Automation equipment for dangerous reaction

Abstract

The utility model relates to the technical field of automation equipment, in particular to automation equipment for dangerous reaction, which comprises pre-split charging equipment, automatic reaction detection equipment, automatic sample post-processing equipment and a rail type mobile robot. The automatic reaction detection equipment comprises a plurality of reaction areas, and each reaction area is provided with a magnetic stirring reaction bottle, a first magnetic stirrer, a Raman detector, a temperature detection device and a feeding transfer device for feeding raw materials into the magnetic stirring reaction bottle; the automatic sample post-processing equipment comprises a magnetic stirring post-processing bottle, a second magnetic stirrer and a negative pressure suction filtration device; the rail-mounted mobile robot realizes material transmission among the pre-split charging equipment, the automatic reaction detection equipment and the automatic sample post-processing equipment. The automatic equipment for dangerous reaction is high in automation degree, manual operation can be reduced, and production efficiency can be improved.

Description

Technical Field

[0001] The utility model relates to the technical field of automation equipment, in particular to an automation equipment used for dangerous reactions. Background Art

[0002] Dangerous reactions are a common production process in the chemical, pharmaceutical, and metallurgical industries. These reactions may produce toxic and hazardous substances, or the reactions themselves are highly dangerous. Traditional manual operation methods not only have safety risks, but are also inefficient. Utility Model Content

[0003] In order to solve the problem in the prior art that dangerous reactions have potential safety hazards due to manual operation, the utility model provides an automated device for dangerous reactions that ensures production safety.

[0004] The technical solution adopted by the utility model to solve its technical problems is:

[0005] An automated device for hazardous response, comprising:

[0006] A pre-packaging device, the pre-packaging device comprising a solid raw material bottle storage area, an empty sample bottle storage area for storing sample bottles, a solid weighing device for weighing the solid raw material, and a liquid filling module for providing liquid raw materials;

[0007] An automated reaction detection device, wherein the automated reaction detection device comprises a plurality of reaction zones, wherein the reaction zones are provided with a magnetic stirring reaction bottle, a first magnetic stirrer, a Raman detector, a temperature detection device, and a feeding and transferring device for feeding raw materials into the magnetic stirring reaction bottle;

[0008] An automated sample post-processing device, the automated sample post-processing device comprising a magnetic stirring post-processing bottle, a second magnetic stirrer and a negative pressure filtration device;

[0009] A track-type mobile robot realizes material transmission between pre-packaging equipment, automated reaction detection equipment and automated sample post-processing equipment.

[0010] Furthermore, the pre-packaging equipment also includes a labeling machine and a first barcode scanner.

[0011] Furthermore, the automated reaction detection equipment also includes a sample bottle storage area, an empty reaction bottle storage area and a second barcode scanner.

[0012] Furthermore, the automated reaction detection equipment also includes a pretreatment area, and the pretreatment area includes a first cooling device for cooling the raw materials in the raw material bottle and a stirring device for stirring the raw materials in the raw material bottle.

[0013] Furthermore, a Buffenhausen funnel for filtration is provided on the negative pressure filtration device, and the automated sample post-processing equipment also includes a Buffenhausen funnel storage area.

[0014] Furthermore, the automated sample post-processing equipment also includes a magnetic stirring reaction bottle storage area and a magnetic stirring post-processing bottle storage area.

[0015] Furthermore, the automated sample post-processing equipment also includes a second cooling device, and the second magnetic stirrer is located in the second cooling device.

[0016] Furthermore, the pre-packaging equipment is also provided with a first static electricity removal device, the automated reaction detection equipment is provided with a second static electricity removal device, and the automated sample post-processing equipment is also provided with a third static electricity removal device.

[0017] Furthermore, the pre-packaging equipment and the automated reaction detection equipment are each provided with tracks, and the tracks are connected front and back to form a walking path for the track-type mobile robot.

[0018] Furthermore, a conveyor belt is provided between the automated reaction detection equipment and the automated sample post-processing equipment.

[0019] Beneficial effects:

[0020] (1) The automated equipment for hazardous reactions of the utility model has a high degree of automation, which can reduce manual operations and improve production efficiency;

[0021] (2) Explosion-proof steel plates are installed on the outside of pre-packaging equipment, automated reaction detection equipment, and automated sample post-processing equipment. The equipment is well sealed to prevent the leakage of toxic and hazardous substances and ensure production safety;

[0022] (3) Pre-packaging equipment, automated reaction detection equipment, and automated sample post-processing equipment are all equipped with anti-static devices, and the equipment has good explosion-proof performance, effectively preventing accidental explosions;

[0023] (4) It can realize real-time temperature control, speed control, and adding raw materials during reaction, which better meets the operational requirements of the reaction;

[0024] (5) The automated reaction detection equipment is equipped with a Raman detection device, which can realize the function of online in-situ detection of the characterization characteristics of the reactants without sampling;

[0025] (6) The control system is highly intelligent and can be precisely controlled according to response requirements;

[0026] (7) The equipment has a compact structure, occupies a small area, and is easy to install and maintain. BRIEF DESCRIPTION OF THE DRAWINGS

[0027] In order to more clearly illustrate the technical solutions of the embodiments of the utility model, the drawings required for use in the description of the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the utility model. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative work.

[0028] Figure 1 It is a schematic diagram of the external structure of the pre-packaging equipment, the automated reaction detection equipment, and the automated sample post-processing equipment;

[0029] Figure 2 It is a schematic diagram of the internal structure of the pre-packaging equipment, the automated reaction detection equipment, and the automated sample post-processing equipment;

[0030] Figure 3 It is a top view of the internal structure of the pre-packaging equipment, the automated reaction detection equipment, and the automated sample post-processing equipment;

[0031] Figure 4 It is a schematic diagram of the internal three-dimensional structure of the pre-packaging equipment;

[0032] Figure 5 It is a schematic diagram of the internal top view structure of the pre-packaging equipment;

[0033] Figure 6 It is a schematic diagram of the internal three-dimensional structure of the automated reaction detection equipment;

[0034] Figure 7 It is a schematic diagram of the internal top view structure of the automated reaction detection equipment;

[0035] Figure 8 It is a schematic diagram of the internal three-dimensional structure of the automated sample post-processing equipment;

[0036] Fig. 9 This is a schematic diagram of the internal top-down structure of the automated sample post-processing equipment.

[0037] 1. Pre-packaging equipment, 11. Solid raw material bottle storage area, 12. Sample bottle, 13. Empty sample bottle storage area, 14. Liquid filling module, 15. Labeling machine, 16. First barcode scanner, 17. First static electricity removal device, 18. Solid weighing device, 2. Automated reaction detection equipment, 21. Reaction area, 22. Magnetic stirring reaction bottle, 23. First magnetic stirrer, 24. Raman detector, 25. Temperature detection device, 26. Sample bottle storage area, 27. Storage area for empty reaction bottles; 28. Second barcode scanner; 29. ​​Pretreatment area; 210. Second static electricity removal device; 3. Automated sample post-processing equipment; 31. Magnetic stirring post-processing bottle; 32. Second magnetic stirrer; 33. Negative pressure filtration device; 34. Buffenhausen funnel; 35. Buffenhausen funnel storage area; 36. Magnetic stirring reaction bottle storage area; 37. Magnetic stirring post-processing bottle storage area; 38. Third static electricity removal device; 4. Track-type mobile robot. DETAILED DESCRIPTION

[0038] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. The following description of at least one exemplary embodiment is actually only illustrative and is by no means a limitation on the utility model and its application or use. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without making creative work are within the scope of protection of the utility model.

[0039] It should be noted that the terms used herein are only for describing specific embodiments and are not intended to limit the exemplary embodiments according to the present application. As used herein, unless the context clearly indicates otherwise, the singular form is also intended to include the plural form. In addition, it should be understood that when the terms "comprise" and / or "include" are used in this specification, it indicates the presence of features, steps, operations, devices, components and / or combinations thereof.

[0040] Unless otherwise specifically stated, the relative arrangement, numerical expressions and numerical values ​​of the parts and steps set forth in these embodiments do not limit the scope of the utility model. At the same time, it should be understood that, for ease of description, the sizes of the various parts shown in the accompanying drawings are not drawn according to the actual proportional relationship. The technology, method and equipment known to those of ordinary skill in the relevant art may not be discussed in detail, but in appropriate cases, the technology, method and equipment should be considered as a part of the specification. In all examples shown and discussed here, any specific value should be interpreted as being merely exemplary, rather than as a limitation. Therefore, other examples of exemplary embodiments may have different values. It should be noted that similar reference numerals and letters represent similar items in the following drawings, and therefore, once a certain item is defined in an accompanying drawing, it does not need to be further discussed in subsequent drawings.

[0041] In the description of the present utility model, it needs to be understood that the directions or positional relationships indicated by directional words such as "front, back, up, down, left, right", "lateral, vertical, perpendicular, horizontal" and "top, bottom" are usually based on the directions or positional relationships shown in the drawings, and are only for the convenience of describing the present utility model and simplifying the description. Unless otherwise specified, these directional words do not indicate or imply that the device or element referred to must have a specific direction or be constructed and operated in a specific direction, and therefore cannot be understood as limiting the scope of protection of the present utility model; the directional words "inside and outside" refer to the inside and outside relative to the contours of each component itself.

[0042] For ease of description, spatially relative terms such as "above", "above", "on the upper surface of", "above", etc. may be used here to describe the spatial positional relationship between a device or feature and other devices or features as shown in the figure. It should be understood that spatially relative terms are intended to include different orientations of the device in use or operation in addition to the orientation described in the figure. For example, if the device in the accompanying drawings is inverted, the device described as "above other devices or structures" or "above other devices or structures" will be positioned as "below other devices or structures" or "below other devices or structures". Thus, the exemplary term "above" can include both "above" and "below". The device can also be positioned in other different ways (rotated 90 degrees or in other orientations), and the spatially relative descriptions used here are interpreted accordingly.

[0043] In addition, it should be noted that the use of terms such as "first" and "second" to limit components is only for the convenience of distinguishing the corresponding components. If not otherwise stated, the above terms have no special meaning and therefore cannot be understood as limiting the scope of protection of the utility model.

[0044] like Figures 1 to 3 , an automated device for hazardous reactions, comprising a pre-packaging device 1, an automated reaction detection device 2, an automated sample post-processing device 3 and a track-type mobile robot 4. The track-type mobile robot 4 realizes the material transmission between the pre-packaging device 1, the automated reaction detection device 2 and the automated sample post-processing device 3. The track-type mobile robot 4 can reach the automated sample post-processing device 3. In the utility model, a conveyor belt is set between the automated reaction detection device 2 and the automated sample post-processing device 3. The track-type mobile robot 4 can reach the conveyor belt, and then, another robot is equipped at the automated sample post-processing device 3. The pre-packaging device 1, the automated reaction detection device 2, and the automated sample post-processing device 3 are all equipped with protective warehouses on the outside.

[0045] like Figures 4-5 The pre-packaging device 1 includes a solid raw material bottle storage area 11, an empty sample bottle storage area 13 for storing sample bottles 12, a solid weighing device 13 for weighing the solid raw material, and a liquid filling module 14 for providing liquid raw materials.

[0046] The pre-packaging device 1 further comprises a labeling machine 15 and a first barcode scanner 16. The pre-packaging device 1 is further provided with a first static electricity removal device 17.

[0047] like Figures 6-7 The automated reaction detection device 2 includes a plurality of reaction zones 21, and the reaction zone 21 is provided with a magnetic stirring reaction bottle 22, a first magnetic stirrer 23, a Raman detector 24, a temperature detection device 25 and a feeding transfer device for feeding raw materials to the magnetic stirring reaction bottle 22. The magnetic stirring reaction bottle 22, i.e., the reaction bottle is provided with a magnet, and the temperature detection device 25 is optional but not limited to an infrared temperature detection sensor. The solid raw material can be fed directly through the track-type mobile robot 4. The feeding transfer device for the liquid raw material can pour the liquid raw material into a needle valve through the track-type mobile robot 4, and then drip the material through the needle valve. Preferably, the feeding device for the liquid raw material of the utility model includes a suction device, which is connected to the dripping needle through a pipeline, and a peristaltic pump is arranged on the pipeline.

[0048] The automated reaction detection device 2 further includes a sample bottle storage area 26 , an empty reaction bottle storage area 27 and a second barcode scanner 28 . The automated reaction detection device 2 is provided with a second static electricity removal device 210 .

[0049] The automated reaction detection device 2 also includes a pretreatment area 29, which includes a first cooling device for cooling the raw materials in the raw material bottle and a stirring device for stirring the raw materials in the raw material bottle. The stirring device can be a stirring rod, etc., and of course it can also be a magnetic stirring structure, that is, a combination structure of a magnetic stirrer and a magnet, and a magnet is arranged in the raw material bottle. The automated reaction detection device 2 can also include a temperature control device for controlling the temperature of the magnetic stirring reaction bottle 22, and water can be used to achieve temperature control. Preferably, the utility model adopts a metal bath structure, and the Raman detection probe of the Raman detector 24 is embedded in the metal bath, which is used to directly characterize the reaction liquid inside the magnetic stirring reaction bottle 22.

[0050] like Figures 8-9 The automated sample post-processing device 3 includes a magnetic stirring post-processing bottle 31, a second magnetic stirrer 32 and a negative pressure filtration device 33. The magnetic stirring post-processing bottle 31, that is, the post-processing bottle has a magnet.

[0051] A Buchner funnel 34 for filtering is provided on the negative pressure filtration device 33 , and the automated sample post-processing equipment 3 further includes a Buchner funnel storage area 35 .

[0052] The automated sample post-processing device 3 further includes a magnetic stirring reaction bottle storage area 36 and a magnetic stirring post-processing bottle storage area 37 .

[0053] The automated sample post-processing device 3 further comprises a second cooling device, in which the second magnetic stirrer 32 is located.

[0054] The automated sample post-processing device 3 is further provided with a third static electricity removal device 38 .

[0055] The pre-packaging device 1 and the automated sample post-processing device 3 are respectively provided with tracks, and the tracks are connected front and back to form a walking path for the track-type mobile robot 4 .

[0056] Working principle:

[0057] The main function of the pre-packaging device 1 is to pre-pack the solid and liquid materials required for the reaction into the sample bottle 12 through the solid weighing device 8 and the liquid filling module 14 respectively; static electricity is a potential safety hazard during the material packaging process. In order to avoid accidents caused by static electricity, the device is equipped with a first static electricity removal device 17. This device can operate continuously and effectively remove possible static electricity, thereby reducing the risk of fire or explosion and ensuring production safety.

[0058] After the pre-packaging of the materials is completed, the automatic door of the pre-packaging equipment 1 is opened, and the track-type mobile robot 4 transports the materials to the automatic reaction detection equipment 2 via the guide rails.

[0059] Take over the pre-packed sample bottle 12 from the previous station. The track-type mobile robot 4 first transfers the magnetic stirring reaction bottle 22 with a magnet to the first magnetic stirrer 23, and the liquid material is slowly dripped through the liquid feeding transfer device; the solid material is clamped by the robot arm of the track-type mobile robot 4 to the top of the magnetic stirring reaction bottle 22, and the solid material is slowly added in a pouring manner; during the entire process of adding liquid and solid, the infrared temperature sensor just above the magnetic stirring reaction bottle 22 monitors the temperature of the reaction liquid in real time. If the temperature rises to the set temperature, the feeding action can be suspended, and the feeding work can be performed again after the temperature drops. When the reaction setting time is reached, the Raman detection probe can detect the reaction liquid in situ. If the reaction is not completed, the reaction continues, and the system recommends the time required to continue the reaction; if the reaction is completed, the track-type mobile robot 4 will move the magnetic stirring reaction bottle 22 to the conveyor belt and transport it to the automated sample post-processing equipment 3.

[0060] Take over the magnetic stirring reaction bottle 22 that has been reacted and transmitted from the previous station. The robot of the automated sample post-processing equipment 3 places the large-volume magnetic stirring post-processing bottle 31 in the low-temperature stirring zone, injects water (which can be installed) into the magnetic stirring post-processing bottle 31, stirs and cools it, and after reaching the temperature, pours the reaction liquid in the magnetic stirring reaction bottle 22 into the magnetic stirring post-processing bottle 31 to complete the quenching work. After the quenching is completed, the liquid in the magnetic stirring post-processing bottle 31 is transferred to the negative pressure filtration device 33 to complete the filtration of the sample. Finally, the robot places the Buchner funnel 34 with the solid sample in the Buchner funnel storage area 35 for manual processing.

[0061] By using the automation equipment of the utility model, the safety and stability of dangerous reaction processes can be significantly improved. The equipment can automatically adjust parameters such as reaction temperature and feeding speed to judge whether the reaction is completed and post-processing operations online, reducing errors and safety risks of manual operations. At the same time, the automated control system can monitor the data of the reaction process in real time, detect abnormal situations in time and take corresponding measures, effectively reducing the possibility of accidents. In addition, special designs such as explosion-proof design and explosion-proof surface further enhance the safety performance of the equipment. When encountering unexpected situations, the equipment can respond quickly and maximize the safety of operators and equipment. Therefore, the utility model is of great significance for improving the safety and efficiency of chemical industry production.

[0062] The utility model is an automated device for dangerous reactions, which is particularly suitable for situations involving flammable and explosive substances in chemical reactions. The device can effectively reduce the risk of operators being exposed to dangerous environments and improve production safety through automated control.

[0063] The above are only preferred specific implementation methods of the utility model, but the protection scope of the utility model is not limited to this. Any technician familiar with the technical field within the technical scope disclosed by the utility model, who makes equivalent replacements or changes based on the technical scheme and utility model concept of the utility model, should be covered by the protection scope of the utility model.

Claims

1. An automated device for hazardous reactions, characterized in that: include: A pre-packaging device (1), the pre-packaging device (1) comprising a solid raw material bottle storage area (11), an empty sample bottle storage area (13) for storing sample bottles (12), a solid weighing device (18) for weighing the solid raw material, and a liquid filling module (14) for providing liquid raw materials; An automated reaction detection device (2), the automated reaction detection device (2) comprising a plurality of reaction zones (21), the reaction zones (21) being provided with a magnetic stirring reaction bottle (22), a first magnetic stirrer (23), a Raman detector (24), a temperature detection device (25) and a feeding transfer device for feeding raw materials into the magnetic stirring reaction bottle (22); An automated sample post-processing device (3), the automated sample post-processing device (3) comprising a magnetic stirring post-processing bottle (31), a second magnetic stirrer (32) and a negative pressure filtration device (33); A track-type mobile robot (4), wherein the track-type mobile robot (4) realizes material transmission between a pre-packaging device (1), an automated reaction detection device (2) and an automated sample post-processing device (3).

2. The automated equipment for dangerous response according to claim 1, characterized in that: The pre-packaging equipment (1) further comprises a labeling machine (15) and a first code scanner (16).

3. The automated equipment for dangerous response according to claim 1, characterized in that: The automated reaction detection device (2) further comprises a sample bottle storage area (26), an empty reaction bottle storage area (27) and a second code scanner (28).

4. The automated equipment for dangerous reactions according to claim 1, characterized in that: The automated reaction detection device (2) further comprises a pretreatment area (29), wherein the pretreatment area (29) comprises a first cooling device for cooling the raw materials in the raw material bottle and a stirring device for stirring the raw materials in the raw material bottle.

5. The automated equipment for dangerous response according to claim 1, characterized in that: A Buchner funnel (34) for filtering is provided on the negative pressure filtration device (33), and the automated sample post-processing equipment (3) further comprises a Buchner funnel storage area (35).

6. The automated equipment for dangerous response according to claim 1, characterized in that: The automated sample post-processing device (3) further comprises a magnetic stirring reaction bottle storage area (36) and a magnetic stirring post-processing bottle storage area (37).

7. The automated equipment for dangerous response according to claim 1, characterized in that: The automated sample post-processing device (3) further comprises a second cooling device, and the second magnetic stirrer (32) is located in the second cooling device.

8. The automated equipment for dangerous response according to claim 1, characterized in that: The pre-packaging equipment (1) is also provided with a first static electricity removal device (17), the automated reaction detection equipment (2) is provided with a second static electricity removal device (210), and the automated sample post-processing equipment (3) is also provided with a third static electricity removal device (38).

9. The automated equipment for dangerous response according to claim 1, characterized in that: The pre-packaging equipment (1) and the automated reaction detection equipment (2) are each provided with a track, and the tracks are connected front and back to form a walking path for the track-type mobile robot (4).

10. The automated equipment for dangerous response according to claim 9, characterized in that: A conveyor belt is provided between the automated reaction detection device (2) and the automated sample post-processing device (3).

Images