Salt dissolving device for ionic membrane caustic soda production

By installing filter barrels and assisting components in the ion membrane caustic soda production device, by-products are removed and stirred without additional power is solved, and the efficiency reduction caused by by-product adsorption is improved, and product purity and production efficiency are improved.

CN222131520UActive Publication Date: 2024-12-10ANHUI DONGZHI GUANGXIN AGROCHEMICAL CO LTD
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Patent Information

Application Number
CN202420363917.7
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-02-27
Publication Date
2024-12-10
Estimated Expiration
2034-02-27

AI Technical Summary

Technical Problem

During the caustic soda production process of ionic membranes, by-products are easily adsorbed on the ionic membrane, reducing separation efficiency, resulting in waste of resources and equipment blockage, affecting production efficiency.

Method used

A salt-chemical device for ion membrane caustic soda production including filter barrels and assisting components is designed to drive the scraper and fan blades to remove by-products through rotating rods, and stir without additional power through thin tubes and stirring plates, thereby improving catalyst use efficiency. and reaction uniformity.

Benefits of technology

Effectively prevent by-product blockage, improve the separation efficiency of the ion film, reduce incomplete reactions and side reactions, improve product purity and production efficiency, and reduce maintenance costs.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a salt dissolving device for ionic membrane caustic soda production, which relates to the technical field of ionic membrane caustic soda, and comprises a box body, a filter barrel is arranged in the box body, an assisting component is arranged in the filter barrel, the assisting component comprises a fixed block, the fixed block is fixedly connected to one side of the box body, a rotating rod is rotatably connected in the fixed block, and the rotating rod is fixedly connected to one side of the box body. A first catalyst flowing pipeline is arranged in the rotating rod, one end of the rotating rod penetrates through the side wall of the box body and extends into the filtering barrel, the other end of the rotating rod is fixedly connected with a thin pipe, the side wall of the end, extending into the filtering barrel, of the rotating rod is fixedly connected with a short rod, and a second catalyst flowing pipeline is arranged in the short rod; a stirring plate is fixedly connected to the side wall of the short rod, and a scraping rod is fixedly connected to the end, away from the rotating rod, of the short rod, so that the technical problem that the separation efficiency of the ionic membrane is reduced due to the fact that a large number of by-products are often generated during electrolysis and are adsorbed on the ionic membrane is solved.
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Description

Technical Field

[0001] The utility model relates to the technical field of ion membrane caustic soda, in particular to a salt-making device for producing ion membrane caustic soda. Background Art

[0002] The salt-making device for ion membrane caustic soda production is a device used to produce caustic soda (sodium hydroxide). Caustic soda is an important chemical raw material, widely used in glass, textile, papermaking, detergent, fertilizer and other industries. The salt-making device for ion membrane caustic soda production mainly consists of the following parts: The brine electrolyzer is the core part of the device, which is used for the electrolysis process. In the electrolyzer, the sodium chloride (salt) solution is decomposed into sodium hydroxide and chlorine by powering on. The ion membrane is a key element in the electrolyzer, which can separate positive and negative ions, allowing only sodium ions to pass through during the electrolysis process and preventing the passage of chloride ions. The membrane chamber is the area separating the positive and negative electrodes of the electrolyzer, and the electrolyzer is divided into the anode membrane chamber and the cathode membrane chamber by the ion membrane. The membrane chamber ensures the separation of cations and anions and avoids the generation and mixing of chlorine. The anode is located in the anode membrane chamber, and after powering on, an oxidation reaction is triggered to produce chlorine and water. The cathode is located in the cathode membrane chamber, and after powering on, a reduction reaction is triggered to produce hydrogen and sodium hydroxide. The ion membrane caustic soda production salt chemical device can realize the process of electrolysis of brine to produce sodium hydroxide and chlorine, and through the selective permeability of the ion membrane, the generated chlorine and hydrogen are collected and utilized separately. This device is highly efficient, environmentally friendly and economical.

[0003] After searching, the patent document (authorization announcement number is CN218795139U) includes: a box body; a connecting column, the connecting column is fixedly installed on the top of both sides of the box body, a placement bucket is fixedly installed on the inner side of the connecting column, a through hole is opened at the bottom of the placement bucket, and a first penetration hole is opened inside the placement bucket; a connecting frame, the connecting frame is fixedly installed on the top of the connecting column, and a motor is fixedly installed on the top of the connecting frame. The utility model provides a salt-making device for ion membrane caustic soda production, which can dissolve its salt in the placement bucket, and then when its volume becomes smaller, it enters the concentration bucket for dissolution, instead of directly in the box body for salt-making work, so there will be no dead angle due to the shape, size, etc. of the box body, resulting in insufficient stirring force, and the inability to effectively and quickly salt-make work, so the work efficiency can be improved.

[0004] However, the above practicality still has shortcomings:

[0005] 1. During the salt treatment, some materials will be on the surface of the liquid, which will cause the materials to fail to be electrolyzed successfully, causing them to be wasted and resulting in a waste of resources.

[0006] 2. During electrolysis, a large amount of by-products are often produced. These by-products will be adsorbed on the ion membrane, thereby reducing the separation efficiency of the ion membrane. Utility Model Content

[0007] The utility model aims to solve at least one of the technical problems existing in the prior art. To this end, the utility model proposes a salt-making device for producing ion membrane caustic soda, which solves the problem that a large amount of by-products are often generated during electrolysis, and these by-products are adsorbed on the ion membrane, thereby reducing the separation efficiency of the ion membrane.

[0008] To achieve the above object, the utility model provides a salt-making device for ion membrane caustic soda production, comprising a box body, a filter barrel is arranged inside the box body, and an auxiliary component is arranged inside the filter barrel, wherein:

[0009] The assisting assembly includes a fixed block, which is fixedly connected to one side of the casing, a rotating rod is rotatably connected inside the fixed block, a first catalyst flow conduit is provided inside the rotating rod, one end of the rotating rod passes through the side wall of the casing and extends into the filter barrel, a thin tube is fixedly connected to the other end of the rotating rod, a short rod is fixedly connected to the side wall of one end of the rotating rod extending into the filter barrel, a second catalyst flow conduit is provided inside the short rod, a stirring plate is fixedly connected to the side wall of the short rod, a scraper rod is fixedly connected to the end of the short rod away from the rotating rod, and a fan blade is fixedly connected to the side wall of the rotating rod extending into the filter barrel.

[0010] Preferably, the short rod is arranged between the fixing block and the fan blade, the second catalyst flow conduit is connected to the first catalyst flow conduit, and the surface of the stirring plate is provided with tiny holes.

[0011] Preferably, the scraper rod is arranged on the inner wall of the filter barrel.

[0012] Preferably, an ion membrane is fixedly connected to the interior of the box, and the ion membrane is arranged just above the filter barrel.

[0013] Preferably, a valve pipeline is fixedly connected to the other side of the box.

[0014] Compared with the prior art, the beneficial effects of the utility model are:

[0015] 1. Through the setting of the assisting component, when feeding, the material will flow into the filter barrel through the valve pipe. Because the material is liquid, the flow rate of the material will drive the fan blades to rotate. During electrolysis, the stirring plate can achieve the stirring effect. In addition, during electrolysis, the catalyst can be injected into the rotating rod through a thin tube, flow through the second catalyst flow pipe and finally flow out from the tiny holes on the stirring plate. The advantage of this design is that stirring can be performed without the need for additional power. Secondly, during stirring, the catalyst will directly contact the material through the stirring plate, so that the use efficiency of the catalyst is maximized. By improving the use efficiency of the catalyst, the reaction process can be better controlled, purer products can be produced, the generation of by-products can be reduced, and the quality of the product can be improved.

[0016] 2. During electrolysis, the material is injected into the box from the valve pipe. At this time, the material will flow from bottom to top. The flow of the material from bottom to top can provide better material transfer and mixing effects, so that the catalyst and the material can be better contacted. This helps to improve the uniformity of the reaction, reduce the occurrence of incomplete reactions and side reactions, and thus improve the selectivity and yield of the reaction.

[0017] 3. When the electrolysis is in progress, the rotation of the rotating rod will drive the short rod to rotate together. At this time, the scraper rod attached to the inner wall of the filter barrel will make a circular motion around the filter barrel. The scraper rod will scrape the by-products produced during the electrolysis process from the filter barrel. This can prevent the by-products from clogging the filter barrel, resulting in the material in the filter barrel being unable to leave the filter barrel after the electrolysis is completed. The advantage of this design is that it can first prevent the by-products from clogging the ion membrane and avoid economic losses. Secondly, ensuring the permeability of the filter barrel can reduce the clogging and blockage of the filter medium and reduce the maintenance and cleaning frequency of the equipment, which reduces the production line downtime and maintenance costs and improves production efficiency. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] Figure 1 It is a three-dimensional structural schematic diagram of the utility model;

[0019] Figure 2 It is a schematic diagram of the internal structure of the utility model;

[0020] Figure 3 This is a schematic diagram of the filter barrel structure of the utility model;

[0021] Figure 4 It is a schematic diagram of the rotating rod structure of the utility model.

[0022] In the figure: 1. box body; 2. ion membrane; 3. valve pipe; 4. filter barrel; 5. assisting component; 51. fixing block; 52. rotating rod; 521. first catalyst flow pipe; 53. capillary; 54. short rod; 541. second catalyst flow pipe; 55. stirring plate; 56. scraper rod; 57. fan blade. DETAILED DESCRIPTION

[0023] The technical solution of the utility model will be described clearly and completely in conjunction with the embodiments below. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of them. Based on the embodiments of the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0024] like Figure 1-4 As shown, a salt-making device for producing caustic soda with an ion membrane includes a housing 1, and an ion membrane 2 is fixedly connected to the interior of the housing 1. The ion membrane 2 is a membrane with selective permeability, which allows a specific type of ions to pass through and prevents the passage of other ions. In the salt-making device for producing caustic soda with an ion membrane 2, the ion membrane 2 is mainly used to separate chloride ions and hydroxide ions, thereby achieving the decomposition of salt and the production of caustic soda. The ion membrane 2 has a low resistance and a high conductivity, and can provide a good ion transfer channel, thereby achieving high electrolysis efficiency.

[0025] A filter barrel 4 is provided inside the housing 1, and the filter barrel 4 can filter out by-products generated during the electrolysis process to prevent these by-products from adhering to the ion membrane 2. Adherence of by-products may reduce the permeability and transfer efficiency of the ion membrane 2 and affect its normal operation.

[0026] The ion membrane 2 is arranged just above the filter barrel 4. When the electrolysis is performed, the material is injected into the box 1 from the valve pipe 3. At this time, the material will flow from bottom to top. The flow of the material from bottom to top can provide better material transfer and mixing effects, so that the catalyst and the material can be better contacted. This helps to improve the uniformity of the reaction, reduce the occurrence of incomplete reactions and side reactions, and thus improve the selectivity and yield of the reaction.

[0027] An assisting assembly 5 is provided inside the filter barrel 4, wherein: the assisting assembly 5 comprises a fixed block 51, the fixed block 51 is fixedly connected to one side of the box body 1, the other side of the box body 1 is fixedly connected to the valve pipe 3, the fixed block 51 is rotatably connected to a rotating rod 52 inside, a first catalyst flow pipe 521 is provided inside the rotating rod 52, one end of the rotating rod 52 passes through the side wall of the box body 1 and extends into the filter barrel 4, a capillary 53 is fixedly connected to the other end of the rotating rod 52, the rotating rod 52 extends to the side wall at one end of the filter barrel 4 and is fixedly connected to a short rod 54, a second catalyst flow pipe 541 is provided inside the short rod 54, and a stirring plate 55 is fixedly connected to the side wall of the short rod 54. When electrolysis is performed When the catalyst is injected into the rotating rod 52 through the capillary 53, it flows through the second catalyst flow conduit 541 and finally flows out from the tiny holes on the stirring plate 55. The end of the short rod 54 away from the rotating rod 52 is fixedly connected to a scraper rod 56, which is arranged on the inner wall of the filter barrel 4. When the electrolysis is carried out, the rotation of the rotating rod 52 will drive the short rod 54 to rotate together. At this time, the scraper rod 56 attached to the inner wall of the filter barrel 4 will make a circular motion around the filter barrel 4. The scraper rod 56 will scrape off the by-products produced during the electrolysis process from the filter barrel 4, so as to prevent the by-products from clogging the filter barrel 4, resulting in the material in the filter barrel 4 being unable to leave the filter barrel 4 after the electrolysis is completed.

[0028] The rotating rod 52 extends to the side wall at one end of the filter barrel 4 and is fixedly connected with a fan blade 57. When feeding, the material will flow into the filter barrel 4 through the valve pipe 3. Because the material is liquid, the flow rate of the material will drive the fan blade 57 to rotate, and the stirring plate 55 can achieve the stirring effect during electrolysis.

[0029] The short rod 54 is disposed between the fixing block 51 and the fan blade 57 , the second catalyst flow conduit 541 is connected to the first catalyst flow conduit 521 , and tiny holes are disposed on the surface of the stirring plate 55 .

[0030] Working principle: when feeding, the material will flow into the filter barrel 4 through the valve pipe 3. Because the material is liquid, the flow rate of the material will drive the fan blade 57 to rotate. During electrolysis, the stirring plate 55 can achieve the stirring effect. In addition, when electrolysis is performed, the catalyst can be injected into the rotating rod 52 through the capillary 53, flow through the second catalyst flow pipe 541 and finally flow out from the tiny holes on the stirring plate 55. The advantage of this design is that stirring can be performed without the need for additional power. Secondly, during stirring, the catalyst will directly contact the material through the stirring plate 55 to improve the catalytic efficiency. Then, the by-products produced during the electrolysis process will be left in the filter barrel 4 due to the action of the filter barrel 4, and the ions will flow through the ion membrane 2 to the top of the ion membrane 2, and the work is completed.

[0031] The above embodiments are only used to illustrate the technical method of the utility model rather than to limit it. Although the utility model is described in detail with reference to the preferred embodiments, ordinary technicians in the field should understand that the technical method of the utility model can be modified or replaced by equivalents without departing from the spirit and scope of the technical method of the utility model.

Claims

1. A salt-making device for producing ion-exchange membrane caustic soda, characterized in that: It comprises a box body (1), a filter barrel (4) is arranged inside the box body (1), and an auxiliary component (5) is arranged inside the filter barrel (4), wherein: The assisting assembly (5) comprises a fixed block (51), the fixed block (51) being fixedly connected to one side of the housing (1), the fixed block (51) being rotatably connected to a rotating rod (52) inside, a first catalyst flow conduit (521) being provided inside the rotating rod (52), one end of the rotating rod (52) passing through the side wall of the housing (1) and extending into the filter barrel (4), the other end of the rotating rod (52) being fixedly connected to a capillary (53), a short rod (54) being fixedly connected to the side wall of one end of the rotating rod (52) extending into the filter barrel (4), a second catalyst flow conduit (541) being provided inside the short rod (54), a stirring plate (55) being fixedly connected to the side wall of the short rod (54), a scraping rod (56) being fixedly connected to the end of the short rod (54) away from the rotating rod (52), and a fan blade (57) being fixedly connected to the side wall of one end of the rotating rod (52) extending into the filter barrel (4).

2. The salt-making device for producing ion-exchange membrane caustic soda according to claim 1, characterized in that: The short rod (54) is arranged between the fixed block (51) and the fan blade (57), the second catalyst flow conduit (541) is connected to the first catalyst flow conduit (521), and the surface of the stirring plate (55) is provided with tiny holes.

3. The salt-making device for producing ion-exchange membrane caustic soda according to claim 1, characterized in that: The scraper rod (56) is arranged on the inner wall of the filter barrel (4).

4. The salt-making device for producing ion-exchange membrane caustic soda according to claim 1, characterized in that: An ion membrane (2) is fixedly connected to the interior of the box (1), and the ion membrane (2) is arranged directly above the filter barrel (4).

5. The salt-making device for producing ion-exchange membrane caustic soda according to claim 1, characterized in that: The other side of the box body (1) is fixedly connected with a valve pipeline (3).