Hydrothermal synthesis workstation

Abstract

The utility model provides a hydrothermal synthesis workstation, and relates to the technical field of experimental equipment. The hydro-thermal synthesis workstation comprises a material storage module, a heating module, a drying module, a driving module and an operation module; the drying module comprises a plurality of gas transmission needles, each gas transmission needle at least can reciprocate in the Z-axis direction so as to extend out of or extend into the reagent bottle, and the gas transmission needles can blow dry gas into the heated reagent bottle; the driving module comprises an X-axis moving guide rail, a Y-axis moving guide rail and a Z-axis moving guide rail which are connected in sequence; the operation module is connected to the Z-axis moving guide rail, the operation module can move among other modules under the action of the driving module, and the operation module is used for clamping reagent bottles and taking or putting raw materials into the reagent bottles. Due to the fact that the drying module promotes the liquid to evaporate rapidly, and the gas transmission needle moves in a reciprocating mode, the drying process and the drying canceling process can be switched freely. The driving module drives the reagent bottles to move freely through the operation module, and the automation degree is improved.

Description

Technical Field

[0001] The present application relates to the technical field of experimental equipment, and in particular to a hydrothermal synthesis workstation. Background Art

[0002] With the continuous deepening of new material research, the demand for efficient and precise hydrothermal synthesis technology is growing. Traditional hydrothermal synthesis processes mostly rely on manual operation, which is not only time-consuming and inefficient, but also has great limitations in high-throughput experiments and precise control. Therefore, the development of an automated, high-throughput hydrothermal synthesis workstation is crucial to improving synthesis efficiency and quality. In recent years, automation and intelligent technologies have been increasingly used in the field of chemical synthesis, such as automated pipetting, precise temperature control, and high-precision actuators. The development of these technologies has greatly improved experimental efficiency and the repeatability of results, while reducing the possibility of human error. However, there is still a lack of rapid drying to obtain samples and the overall degree of automation. Utility Model Content

[0003] Based on this, it is necessary to provide a hydrothermal synthesis workstation to improve the degree of automation and quickly dry to obtain samples.

[0004] A hydrothermal synthesis workstation comprises a material storage module, a heating module, a drying module, a driving module and an operating module; the material storage module has a material storage station for storing reagent bottles; the heating module is used to heat the reagent bottles; the drying module comprises a plurality of gas delivery needles arranged at intervals, each of the gas delivery needles can at least reciprocate along the Z-axis direction to extend out of or extend into the reagent bottle, and the gas delivery needles can blow dry gas into the heated reagent bottle; the driving module comprises an X-axis movable guide rail, a Y-axis movable guide rail and a Z-axis movable guide rail connected in sequence; the operating module is connected to the Z-axis movable guide rail, the operating module can flow and move between the material storage module, the heating module and the drying module under the action of the driving module, and the operating module is used to clamp the reagent bottle and take or put raw materials in the reagent bottle.

[0005] It is understandable that a storage module is provided to centrally place reagent bottles. The drive assembly controls the operation module through the X-axis moving guide rail, the Y-axis moving guide rail and the Z-axis moving guide rail. The reagent bottle is clamped by the operation module and transferred to each different module. The operation module can also add raw materials to the reagent bottle or take the raw materials in the reagent bottle to facilitate mixing between the raw materials to form a chemical reaction. The heating module can heat the reagent bottle to meet the temperature conditions required for the chemical reaction. The drying module blows dry gas into the reagent bottle through the gas delivery needle to promote the rapid evaporation of the liquid in the reagent bottle, so as to quickly obtain the required sample, and the drying process and the process of canceling the drying process can be switched freely by moving the gas delivery needle up and down, and the operation is simple. The drive module is connected to the operation module to drive the reagent bottle to flow freely in other modules, which improves the overall automation of the hydrothermal synthesis workstation and can meet the needs of high-throughput and high-efficiency hydrothermal synthesis.

[0006] In one embodiment, the drying module includes a mounting bracket and a Z-axis driving mechanism connected to the mounting bracket, the Z-axis driving mechanism is used to drive the mounting bracket to move along the Z-axis, the mounting bracket is constructed with a plurality of mounting holes arranged at intervals, and each of the mounting holes is correspondingly installed with the gas supply needle.

[0007] It can be understood that the arrangement of the mounting bracket facilitates the installation of multiple gas delivery needles, and the Z-axis driving mechanism provides a power source for the movement of the mounting bracket, thereby facilitating the synchronous movement of multiple gas delivery needles along the Z-axis.

[0008] In one embodiment, the drying module further includes an X-axis driving mechanism, which is connected to the Z-axis driving mechanism and is used to drive the Z-axis driving mechanism to move along the X-axis, and the mounting bracket moves synchronously with the Z-axis driving mechanism.

[0009] It can be understood that the X-axis drive mechanism is configured so that the mounting bracket and the Z-axis drive mechanism can move synchronously along the X-axis to move closer to or farther away from the reagent bottle along the X-axis, so as to facilitate the placement and removal of the reagent bottle.

[0010] In one embodiment, the mounting bracket is connected to a sliding rod, the sliding rod is slidably connected to the Z-axis driving mechanism, and the Z-axis driving mechanism is slidably connected to the X-axis driving mechanism.

[0011] It can be understood that the sliding connection is set to facilitate the stable reciprocating movement of the sliding rod along the Z axis, and the Z axis driving mechanism is slidably connected to the X axis driving mechanism to drive the sliding rod to move synchronously along the X axis.

[0012] In one embodiment, the hydrothermal synthesis workstation further includes a shaking module, wherein the shaking module has a shaking station for placing the reagent bottle, and the shaking module can drive the reagent bottle to shake.

[0013] It can be understood that the shaking module is provided to shake the reagent bottle to promote uniform mixing of the raw materials in the reagent bottle, which is beneficial to accelerate the reaction rate.

[0014] In one embodiment, the shaking module also includes a shaking drive, a shaking transmission mechanism and a shaking table. The shaking transmission mechanism is connected between the shaking drive and the shaking table. The shaking transmission mechanism drives the shaking table to shake under the action of the shaking drive. The shaking table is constructed with a plurality of shaking stations arranged at intervals.

[0015] It can be understood that the shaking driving member provides a power source for the shaking of the shaking table, and the shaking transmission mechanism transmits the power of the shaking driving member to the shaking table to make the shaking table shake.

[0016] In one embodiment, the vibration transmission mechanism includes a transmission belt assembly and multiple transmission shafts, each of the transmission shafts is connected between the transmission belt assembly and the vibration table, the transmission belt assembly is connected to the vibration driving member, and can drive the multiple transmission shafts to rotate; wherein each of the transmission shafts includes a first shaft section and a second shaft section, the first shaft section and the second shaft section are connected and eccentrically arranged, the first shaft section is connected to the transmission belt assembly, and the second shaft section is connected to the vibration table.

[0017] It can be understood that the transmission belt assembly transmits power to the transmission shaft smoothly. Since the first shaft section and the second shaft section of the transmission shaft are eccentrically arranged, the second shaft section rotates around the axis of the first shaft section to drive the shaking table to swing.

[0018] In one embodiment, the transmission belt assembly includes a driving pulley, a plurality of driven pulleys and at least two transmission belts. The driving pulley is connected to the vibration drive element and is transmission-connected to one of the driven pulleys through a transmission belt. A transmission connection is formed between the plurality of driven pulleys through at least one transmission belt. The plurality of driven pulleys are circumferentially arranged around the axis of the vibration table.

[0019] It is understandable that, with such an arrangement, the driving pulley transmits power to multiple driven pulleys through the transmission belt, so that the multiple driven pulleys respectively drive the transmission shafts to rotate, which is beneficial to the synchronous rotation of multiple transmission shafts and promotes the circumferential swinging of the shaking table.

[0020] In one embodiment, the reagent bottle includes a bottle body and a cover body, and the hydrothermal synthesis workstation also includes a capping module; the capping module has a second gripping clamp, which is used to clamp the bottle body and cooperate with the operating module to clamp the cover body and rotate it relative to the bottle body; or, the capping module has a second gripping clamp and a third gripping clamp arranged at intervals, the second gripping clamp is used to clamp the bottle body, and the third gripping clamp is used to clamp the cover body and rotate it relative to the bottle body.

[0021] It is understandable that the automatic screwing of the cap body relative to the bottle body can be realized by setting the cap screwing module, thereby improving the degree of automation. The second gripping clamp cooperates with the first gripping clamp or the second gripping clamp cooperates with the third gripping clamp, which is easy to operate.

[0022] In one embodiment, the operation module includes a first gripper, which is at least used to grip the reagent bottle; and / or the operation module includes a pipette, which is used to absorb raw materials in the reagent bottle or add raw materials to the reagent bottle.

[0023] It can be understood that the first gripper is provided to facilitate the movement of the reagent bottle, and the pipette is provided to facilitate the addition and mixing of raw materials to promote the chemical reaction. BRIEF DESCRIPTION OF THE DRAWINGS

[0024] In order to more clearly illustrate the technical solutions in the embodiments of the present application or the conventional technology, the drawings required for use in the embodiments or the conventional technology descriptions are briefly introduced below. Obviously, the drawings described below are only some embodiments of the present application. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work.

[0025] Figure 1 A schematic diagram of the structure of a hydrothermal synthesis workstation provided in this application;

[0026] Figure 2 This is a schematic diagram of the structure of the drying module in the hydrothermal synthesis workstation provided in this application;

[0027] Figure 3 A schematic diagram of another structural orientation of the hydrothermal synthesis workstation provided in this application;

[0028] Figure 4 A schematic diagram of the structure of the shaking module in the hydrothermal synthesis workstation provided in this application;

[0029] Figure 5 A cross-sectional view of a shaking module in a hydrothermal synthesis workstation provided in the present application;

[0030] Figure 6This is a schematic diagram of the structure of the transmission shaft of the shaking module in the hydrothermal synthesis workstation provided in this application.

[0031] 1. The invention relates to a hydrothermal synthesis workstation; 2. a material storage module; 3. a reagent bottle; 4. a heating module; 5. a drying module; 6. a gas supply needle; 7. a mounting bracket; 8. a sliding rod; 9. a driving module; 10. a moving guide rail for an X-axis; 11. a moving guide rail for an Y-axis; 12. a moving guide rail for an Z-axis; 13. a first gripping clamp; 14. a pipette; 15. a shaking module; 16. a shaking driving member; 17. a shaking transmission mechanism; 18. a shaking transmission assembly; 19. a driving pulley; 20. a driven pulley; 21. a second transmission belt; 22. a transmission shaft; 23. a bearing seat; 24. a bearing; 25. a shaking table; 26. a capping module; 27. a housing; 28. an interface; 29. ​​a start / stop switch. DETAILED DESCRIPTION

[0032] In order to make the above-mentioned purposes, features and advantages of the present application more obvious and easy to understand, the specific implementation methods of the present application are described in detail below in conjunction with the accompanying drawings. In the following description, many specific details are set forth to facilitate a full understanding of the present application. However, the present application can be implemented in many other ways different from those described herein, and those skilled in the art can make similar improvements without violating the connotation of the present application, so the present application is not limited by the specific embodiments disclosed below.

[0033] It should be noted that when a component is referred to as being "fixed to" or "disposed on" another component, it may be directly on the other component or there may also be a central component. When a component is considered to be "connected to" another component, it may be directly connected to the other component or there may be a central component at the same time. The terms "vertical", "horizontal", "upper", "lower", "left", "right" and similar expressions used in the specification of this application are for illustrative purposes only and do not represent the only implementation method.

[0034] In addition, the terms "first" and "second" are used for descriptive purposes only and should not be understood as indicating or implying relative importance or implicitly indicating the number of the indicated technical features. Therefore, the features defined as "first" and "second" may explicitly or implicitly include at least one of the features. In the description of this application, the meaning of "plurality" is at least two, such as two, three, etc., unless otherwise clearly and specifically defined.

[0035] In the present application, unless otherwise clearly specified and limited, a first feature being “above” or “below” a second feature may mean that the first feature is directly in contact with the second feature, or the first feature and the second feature are indirectly in contact through an intermediate medium. Moreover, a first feature being “above”, “above” or “above” a second feature may mean that the first feature is directly above or obliquely above the second feature, or simply means that the first feature is higher in level than the second feature. A first feature being “below”, “below” or “below” a second feature may mean that the first feature is directly below or obliquely below the second feature, or simply means that the first feature is lower in level than the second feature.

[0036] Unless otherwise defined, all technical and scientific terms used in the specification of this application have the same meaning as those commonly understood by those skilled in the art to which this application belongs. The terms used in the specification of this application are only for the purpose of describing specific embodiments and are not intended to limit this application. The term "and / or" used in the specification of this application includes any and all combinations of one or more related listed items.

[0037] See also Figures 1 to 6 The present application provides a hydrothermal synthesis workstation 100, which includes a material storage module 10, a heating module 20, a drying module 30, a driving module 40 and an operating module; the material storage module 10 has a material storage station for storing a reagent bottle 11; the heating module 20 is used to heat the reagent bottle 11; the drying module 30 includes a plurality of gas delivery needles arranged at intervals, each of which can at least reciprocate along the Z-axis direction to extend out or extend into the reagent bottle, and the gas delivery needle can blow dry gas into the heated reagent bottle; the driving module 40 includes an X-axis moving guide rail 41, a Y-axis moving guide rail 42 and a Z-axis moving guide rail 43 connected in sequence; the operating module is connected to the Z-axis moving guide rail 43, and the operating module can flow and move between the material storage module 10, the heating module 20 and the drying module 30 under the action of the driving module 40, and the operating module is used to clamp the reagent bottle 11 and take or put raw materials in the reagent bottle 11.

[0038] In this way, the material storage module 10 is provided with a material storage station to facilitate the stable placement of the reagent bottle 11. A plurality of material storage stations arranged at intervals can be provided to centrally place a plurality of reagent bottles 11, so as to facilitate centralized taking and more convenient operation. Among them, the operating module can take the reagent bottle 11, and can also take out the raw materials in the reagent bottle 11 and add them to another reagent bottle 11 to mix and react. The driving module 40 is connected to the operating module to control the operation module to circulate in other modules. Specifically, the driving module 40 controls the movement of the operating module to realize the taking and adding of the raw materials. After the raw materials in the reagent bottle 11 are mixed in proportion, the driving module 40 can control it to move to the heating module 20 for heating, so that the temperature is increased and the reaction conditions are reached. After the heating is completed, the driving module 40 continues to drive the operating module to move the reagent bottle 11 to the drying module 30. At this time, the gas delivery needle moves downward along the Z axis so that the gas delivery needle extends into the reagent bottle 11, and then the drying gas is input into the reagent bottle 11. The drying gas can promote the rapid evaporation of the liquid in the reagent bottle 11 to quickly obtain the sample. After drying is completed, the gas delivery needle moves upward along the Z axis and extends out of the reagent bottle 11 to facilitate taking out the reagent bottle 11 .

[0039] In summary, it is precisely because of the setting of each module that different functions can be realized clearly and reasonably. The driving module 40 can realize free movement in three dimensions of X-axis, Y-axis and Z-axis, improve the degree of automation, and the setting of the drying module 30 speeds up the process of obtaining samples. The cooperation of the driving module 40, the operating module and the drying module 30 is conducive to automatic and rapid drying to obtain samples, so as to meet the needs of high-throughput and high-efficiency hydrothermal synthesis.

[0040] In a specific embodiment, the reagent bottle 11 includes a bottle body and a bottle cap, and a plurality of material storage stations are provided, and the material storage station can place the bottle body or the cap.

[0041] like Figure 1 As shown, in a specific embodiment, the operation module includes a pipette 52, and the pipette 52 is used to absorb the raw materials in the reagent bottle 11 or add raw materials to the reagent bottle 11, so as to realize the transfer of raw materials and mix different raw materials to produce reactions. In a more specific embodiment, the material storage module 10 also includes a suction head, which can be placed on the material storage station. The pipette 52 is first assembled with the suction head, and then the raw materials are absorbed. The suction head is usually a disposable item, and multiple pipettes can be provided to facilitate the replacement of the pipette 52, which is conducive to reducing pollution and ensuring the normal progress of the reaction.

[0042] like Figure 1 As shown, in some embodiments, the operation module includes a first gripper 51 , which is at least used to grip the reagent bottle 11 , and driven by the driving module 40 , can move the reagent bottle 11 to other modules.

[0043] like Figure 1 As shown, in a specific embodiment, the heating module 20 is provided with a heating platform, on which a plurality of heating stations arranged at intervals are constructed, and the reagent bottle 11 is placed on the heating station for heating.

[0044] like Figure 1 As shown, in an optional embodiment, the hydrothermal synthesis workstation 100 also includes a shaking module 60, which has a shaking station for placing the reagent bottle 11. The shaking module 60 can drive the reagent bottle 11 to shake, thereby promoting the different raw materials in the reagent bottle 11 to be mixed evenly, which is beneficial to accelerate the reaction rate and promote the progress of the reaction.

[0045] like Figure 4 and Figure 5 As shown, in a further embodiment, the shaking module 60 further includes a shaking drive 61, a shaking transmission mechanism 62 and a shaking table 63, wherein the shaking transmission mechanism 62 is connected between the shaking drive 61 and the shaking table 63, and the shaking transmission mechanism 62 drives the shaking table 63 to shake under the action of the shaking drive 61, and the shaking table 63 is configured with a plurality of shaking stations arranged at intervals. In this way, the shaking station can place the corresponding reagent bottle 11, the shaking drive 61 provides a power source for shaking, and the shaking transmission mechanism 62 transmits power to the shaking table 63, so that the shaking table 63 shakes.

[0046] like Figure 5 and Figure 6 As shown, in a specific embodiment, in a specific embodiment, the shaking transmission mechanism 62 includes a shaking transmission component 621, a first transmission belt and multiple transmission shafts 622, the multiple transmission shafts 622 are circumferentially arranged around the axis of the shaking table 63 and connected to the shaking table 63, the first transmission belt is tensioned between the multiple transmission shafts 622, the transmission shafts 622 are also connected to the shaking transmission component 621, the shaking transmission component 621 is connected to the shaking drive member 61, and can drive the multiple transmission shafts 622 to rotate; wherein, each transmission shaft 622 includes a first shaft section 6221 and a second shaft section 6222, the first shaft section 6221 and the second shaft section 6222 are connected and eccentrically arranged, the first shaft section 6221 is connected to the shaking transmission component 621, and the second shaft section 6222 is connected to the shaking table 63.

[0047] In this way, the shaking transmission assembly 621 transmits the power of the shaking drive member 61 to the transmission shaft 622, and driven by the first transmission belt, the first shaft segments 6221 in the plurality of transmission shafts 622 rotate synchronously. Since the second shaft segment 6222 is eccentrically arranged relative to the first shaft segment 6221, the second shaft segment 6222 rotates around the axis of the first shaft segment 6221. Since the transmission shaft 622 is circumferentially arranged around the axis of the shaking table 63, the shaking table 63 is shaken and swayed under the joint action of the plurality of second shaft segments 6222.

[0048] In a specific embodiment, three transmission shafts 622 are provided, and the three transmission shafts 622 are staggered along the X-axis and the Y-axis to form a circle, so that the vibration table 63 can swing and sway circumferentially under the eccentricity of the second shaft section 6222 relative to the first shaft section 6221. In other embodiments, four, five, etc. transmission shafts 622 can also be provided, as long as the vibration table 63 can swing and sway circumferentially.

[0049] like Figure 5 As shown, in a specific embodiment, the vibration transmission assembly 621 includes a driving pulley 6211, a driven pulley 6212 and a second transmission belt 6213. The driving pulley 6211 is connected to the vibration driving member 61. The second transmission belt 6213 is tightened between the driving pulley 6211 and the driven pulley 6212. The driven pulley 6212 is in transmission connection with one of the transmission shafts 622. In this way, the vibration driving member 61 drives the driving pulley 6211 to rotate, and the driving pulley 6211 drives the driven pulley 6212 to rotate through the second transmission belt 6213. Then, the synchronous rotation of multiple transmission shafts 622 is realized through the first transmission belt, and the vibration platform 63 is driven to swing and shake together. In a specific embodiment, each transmission shaft 622 is connected to a driven pulley 6212, the driving pulley 6211 is connected to one of the driven pulleys 6212 through a second transmission belt 6213, and a first transmission belt is tensioned between multiple driven pulleys 6212 to achieve synchronous rotation of multiple driven pulleys 6212, thereby achieving synchronous rotation of multiple transmission shafts 622.

[0050] like Figure 4 and Figure 5 As shown, in a specific embodiment, the vibration transmission mechanism 62 includes a bearing seat 623, the bearing seat 623 is provided with a mounting hole, a bearing 624 is installed in the mounting hole, each transmission shaft 622 is installed in the mounting hole and passes through the bearing 624, and the bearing 624 is arranged to promote the stable rotation of the transmission shaft 622 and avoid direct contact with the bearing seat 623.

[0051] like Figure 1 As shown, in an optional embodiment, the hydrothermal synthesis workstation 100 also includes a capping module 70; the capping module 70 has a second gripper, the second gripper is used to clamp the bottle body, and cooperate with the operating module to clamp the cover body to rotate relative to the bottle body, that is, the operating module moves the bottle body into the second gripper, the second gripper clamps the bottle body, and the operating module continues to move the cover body to the bottle mouth of the bottle body, and drives the cover body to rotate relative to the bottle body to achieve the tightening of the cover body. In this process, the second gripper clamps the bottle body to prevent the bottle body from rotating, so that the operating module can smoothly drive the cover body to rotate. In a specific embodiment, the first gripper 51 in the operating module clamps the bottle body and the cover body, and the first gripper 51 can rotate around the axis to achieve the rotation of the cover body.

[0052] In another optional embodiment, the capping module 70 has a second gripper and a third gripper that are spaced apart, the second gripper is used to clamp the bottle body, and the third gripper is used to clamp the cap body and rotate relative to the bottle body. In this way, the operating module moves the bottle body into the second gripper, the second gripper clamps the bottle body, the operating module continues to move the cap body to the bottle mouth of the bottle body, and then the third gripper clamps the cap body and drives the cap body to rotate, so that the cap body rotates relative to the bottle body.

[0053] In a specific embodiment, the second gripper and / or the third gripper can be configured as a pneumatic gripper, and the hydrothermal synthesis workstation 100 further includes a gas pressure regulating valve connected to the pneumatic gripper to control the clamping force of the pneumatic gripper. At the same time, the pneumatic gripper can also be connected to a dry gas source in the drying module 30 to control the output pressure of the dry gas.

[0054] In an optional embodiment, the drying module 30 includes a mounting bracket 32 ​​and a Z-axis driving mechanism connected to the mounting bracket 32. The Z-axis driving mechanism is used to drive the mounting bracket 32 ​​to move along the Z-axis. The mounting bracket 32 ​​is configured with a plurality of mounting holes arranged at intervals, and each mounting hole is correspondingly installed with a gas delivery needle 31. In this way, the Z-axis driving mechanism provides a power source for the movement of the mounting bracket 32 ​​along the Z-axis. The setting of the mounting bracket 32 ​​facilitates the joint installation of a plurality of gas delivery needles 31 on the mounting bracket 32. Under the drive of the Z-axis driving mechanism, the synchronous movement of the plurality of gas delivery needles 31 can be achieved.

[0055] In a further embodiment, the drying module further includes an X-axis driving mechanism, which is connected to the Z-axis driving mechanism and is used to drive the Z-axis driving mechanism to move along the X-axis, and the mounting bracket 32 ​​moves synchronously with the Z-axis driving mechanism.

[0056] Thus, when the drying process begins, the Z-axis drive mechanism drives the mounting bracket 32 ​​to move upward along the Z-axis, then drives the mounting bracket 32 ​​to move closer to the reagent bottle along the X-axis, and finally drives the mounting bracket 32 ​​to move downward along the Z-axis to allow the gas delivery needle 31 to extend into the reagent bottle. After the drying is completed, the Z-axis drive mechanism drives the mounting bracket 32 ​​to move in the opposite direction, that is, first move upward along the Z-axis to allow the gas delivery needle 31 to extend out of the reagent bottle, then move away from the reagent bottle along the X-axis to facilitate the removal of the reagent bottle, and finally move downward along the Z-axis to reduce the height of the mounting bracket 32 ​​along the Z-axis direction, reduce bumps, and help protect the structure of the mounting bracket 32 ​​and the gas delivery needle 31.

[0057] In a specific embodiment, the mounting bracket 32 ​​is connected to a sliding rod 33, the sliding rod 33 is slidably connected to the Z-axis driving mechanism, and the Z-axis driving mechanism is slidably connected to the X-axis driving mechanism, so that the Z-axis driving mechanism and the sliding rod 33 can move synchronously along the X-axis direction.

[0058] In a specific embodiment, the drying module 30 is configured with a plurality of spaced gas delivery ports and a plurality of gas delivery pipes, each gas delivery pipe being connected to the gas delivery port and the end of the gas delivery needle 31 away from the reagent bottle, so as to facilitate the delivery of the drying gas. Further, the drying gas may be an inert gas such as nitrogen.

[0059] like Figure 1 As shown, in a possible embodiment, along the X-axis direction, the storage module 10, the heating module 20, the shaking module 60 and the drying module 30 are arranged in sequence to conform to the reaction process, shorten the moving path of the driving module 40, improve the overall efficiency, and facilitate precise control. Further, along the X-axis direction, the shaking module 60 overlaps with the capping module 70, and along the Y-axis direction, the shaking module 60 and the capping module 70 are arranged at intervals to reduce the size along the X-axis, so as to facilitate shaking after the capping, and avoid liquid splashing during shaking. Further, along the Z-axis direction, the driving module 40 is located above the storage module 10, the heating module 20, the shaking module 60, the capping module 70 and the drying module 30, so as to facilitate circulation in each module.

[0060] like Figure 1 As shown, in a specific embodiment, the hydrothermal synthesis workstation 100 also includes a shell 80, and the shell 80 is configured with an installation space, and the material storage module 10, the heating module 20, the shaking module 60, the capping module 70, the drying module 30 and the driving module 40 are all located in the installation space.

[0061] In a specific embodiment, the hydrothermal synthesis workstation 100 further includes a fan, which is installed at the bottom of the heating module 20 and the drying module 30 to dissipate heat for the drying drive components in the heating module 20 and the drying module 30 and extend their service life.

[0062] like Figure 1 As shown, in a specific embodiment, an interface 81 is installed on the shell 80 to facilitate external power supply, and a start-stop switch 82 is also provided on the shell 80 to control the start and stop of the entire hydrothermal synthesis workstation 100.

[0063] In the present application, the hydrothermal synthesis workstation 100 includes a controller, which is connected to a fan, an air pressure regulating valve, and various modules to control the smooth progress of the entire workflow. The specific control content is a technology well known to those skilled in the art, so it will not be repeated here.

[0064] The technical features of the above-described embodiments may be arbitrarily combined. To make the description concise, not all possible combinations of the technical features in the above-described embodiments are described. However, as long as there is no contradiction in the combination of these technical features, they should be considered to be within the scope of this specification.

[0065] The above-described embodiments only express several implementation methods of the present application, and the descriptions thereof are relatively specific and detailed, but they cannot be understood as limiting the scope of the patent application. It should be pointed out that, for a person of ordinary skill in the art, several variations and improvements can be made without departing from the concept of the present application, and these all belong to the protection scope of the present application. Therefore, the scope of patent protection of the present application shall be subject to the attached claims.

Claims

1. A hydrothermal synthesis workstation, characterized in that: include: A material storage module (10) having a material storage station for storing reagent bottles (11); A heating module (20), used for heating the reagent bottle (11); A drying module (30) comprising a plurality of gas delivery needles (31) arranged at intervals, each of the gas delivery needles (31) being capable of reciprocating along at least a Z-axis direction to extend out of or into the reagent bottle (11), and the gas delivery needle (31) being capable of blowing dry gas into the heated reagent bottle (11); A driving module (40) comprising an X-axis moving guide rail (41), a Y-axis moving guide rail (42) and a Z-axis moving guide rail (43) which are connected in sequence; An operating module is connected to the Z-axis movable guide rail (43). The operating module can be moved between the material storage module (10), the heating module (20) and the drying module (30) under the action of the driving module (40). The operating module is used to clamp the reagent bottle (11) and take or put the raw material in the reagent bottle (11).

2. The hydrothermal synthesis workstation according to claim 1, characterized in that: The drying module (30) comprises a mounting bracket (32) and a Z-axis driving mechanism connected to the mounting bracket (32), wherein the Z-axis driving mechanism is used to drive the mounting bracket (32) to move along the Z-axis, and the mounting bracket (32) is configured with a plurality of mounting holes arranged at intervals, and each of the mounting holes is correspondingly mounted with the gas delivery needle (31).

3. The hydrothermal synthesis workstation according to claim 2, characterized in that: The drying module also includes an X-axis driving mechanism, which is connected to the Z-axis driving mechanism and is used to drive the Z-axis driving mechanism to move along the X-axis, and the mounting bracket (32) moves synchronously with the Z-axis driving mechanism.

4. The hydrothermal synthesis workstation according to claim 3, characterized in that: The mounting bracket (32) is connected to a sliding rod (33), the sliding rod (33) is slidably connected to the Z-axis driving mechanism, and the Z-axis driving mechanism is slidably connected to the X-axis driving mechanism.

5. The hydrothermal synthesis workstation according to claim 1, characterized in that: The hydrothermal synthesis workstation further comprises a shaking module (60), wherein the shaking module (60) has a shaking station for placing the reagent bottle (11), and the shaking module (60) can drive the reagent bottle (11) to shake.

6. The hydrothermal synthesis workstation according to claim 5, characterized in that: The shaking module (60) further comprises a shaking driving member (61), a shaking transmission mechanism (62) and a shaking table (63); the shaking transmission mechanism (62) is connected between the shaking driving member (61) and the shaking table (63); the shaking transmission mechanism (62) drives the shaking table (63) to shake under the action of the shaking driving member (61); and the shaking table (63) is constructed with a plurality of shaking stations arranged at intervals.

7. The hydrothermal synthesis workstation according to claim 6, characterized in that: The shaking transmission mechanism (62) comprises a shaking transmission assembly (621), a first transmission belt and a plurality of transmission shafts (622); the plurality of transmission shafts (622) are circumferentially arranged around the axis of the shaking platform (63) and connected to the shaking platform (63); the first transmission belt is tensioned between the plurality of transmission shafts (622); the transmission shafts (622) are also connected to the shaking transmission assembly (621); the shaking transmission assembly (621) is connected to the shaking driving member (61) and can drive the plurality of transmission shafts (622) to rotate; Wherein, each of the transmission shafts (622) comprises a first shaft section (6221) and a second shaft section (6222), the first shaft section (6221) and the second shaft section (6222) are connected and eccentrically arranged, the first shaft section (6221) is connected to the shaking transmission assembly (621), and the second shaft section (6222) is connected to the shaking table (63).

8. The hydrothermal synthesis workstation according to claim 7, characterized in that: The vibration transmission assembly (621) includes a driving pulley (6211), a driven pulley (6212) and a second transmission belt (6213), wherein the driving pulley (6211) is connected to the vibration drive member (61), the second transmission belt (6213) is tensioned between the driving pulley (6211) and the driven pulley (6212), and the driven pulley (6212) is in transmission connection with one of the transmission shafts (622).

9. The hydrothermal synthesis workstation according to claim 1, characterized in that: The reagent bottle (11) comprises a bottle body and a cover body, and the hydrothermal synthesis workstation further comprises a capping module (70); The capping module (70) comprises a second gripping clamp (71), the second gripping clamp (71) is used to clamp the bottle body and cooperate with the operating module to clamp the cap body and rotate relative to the bottle body; or, the capping module (70) comprises a second gripping clamp (71) and a third gripping clamp arranged at intervals, the second gripping clamp (71) is used to clamp the bottle body, and the third gripping clamp is used to clamp the cap body and rotate relative to the bottle body.

10. The hydrothermal synthesis workstation according to any one of claims 1 to 9, characterized in that: The operation module comprises a first gripper (51), the first gripper (51) being at least used to grip the reagent bottle (11); and / or the operation module comprises a pipette (52), the pipette (52) being used to absorb raw materials in the reagent bottle (11) or to add raw materials to the reagent bottle (11).

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