circles of the top and bottom of the pipe body (331).

5. The monitoring and sampling device for lithium hexafluorophosphate according to claim 4, characterized in that, The frame (41) includes a bottom plate (411). Side plates (412) are welded to the front and rear sides of the bottom plate (411). A cross plate (413) is provided above the bottom plate (411) between the two side plates (412). The cross plate (413) is used to carry the sample temporary storage component (5). A rectangular through slot is formed in the cross plate (413); The conveying member (42) is located between the bottom plate (411) and the cross plate (413). The conveying member (42) includes two movable rollers and a conveyor belt. Among them, the two movable rollers are respectively arranged on the inner wall of the corresponding side plate (412) through a carrier, and the two movable rollers are connected by a conveyor belt. A plurality of bases are equidistantly arranged on the outer surface of the conveyor belt. A push top plate is movably connected to each base through a pin shaft. A torsion spring for reset adjustment of the push top plate is also sleeved on the pin shaft. A groove is formed on each side plate (412).

6. The monitoring and sampling device for lithium hexafluorophosphate according to claim 5, characterized in that, The pushing member (43) includes a sliding plate (431) slidably connected to the groove. A contact rod (432) for pushing the sampling mechanism (3) is arranged between the two sliding plates (431). A bent rod (433) is installed on the outer wall of each sliding plate (431). The two bent rods (433) are connected by a driven wedge block (434). The driven wedge block (434) is slidably connected to the top shell wall of the bottom plate (411), and the inclined surface of the driven wedge block (434) is in sliding contact with the inclined surface of the driving wedge block (68).

7. The monitoring and sampling device for lithium hexafluorophosphate according to claim 6, characterized in that, The sample temporary storage assembly (5) includes a carrier plate (51) placed on the cross plate (413). A convex block (52) is integrally arranged at the center of the bottom of the carrier plate (51). The bottom of the convex block (52) penetrates through the rectangular through groove and contacts the corresponding push top plate. A plurality of placement frames (53) are linearly distributed on the top of the carrier plate (51). Sample bottles (54) for temporarily storing samples are placed in the placement frames (53). The sample bottle (54) includes a bottle body (541) placed in the placement frame (53). A sealing member (542) is installed at the bottle mouth of the bottle body (541). The sealing member (542) includes a sealing cover box (5421) threadedly connected to the bottle mouth of the bottle body (541). An accommodation chamber is formed inside the sealing cover box (5421). Cavities are formed on the inner walls on both sides of the accommodation chamber. A round rod (5423) is arranged in the cavity. Sealing baffles (5422) for blocking are symmetrically arranged on the left and right in the accommodation chamber. A slider movably connected to the corresponding round rod (5423) is installed on the front and rear sides of each sealing baffle (5422). A return spring located on the corresponding round rod (5423) is sleeved on the side wall of each slider. One side of the two sealing baffles (5422) away from each other penetrates through the corresponding side wall of the accommodation chamber, and a U-shaped groove for assembling the lifting member (3262) is formed.

8. The monitoring and sampling device for lithium hexafluorophosphate according to claim 7, characterized in that, A placement plate is integrally arranged on the side wall of the bottom plate (411). The motor (61) is arranged on the top shell wall of the placement plate through a cushion seat. The left end of the transmission shaft is installed with an L-shaped plate through a bearing. The bottom of the L-shaped plate is fixedly connected to the top of the placement plate by bolts. The driven gear (63) is arranged at the left end of the front movable roller. The driven gear (63) is in meshing transmission with the half gear (62), and the half gear (62) is also in meshing transmission with the transmission gear (64). A convex rod is installed on the right shell wall of the disc (65). A vertical groove is formed in the moving plate (66). The convex rod is movably connected in the vertical groove, and the bottom of the moving plate (66) is slidably connected to the bottom plate (411).

9. The monitoring and sampling device for lithium hexafluorophosphate according to claim 8, characterized in that, The inflation mechanism (7) includes an inflation pump body (71) arranged on the bottom plate (411). An inflation main pipe (72) is arranged on the air outlet port of the inflation pump body (71). A plurality of branch pipes are linearly distributed on the inflation main pipe (72). The plurality of intake pipes (36) and the corresponding branch pipes are connected by hoses. The liquid pumping mechanism (8) includes a liquid pumping pump body (81) arranged on the bottom plate (411). A liquid pumping main pipe (82) is arranged on the feed port of the liquid pumping pump body (81). One end of each of the plurality of liquid pumping pipes (35) far away from the corresponding vertical component (32) is arranged on the liquid pumping main pipe (82).

Citation Information

Patent Citations

  • Lithium hexafluorophosphate detection sampling device

    CN216847033U

  • Controllable-temperature passive sample conveying tank

    CN102375072A

  • Sampler and sampling tube thereof

    CN103512779A

  • Method for detecting phase purity of lithium titanate composition

    CN106053500A

  • Inverted sample loading device

    CN106645771A