Skid-mounted continuous rectification system for silane product and sulfite product

By designing closely arranged skid-mounted equipment in the continuous distillation system of silane and sulfite products, the installation difficulties and large land occupation caused by the numerous and scattered equipment are solved, and efficient component separation and convenient equipment operation are achieved. .

CN222238845UActive Publication Date: 2024-12-27SHANDONG PENGRUN NEW MATERIALS CO LTD
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Patent Information

Application Number
CN202421032641.0
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-05-13
Publication Date
2024-12-27
Estimated Expiration
2034-05-13

AI Technical Summary

Technical Problem

The existing continuous distillation system of silane products and sulfite products has many equipment and is distributed scattered, resulting in installation difficulties and large area.

Method used

A skid-mounted continuous distillation system is designed, including a base, a connecting frame, a light component box, a heavy component box, a super gravity distillation bed body, a condensation component and an evaporation component. All components are closely installed on the base and utilize servo. Motors and transmission mechanisms simplify movement and maintenance and reduce footprint.

Benefits of technology

It realizes a tightly arranged installation, reduces the difficulty of equipment installation and footprint, further separates components through countercurrent contact and material energy transfer, improves the distillation effect, and facilitates movement and maintenance.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a skid-mounted continuous rectification system for silane products and sulfite products, which relates to the technical field of rectification reaction equipment and comprises a base, a connecting frame, a light component box and a heavy component box are respectively arranged at the top end of the base, and a supergravity rectification bed body is arranged at the top end of the connecting frame. A movable disc is rotationally arranged in the supergravity rectification bed body, and a gas collecting pipe, a return pipe, a feeding pipe, a gas inlet pipe and a turbidity collecting pipe are respectively arranged on the surface of the supergravity rectification bed body; the supergravity rectification bed has the beneficial effects that the connecting frame, the supergravity rectification bed body, the light component box, the heavy component box, the condensation assembly and the evaporation assembly are all mounted on the base, the layout is compact, the mounting difficulty is reduced, the occupied space is reduced, volatile components in reflux liquid can be subjected to countercurrent contact and substance and energy transfer when being in contact with rising steam, and the working efficiency is improved. Therefore, components difficult to volatilize are further separated out, supergravity rectification is achieved, and the rectification effect is improved.
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Description

Technical Field

[0001] The utility model relates to a continuous distillation system, in particular to a skid-mounted continuous distillation system for silane products and sulfite products, belonging to the technical field of distillation reaction equipment. Background Art

[0002] Distillation is a separation process that uses the different volatilities of the components in a mixture to separate them. Common equipment for distillation includes plate distillation towers and packed distillation towers. In the production process of silane products and sulfite products, traditional intermittent distillation methods are usually used. Silane products include mercaptopropyltrimethoxysilane, mercaptopropyltriethoxysilane, chloropropyltrimethoxysilane, chloropropyltriethoxysilane, vinyltriethoxysilane, vinyltrimethoxysilane, etc. Sulfite products include vinyl sulfite, propylene sulfite, butylene sulfite, 4-methyl vinyl sulfite, 4-propyl vinyl sulfite, etc.

[0003] Among them, the "a kind of silane continuous distillation device" disclosed in the application number "CN202022251803.8" "comprises a distillation bottom kettle, the upper end of the distillation bottom kettle is connected to a heat exchanger, the heat exchanger is connected to a temperature control valve, a sampling tube and a liquid nitrogen control valve, the lower end of the heat exchanger is provided with a bottom kettle, and a liquid phase extraction control valve is provided between the heat exchanger and the bottom kettle; by adding crude silane into the distillation bottom kettle, opening the liquid nitrogen control valve and the temperature control valve, and controlling the specified temperature, the continuous distillation of silane is realized, the cost is reduced and the quality is improved, and the interlocking of the temperature-raising full reflux control valve and the liquid phase extraction control valve avoids manual operation, so that the production capacity and quality of the entire distillation process reach a new height to meet customer requirements", and further search found that the "a kind of continuous distillation device" disclosed in the application number "CN202122099701.3" It "comprises an ultra-gravity distillation bed body, the distillation port on the ultra-gravity distillation bed body is connected to the air inlet of the gas-liquid separator, the liquid outlet at the bottom of the gas-liquid separator is connected to the reflux port on the ultra-gravity distillation bed body through a pipeline, the distillate outlet at the bottom of the ultra-gravity distillation bed body is connected to the distillate storage tank and the circulation pump through branch pipelines, the liquid outlet of the circulation pump is connected to the circulation pipeline, the circulation pipeline is provided with a feed-liquid mixing inlet, and the end of the circulation pipeline is connected to the feeding port on the ultra-gravity distillation bed body. This device has the characteristics of low investment and low energy consumption. The use of a complete set of continuous distillation devices replaces the traditional parallel concentrator process, which greatly increases the processing capacity. This equipment is particularly suitable for the distillation treatment of desulfurized ammonia waste liquid in coking enterprises, thereby reducing the production cost of coking enterprises, reducing the energy consumption of enterprises, and increasing the economic benefits of enterprises."

[0004] However, the above two methods still have the following defects: there are many devices and they are scattered, so the traditional installation method is very troublesome to install and occupies a large area. Utility Model Content

[0005] The utility model aims to provide a skid-mounted continuous distillation system for silane products and sulfite products, so as to solve the problems of inconvenient installation and large floor space caused by the large number of existing equipments and their scattered distribution.

[0006] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a skid-mounted continuous distillation system for silane products and sulfite products, comprising a base, a connecting frame, a light component box and a heavy component box are respectively arranged on the top of the base, a supergravity distillation bed body is arranged on the top of the connecting frame, a moving disk is rotatably arranged inside the supergravity distillation bed body, a moving baffle ring is arranged on the upper surface of the moving disk, a static disk is arranged above the moving disk, and a static baffle ring is arranged on the lower surface of the static disk, a gas collecting pipe, a reflux pipe, a feed pipe, an air inlet pipe and a turbidity collecting pipe are respectively arranged on the surface of the supergravity distillation bed body, a condensation assembly is arranged on the top of the light component box, an evaporation assembly is arranged on the top of the heavy component box, an auxiliary groove is opened inside the base, an auxiliary assembly is arranged inside the auxiliary groove, and an adjustment assembly is arranged on one side of the base.

[0007] As a preferred technical solution of the utility model, the condensation component includes a condensation box, which is arranged at the top of the light component box. The inner wall of the condensation box is provided with a first S-shaped heat exchange tube, one end of the first S-shaped heat exchange tube passes through the top of the light component box and is placed at the top inside the light component box, the other end of the first S-shaped heat exchange tube is provided with a first auxiliary pipe, one end of the first auxiliary pipe is connected to one end of the gas collecting pipe, a water inlet pipe is provided at the bottom of the front side of the condensation box, and a water outlet pipe is provided at the top of the back side of the condensation box.

[0008] As a preferred technical solution of the utility model, a discharge pipe is provided on one side of the light component box, a first submersible pump is provided on the inner wall of the bottom end of the light component box, a liquid supply pipe is provided at the liquid outlet end of the first submersible pump, one end of the liquid supply pipe passes through the inner wall of one side of the light component box and is connected to one end of a return pipe, the other end of the return pipe and one end of the feed pipe are both provided with shower nozzles, the return pipe, feed pipe and air collecting pipe are all placed above the moving plate, and the air inlet pipe and turbidity collecting pipe are both placed below the moving plate.

[0009] As a preferred technical solution of the utility model, the evaporation component includes a heating box, which is arranged at the top of the heavy component box, and the inner wall of the heavy component box is provided with a second S-shaped heat exchange tube, one end of the second S-shaped heat exchange tube passes through the top of the heavy component box and is placed at the top inside the heavy component box, a steam pipe is provided at the top of the front of the heating box, one end of the steam pipe is connected to one end of the air inlet pipe, a turbidity outlet pipe is provided at the bottom of the front of the heating box, and a turbidity inlet pipe is provided in the middle of the back of the heating box.

[0010] As a preferred technical solution of the utility model, the inner walls of the recombinant tank are respectively provided with a partition and a second submersible pump, the partition is arranged in a Z shape, the partition divides the interior of the recombinant tank into a steam storage chamber and a turbidity storage chamber connected to the interior of the turbidity collecting pipe, the second submersible pump is placed inside the turbidity storage chamber, a second auxiliary pipe is provided at the liquid outlet end of the second submersible pump, one end of the second auxiliary pipe passes through the inner wall of one side of the recombinant tank and is connected to one end of the turbidity inlet pipe, a steam outlet pipe is provided on one side of the recombinant tank, and the interior of the steam outlet pipe is connected to the interior of the steam storage chamber.

[0011] As a preferred technical solution of the utility model, the auxiliary component includes a driving component and two slide grooves, the two slide grooves are both opened at the bottom end of the base, the interiors of the two slide grooves are connected with the interior of the auxiliary groove, the inner walls of the two slide grooves are slidably connected with a lifting plate, the bottom ends of the two lifting plates are provided with universal wheels, and a transmission frame sliding with the auxiliary groove is provided between the two lifting plates, the inner wall of the transmission frame is threadedly connected with a transmission screw through a screw nut, and both ends of the transmission screw are rotatably connected to the inner wall of the auxiliary groove through sealed bearings.

[0012] As a preferred technical solution of the utility model, the driving assembly includes a groove and a worm, the groove is opened on one side of the base, the inner wall of the groove is provided with a servo motor, the servo motor is a forward and reverse motor, the worm is rotatably arranged on the inner wall of the auxiliary groove through a sealed bearing, one end of the worm is connected to the transmission shaft of the servo motor, the front side of the worm is meshed with a worm wheel, and the inner wall of the worm wheel is connected to the surface of the transmission screw.

[0013] As a preferred technical solution of the utility model, the adjustment component includes two storage boxes, one of which is arranged on the front side of the base, and the other is arranged on the back side of the base, through holes are provided on the surfaces of the two storage boxes, adjustment plates are slidably connected to the inner walls of the two storage boxes, threaded holes are provided on the surfaces of the two adjustment plates, vertical rods are provided on one side of the two adjustment plates, gripping rods are provided at one end of the two vertical rods, and anti-slip sleeves are provided on the surfaces of the gripping rods.

[0014] Compared with the related art, the skid-mounted continuous distillation system for silane products and sulfite products provided by the utility model has the following beneficial effects:

[0015] 1. The connecting frame, the ultra-gravity distillation bed body, the light component box, the heavy component box, the condensation component and the evaporation component are all installed on the base. The layout is compact, which reduces the difficulty of installation and reduces the space occupied. The volatile components in the reflux liquid will undergo countercurrent contact and material and energy transfer when contacting the rising steam, thereby volatilizing again, further separating the non-volatile components, realizing ultra-gravity distillation and improving the distillation effect;

[0016] 2. The servo motor drives the worm to rotate, and the worm drives the transmission screw to rotate through the worm wheel to realize the driving of the transmission screw. The transmission screw drives the transmission frame to move downward, and the transmission frame drives two lifting plates and multiple universal wheels to move downward, causing the universal wheels to extend from the inside of the slide and grounded, which is convenient for moving the base. The servo motor is set outside the auxiliary slot for easy maintenance. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 It is a structural schematic diagram of the utility model;

[0018] Figure 2 This is a schematic diagram of the back structure of the utility model;

[0019] Figure 3 It is a schematic diagram of the cross-sectional structure of the utility model;

[0020] Figure 4 It is a schematic diagram of the side cross-sectional structure of the light component box of the utility model;

[0021] Figure 5 It is a schematic diagram of the side cross-section structure of the reorganization and distribution box of the utility model;

[0022] Figure 6 This is one of the schematic diagrams of the top cross-sectional structure of the base of the utility model;

[0023] Figure 7 This is the second schematic diagram of the top cross-sectional structure of the base of the utility model.

[0024] In the figure: 1, base; 2, connecting frame; 3, condensing assembly; 301, condensing box; 302, first S-shaped heat exchange tube; 303, first auxiliary pipe; 304, water inlet pipe; 305, water outlet pipe; 4, evaporating assembly; 401, heating box; 402, second S-shaped heat exchange tube; 403, steam transmission pipe; 404, turbidity outlet pipe; 405, turbidity inlet pipe; 5, light component box; 6, auxiliary assembly; 601, slide; 602, lifting plate; 603, universal wheel; 604, transmission frame; 605, transmission screw; 7, driving assembly; 701, groove; 702, worm Rod; 703, servo motor; 704, worm gear; 8, adjustment assembly; 801, storage box; 802, adjustment plate; 803, vertical rod; 804, auxiliary grip rod; 9, re-combination box; 10, ultra-gravity distillation bed body; 11, moving plate; 12, gas collecting pipe; 13, reflux pipe; 14, feed pipe; 15, air inlet pipe; 16, turbidity collecting pipe; 17, auxiliary tank; 18, discharge pipe; 19, first submersible pump; 20, liquid supply pipe; 21, partition; 22, second submersible pump; 23, turbidity storage chamber; 24, steam storage chamber; 25, second auxiliary pipe; 26, steam outlet pipe. DETAILED DESCRIPTION

[0025] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0026] See also Figure 1-7The utility model provides a skid-mounted continuous distillation system for silane products and sulfite products, comprising a base 1, a connecting frame 2, a light component box 5 and a heavy component box 9 are fixedly arranged on the top of the base 1, a supergravity distillation bed body 10 is fixedly arranged on the surface of the connecting frame 2, a moving plate 11 is fixedly arranged on the inner wall of the supergravity distillation bed body 10, a moving baffle ring is arranged on the upper surface of the moving plate 11, a static plate is arranged above the moving plate 11, a static baffle ring is arranged on the lower surface of the static plate, and the surface of the supergravity distillation bed body 10 is fixedly arranged on the inner wall of the supergravity distillation bed body 10 A gas collecting pipe 12, a reflux pipe 13, a feed pipe 14, an air inlet pipe 15 and a turbidity collecting pipe 16 are arranged, a condensation assembly 3 is arranged on the top of the light component box 5, an evaporation assembly 4 is arranged on the top of the heavy component box 9, an auxiliary tank 17 is opened inside the base 1, an auxiliary assembly 6 is arranged inside the auxiliary tank 17, and an adjustment assembly 8 is arranged on one side of the base 1. The raw materials are distilled by the supergravity distillation bed body 10, and the gas collecting pipe 12 discharges the gaseous volatile components (silane or sulfite) and the misty non-volatile components, and the condensation assembly Component 3 and light component box 5 condense and reflux the gaseous volatile components and the misty non-volatile components. The volatile components in the reflux liquid will undergo countercurrent contact and material and energy transfer when contacting the rising steam, thereby volatilizing again, further separating the non-volatile components, and realizing supergravity distillation. Specifically, the rising steam is partially condensed multiple times, the temperature gradually decreases, the non-volatile components are liquefied before the volatile components, and the liquefied non-volatile components fall due to weight loss, so that the concentration of the volatile components in the steam gradually increases; The descending reflux liquid is partially vaporized multiple times, and the temperature gradually increases due to heat exchange. The volatile components evaporate before the less volatile components, and the vaporized volatile components rise due to overweight (upward acceleration). Therefore, the concentration of the less volatile components in the descending reflux liquid gradually increases, and the concentration of the volatile components in the liquid gradually decreases, thereby achieving supergravity distillation. The turbidity collecting pipe 16 discharges the liquid less volatile components, and the liquid less volatile components are heated by the cooperation of the recombination box 9, the evaporation component 4 and the external steam generator to generate high-temperature steam.

[0027] The condensation assembly 3 includes a condensation box 301, which is fixedly arranged at the top of the light component box 5. The inner wall of the condensation box 301 is fixedly provided with a first S-shaped heat exchange tube 302. One end of the first S-shaped heat exchange tube 302 passes through the top of the light component box 5 and is placed on the top of the light component box 5. The other end of the first S-shaped heat exchange tube 302 is fixedly provided with a first auxiliary tube 303. One end of the first auxiliary tube 303 is fixedly connected to one end of the gas manifold 12. A water inlet pipe 304 is fixedly provided at the bottom of the front of the condensation box 301. The condensation box 3 A water outlet pipe 305 is fixedly provided on the top of the back side of 01. The gaseous volatile components and the misty non-volatile components enter the interior of the first S-type heat exchange tube 302 through the first auxiliary pipe 303, and are injected with cold water through the water inlet pipe 304. The temperature of the gaseous volatile components and the misty non-volatile components is reduced by the cold water and the first S-type heat exchange tube 302, so that the volatile components are liquefied. The liquefied volatile components and liquid non-volatile components are injected into the interior of the light component box 5, and the cold water after heat exchange is discharged through the water outlet pipe 305.

[0028] A discharge pipe 18 is provided on one side of the light component box 5, and a first submersible pump 19 is fixedly provided on the inner wall of the bottom end of the light component box 5. A liquid supply pipe 20 is fixedly provided at the liquid outlet end of the first submersible pump 19. One end of the liquid supply pipe 20 passes through the inner wall of one side of the light component box 5 and is fixedly connected to one end of the reflux pipe 13. The other end of the reflux pipe 13 and one end of the feed pipe 14 are fixedly provided with a shower nozzle. The reflux pipe 13, the feed pipe 14 and the gas collecting pipe 12 are all placed above the moving disk 11, and the gas intake pipe 15 and the turbidity collecting pipe 16 are all placed below the moving disk 11. The liquefied volatile components and liquid non-volatile components are pumped into the interior of the liquid supply pipe 20, and then enter the interior of the supergravity distillation bed body 10 through the interior of the reflux pipe 13, so that the volatile components in the reflux liquid are countercurrently contacted and matter and energy are transferred when contacting the rising steam, so as to further separate the liquid non-volatile components and improve the distillation effect.

[0029] The evaporation assembly 4 includes a heating box 401, which is fixedly arranged at the top of the recombinant tank 9. A second S-shaped heat exchange tube 402 is fixedly arranged on the inner wall of the recombinant tank 9. One end of the second S-shaped heat exchange tube 402 passes through the top of the recombinant tank 9 and is placed at the top inside the recombinant tank 9. A steam delivery pipe 403 is fixedly arranged at the top of the front face of the heating box 401. One end of the steam delivery pipe 403 is fixedly connected to one end of the air inlet pipe 15. A turbidity outlet pipe 404 is fixedly arranged at the bottom of the front face of the heating box 401. A turbidity inlet pipe 405 is fixedly arranged in the middle of the back face of the heating box 401, and the steam outlet end of the external steam generator is connected to one end of the second S-shaped heat exchange tube 402. When the steam passes through the second S-shaped heat exchange tube 402, the liquid non-volatile components in the heating box 401 are heated, and the liquid non-volatile components enter the heating box 401 through the turbidity inlet pipe 405. A part of the liquid non-volatile components are heated and evaporated, and the generated steam is blown into the interior of the ultra-gravity distillation bed body 10 through the steam transmission pipe 403 and the air inlet pipe 15. The rotating disk 11 in the ultra-gravity distillation bed body 10 rotates to generate centrifugal force. Under the action of the moving baffle ring on the surface of the moving disk 11 and the static baffle ring on the surface of the static disk, the gas and liquid are continuously contacted to transfer mass and heat for distillation, and the other part of the liquid non-volatile components are discharged through the turbidity outlet pipe 404.

[0030] The inner wall of the recombinant tank 9 is fixedly provided with a partition 21 and a second submersible pump 22, and the partition 21 is arranged in a Z shape. The partition 21 divides the interior of the recombinant tank 9 into a steam storage chamber 24 and a turbidity storage chamber 23 connected to the interior of the turbidity collecting pipe 16. The second submersible pump 22 is placed in the turbidity storage chamber 23. The liquid outlet end of the second submersible pump 22 is fixedly provided with a second auxiliary pipe 25. One end of the second auxiliary pipe 25 passes through the inner wall of one side of the recombinant tank 9 and is fixedly connected to one end of the turbidity inlet pipe 405. A steam outlet pipe 26 is fixedly provided on one side of the recombinant tank 9. The interior of the steam outlet pipe 26 is connected to the interior of the steam storage chamber 24. The second submersible pump 22 pumps the liquid non-volatile components introduced by the turbidity collecting pipe 16 into the turbidity inlet pipe 405. The interior of the second S-shaped heat exchange tube 402 is connected to the interior of the steam storage chamber 24, thereby discharging the steam passing through the second S-shaped heat exchange tube 402 through the steam outlet pipe 26.

[0031] The auxiliary assembly 6 includes a driving assembly 7 and two slide grooves 601. The two slide grooves 601 are both opened at the bottom end of the base 1. The interiors of the two slide grooves 601 are connected to the interior of the auxiliary groove 17. The inner walls of the two slide grooves 601 are slidably connected with a lifting plate 602. The bottom ends of the two lifting plates 602 are fixed with universal wheels 603. There are six universal wheels 603 at the bottom end of each lifting plate 602. A transmission frame 6 that slides with the auxiliary groove 17 is fixed between the two lifting plates 602. 04, the inner wall of the transmission frame 604 is threadedly connected with a transmission screw 605 through a screw nut, and both ends of the transmission screw 605 are rotatably connected to the inner wall of the auxiliary groove 17 through sealed bearings. The transmission screw 605 is rotated to drive the transmission frame 604 to move downward through the transmission screw 605, and the transmission frame 604 drives the two lifting plates 602 and multiple universal wheels 603 to move downward, causing the universal wheels 603 to extend from the inside of the slide groove 601, and the universal wheels 603 are grounded, which is convenient for moving the base 1.

[0032] The driving assembly 7 includes a groove 701 and a worm 702. The groove 701 is opened on one side of the base 1. A servo motor 703 is fixedly arranged on the inner wall of the groove 701. The servo motor 703 is a forward and reverse motor. The worm 702 is rotatably arranged on the inner wall of the auxiliary groove 17 through a sealed bearing. One end of the worm 702 is fixedly connected to the transmission shaft of the servo motor 703. The front of the worm 702 is meshed with a worm wheel 704. The inner wall of the worm wheel 704 is fixedly connected to the surface of the transmission screw 605. When the servo motor 703 is started, the servo motor 703 will drive the worm 702 to rotate. The worm 702 drives the transmission screw 605 to rotate through the worm wheel 704, thereby realizing the driving of the transmission screw 605. The servo motor 703 is arranged outside the auxiliary groove 17 for easy maintenance.

[0033] The adjustment assembly 8 includes two storage boxes 801, one of which is fixedly arranged on the front side of the base 1, and the other is fixedly arranged on the back side of the base 1. Through holes are provided on the surfaces of the two storage boxes 801. Adjustment plates 802 are slidably connected to the inner walls of the two storage boxes 801. Threaded holes are provided on the surfaces of the two adjustment plates 802. Vertical rods 803 are fixedly arranged on one side of the two adjustment plates 802. A gripping rod 804 is fixedly arranged on one end of the two vertical rods 803. The surface of the auxiliary grip rod 804 is fixed with an anti-slip cover. When the auxiliary grip rod 804 is pulled, the auxiliary grip rod 804 drives the adjustment plate 802 to slide through the vertical rod 803, and the relative position of the adjustment plate 802 and the storage box 801 is adjusted. Then, bolts are screwed into the through holes and the threaded holes to fix the adjustment plate 802 and the storage box 801. Then, the base 1 is pushed by the auxiliary grip rod 804, which is very convenient. By selecting different through holes, the adjustment plate 802 can be stored inside the storage box 801, reducing the use of space.

[0034] When in use, the raw material is distilled by the supergravity distillation bed body 10, and the gaseous volatile components (silane or sulfite) and the misty non-volatile components are discharged by the gas manifold 12. The gaseous volatile components and the misty non-volatile components are condensed and refluxed by the condensation component 3 and the light component box 5. The volatile components in the reflux liquid will be countercurrently contacted and transfer substances and energy when contacting the rising steam, so as to volatilize again, and the non-volatile components are further separated, thus realizing supergravity distillation. After multiple refluxes and ultra-gravity distillations, the liquid silane product or sulfite product is discharged through the discharge pipe 18. The liquid non-volatile components are heated by the cooperation of the recombination box 9, the evaporation component 4 and the external steam generator to generate high-temperature steam to cooperate with the reflux liquid to achieve ultra-gravity distillation. The connecting frame 2, the ultra-gravity distillation bed body 10, the light component box 5, the recombination box 9, the condensation component 3 and the evaporation component 4 are all installed on the base 1, with a compact layout, which reduces the difficulty of installation and reduces the space occupied.

[0035] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A skid-mounted continuous distillation system for silane products and sulfite products, comprising a base (1), characterized in that: The top of the base (1) is provided with a connecting frame (2), a light component box (5) and a heavy component box (9), the top of the connecting frame (2) is provided with an ultra-gravity distillation bed body (10), a moving disk (11) is rotatably provided inside the ultra-gravity distillation bed body (10), a moving baffle ring is provided on the upper surface of the moving disk (11), a static disk is provided above the moving disk (11), and a static baffle ring is provided on the lower surface of the static disk, a gas collecting pipe (12), a reflux pipe (13), a feed pipe (14), an air inlet pipe (15) and a turbidity collecting pipe (16) are provided on the surface of the ultra-gravity distillation bed body (10), a condensation assembly (3) is provided on the top of the light component box (5), an evaporation assembly (4) is provided on the top of the heavy component box (9), an auxiliary groove (17) is provided inside the base (1), an auxiliary assembly (6) is provided inside the auxiliary groove (17), and an adjustment assembly (8) is provided on one side of the base (1).

2. The skid-mounted continuous distillation system for silane products and sulfite products according to claim 1, characterized in that: The condensation assembly (3) comprises a condensation box (301), the condensation box (301) is arranged at the top of the light component box (5), the inner wall of the condensation box (301) is provided with a first S-shaped heat exchange tube (302), one end of the first S-shaped heat exchange tube (302) passes through the top of the light component box (5) and is placed at the top of the light component box (5), the other end of the first S-shaped heat exchange tube (302) is provided with a first auxiliary tube (303), one end of the first auxiliary tube (303) is connected to one end of the gas collecting pipe (12), a water inlet pipe (304) is provided at the bottom of the front side of the condensation box (301), and a water outlet pipe (305) is provided at the top of the back side of the condensation box (301).

3. The skid-mounted continuous distillation system for silane products and sulfite products according to claim 1, characterized in that: A discharge pipe (18) is provided on one side of the light component tank (5), a first submersible pump (19) is provided on the inner wall of the bottom end of the light component tank (5), a liquid supply pipe (20) is provided at the liquid outlet end of the first submersible pump (19), one end of the liquid supply pipe (20) passes through the inner wall of one side of the light component tank (5) and is connected to one end of the return pipe (13), the other end of the return pipe (13) and one end of the feed pipe (14) are both provided with a shower nozzle, the return pipe (13), the feed pipe (14) and the air collecting pipe (12) are all placed above the moving plate (11), and the air inlet pipe (15) and the turbidity collecting pipe (16) are both placed below the moving plate (11).

4. The skid-mounted continuous distillation system for silane products and sulfite products according to claim 1, characterized in that: The evaporation component (4) comprises a heating box (401), the heating box (401) being arranged at the top of a recombinant component box (9), the inner wall of the recombinant component box (9) being provided with a second S-shaped heat exchange tube (402), one end of the second S-shaped heat exchange tube (402) passing through the top of the recombinant component box (9) and being arranged at the top of the interior of the recombinant component box (9), a steam transmission pipe (403) being arranged at the top of the front face of the heating box (401), one end of the steam transmission pipe (403) being connected to one end of an air inlet pipe (15), a turbidity outlet pipe (404) being arranged at the bottom of the front face of the heating box (401), and a turbidity inlet pipe (405) being arranged at the middle of the back face of the heating box (401).

5. A skid-mounted continuous distillation system for silane products and sulfite products according to claim 4, characterized in that: The inner wall of the recombinant tank (9) is provided with a partition (21) and a second submersible pump (22), the partition (21) being arranged in a Z shape, the partition (21) dividing the interior of the recombinant tank (9) into a steam storage chamber (24) and a turbidity storage chamber (23) connected to the interior of the turbidity collecting pipe (16), the second submersible pump (22) being placed inside the turbidity storage chamber (23), the liquid outlet end of the second submersible pump (22) being provided with a second auxiliary pipe (25), one end of the second auxiliary pipe (25) passing through the inner wall of one side of the recombinant tank (9) and being connected to one end of the turbidity inlet pipe (405), a steam outlet pipe (26) being provided on one side of the recombinant tank (9), the interior of the steam outlet pipe (26) being connected to the steam storage chamber (24).

6. The skid-mounted continuous distillation system for silane products and sulfite products according to claim 1, characterized in that: The auxiliary component (6) comprises a driving component (7) and two slide grooves (601), the two slide grooves (601) are both arranged at the bottom end of the base (1), the interiors of the two slide grooves (601) are both connected to the interior of the auxiliary groove (17), the inner walls of the two slide grooves (601) are both slidably connected with a lifting plate (602), the bottom ends of the two lifting plates (602) are both provided with a universal wheel (603), a transmission frame (604) sliding with the auxiliary groove (17) is provided between the two lifting plates (602), the inner wall of the transmission frame (604) is threadedly connected with a transmission screw (605) through a screw nut, and both ends of the transmission screw (605) are rotatably connected to the inner wall of the auxiliary groove (17) through a sealed bearing.

7. A skid-mounted continuous distillation system for silane products and sulfite products according to claim 6, characterized in that: The driving assembly (7) comprises a groove (701) and a worm (702), wherein the groove (701) is provided on one side of the base (1), and a servo motor (703) is provided on the inner wall of the groove (701), wherein the servo motor (703) is a forward and reverse motor, and the worm (702) is rotatably arranged on the inner wall of the auxiliary groove (17) via a sealed bearing, and one end of the worm (702) is connected to a transmission shaft of the servo motor (703), and a worm wheel (704) is meshedly connected to the front side of the worm (702), and the inner wall of the worm wheel (704) is connected to the surface of a transmission screw (605).

8. The skid-mounted continuous distillation system for silane products and sulfite products according to claim 1, characterized in that: The adjustment assembly (8) comprises two storage boxes (801), wherein one of the storage boxes (801) is arranged on the front side of the base (1), and the other storage box (801) is arranged on the back side of the base (1), through holes are provided on the surfaces of the two storage boxes (801), adjustment plates (802) are slidably connected to the inner walls of the two storage boxes (801), threaded holes are provided on the surfaces of the two adjustment plates (802), vertical rods (803) are provided on one side of the two adjustment plates (802), and gripping rods (804) are provided at one end of the two vertical rods (803), and anti-slip sleeves are provided on the surfaces of the gripping rods (804).