A phenol water recycling device
By designing a phenol water recycling device, and utilizing the combination of a spiral evaporation channel and a puncture head, the problems of high cost and low efficiency in existing phenol water treatment technologies have been solved, achieving efficient phenol water recycling and treatment.
Patent Information
- Application Number
- CN202510890877.0
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2025-06-30
- Publication Date
- 2025-11-04
- Estimated Expiration
- 2045-06-30
AI Technical Summary
Existing technologies for treating phenol-containing wastewater require prolonged heating and cannot effectively remove oils and tar, resulting in high phenol removal costs and reduced treatment efficiency.
A phenol water recycling device was designed, including a tar pool, an evaporator, a liquid pumping mechanism, an evaporation mechanism, an oil discharge mechanism, and an exhaust mechanism. By using a spiral evaporation channel and a puncture head in combination, the device achieves efficient evaporation of phenol water and separation of oily liquids.
It shortens the phenol water treatment time, reduces costs, improves the quality and efficiency of phenol water recovery, alleviates the treatment burden, and increases treatment efficiency.
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Figure CN120463278B_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The present application belongs to the technical field of sewage treatment, and particularly relates to a phenolic water recycling device. BACKGROUND
[0002] Phenolic wastewater refers to industrial wastewater containing phenolic compounds, mainly from petroleum refining, coking, chemical, pharmaceutical, pesticide, dye and other production processes; among them, phenols are mainly monohydric phenols, with the highest content of phenol, followed by m-cresol and p-cresol, which are generated from the scrubbing water and phenolic condensate water in the cooling and purification of coal gas, and the generation of phenolic condensate water depends on the quality of gasified coal and the gasification process. The treatment method of phenolic wastewater is as follows: steam chemical phenol removal method: use strong high-temperature steam to heat the phenolic wastewater, so that the phenol in the wastewater evaporates and escapes with the steam, and then the alkali solution is introduced to absorb it into phenyl sodium salt, so as to achieve the purpose of removing phenol; steam phenol removal method: steam phenol removal method is also called gas removal method, the phenolic wastewater is heated, and the phenol is volatilized with water vapor, and then the part of the phenolic steam is introduced into the furnace bottom of the generating furnace and mixed with air as a gasification agent, and the phenol is burned and decomposed into carbon dioxide and water in the furnace at high temperature to ultimately achieve the purpose of removing phenol; incineration method: the phenolic wastewater is sprayed into the incinerator, so that the phenolic organic matter is oxidized at a high temperature of about 1100 DEG C, and finally generates carbon dioxide and water for discharge.
[0003] At present, when the existing technology removes phenols by gas removal method, the phenolic wastewater is generally directly heated or stirred in the heating process until the phenolic wastewater no longer generates steam. Although this method can achieve the purpose of removing phenol, it needs to heat the phenolic wastewater for a long time, and because the phenolic wastewater contains oil, tar and other substances, as the heating time is prolonged, the water content will gradually decrease, and the density of the oil is lower than that of the water, which will cause the water to be below the oil, so that the water is difficult to evaporate, resulting in high cost of phenol removal, and the process of heating the phenolic wastewater cannot discharge the tar and other impurities at the same time, so it is impossible to continuously remove the phenolic wastewater by gas, which increases the burden of treating the phenolic wastewater and affects the efficiency of treating the phenolic wastewater. Based on this, a phenolic water recycling device is proposed. SUMMARY
[0004] The purpose of the present application is to provide a phenolic water recycling device with simple structure and reasonable design to solve the above problems.
[0005] The present application realizes the above-mentioned purpose through the following technical solutions:
[0006] A phenolic water recycling device, comprising a tar pool and an evaporation tank, further comprising:
[0007] A liquid pumping mechanism for connecting the tar pool and the evaporation tank, the liquid pumping mechanism is used for pumping the phenolic wastewater in the tar pool into the evaporation tank;
[0008] The liquid pumping mechanism is used for pumping the phenol-containing wastewater in the evaporation tank into the top of the evaporation mechanism;
[0009] The oil discharging mechanism is fixedly connected with the bottom of the evaporation tank, and is used for pumping the liquid remaining after the evaporation of the phenol-containing wastewater and heating the phenol-containing wastewater in the tar pool;
[0010] The gas discharging mechanism is fixedly connected with the evaporation tank, and is used for driving the evaporation mechanism to rotate and discharging the water vapor generated by heating the phenol-containing wastewater in the evaporation tank.
[0011] As a further optimization scheme of the present application, the evaporation mechanism comprises an electric heater fixedly connected with the evaporation tank, the evaporation tank is sealingly and rotatably connected with an evaporation disc, the evaporation disc is arranged at the top of the electric heater, the top of the evaporation disc is provided with an evaporation channel, the top of the evaporation disc is fixedly connected with a plurality of piercing heads, and the middle of the evaporation disc is fixedly connected with an oil discharging pipe.
[0012] As a further optimization scheme of the present application, the evaporation channel is arranged in a spiral type, and the plurality of piercing heads are fixedly connected in the evaporation channel.
[0013] As a further optimization scheme of the present application, the liquid pumping mechanism comprises a water pump fixedly connected with the top of the tar pool, one end of the water pump is fixedly connected with a water pumping pipe, the water pumping pipe extends into the tar pool, the end of the water pumping pipe away from the water pump is fixedly connected with a filter ball, the other end of the water pump is fixedly connected with a liquid injecting pipe, the end of the liquid injecting pipe away from the water pump is fixedly connected with a liquid conveying pipe, and the bottom of the liquid conveying pipe is fixedly connected with a liquid discharging pipe.
[0014] As a further optimization scheme of the present application, the liquid injecting pipe is fixedly connected with the evaporation tank, the liquid conveying pipe is arranged in a spiral type, and the liquid conveying pipe is fixedly connected with the inner surface of the evaporation tank, the liquid discharging pipe is arranged at the top of the evaporation disc, and the liquid discharging pipe is fixedly connected with the inner surface of the evaporation tank.
[0015] As a further optimization scheme of the present application, the oil discharging mechanism comprises an oil pump fixedly connected with the outer surface of the tar pool, one end of the oil pump is fixedly connected with a heat exchanging pipe, the other end of the oil pump is fixedly connected with an oil pumping pipe, the end of the oil pumping pipe away from the oil pump is fixedly connected with an oil storing pipe, and the oil storing pipe is fixedly connected with the bottom of the evaporation tank.
[0016] As a further optimization scheme of the present application, the heat exchanging pipe is arranged in an "S" type, the heat exchanging pipe is arranged in the tar pool and fixedly connected with the tar pool, the oil discharging end of the heat exchanging pipe extends out of the tar pool, and the oil storing pipe is sealingly and rotatably connected with the oil discharging pipe.
[0017] As a further optimization scheme of the present application, the exhaust mechanism comprises a servo motor fixedly connected to the outer surface of the evaporation tank through the motor base, the output end of the servo motor is fixedly connected with a rotating shaft, the end of the rotating shaft is fixedly connected with a first bevel gear, the inner surface of the evaporation tank is fixedly connected with a protective shell, the middle part of the protective shell is fixedly connected with a transmission shaft, the transmission shaft is rotatably connected with the evaporation tank, the outer surface of the transmission shaft is fixedly connected with a second bevel gear, the second bevel gear is meshed with the first bevel gear, and the outer surface of the transmission shaft is fixedly connected with a fan blade.
[0018] As a further optimization scheme of the present application, the fan blade is located at the top of the evaporation disc, the first bevel gear and the second bevel gear are located in the protective shell, the transmission shaft is fixedly connected with the oil discharge pipe, the rotating shaft penetrates through the evaporation tank and is rotatably connected with the evaporation tank, and the rotating shaft penetrates through the protective shell and is rotatably connected with the protective shell.
[0019] As a further optimization scheme of the present application, the tar pool is fixedly connected with a liquid feeding pipe, the outer surface of the evaporation tank is fixedly connected with an observation window, the top of the evaporation tank is fixedly connected with a steam pipe, the top of the tar pool is hingedly connected with a pool cover, the pool cover is sealingly attached to the tar pool, the top of the tar pool is fixedly connected with a one-way exhaust pipe, the one-way exhaust pipe is fixedly connected with the evaporation tank, and the sidewall of the tar pool is fixedly connected with a residue discharge pipe.
[0020] The present application has the following advantages:
[0021] 1. The present application can continuously inject phenolic wastewater into the evaporation mechanism through the cooperation of the liquid pumping mechanism and the evaporation mechanism, and the evaporation mechanism can evaporate the phenolic water in the phenolic wastewater through the spiral evaporation channel, while the oil, tar and other liquids in the phenolic wastewater can be discharged during the evaporation of the phenolic water, avoiding the accumulation of oil, tar and other liquids in the phenolic wastewater, thereby shortening the time for the recovery and treatment of the phenolic wastewater, saving costs, reducing the burden of treating the phenolic wastewater, and improving the treatment efficiency.
[0022] 2. The present application can further improve the evaporation efficiency by using the evaporation disc, the spiral evaporation channel and the piercing head in cooperation. When the phenolic wastewater flows in the evaporation channel, the evaporation disc evaporates the phenolic water in the phenolic wastewater, and at the same time, the multiple piercing heads can divert the phenolic wastewater. As the phenolic water in the phenolic wastewater is gradually evaporated, there will be large droplets of phenolic water wrapped in tar. At this time, when the phenolic wastewater passes through the piercing head, the piercing head pierces the large droplets of phenolic water wrapped in tar, so that the phenolic water in the large droplets can flow out, thereby further evaporating the phenolic water, and completely evaporating the phenolic water in the phenolic wastewater, thereby shortening the treatment time of the phenolic wastewater, saving costs, and improving the recovery quality and efficiency of the phenolic water in the phenolic wastewater.
[0023] 3. The present application is provided by the spiral form of the infusion tube, so that the phenolic wastewater in the spiral form of the infusion tube, at this time due to the high temperature inside the evaporation tank, and the high temperature of the phenolic water vapor, at this time the evaporation tank and the high temperature of the phenolic water vapor will be heated to the phenolic wastewater in the infusion tube, improve the initial temperature of the phenolic wastewater, shorten the residence time of the phenolic water in the evaporation channel of the evaporation disc, thereby further improving the evaporation efficiency of the phenolic water in the phenolic wastewater, shorten the evaporation time of the phenolic water, save the cost.
[0024] 4. The present application is provided by the heat exchange pipe, the oil, tar and other unevaporated liquid will be discharged through the heat exchange pipe, at this time due to the oil, tar and other unevaporated liquid is the liquid produced after the phenolic wastewater is evaporated, so the oil, tar and other unevaporated liquid has high temperature, so when discharging through the heat exchange pipe, the phenolic wastewater in the tar pool will be heated, the initial temperature of the phenolic wastewater is improved, the evaporation time of the phenolic wastewater in the evaporation tank is shortened, thereby improving the flowability of the oil, tar and other substances in the phenolic wastewater, facilitating the subsequent evaporation of the phenolic water in the phenolic wastewater, and further improving the recycling efficiency of the phenolic water in the phenolic wastewater.
[0025] 5. The present application is provided by the exhaust mechanism, which can extract the phenolic water vapor formed by the evaporation of the phenolic wastewater in the evaporation tank, inject the phenolic water vapor into the kiln through the steam pipe, avoid the accumulation of the phenolic water vapor in the evaporation tank, cause the phenolic water vapor to recondense, thereby avoiding the need for the evaporation disc to evaporate the recondensed phenolic water vapor, further improving the treatment efficiency of the phenolic wastewater, saving resources, on the other hand, the evaporation disc can be driven to rotate, ensuring the uniformity of the heating of the evaporation disc, and making the phenolic wastewater flowing in the evaporation channel separate from other liquids under the action of centrifugal force, facilitating the evaporation of the phenolic water by the evaporation disc, further improving the evaporation efficiency of the phenolic water, shortening the treatment time of the phenolic water, and improving the treatment efficiency of the phenolic water. BRIEF DESCRIPTION OF DRAWINGS
[0026] Figure 1 is the overall front three-dimensional structure schematic diagram of the present application;
[0027] Figure 2 is the overall three-dimensional structure schematic diagram of the present application;
[0028] Figure 3 is the three-dimensional local sectional view of the present application;
[0029] Figure 4 is the three-dimensional local sectional view of the present application; Figure 3 is the three-dimensional local sectional view of the present application;
[0030] Figure 5is a schematic diagram of a positive middle part cut structure of the present application;
[0031] Figure 6 is a schematic diagram of a top cut structure of the present application;
[0032] Figure 7 is a schematic diagram of a three-dimensional structure of the infusion tube of the present application;
[0033] Figure 8 is a schematic diagram of a three-dimensional structure of the evaporation disc of the present application.
[0034] In the figure: 1, tar pool; 2, evaporation tank; 3, observation window; 4, steam pipe; 5, liquid adding pipe; 6, liquid pumping mechanism; 601, water pump; 602, water pumping pipe; 603, filter ball; 604, liquid injection pipe; 605, infusion tube; 606, liquid discharging pipe; 7, evaporation mechanism; 701, electric heater; 702, evaporation disc; 703, evaporation channel; 704, piercing head; 705, oil discharging pipe; 8, oil discharging mechanism; 801, oil pump; 802, oil pumping pipe; 803, oil storage pipe; 804, heat exchange pipe; 9, air discharging mechanism; 901, servo motor; 902, rotating shaft; 903, first bevel gear; 904, protective shell; 905, second bevel gear; 906, transmission shaft; 907, fan blade; 10, pool cover; 11, one-way air discharging pipe; 12, slag discharging pipe. DETAILED DESCRIPTION
[0035] It is necessary to point out here that the following detailed description is only used to further illustrate the present application and cannot be understood as limiting the protection scope of the present application. Those skilled in the art can make some non-essential improvements and adjustments to the present application according to the above application content.
[0036] Embodiment: as Figure 1 , Figure 2 , Figure 3 , Figure 5 , Figure 6 , Figure 7 and Figure 8As shown, a phenol water recycling device, including tar pool 1 and evaporation tank 2, the tar pool 1 is fixedly connected with liquid adding pipe 5, liquid adding pipe 5 is used for adding phenolic sewage to tar pool 1, and the particulate impurities in the phenolic sewage will be precipitated in the tar pool 1, the outer surface of the evaporation tank 2 is fixedly connected with the observation window 3, the observation window 3 is used for observing the evaporation of the phenolic sewage in the evaporation tank 2, the top of the evaporation tank 2 is fixedly connected with the steam pipe 4, the steam pipe 4 is fixedly connected with the kiln, the kiln is used for burning the phenolic water vapor generated by the evaporation of the phenolic sewage (the kiln is prior art, not shown in the figure, not described in detail), the top of the tar pool 1 is hingedly connected with the pool cover 10, and the pool cover 10 is sealingly attached to the tar pool 1, the pool cover 10 is provided to facilitate cleaning the tar pool 1, the top of the tar pool 1 is fixedly connected with the one-way exhaust pipe 11, the one-way exhaust pipe 11 is fixedly connected with the evaporation tank 2, a one-way valve is installed in the one-way exhaust pipe 11, so that the gas in the tar pool 1 can only be discharged to the evaporation tank 2 through the one-way exhaust pipe 11, the sidewall of the tar pool 1 is fixedly connected with the deslagging pipe 12, a valve is installed in the deslagging pipe 12, which facilitates periodic cleaning of the precipitate in the tar pool 1, and further comprises: a liquid pumping mechanism 6 for connecting the tar pool 1 and the evaporation tank 2, the liquid pumping mechanism 6 is used to pump the phenolic sewage in the tar pool 1 into the evaporation tank 2, the evaporation tank 2 is fixedly connected with an evaporation mechanism 7, the liquid pumping mechanism 6 injects the phenolic sewage pumped into the evaporation tank 2 into the top of the evaporation mechanism 7, the evaporation mechanism 7 is used to evaporate the phenolic sewage, the evaporation mechanism 7 includes an electric heater 701 fixedly connected in the evaporation tank 2, a temperature sensor is installed in the evaporation tank 2 (the temperature sensor is prior art, not shown in the figure, not described in detail), which is used to detect the temperature inside the evaporation tank 2, the evaporation tank 2 is sealingly rotatably connected with an evaporation disc 702, the evaporation disc 702 is provided in a funnel-shaped structure, the evaporation disc 702 is provided at the top of the electric heater 701, the top of the evaporation disc 702 is provided with an evaporation channel 703, the top edge position of the evaporation disc 702 is provided in a concave shape and is communicated with the evaporation channel 703, in addition, a through slot is provided at the top of the evaporation disc 702, the through slot is used to communicate the top edge position of the evaporation disc 702 and the evaporation channel 703, the evaporation channel 703 is provided in a spiral shape, a plurality of piercing heads 704 are fixedly connected in the evaporation channel 703, the evaporation disc 702 is fixedly connected with an oil discharge pipe 705 at the middle part, the evaporation channel 703 is in communication with the inside of the oil discharge pipe 705, the oil discharge pipe 705 penetrates through the electric heater 701 and does not contact the electric heater 701.
[0037] In use, the phenolic wastewater is added into the tar pool 1 through the liquid adding pipe 5, and the particulate impurities in the phenolic wastewater will be precipitated in the tar pool 1, and then the electric heater 701 is started, and the temperature capable of evaporating the phenol water in the phenolic wastewater is set, the temperature sensor detects the temperature inside the evaporation tank 2, until the evaporation disc 702 reaches the corresponding temperature, at which time the liquid pumping mechanism 6 is started to pump the phenolic wastewater in the tar pool 1, and the phenolic wastewater is injected into the evaporation passage 703 opened at the top of the evaporation disc 702, so that the phenolic wastewater flows into the oil discharge pipe 705 through the spiral evaporation passage 703, and the phenolic wastewater entering the evaporation passage 703 will not overflow the evaporation passage 703. In this process, since the temperature of the evaporation disc 702 can evaporate the phenol water, the phenolic wastewater flowing in the evaporation passage 703 will evaporate the phenol water in the evaporation disc 702. During the evaporation and flow of the phenolic wastewater in the evaporation passage 703, the multiple piercing heads 704 will cause the phenolic wastewater to branch, and as the phenol water in the phenolic wastewater is gradually evaporated, there will be large droplets of phenol water wrapped in tar. At this time, when the phenolic wastewater passes through the piercing head 704, the piercing head 704 can pierce the large droplets of phenol water wrapped in tar, so that the phenol water in the large droplets can flow out, thereby further evaporating the phenol water, so that the phenol water in the phenolic wastewater can be completely evaporated, shortening the treatment time of the phenolic wastewater, saving the cost, improving the recovery quality and recovery efficiency of the phenol water in the phenolic wastewater, and the phenol water vapor formed by the evaporation of the phenol water will be discharged into the kiln through the steam pipe 4 for combustion in the kiln, thereby reducing the disposal cost of the phenolic wastewater and reducing the production cost.
[0038] The oil, tar and other liquids not evaporated after the evaporation of the phenol water will flow into the oil discharge pipe 705.
[0039] As Figure 1 , Figure 2 , Figure 3 , Figure 5 , Figure 6 and Figure 7As shown, the liquid pumping mechanism 6 includes a water pump 601 fixedly connected to the top of the tar pool 1, one end of the water pump 601 is fixedly communicated with a water pumping pipe 602, the water pumping pipe 602 extends into the tar pool 1, the end of the water pumping pipe 602 away from the water pump 601 is fixedly communicated with a filter ball 603, the other end of the water pump 601 is fixedly communicated with a liquid injection pipe 604, the liquid injection pipe 604 is fixedly connected with the evaporation tank 2, the end of the liquid injection pipe 604 away from the water pump 601 is fixedly communicated with a liquid conveying pipe 605, the liquid conveying pipe 605 is arranged in a spiral form, and the liquid conveying pipe 605 is fixedly connected to the inner surface of the evaporation tank 2, the bottom of the liquid conveying pipe 605 is fixedly communicated with a liquid discharging pipe 606, the liquid discharging pipe 606 is arranged at the top of the evaporation disc 702, and the liquid discharging pipe 606 is fixedly connected with the inner surface of the evaporation tank 2, the top edge of the evaporation disc 702 is arranged in a concave shape to guide the phenolic wastewater discharged by the liquid discharging pipe 606 to enter the evaporation channel 703, and the plurality of through grooves can make the phenolic wastewater discharged by the liquid discharging pipe 606 quickly enter the evaporation channel 703, avoiding the accumulation of the phenolic wastewater and directly jumping over the evaporation channel 703 to enter the oil discharging pipe 705.
[0040] When the evaporation disc 702 reaches the corresponding temperature and the phenolic wastewater in the tar pool 1 needs to be pumped out, the water pump 601 is started to make the water pumping pipe 602 pump out the phenolic wastewater in the tar pool 1, and in the process of pumping, the filter ball 603 filters the phenolic wastewater to avoid the particulate impurities in the phenolic wastewater entering the evaporation tank 2 together with the phenolic wastewater, and avoid the particulate impurities polluting the evaporation tank 2, the phenolic wastewater pumped out by the water pump 601 through the water pumping pipe 602 will be discharged into the liquid conveying pipe 605 through the liquid injection pipe 604, at this time, since the liquid conveying pipe 605 is in a spiral form, the temperature inside the evaporation tank 2 is high, and high-temperature phenolic water vapor is generated, at this time, the evaporation tank 2 and the high-temperature phenolic water vapor will heat the phenolic wastewater in the liquid conveying pipe 605, increase the initial temperature of the phenolic wastewater, and further improve the evaporation efficiency of the phenolic water in the phenolic wastewater, shorten the evaporation time of the phenolic water, and save the cost, the phenolic wastewater entering the liquid conveying pipe 605 will be discharged into the evaporation disc 702 through the liquid discharging pipe 606 and enter the evaporation channel 703.
[0041] As shown in the drawings, Figure 1 , Figure 2 , Figure 3 , Figure 5 and Figure 6As shown, the device further comprises an oil discharging mechanism 8 fixedly connected to the bottom of the evaporation tank 2, which is used to discharge the liquid remaining after the phenolic wastewater is evaporated and heat the phenolic wastewater in the tar pool 1. The oil discharging mechanism 8 comprises an oil pump 801 fixedly connected to the outer surface of the tar pool 1. One end of the oil pump 801 is fixedly connected to a heat exchange pipe 804 arranged in an "S" shape. The heat exchange pipe 804 is arranged in the tar pool 1 and fixedly connected to the tar pool 1. The oil discharging end of the heat exchange pipe 804 extends out of the tar pool 1. The liquid feeding pipe 5 is located below the heat exchange pipe 804. The end of the heat exchange pipe 804 extending out of the tar pool 1 is fixedly connected to an oil storage tank, which is convenient for personnel to collect and process the oil, tar and other liquids not evaporated after the phenolic wastewater is evaporated (the oil storage tank is prior art and not shown in the figure, and will not be described in detail). The other end of the oil pump 801 is fixedly connected to an oil pumping pipe 802. The end of the oil pumping pipe 802 away from the oil pump 801 is fixedly connected to an oil storage pipe 803. The oil storage pipe 803 is sealingly and rotatably connected to the oil discharging pipe 705. The oil storage pipe 803 is fixedly connected to the bottom of the evaporation tank 2.
[0042] The oil, tar and other liquids not evaporated entering the oil discharging pipe 705 will fall into the oil storage pipe 803. After the phenolic wastewater is evaporated for a period of time, the oil pump 801 is started to draw the oil, tar and other liquids not evaporated in the oil storage pipe 803 through the oil pumping pipe 802. The drawn liquid will be discharged through the heat exchange pipe 804. At this time, since the oil, tar and other liquids not evaporated have a high temperature, when they are discharged through the heat exchange pipe 804, they will heat the phenolic wastewater in the tar pool 1, increase the initial temperature of the phenolic wastewater, and thus improve the flowability of the oil, tar and other liquids in the phenolic wastewater, which is convenient for subsequent evaporation of the phenolic wastewater, and further improves the recycling efficiency of the phenolic wastewater. The phenolic wastewater heated in the tar pool 1 will be partially evaporated under the action of temperature, and the gas formed by evaporation will be discharged into the evaporation tank 2 through the one-way exhaust pipe 11.
[0043] As Figure 3 , Figure 4 , Figure 5 , Figure 6 , Figure 7 and Figure 8Also shown, further comprising: an exhaust mechanism 9 fixedly connected in the evaporation tank 2, the exhaust mechanism 9 is used to drive the evaporation mechanism 7 to rotate and discharge the water vapor generated by heating the phenolic sewage in the evaporation tank 2, the exhaust mechanism 9 comprises a servo motor 901 fixedly connected on the outer surface of the evaporation tank 2 through a motor base, the output end of the servo motor 901 is fixedly connected with a rotating shaft 902, the rotating shaft 902 penetrates the evaporation tank 2 and is sealingly rotatably connected with the evaporation tank 2, the end of the rotating shaft 902 is fixedly connected with a first bevel gear 903, the inner surface of the evaporation tank 2 is fixedly connected with a protective shell 904, the rotating shaft 902 penetrates the protective shell 904 and is sealingly rotatably connected with the protective shell 904, the middle part of the protective shell 904 is penetratingly and sealingly rotatably connected with a transmission shaft 906, the transmission shaft 906 is rotatably connected with the evaporation tank 2, the transmission shaft 906 is fixedly connected with the oil discharge pipe 705, the outer surface of the transmission shaft 906 is fixedly connected with a second bevel gear 905, the second bevel gear 905 is engaged with the first bevel gear 903, the first bevel gear 903 and the second bevel gear 905 are located in the protective shell 904, the top end of the transmission shaft 906 is fixedly connected with a fan blade 907, the fan blade 907 is located at the top of the evaporation tank 2, and the one-way exhaust pipe 11 is located below the fan blade 907.
[0044] When the evaporation disc 702 reaches the corresponding temperature, the servo motor 901 is started, the working of the servo motor 901 will drive the first bevel gear 903 to rotate through the rotating shaft 902, the first bevel gear 903 will drive the transmission shaft 906 to rotate through the second bevel gear 905, the rotation of the transmission shaft 906 will drive the fan blade 907 and the oil discharge pipe 705 to rotate, the rotation of the fan blade 907 will extract the phenolic water vapor formed by the evaporation of the phenolic sewage in the evaporation tank 2, and the phenolic water vapor will be injected into the kiln through the steam pipe 4, avoiding the accumulation of the phenolic water vapor in the evaporation tank 2, causing the phenolic water vapor to recondense, thereby avoiding the evaporation disc 702 needing to evaporate the recondensed phenolic water vapor, further improving the treatment efficiency of the phenolic sewage, saving resources, and the rotation of the oil discharge pipe 705 will drive the evaporation disc 702 to rotate, ensuring the uniformity of the heating of the evaporation disc 702, and making the flowing phenolic sewage in the evaporation channel 703 separate the phenolic water and other liquids under the action of centrifugal force, facilitating the evaporation of the phenolic water by the evaporation disc 702, further improving the evaporation efficiency of the phenolic water, shortening the phenolic water treatment time and improving the phenolic water treatment efficiency.
[0045] The specific working principle of the present application is as follows:
[0046] In use, the phenolic wastewater is added to the tar pool 1 through the liquid adding pipe 5, and the particulate impurities in the phenolic wastewater will precipitate in the tar pool 1, and then the electric heater 701 is started, and the temperature capable of evaporating the phenolic water in the phenolic wastewater is set, until the evaporation disc 702 reaches the corresponding temperature, the water pump 601 and the servo motor 901 are started, so that the water suction pipe 602 sucks the phenolic wastewater in the tar pool 1, and in the process of sucking, the filter ball 603 filters the phenolic wastewater to avoid the particulate impurities in the phenolic wastewater entering the evaporation tank 2 together with the phenolic wastewater, the phenolic wastewater sucked by the water pump 601 through the water suction pipe 602 will be discharged into the liquid conveying pipe 605 through the liquid injection pipe 604, at this time, since the liquid conveying pipe 605 is in a spiral form, and the temperature inside the evaporation tank 2 is high, and contains high-temperature phenolic water vapor, at this time, the evaporation tank 2 and the high-temperature phenolic water vapor will heat the phenolic wastewater in the liquid conveying pipe 605, to improve the initial temperature of the phenolic wastewater, thereby further improving the evaporation efficiency of the phenolic water in the phenolic wastewater, shortening the evaporation time of the phenolic water, saving the cost, and the phenolic wastewater entering the liquid conveying pipe 605 will be discharged into the top of the evaporation disc 702 through the liquid discharge pipe 606 and enter the evaporation channel 703;
[0047] The phenolic wastewater flows into the oil discharge pipe 705 through the spiral evaporation channel 703, and the phenolic wastewater entering the evaporation channel 703 will not overflow the evaporation channel 703, in this process, since the temperature of the evaporation disc 702 can evaporate the phenolic water, therefore, when the phenolic wastewater flows in the evaporation channel 703, the evaporation disc 702 will evaporate the phenolic water in the phenolic wastewater, and in the process of evaporation and flow of the phenolic wastewater in the evaporation channel 703, the multiple piercing heads 704 will cause the phenolic wastewater to branch, and as the phenolic water in the phenolic wastewater is gradually evaporated, there will be large droplets of phenolic water wrapped in tar, at this time, when the phenolic wastewater passes through the piercing head 704, the piercing head 704 can pierce the large droplets of phenolic water wrapped in tar, so that the phenolic water in the large droplets can flow out, thereby further evaporating the phenolic water, so that the phenolic water in the phenolic wastewater can be completely evaporated, shortening the treatment time of the phenolic wastewater, saving the cost, improving the recovery quality and recovery efficiency of the phenolic water in the phenolic wastewater, and the phenolic water vapor formed by the evaporation of the phenolic water will be discharged into the kiln through the vapor pipe 4 for combustion, thereby reducing the disposal cost of the phenolic wastewater and reducing the production cost;
[0048] Meanwhile, the operation of the servo motor 901 will drive the first bevel gear 903 to rotate through the rotating shaft 902, the first bevel gear 903 will drive the transmission shaft 906 to rotate through the second bevel gear 905, the rotation of the transmission shaft 906 will drive the fan blade 907 and the oil discharge pipe 705 to rotate, the rotation of the fan blade 907 will extract the phenol water steam formed by the evaporation of the phenol-containing sewage in the evaporation tank 2, and the phenol water steam will be injected into the kiln through the steam pipe 4, avoiding the accumulation of the phenol water steam in the evaporation tank 2, causing the phenol water steam to re-condense, thereby avoiding the evaporation disc 702 from evaporating the re-condensed phenol water steam, further improving the treatment efficiency of the phenol-containing sewage, saving resources, and the rotation of the oil discharge pipe 705 will drive the evaporation disc 702 to rotate, ensuring the uniformity of the heating of the evaporation disc 702, and at the same time, the phenol-containing sewage flowing in the evaporation channel 703 is separated from other liquids under the action of centrifugal force, facilitating the evaporation of the phenol water by the evaporation disc 702, further improving the evaporation efficiency of the phenol water, shortening the phenol water treatment time, and improving the phenol water treatment efficiency;
[0049] After the phenol water is evaporated, the oil, tar and other non-evaporated liquids formed will flow into the oil discharge pipe 705, the oil, tar and other non-evaporated liquids entering the oil discharge pipe 705 will fall into the oil storage pipe 803, and after the phenol-containing sewage is evaporated for a period of time, the oil pump 801 is started, so that the oil pump 801 extracts the oil, tar and other non-evaporated liquids in the oil storage pipe 803 through the oil extraction pipe 802, and the extracted liquids will be discharged through the heat exchange pipe 804, at this time, since the oil, tar and other non-evaporated liquids are liquids generated after the evaporation of the phenol-containing sewage, they have a high temperature, and when they are discharged through the heat exchange pipe 804, they will heat the phenol-containing sewage in the tar pool 1, increase the initial temperature of the phenol-containing sewage, and thus improve the fluidity of the oil, tar and other substances in the phenol-containing sewage, facilitate the subsequent evaporation of the phenol water in the phenol-containing sewage, and further improve the recycling efficiency of the phenol water in the phenol-containing sewage, and the heated phenol-containing sewage in the tar pool 1 will be partially evaporated under the action of temperature, and the gas formed by evaporation will be discharged through the one-way exhaust pipe 11 into the evaporation tank 2 and then discharged into the kiln through the steam pipe 4.
[0050] The above-described embodiments only express several embodiments of the present application, and the description is more specific and detailed, but it cannot be understood as a limitation on the scope of the present application. It should be noted that for ordinary skilled persons in the art, without departing from the concept of the present application, a number of modifications and improvements can be made, which are within the scope of protection of the present application.
Claims
1. A phenol water recycling device, comprising a tar tank (1) and an evaporator (2), characterized in that, Also includes: A pumping mechanism (6) for connecting the tar pool (1) and the evaporator (2) is used to pump phenol-containing wastewater from the tar pool (1) into the evaporator (2); An evaporation mechanism (7) is fixedly connected inside an evaporator (2) for evaporating phenol-containing wastewater. The pumping mechanism (6) pumps the phenol-containing wastewater into the evaporator (2) into the top of the evaporation mechanism (7). The evaporation mechanism (7) includes an electric heater (701) fixedly connected inside the evaporator (2). An evaporation plate (702) is rotatably connected inside the evaporator (2). The evaporation plate (702) is located on top of the electric heater (701). An evaporation channel (703) is opened on the top of the evaporation plate (702). The evaporation channel (703) is spiral-shaped. Multiple piercing heads (704) are fixedly connected to the top of the evaporation plate (702). Multiple piercing heads (704) are fixedly connected inside the evaporation channel (703). An oil drain pipe (705) is fixedly connected to the middle of the evaporation plate (702). An oil draining mechanism (8) is fixedly connected to the bottom of the evaporator (2). The oil draining mechanism (8) is used to extract the liquid remaining after the phenol-containing wastewater is evaporated and to heat the phenol-containing wastewater in the tar pool (1). An exhaust mechanism (9) is fixedly connected inside the evaporator (2). The exhaust mechanism (9) is used to drive the evaporator (7) to rotate and discharge the water vapor generated by heating the phenol-containing wastewater inside the evaporator (2).
2. The phenol water recycling device according to claim 1, characterized in that: The pumping mechanism (6) includes a water pump (601) fixedly connected to the top of the tar tank (1). One end of the water pump (601) is fixedly connected to a water pumping pipe (602). The water pumping pipe (602) extends into the tar tank (1). The end of the water pumping pipe (602) away from the water pump (601) is fixedly connected to a filter ball (603). The other end of the water pump (601) is fixedly connected to an injection pipe (604). The end of the injection pipe (604) away from the water pump (601) is fixedly connected to an infusion pipe (605). The bottom of the infusion pipe (605) is fixedly connected to a drain pipe (606).
3. The phenol water recycling device according to claim 2, characterized in that: The injection pipe (604) is fixedly connected to the evaporator (2), the delivery pipe (605) is set in a spiral shape and is fixedly connected to the inner surface of the evaporator (2), the drain pipe (606) is set on the top of the evaporation plate (702) and is fixedly connected to the inner surface of the evaporator (2).
4. The phenol water recycling device according to claim 1, characterized in that: The oil discharge mechanism (8) includes an oil pump (801) fixedly connected to the outer surface of the tar pool (1). One end of the oil pump (801) is fixedly connected to a heat exchange tube (804), and the other end of the oil pump (801) is fixedly connected to an oil extraction tube (802). The end of the oil extraction tube (802) away from the oil pump (801) is fixedly connected to an oil storage tube (803), and the oil storage tube (803) is fixedly connected to the bottom of the evaporator (2).
5. The phenol water recycling device according to claim 4, characterized in that: The heat exchange tube (804) is configured as an "S" shape. The heat exchange tube (804) is installed in the tar pool (1) and fixedly connected to the tar pool (1). The oil discharge end of the heat exchange tube (804) extends out of the tar pool (1). The oil storage tube (803) is sealed and rotatably connected to the oil discharge tube (705).
6. The phenol water recycling device according to claim 1, characterized in that: The exhaust mechanism (9) includes a servo motor (901) fixedly connected to the outer surface of the evaporator (2) via a motor mount. The output end of the servo motor (901) is fixedly connected to a rotating shaft (902). The end of the rotating shaft (902) is fixedly connected to a first bevel gear (903). The inner surface of the evaporator (2) is fixedly connected to a protective shell (904). The middle part of the protective shell (904) is rotatably connected to a transmission shaft (906). The transmission shaft (906) is rotatably connected to the evaporator (2). The outer surface of the transmission shaft (906) is fixedly connected to a second bevel gear (905). The second bevel gear (905) meshes with the first bevel gear (903). The top outer surface of the transmission shaft (906) is fixedly connected to a fan blade (907).
7. A phenol water recycling device according to claim 6, characterized in that: The first bevel gear (903) and the second bevel gear (905) are both located inside the protective shell (904). The drive shaft (906) is fixedly connected to the oil drain pipe (705). The rotating shaft (902) passes through the evaporator (2) and is rotatably and sealed to the evaporator (2). The rotating shaft (902) passes through the protective shell (904) and is rotatably and sealed to the protective shell (904).
8. The phenol water recycling device according to claim 1, characterized in that: A liquid addition pipe (5) is fixedly connected to the tar tank (1), an observation window (3) is fixedly connected to the outer surface of the evaporator (2), a steam pipe (4) is fixedly connected to the top of the evaporator (2), a tank cover (10) is hinged to the top of the tar tank (1), and the tank cover (10) is sealed and fitted to the tar tank (1), a one-way exhaust pipe (11) is fixedly connected to the top of the tar tank (1), the one-way exhaust pipe (11) is fixedly connected to the evaporator (2), and a slag discharge pipe (12) is fixedly connected to the side wall of the tar tank (1).
Citation Information
Patent Citations
Treatment method and device for phenol-containing water of gas generator
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