Separation device for production of antibacterial composition and preparation process
By designing a separation device with an automatic discharge mechanism, the problem of impurities not being automatically removed in existing technologies has been solved, achieving efficient solid-liquid separation and component recovery, and improving production efficiency.
Patent Information
- Application Number
- CN202511111212.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-08-08
- Publication Date
- 2025-11-07
AI Technical Summary
Existing separation devices used in the production of antibacterial compositions cannot automatically remove impurities during the separation process, resulting in low production efficiency.
A separation device comprising a separation tank, a storage tank, a flow guide ring groove, a discharge mechanism, and a drive assembly is designed. It achieves solid-liquid separation through high-speed rotation and centrifugal force, and is equipped with an automatic discharge mechanism that can remove residues without manual intervention.
It significantly improves solid-liquid separation efficiency, reduces component residue rate, increases the recovery rate of target components, and greatly shortens impurity cleaning time, thereby improving overall production efficiency.
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Figure CN120900286A_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The present application relates to the technical field of sugar derivatives, in particular to a separation device for producing an antibacterial composition and a preparation process. BACKGROUND
[0002] The antibacterial composition is obtained by extracting a plurality of traditional Chinese medicines by high-concentration ethanol (at least 92 vol %). The traditional Chinese medicines involved include clove, purple flower, cumin, prepared aconite, prepared Sichuan aconite, Sichuan pepper, asarum, cardamom, seven-leaf one-stemmed flower, indigo, borneol, henbane, dragon's blood, and tianbeimu. The extracts of these traditional Chinese medicines are the core basis for exerting antibacterial effect. They have significant curative effect on common gynecological inflammation and can inhibit common pathogenic bacteria of gynecological diseases (such as bacteria and fungi that may cause infection).
[0003] Chinese Patent No. CN219630787U discloses an antibacterial composition production separation device, which comprises a heating box, an adjusting column is rotatably connected to the inner side wall of the heating box, a drying column is rotatably connected to the inner side wall of the adjusting column, a plurality of liquid outlet holes are formed in the outer sides of the adjusting column and the drying column, a feeding funnel is fixedly installed on the top inner wall of the heating box, the outer sides of the feeding funnel are rotatably connected to the top outer sides of the adjusting column and the drying column, and a sealing plate is slidably connected to the inner side wall of the drying column. The patent document has the following beneficial effects: the adjusting column is rotatable outside the drying column. When the liquid outlet holes of the adjusting column and the drying column correspond, the filtrate and the filter residue can be preliminarily separated through the liquid outlet holes. The filtrate and the filter residue in the drying column can be further separated more efficiently through the high-speed rotation of the drying column outside the adjusting column. The water content in the filter residue can be greatly reduced, thereby improving the efficiency of the overall separation device in separating the antibacterial composition.
[0004] However, the above-mentioned patent document still has the following defects in the implementation process. Although the above-mentioned patent document can separate the antibacterial composition, it cannot remove the impurities generated during the separation process, and manual cleaning is still required, which reduces the overall production efficiency. SUMMARY
[0005] The main purpose of the present application is to provide a separation device for producing an antibacterial composition and a preparation process, which can effectively solve the problems raised in the background art.
[0006] To achieve the above-mentioned purpose, the technical scheme adopted by the present application is as follows: The utility model provides an anti -bacterial composition production is with separating device, including support frame, the middle part fixed mounting of support frame has the separation jar, the top of separation jar is provided with the feed pipe, the outside surface one side of separation jar is installed with the storage bucket, the other side of separation jar outside surface is provided with the storage box, the separation jar inner chamber upper portion is installed with the separating mechanism that the anti -bacterial composition is separated, the storage bucket inner chamber middle part upper side is installed with the flow guiding ring groove, the separation jar inner chamber is provided with the discharge mechanism, the separation jar inner chamber bottom is provided with drive assembly, The bottom wall of the flow guiding ring groove is inclined towards the storage bucket and is connected to the inner cavity of the storage bucket through an elbow pipe.
[0007] Preferably, the separating mechanism comprises a filter cartridge and a rotating shaft, the filter cartridge is rotatably installed at the top of the inner cavity of the separation jar, a plurality of clamping grooves are arranged in the lower end of the filter cartridge in a ring shape, the rotating shaft is rotatably installed at the top of the inner cavity of the separation jar, a plurality of fixed blocks are arranged on the outer surface of the rotating shaft in a ring shape, a plurality of rotating rods are rotatably installed in the fixed blocks, a plurality of pressure rollers are rotatably installed on the side of the rotating rods away from the fixed blocks, a plurality of elastic assemblies are arranged on the side of the pressure rollers close to the rotating shaft, and a clamping groove is arranged at the bottom of the rotating shaft.
[0008] Preferably, the elastic assembly comprises a guide pipe, the guide pipe is arranged on the outer surface of the rotating shaft, a spring is arranged in the inner cavity of the guide pipe, a sliding column is arranged on the side of the spring away from the rotating shaft, and the sliding column is arranged on the side of the pressure roller away from the rotating shaft.
[0009] Preferably, the discharge mechanism comprises a ring-shaped groove, the ring-shaped groove is arranged at the lower part of the inner cavity of the separation jar, a support turntable is rotatably installed in the ring-shaped groove, a plurality of springs are arranged on the upper part of the support turntable in a ring shape, a support disc is rotatably installed on the upper part of the springs, a clamping assembly is arranged at the middle part of the support disc, a scraping assembly is arranged on the upper part of the support disc, a plurality of clamping assemblies are arranged on the side of the support disc away from the axis in a ring shape, a scraper is arranged on the side of the support turntable away from the axis, the scraper slides in the inner cavity of the ring-shaped groove, and a discharge frame is arranged on one side of the bottom of the ring-shaped groove.
[0010] Preferably, the scraping assembly comprises a plurality of sliding rods, a plurality of scraping rings slide in the inner part of the support disc in a ring shape, the upper part of the sliding rods is rotatably installed with the scraping rings, and the lower end of the scraping rings is rotatably installed with a plurality of pressing columns.
[0011] Preferably, the clamping assembly comprises a plurality of fixed pipes, the fixed pipes are arranged on the side of the upper part of the support disc away from the axis in a ring shape, a spring is arranged in the inner cavity of the fixed pipes, the upper part of the spring is rotatably installed with a clamping column, the clamping column slides in the inner cavity of the fixed pipe, and the clamping column and the fixed pipe correspond to the inner cavity of the clamping groove.
[0012] Preferably, the clamping assembly two comprises a rotating cylinder, the rotating cylinder is rotatably installed in the middle of the supporting disc, a spring four is installed in the inner cavity of the rotating cylinder, a telescopic column is arranged in the inner part of the spring four, a clamping block is fixedly installed on the upper part of the telescopic column and the spring four, and the outer surface of the clamping block is corresponding to the inner cavity of the clamping groove two.
[0013] Preferably, the driving assembly comprises a partition plate, a motor and an electric telescopic cylinder, the partition plate is installed in the lower part of the separation tank, the motor is installed on one side of the bottom wall of the separation tank, the electric telescopic cylinder is installed on the other side of the bottom wall of the separation tank, a transmission assembly is arranged in the middle of the partition plate, a gear set is fixedly installed on the output end of the motor through a shaft coupling, a top plate is fixedly installed on the output end of the electric telescopic cylinder and penetrates the lower part of the partition plate, rotating columns are rotatably installed on the upper part of the top plate and the two sides thereof are symmetrical, a circular ring is arranged on the outer surfaces of the two rotating columns, the circular ring is fixedly installed on the lower ends of a plurality of sliding rods, and the gear set is composed of three meshing conical gears.
[0014] Preferably, the driving assembly comprises a transmission rod one, the transmission rod one is fixedly installed on the lower part of the supporting disc, a transmission column one is slidably installed in the inner cavity of the transmission rod one, a transmission rod two is movably installed in the inner cavity of the transmission column one, a transmission column two is slidably installed in the inner cavity of the transmission rod two, the upper end of the transmission rod two is fixedly installed on the lower end of the rotating cylinder, the lower part of the transmission column two penetrates the middle part of the lower conical gear and is fixedly installed on the middle part of the upper conical gear, and the lower part of the transmission column one is fixedly installed on the middle part of the upper conical gear.
[0015] An antibacterial composition preparation process based on a separation device for producing the antibacterial composition, characterized by the following specific production steps: S1, select the following combination of traditional Chinese medicinal materials: clove, purple night flower, cumin, prepared fuzi, prepared chuanwu, chuanjiao, fine xing, sand ginger, seven-leaf one-stemmed flower, green daub, ice piece, tianshenzi, blood oozing, earth beimu, then weigh and match the traditional Chinese medicinal materials according to the conventional dosage; S2, put the mixed traditional Chinese medicinal raw materials into the extraction tank, add at least 92vol% of ethanol solution, control the solid-liquid ratio to be 1:8-1:15, and constant-temperature stirring extraction is carried out at 60-70℃ for 1-2 hours, and the alcohol extraction mixed liquor containing medicinal residues is obtained after extraction is completed; S3, according to the ratio of traditional Chinese medicinal extract: synergistic component = 1-20:1, carboxymethyl konjac oligosaccharide L-guluronate octasaccharide is added into the above alcohol extraction liquid and stirred uniformly to form an antibacterial combination liquid; S4, through the connecting pipeline or manual filling mode, the antibacterial combination liquid is sent into the inner cavity of the separation tank of the separation device through the feeding pipe; S5, start the driving assembly to drive the separation mechanism to rotate at high speed to separate the antibacterial mixed liquid; S6, then start the drive assembly to drive the discharge mechanism movement to scrape off the separated residue, then through the discharge mechanism rotation makes the impurities through the centrifugal force to throw out the inside of the separation tank into the storage box, realizes the automatic slagging under the non-manual intervention.
[0016] Compared with the prior art, the present application has the following beneficial effects: 1、 In the present application, the separation mechanism can roll and extrude the attached residue during the separation of the antibacterial composition, can perform secondary deep separation on the solid impurities in the viscous material, effectively breaks the adsorption and combination of the solid impurities and the liquid, significantly improves the separation efficiency of the solid impurities and the liquid, reduces the residual rate of the components, and effectively improves the recovery rate of the target components.
[0017] 2、 In the present application, the discharge mechanism and the drive assembly cooperate to scrape off the residual impurities in the antibacterial composition after separation, avoid the component loss caused by the adhesion of the viscous material to the inner wall, and significantly improve the recovery rate of the effective components in the antibacterial composition.
[0018] 3、 In the present application, the discharge mechanism and the drive structure can be automatically completed through mechanical structure without manual intervention, greatly shortens the impurity cleaning time, reduces the downtime caused by manual cleaning, and effectively improves the overall production efficiency. BRIEF DESCRIPTION OF DRAWINGS
[0019] Figure 1 It is a schematic view of the overall structure of the present application; Figure 2 It is another view of the overall structure of the present application; Figure 3 It is a sectional structure schematic view of the separation mechanism of the present application; Figure 4 It is a sectional structure schematic view of the elastic assembly of the present application; Figure 5 It is a sectional structure schematic view of the discharge mechanism of the present application; Figure 6 It is a sectional structure schematic view of the scraping assembly of the present application; Figure 7 It is a sectional structure schematic view of the annular groove of the present application; Figure 8 It is a sectional structure schematic view of the Figure 5 It is an enlarged view schematic view of A in the present application; Figure 9 It is an enlarged view schematic view of B in the present application; Figure 5 Figure 10 It is a sectional structure schematic view of the drive assembly of the present application; Figure 11 It is a sectional structure schematic view of the transmission assembly of the present application.
[0020] In the diagram: 1. Support frame; 2. Separating tank; 3. Storage tank; 4. Storage box; 5. Separating mechanism; 51. Filter cartridge; 52. Slot 1; 53. Rotating shaft; 54. Fixing block; 55. Rotating rod; 56. Elastic component; 561. Guide tube; 562. Spring 1; 563. Sliding column; 57. Pressure roller; 58. Slot 2; 6. Guide ring groove; 7. Discharge mechanism; 71. Annular groove; 72. Support turntable; 73. Spring 2; 74. Support plate; 75. Scraping component; 751. Scraper ring; 752. Sliding rod; 753. Pressure column; 76 77. Scraper; 78. Discharge frame; 79. Engaging assembly one; 70. Fixing pipe; 71. Spring three; 72. Locking column; 73. Engaging assembly two; 74. Rotary drum; 75. Spring four; 76. Telescopic column; 77. Locking block; 88. Drive assembly; 89. Partition plate; 80. Motor; 81. Gear set; 80. Electric telescopic cylinder; 81. Ring; 82. Top plate; 83. Rotary column; 84. Transmission assembly; 85. Transmission rod one; 86. Transmission column one; 87. Transmission column two; 88. Transmission rod two; 9. Feed pipe. Detailed Implementation
[0021] To make the technical means, creative features, objectives and effects of this invention easier to understand, the invention will be further described below in conjunction with specific embodiments.
[0022] Example 1, as Figures 1 to 11 As shown, a separation device for producing antibacterial compositions includes a support frame 1, a separation tank 2 fixedly installed in the middle of the support frame 1, a feed pipe 9 provided at the top of the separation tank 2, a storage tank 3 installed on one side of the outer surface of the separation tank 2, a storage box 4 provided on the other side of the outer surface of the separation tank 2, a separation mechanism 5 for separating antibacterial compositions installed in the upper part of the inner cavity of the separation tank 2, a flow guide ring groove 6 installed on the upper side of the middle part of the inner cavity of the storage tank 3, a discharge mechanism 7 provided in the inner cavity of the separation tank 2, and a drive assembly 8 provided at the bottom of the inner cavity of the separation tank 2. The bottom wall of the flow guide ring groove 6 is inclined toward the storage tank 3 and is connected to the inner cavity of the storage tank 3 through a bend.
[0023] The antibacterial composition to be separated is first put into the separation mechanism 5 by the operator through the feeding pipe 9, then the driving structure of the driving assembly 8 is started to drive the internal structure of the separation mechanism 5 to rotate at high speed, and then the centrifugal force generated during the high-speed rotation of the internal structure of the separation mechanism 5 realizes efficient separation of the antibacterial composition by using the density difference between solid and liquid, and at the same time, the solid impurities contained in the antibacterial composition are thrown to the inner wall of the internal structure of the separation mechanism 5 under the action of the centrifugal force. At the same time, the internal structure of the separation mechanism 5 is driven to rotate in the opposite direction under the action of the internal structure of the driving assembly 8, which rolls and extrudes the residues attached to the inner wall of the separation mechanism 5 under the action of the reverse rotation of the internal structure of the separation mechanism 5, effectively breaking the adsorption and combination of the solid impurities and the liquid, significantly improving the separation efficiency of the solid impurities and the liquid, and reducing the residual rate of the components. Then the antibacterial composition separated by centrifugation falls into the flow guide ring groove 6 through the surface of the separation mechanism 5, and then flows into the storage barrel 3 through the elbow pipe under the action of the inclined bottom wall of the flow guide ring groove 6 for storage. Then when the antibacterial composition is separated, the impurities remaining in the separation mechanism 5 need to be cleaned. At this time, the internal structure of the driving assembly 8 is started again to drive the internal structure of the discharge mechanism 7 to rise, which can tightly fit the internal structure wall of the separation mechanism 5 during the rising process, so as to scrape off the impurities attached to the internal structure and fall off. When the internal structure of the separation mechanism 5 is scraped off, the internal structure of the discharge mechanism 7 is lowered again by the driving assembly 8, and when the internal structure of the discharge mechanism 7 is lowered to a certain extent, it is extruded to lower a certain distance. The dropped residues are also lowered a certain distance at the same time, and the residues are lowered to the lower part of the flow guide ring groove 6. Then the internal structure of the discharge mechanism 7 is rotated by the internal structure of the driving assembly 8, so that the residues falling on the surface of the discharge mechanism 7 are thrown to the surrounding by centrifugal force. At the same time, the internal structure of the discharge mechanism 7 rotates around its axis during the rotation process, and at the same time, the impurities thrown to the surrounding are scraped into the storage box 4 for storage. The whole process does not need manual intervention. After the impurities are cleaned, the internal structure of the discharge mechanism 7 is raised by the internal structure of the driving assembly 8, so that the internal structure is reset. The internal structure can be smoothly and accurately engaged with the bottom of the separation mechanism 5, so as to ensure stable transmission of driving force during the next separation.
[0024] In order to achieve the purpose of separating the antibacterial composition, reference is made to Figure 3 and Figure 4In the scheme, the separating mechanism 5 comprises a filter cartridge 51 and a rotating shaft 53, the filter cartridge 51 is rotatably installed at the top of the inner cavity of the separation tank 2, a plurality of clamping grooves one 52 are arranged at the lower end of the filter cartridge 51 in a ring shape, the rotating shaft 53 is rotatably installed at the top of the inner cavity of the separation tank 2, a plurality of fixed blocks 54 are arranged on the outer surface of the rotating shaft 53 in a ring shape, a rotating rod 55 is rotatably installed in each of the fixed blocks 54, a pressing roller 57 is rotatably installed on the side of each of the two adjacent rotating rods 55 away from the same side fixed block 54, an elastic assembly 56 is arranged on the side of each of the pressing rollers 57 close to the rotating shaft 53, and a clamping groove two 58 is arranged at the bottom of the rotating shaft 53.
[0025] In the above, first, the antibacterial composition is poured into the filter cartridge 51 through the feeding pipe 9, then the internal structure of the discharging mechanism 7 is driven to rotate by the driving assembly 8, then the internal structure of the discharging mechanism 7 is clamped in the inner cavities of the clamping grooves one 52 and the clamping grooves two 58, then the filter cartridge 51 starts to rotate by the rotation of the internal structure of the discharging mechanism 7, and the antibacterial composition is separated, at the same time, the rotating shaft 53 is driven to rotate in the opposite state by the internal structure of the discharging mechanism 7 clamped in the inner cavity of the clamping groove two 58 while the filter cartridge 51 rotates, then the rotating shaft 53 drives the rotating rods 55 to rotate synchronously in the high-speed rotating process, then the pressing rollers 57 are thrown outward with the rotating shaft 53 as the axis under the action of the high-speed rotating centrifugal force, and the pressing rollers 57 rotate by tightly adhering to the wall surface of the filter cartridge 51 through the centrifugal force, so that the pressing rollers 57 roll and extrude the solid impurities thrown on the surface of the filter cartridge 51 by the centrifugal force, thereby performing secondary deep separation on the solid impurities in the viscous material, and significantly improving the separation efficiency of the solid impurities and the liquid.
[0026] Specifically, in order to achieve the purpose of throwing the pressing roller 57 to the wall surface of the filter cartridge 51, referring to Figure 4 In the scheme, the elastic assembly 56 comprises a guide pipe 561, the guide pipe 561 is arranged on the outer surface of the rotating shaft 53, a spring one 562 is arranged in the inner cavity of the guide pipe 561, a sliding column 563 is arranged on the side of the spring one 562 away from the rotating shaft 53, and the sliding column 563 is arranged on one side of the pressing roller 57 away from the rotating shaft 53.
[0027] In the above, the rotating rods 55 are thrown outward in the high-speed rotating process of the rotating shaft 53, the pressing roller 57 pulls the sliding column 563 to move outward in the inner cavity of the guide pipe 561 in the throwing process, then the sliding column 563 pulls the spring one 562 to deform, and the rotating shaft 53 can pull the pressing roller 57 back to the initial position under the action of the spring one 562 when it stops rotating, which can prevent the filter cartridge 51 from being scraped and collided after separation.
[0028] In order to achieve the purpose of automatically scraping and collecting the separated solid residues, referring toFigure 5 、 Figure 6 、 Figure 7 、 Figure 8 and Figure 9 In the scheme, the discharging mechanism 7 comprises an annular groove 71 arranged at the lower part of the inner cavity of the separation tank 2, a support turntable 72 rotatably arranged inside the annular groove 71, a plurality of spring II 73 arranged in an annular distribution on the upper part of the support turntable 72, a support disc 74 commonly arranged on the upper part of the plurality of spring II 73, a clamping assembly II 79 arranged at the middle part of the support disc 74, a scraping assembly 75 arranged on the upper part of the support disc 74, a plurality of clamping assembly I 78 arranged in an annular distribution on the side of the upper part of the support disc 74 away from the axis thereof, a scraper 76 arranged on the side of the upper part of the support turntable 72 away from the axis thereof, the scraper 76 sliding in the inner cavity of the annular groove 71, and a discharging frame 77 arranged at one side of the bottom of the annular groove 71.
[0029] After the separation of the antibacterial mixture, first, the internal structure of the driving assembly 8 is started to drive the scraping assembly 75 to move upward, and in the process of upward movement of the internal components of the scraping assembly 75, the internal structure of the scraping assembly 75 is attached to the wall surface of the filter cartridge 51 to scrape upward, then the scraped solid residues directly fall on the upper part of the support disc 74, after the scraping of the residues is completed, the internal structure of the driving assembly 8 is driven to lower the scraping assembly 75, then when the scraping assembly 75 is lowered to a certain extent, the upper end of the support disc 74 is pressed to continue to lower, so that the upper part of the support disc 74 is separated from the lower part of the shaft 53 and the filter cartridge 51, the support disc 74 is pressed by the spring II 73, then when the support disc 74 is lowered by a certain distance beyond the bottom of the flow guide ring groove 6, the internal structure of the driving assembly 8 is started to rotate, thereby driving the support disc 74 and the support turntable 72 to rotate, then in the process of synchronous rotation of the support disc 74, the residues hanging on the upper part are thrown to the inner cavity of the annular groove 71 by the centrifugal force, then in the process of synchronous rotation of the support turntable 72, the scraper 76 is synchronously rotated, so that the scraper 76 rotates around the axis of the support turntable 72 to scrape the impurities falling in the inner cavity of the annular groove 71 into the internal part of the discharging frame 77, then the impurities are stored in the internal part of the storage box 4 through the sliding of the discharging frame 77.
[0030] Specifically, in order to achieve the purpose of scraping the inner wall of the filter cartridge 51, with reference to Figure 6 In the scheme, the scraping assembly 75 comprises a plurality of sliding rods 752, a plurality of scraping rings 751 arranged in an annular distribution inside the support disc 74, the scraping rings 751 commonly arranged on the upper part of the plurality of sliding rods 752, and a plurality of pressing columns 753 arranged in an annular distribution on the lower end of the scraping rings 751.
[0031] In the above, the internal structure of the driving assembly 8 simultaneously pushes the plurality of slide rods 752 to move upward, and then the plurality of slide rods 752 are simultaneously slid upward in the support disc 74 to push the scraping ring 751 to move and scrape the wall surface of the filter drum 51, so as to scrape off the solid impurities attached to the surface of the filter drum 51, and then after the scraping is completed, the internal structure of the driving assembly 8 simultaneously drives the plurality of slide rods 752 to descend, and then when the slide rods 752 descend to a certain distance, the pressure column 753 is lowered to lower the support disc 74, so as to realize the lowering of the support disc 74 to the lower side of the flow guide ring groove 6.
[0032] Specifically, in order to achieve the purpose of returning the support disc 74 to the original position after the solid impurities are cleaned, with the purpose of facilitating the next separation, referring to Figure 8 and Figure 9 In the present scheme, the clamping assembly one 78 comprises a plurality of fixed pipes 781, which are annularly arranged on one side of the upper part of the support disc 74 away from the shaft center, the inner cavities of the plurality of fixed pipes 781 are provided with springs three 782 at the bottom, the upper parts of the plurality of springs three 782 are fixedly installed with clamping columns 783, the plurality of clamping columns 783 are slidably connected to the inner cavities of the same side fixed pipes 781, and the plurality of clamping columns 783 and fixed pipes 781 correspond to the inner cavities of the same side clamping grooves one 52.
[0033] Further, the clamping assembly two 79 comprises a rotating drum 791 rotatably installed in the middle part of the support disc 74, the rotating drum 791 is installed with springs four 792 in the inner cavity, the springs four 792 are provided with telescopic columns 793 inside, the telescopic columns 793 and the springs four 792 are fixedly installed with clamping blocks 794 at the upper parts, and the outer surfaces of the clamping blocks 794 correspond to the inner cavities of the clamping grooves two 58.
[0034] In the above, after the impurities are thrown off by the falling support disc 74 driven by the internal structure of the driving assembly 8, the driving assembly 8 lifts the plurality of slide rods 752 to a certain height to release the downward pressure of the support disc 74 by the pressure column 753, and then the plurality of springs 73 release the compressed force to push the support disc 74 upward, while moving upward, the plurality of clamping columns 783 contact the bottom wall of the clamping groove one 52, and the plurality of clamping blocks 794 are released from the bottom of the clamping groove two 58, then the internal driving structure of the driving assembly 8 drives the support disc 74 to rotate, the support disc 74 rotates to drive the plurality of fixed pipes 781 to rotate, then the plurality of fixed pipes 781 drive the plurality of clamping columns 783 to rotate synchronously, then when the clamping columns 783 rotate to a certain position, the plurality of clamping columns 783 are pushed into the internal cavity of the clamping groove one 52 on the same side under the action of the spring three 782, and the rotating drum 791 is driven to rotate in the opposite direction of the support disc 74 by the internal structure of the driving assembly 8, so that the clamping block 794 is driven to rotate synchronously by the telescopic column 793, and then the clamping block 794 is clamped into the internal cavity of the clamping groove two 58 under the action of the spring four 792 after rotating by a certain angle. Then, after clamping, the fixed pipe 781 and the rotating drum 791 enter the internal cavities of the clamping groove one 52 and the clamping groove two 58 respectively under the action of the spring two 73, and the support disc 74 is tightly attached to the lower end of the filter cartridge 51.
[0035] In order to achieve the purpose of driving the filter cartridge 51 to rotate in the opposite direction of the rotating shaft 53, reference is made to Figure 10 and Figure 11 In the present scheme, the driving assembly 8 comprises a partition plate 81, a motor 82 and an electric telescopic cylinder 84, the partition plate 81 is installed in the lower part of the internal cavity of the separation tank 2, the motor 82 is installed on one side of the bottom wall of the separation tank 2, the electric telescopic cylinder 84 is installed on the other side of the bottom wall of the separation tank 2, the partition plate 81 is provided with a transmission assembly 88 in the middle part, the output end of the motor 82 is fixedly installed with a gear set 83 through a shaft coupling, the output end of the electric telescopic cylinder 84 penetrates the lower part of the partition plate 81 and is fixedly installed with a top plate 86, the upper part of the top plate 86 is symmetrically provided with rotatingly installed rotating columns 87 on both sides, the outer surfaces of the two rotating columns 87 are commonly provided with a circular ring 85, the circular ring 85 is fixedly installed at the lower end of the plurality of slide rods 752, and the gear set 83 is composed of three meshing conical gears.
[0036] In the above, the lower parts of the plurality of slide rods 752 are fixedly installed on the upper part of the circular ring 85, then when it is necessary to scrape the wall surface of the filter cartridge 51, the top plate 86 is lifted by starting the electric telescopic cylinder 84 to drive the two rotating columns 87 to lift upward, so that the two rotating columns 87 push the circular ring 85 to lift, and at the same time during the rotating separation, the plurality of slide rods 752 drive the circular ring 85 to rotate by rotating, so that the lower part of the circular ring 85 slides on the surface of the rotating column 87.
[0037] Specifically, in order to achieve the purpose of being able to drive rotation when the support disc 74 rises or falls, with reference to Figure 10 and Figure 11 In the scheme, the driving assembly 8 includes a transmission rod one 881, which is fixedly installed at the lower part of the support disc 74, a transmission column one 882 is slidably installed in the inner cavity of the transmission rod one 881, a transmission rod two 884 is movably installed in the inner cavity of the transmission column one 882, a transmission column two 883 is slidably installed in the inner cavity of the transmission rod two 884, and the upper end of the transmission rod two 884 is fixedly installed at the lower end of the rotating drum 791. The lower part of the transmission column two 883 penetrates the upper conical gear and is fixedly installed in the middle of the lower conical gear, and the lower part of the transmission column one 882 is fixedly installed in the middle of the upper conical gear.
[0038] In the above, the transmission rod one 881 is driven to descend synchronously during the descent of the support disc 74, so that the transmission rod one 881 descends synchronously on the outer surface of the transmission column one 882, and at the same time the rotating drum 791 is pressed to descend and the transmission rod two 884 is pressed to descend on the surface of the transmission column two 883. Then the motor 82 is started to drive the vertical conical gear to rotate, thereby driving the two horizontal conical gears meshing with it to rotate at the same time, the transmission column one 882 is driven to rotate by the upper horizontal conical gear, and the transmission column two 883 is driven to reverse by the lower conical gear. The texture blocks on the surface can stabilize the transmission of the transmission rod one 881 and the transmission rod two 884 during rotation.
[0039] The present application also discloses an antibacterial composition preparation process with a separation device for producing an antibacterial composition. In particular, the antibacterial composition based on konjac oligosaccharide derivatives and the application thereof, the antibacterial composition comprises: a base ingredient of traditional Chinese medicine extract, specifically at least 92vol% of alcohol-extracted products of clove, purple nightshade flower, corydalis, prepared aconite tablet, prepared Szechuan aconite, Szechuan pepper, asarum, cardamom, seven-bark flower, indigo, borneol, henbane, dragon's blood and tianxianzi; and a synergistic ingredient of carboxymethyl konjac oligosaccharide and L-guluronic acid octasaccharide in a weight ratio of 1-20:1.
[0040] The antibacterial composition has significant curative effect on common gynecological inflammation, has short treatment course, high curative effect, fast healing time, and is not easy to relapse after healing, and has no obvious side effects. In addition, the composition also has excellent inhibitory effect on common pathogenic bacteria of gynecological diseases.
[0041] S1, select the following combination of traditional Chinese medicinal materials: clove, purple nightshade flower, corydalis, prepared aconite tablet, prepared Szechuan aconite, Szechuan pepper, asarum, cardamom, seven-bark flower, indigo, borneol, henbane, dragon's blood, and tianxianzi, then weigh and match the traditional Chinese medicinal materials according to the conventional dosage; S2, put the mixed traditional Chinese medicine raw materials into the extraction tank, add at least 92vol% ethanol solution, control the solid-liquid ratio to be 1:8~1:15, and extract at 60~70°C for 1~2 hours, to obtain an alcohol extraction mixture containing residues; S3, add carboxymethyl konjac oligosaccharide L-guluronate octasaccharide to the alcohol extraction mixture in a proportion of traditional Chinese medicine extract: synergistic component = 1~20:1, stir uniformly, and form an antibacterial mixture; S4, first, through a connecting pipe or manual injection, the antibacterial mixture is sent into the separation mechanism 5 inside the separation tank 2 through the feed pipe 9 for separation; S5, then start the motor 82 inside the driving assembly 8 to drive the transmission assembly 88 to rotate, then drive the rotating shaft 53 inside the separation mechanism 5 to rotate at high speed, and then drive the filter cylinder 51 to rotate at high speed to separate the antibacterial mixture; S6, then start the electric telescopic cylinder 84 inside the driving assembly 8 to push the circular ring 85 upward, then drive the slide rod 752 to rise by lifting the circular ring 85 upward, then drive the scraper ring 751 to rise by lifting the slide rod 752 upward, and scrape off the residues attached to the inner wall of the filter cylinder 51, then after the residues fall off, drive the scraper ring 751 to descend by the electric telescopic cylinder 84, and at the same time, drive the residues on the support disc 74 to descend to the lower part of the flow guide ring groove 6, then drive the support disc 74 to rotate by starting the motor 82, so that the impurities are thrown into the annular groove 71 by centrifugal force, then drive the scraper 76 to rotate by the rotation of the support disc 74, and scrape the residues to the storage box 4 for storage, realizing automatic residue cleaning without manual intervention.
[0042] The amount of raw materials used in traditional Chinese medicine alcohol extraction needs to consider both the effective component dissolution rate and the cost. Combined with the common formula of gynecological external preparations (such as suppositories and lotions), the conventional dosage range of single herb is approximately: Clove, Cnidium, Sichuan pepper: This type of medicine contains volatile oil or strong antibacterial components, and the dosage is usually moderate. The extraction amount of single herb is about 10~30g (for example, Cnidium is commonly used in 20~30g in gynecological preparations to ensure the dissolution of cnidim). Prepared Fuzi and prepared Sichuan aconite: This type of medicine has reduced toxicity after processing, and the dosage needs to be strictly controlled. The extraction amount of single herb is about 3~10g (to avoid residual toxic components, in line with the dosage requirements of processed aconite in the Chinese Pharmacopoeia); Paris polyphylla, indigo, and dragon's blood: The saponins in Paris polyphylla and the indigo components in indigo are the core antibacterial components, and the dosage is usually 5~20g. Dragon's blood is used as a blood-activating component, and the dosage is light, about 1~5g; Borneol, Fructus Amomi, Asarum: Borneol is a volatile component, and its dosage should be small (avoid excessive stimulation of mucous membranes), about 0.5-3 g; Fructus Amomi and Asarum contain volatile oil, and their dosages are about 3-10 g; Calceolaria, Semen Hyoscyami, Bolbostemma: Calceolaria (commonly used as an astringent component for external use) is about 2-8 g; Semen Hyoscyami (containing alkaloids, which need to be controlled in amount) is about 0.5-2 g; Bolbostemma (dispersing and antibacterial) is about 5-15 g; Alcohol extraction material liquid ratio: the ratio of traditional Chinese medicine to 92vol% ethanol is usually 1:8-1:15 (i.e. 1 g of medicinal material plus 8-15 mL of 92% ethanol), so as to ensure that the effective components are fully dissolved (for example, 300 g of mixed traditional Chinese medicine raw materials need to be added with 2400-4500 mL of 92% ethanol).
[0043] The above shows and describes the basic principles and main features of the present application and the advantages of the present application. Those skilled in the art should understand that the present application is not limited by the above examples, and the above examples and descriptions in the specification are only to illustrate the principles of the present application. Without departing from the spirit and scope of the present application, various changes and improvements can be made to the present application, and these changes and improvements all fall within the scope of the present application. The scope of protection of the present application is defined by the appended claims and their equivalents.
Claims
1. A separation device for the production of an antibacterial composition, comprising a support frame (1), characterized in that: The support frame (1) middle fixed mounting has separation tank (2), separation tank (2) top is provided with feed pipe (9), separation tank (2) outer surface one side is installed with storage bucket (3), separation tank (2) outer surface the other side is provided with storage box (4), separation tank (2) inner chamber upper portion is installed with the separation mechanism (5) that the antagonistic bacteria composition is separated, the storage bucket (3) inner chamber middle upper side is installed with the flow guiding ring groove (6), separation tank (2) inner chamber is provided with discharge mechanism (7), separation tank (2) inner chamber bottom is provided with drive assembly (8). The bottom wall of the flow guiding ring groove (6) is inclined towards the storage bucket (3) and is connected with the inner cavity of the storage bucket (3) through a bent pipe.
2. A separation device for the production of an antibacterial composition according to claim 1, characterized in that: The separation mechanism (5) comprises a filter cartridge (51) and a rotating shaft (53), the filter cartridge (51) is rotatably installed on the inner cavity top of the separation tank (2), a plurality of clamping grooves (52) are arranged on the lower end of the filter cartridge (51) in a ring shape, the rotating shaft (53) is rotatably installed on the inner cavity top of the separation tank (2), a plurality of fixed blocks (54) are arranged on the outer surface of the rotating shaft (53) in a ring shape, a plurality of rotating rods (55) are rotatably installed in the fixed blocks (54), a plurality of pressure rollers (57) are rotatably installed on the side of the rotating rods (55) away from the same side fixed block (54), a plurality of elastic assemblies (56) are arranged on the side of the pressure rollers (57) close to the rotating shaft (53), and a clamping groove (58) is arranged on the bottom of the rotating shaft (53).
3. A separation device for the production of an antibacterial composition according to claim 2, characterized in that: The elastic assembly (56) comprises a guide pipe (561), the guide pipe (561) is arranged on the outer surface of the rotating shaft (53), a spring (562) is arranged in the inner cavity of the guide pipe (561), a sliding column (563) is arranged on the side of the spring (562) away from the rotating shaft (53), and the sliding column (563) is arranged on the side of the pressure roller (57) away from the rotating shaft (53).
4. A separation device for the production of an antibacterial composition according to claim 2, characterized in that: The discharge mechanism (7) comprises a ring groove (71), the ring groove (71) is arranged on the lower part of the inner cavity of the separation tank (2), a support turntable (72) is rotatably installed in the ring groove (71), a plurality of springs (73) are arranged on the upper part of the support turntable (72) in a ring shape, a support disc (74) is rotatably installed on the upper part of the springs (73), a clamping assembly (79) is arranged on the middle part of the support disc (74), a scraping assembly (75) is arranged on the upper part of the support disc (74), a plurality of clamping assemblies (78) are arranged on the side of the support disc (74) away from the axis in a ring shape, a scraper (76) is arranged on the side of the support turntable (72) away from the axis, the scraper (76) slides in the inner cavity of the ring groove (71), and a discharge frame (77) is arranged on one side of the bottom of the ring groove (71). 5.The scraping assembly (75) comprises a plurality of sliding rods (752), a plurality of scraping rings (751) are annularly distributed and slide in the inner portion of the support disc (74), a plurality of the sliding rods (752) are commonly provided with the scraping rings (751) at the upper portion, and a plurality of the scraping rings (751) are annularly distributed and provided with a plurality of pressing columns (753) at the lower end.
6. A separation device for the production of an antibacterial composition according to claim 4, characterized in that: The first clamping assembly (78) comprises a plurality of fixed tubes (781), a plurality of the fixed tubes (781) are annularly distributed and arranged on the upper portion of the support disc (74) away from the axis, the inner cavity bottom of each of the fixed tubes (781) is provided with a spring three (782), the upper portion of each of the spring threes (782) is fixedly provided with a clamping column (783), each of the clamping columns (783) is slidingly connected to the inner cavity of the same side fixed tube (781), and each of the clamping columns (783) and the fixed tube (781) corresponds to the inner cavity of the same side clamping groove one (52).
7. A separation device for the production of an antibacterial composition according to claim 4, characterized in that: The second clamping assembly (79) comprises a rotating barrel (791), the rotating barrel (791) is rotatably installed at the middle portion of the support disc (74), the inner cavity of the rotating barrel (791) is provided with a spring four (792), the inner portion of the spring four (792) is provided with a telescopic column (793), the upper portion of the telescopic column (793) and the spring four (792) are commonly fixedly provided with a clamping block (794), and the outer surface of the clamping block (794) corresponds to the inner cavity of the clamping groove two (58).
8. A separation device for the production of an antibacterial composition according to claim 5, characterized in that: The driving assembly (8) comprises a partition plate (81), a motor (82) and an electric telescopic cylinder (84), the partition plate (81) is installed at the lower portion of the inner cavity of the separation tank (2), the motor (82) is installed on one side of the bottom wall of the separation tank (2), the electric telescopic cylinder (84) is installed on the other side of the bottom wall of the separation tank (2), the middle portion of the partition plate (81) is provided with a transmission assembly (88), the output end of the motor (82) is fixedly provided with a gear set (83) through a shaft coupling, the output end of the electric telescopic cylinder (84) penetrates the lower portion of the partition plate (81) and is fixedly provided with a top plate (86), the upper portion of the top plate (86) is symmetrically provided with two rotating columns (87) on both sides, the outer surfaces of the two rotating columns (87) are commonly provided with a circular ring (85), the circular ring (85) is fixedly installed at the lower end of a plurality of sliding rods (752), and the gear set (83) is composed of three meshing conical gears.
9. A separation device for the production of an antibacterial composition according to claim 8, characterized in that: The driving assembly (8) comprises a transmission rod one (881), the transmission rod one (881) is fixedly installed at the lower portion of the support disc (74), the inner cavity of the transmission rod one (881) is slidingly provided with a transmission column one (882), the inner cavity of the transmission column one (882) is movably provided with a transmission rod two (884), the inner cavity of the transmission rod two (884) is slidingly provided with a transmission column two (883), the upper end of the transmission rod two (884) is fixedly installed at the lower end of the rotating barrel (791), the lower portion of the transmission column two (883) penetrates the upper conical gear and is fixedly installed at the middle portion of the lower conical gear, and the lower portion of the transmission column one (882) is fixedly installed at the middle portion of the upper conical gear.
10. A process for the preparation of an antibacterial composition based on the antibacterial composition produced by the separation device according to any one of claims 1 to 9, characterized in that, The specific production steps are as follows: S1, select the following combination of Chinese herbal medicine: clove, purple night-blooming cereus, cumin, prepared appendage, prepared Sichuan aconite, Sichuan pepper, asarum, sand, seven-leaf branch flower, indigo, borneol, henbane, dragon's blood, earth peony, then the traditional dosage of Chinese herbal medicine weighing ratio; S2, the mixed Chinese herbal medicine into the extraction tank, add at least 92vol% ethanol solution, control the ratio of solid to liquid is 1:8~1:15 at 60~70℃ constant temperature stirring extraction 1~2 hours, after extraction obtained containing drug residue alcohol extract mixture; S3, to the above alcohol extract liquid according to the proportion of Chinese herbal medicine extract: synergistic component = 1~20:1 add: carboxymethyl konjac oligosaccharide L-guluronate octasaccharide stirring uniform, form antibacterial combination liquid; S4, through the connection pipeline or artificial injection, the antibacterial combination liquid through the feed pipe (9) into the separation tank (2) of the separation device inner chamber; S5, start the drive assembly (8), drive the separation mechanism (5) high speed rotation for antibacterial mixture separation; S6, then start the drive assembly (8) drive discharge mechanism (7) movement will be separated after the residue, then through the discharge mechanism (7) rotation makes impurities by centrifugal force throw out the separation tank (2) inside into the storage tank (4), realize automatic cleaning slag without manual intervention.
Citation Information
Patent Citations
Separating device for antibacterial composition production
CN219630787U