Pure ethanol gas sterilizer
Through the combination of tank rotation and hot water circulation by pure ethanol gas sterilization machines, the problem of the problem of lumps and active component losses in the thermal pressure sterilization method is solved, and the efficient and uniform sterilization effect is achieved.
Patent Information
- Application Number
- CN202420701177.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-04-08
- Publication Date
- 2025-01-28
- Estimated Expiration
- 2034-04-08
AI Technical Summary
The existing hot press sterilization methods have the problem that solid materials are prone to agglomeration and large losses of active ingredients, which are especially unfavorable for Chinese medicinal materials.
The pure ethanol gas sterilization machine, through ethanol gas sterilization, combined with tank rotation and hot water circulation to achieve uniform heating and rapid drying of the material.
Effectively avoid the loss of material blocks and effective ingredients, achieve a sufficient sterilization effect, and reduce the subsequent drying and crushing steps, and reduce the risk of dyeing bacteria.
Smart Images

Figure CN222399601U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of pure ethanol gas sterilizers, in particular to a pure ethanol gas sterilizer. Background Art
[0002] "Sterilization" is an important means to ensure that the microbial index of pharmaceutical and health care solid preparations meets the standard. In the process of manufacturing solid preparations, pharmaceutical factories must perform "hot pressure sterilization" (121℃ / 30min) on the materials to ensure that the microbial index of the finished products meets the standard. The sterilization effect is reliable, so it is widely used.
[0003] Hot pressure sterilization, also known as moist heat sterilization or moist heat steam sterilization, is a sterilization method that uses steam provided by a boiler for sterilization. In actual applications, it is found that "hot pressure sterilization" has the following defects:
[0004] 1. Solid materials tend to clump after sterilization, so the materials need to be dried and crushed again. This not only adds two processes, but also increases the risk of re-contamination;
[0005] 2. The "temperature of hot pressing sterilization is too high" (121℃), which also causes great damage to some effective ingredients in traditional Chinese medicine. For example, the content of gardenia glycoside contained in Huangzhizi is lost by nearly 30% after hot pressing sterilization.
[0006] Studies have shown that ethanol can effectively kill microorganisms in traditional Chinese medicine by penetrating microbial cells and their spore walls to denature proteins. Utility Model Content
[0007] The technical problem to be solved by the utility model is to overcome the defects of the above-mentioned technology and provide a pure ethanol gas sterilizer.
[0008] In order to solve the above technical problems, the technical solution provided by the utility model is a pure ethanol gas sterilizer: comprising a tank body and a bracket, the left and right ends of the tank body are in a frustum shape, the shaft tubes at both ends of the tank body are rotatably connected to the bearing seat of the bracket, the outside of the tank body is provided with a jacket, the jacket and the tank body form a closed interlayer, the lower end of the tank body is provided with a discharge butterfly valve, the upper end is provided with a top cover, the shaft tube on one side of the tank body is provided with a fixed gas inlet and outlet pipe and a hot water return pipe, and the shaft tube on the other side of the tank body is provided with a hot water pipe; the gas inlet and outlet pipe passes through the inside of the shaft tube, and three pipe openings are provided at the outer end, each of which is provided with a valve; the shaft tube is a double-layer tube, and the hot water return pipe and the hot water pipe are both rotatably connected to the shaft tube;
[0009] A hydraulic motor is provided on the upper part of one side of the bracket, and the hydraulic motor is connected to the gear transmission of the shaft tube;
[0010] It also includes an ethanol vaporizer and a hot water generator. The ethanol vaporizer, gas inlet and outlet pipes, and a titanium filter rod in the tank body are connected in sequence, and the hot water generator, hot water pipe, interlayer, and hot water reflux pipe are connected in a closed loop in sequence.
[0011] As an improvement, automatic cleaning nozzles are provided on the conical surfaces at both ends of the tank body, and the automatic cleaning nozzles extend to the inner wall of the tank body. The tank body is also provided with a cleaning pipe, which is located in the axial tube close to the hot water pipe and is connected to the two automatic cleaning nozzles.
[0012] As an improvement, the top cover is provided with a cover-tightening handle, and a hanging ear is provided on one side of the top cover, and the hanging ear is fixedly connected to the tank body.
[0013] As an improvement, a step ladder is provided on one side of the bracket, a platform is provided at the upper end of the step ladder, the hydraulic motor is provided on the platform, and the platform is provided with a fence.
[0014] As an improvement, the hydraulic motor is on the same side as the hot water pipe.
[0015] As an improvement, a retractable water receiving hopper is provided at the lower part of the unloading butterfly valve.
[0016] As an improvement, a water dividing plate is provided at the inner end of the shaft tube of the hot water pipe, and the water dividing plate enters the interlayer and is fixedly connected to the tank body.
[0017] As an improvement, an outer sheath is provided outside the jacket.
[0018] Compared with the prior art, the utility model has the following advantages: going up to the platform from the step ladder, opening the top cover, putting materials into the tank body, closing the top cover, starting the ethanol vaporizer and the hot water generator, starting the hydraulic motor to drive the tank body to rotate in one direction at a speed of 8-10 revolutions / min, starting the vacuum pump to evacuate the gas inlet and outlet pipes to the maximum limit and then closing the vacuum pump, connecting the nitrogen bottle to the gas inlet and outlet pipes, opening the valve to fill nitrogen until the vacuum degree in the tank body drops to 0 and then closing it, and then using the vacuum pump to evacuate the tank body to the maximum limit from the gas inlet and outlet pipes and then closing the vacuum pump. Start the ethanol vaporizer, hot water generator and hydraulic motor. After preheating for a few minutes, inject ethanol through the ethanol vaporizer until ethanol no longer enters. Turn off the ethanol vaporizer, hot water generator and hydraulic motor. After standing for 1-2 hours, restart the hot water generator, vacuum pump and hydraulic motor, drive the tank body to rotate in one direction at a speed of 8-10 rpm, and then keep hot water circulating in the interlayer. After running for 0.5-1 hour, turn off the hot water generator, vacuum pump and hydraulic motor, open the nitrogen valve, fill with nitrogen until the pressure inside and outside the tank is balanced, then close it, open the top cover, and finally open the unloading butterfly valve to unload the material. The titanium filter rod is used to intake air into the tank body and check the discharge of materials at the same time.
[0019] Practical application test results: Taking Huangzhizi as an example, after sterilization with ethanol gas, the loss of gardenia glycoside content is less than 5%.
[0020] This pure ethanol gas sterilizer utilizes ethanol gas for sterilization and quickly dries the material after sterilization. During drying, the tank rotates to heat the material evenly without agglomeration. It not only fully achieves the effect of full sterilization, but also saves the trouble of re-drying and crushing the material after the original hot pressure sterilization, and avoids the risk of re-contamination. At the same time, the "low temperature" (≤80 degrees) of ethanol gas sterilization can effectively prevent some effective ingredients in traditional Chinese medicine from being destroyed. It can be widely used in the sterilization of solid materials and has high practical value and promotion value. BRIEF DESCRIPTION OF THE DRAWINGS
[0021] Figure 1 The utility model is a front view of a pure ethanol gas sterilizer.
[0022] Figure 2 The utility model is a side view of a bracket of a pure ethanol gas sterilizer.
[0023] Figure 3 The utility model is a structural schematic diagram of the left side shaft tube of a pure ethanol gas sterilizer.
[0024] Figure 4 The utility model is a structural schematic diagram of the right side shaft tube of a pure ethanol gas sterilizer.
[0025] As shown in the figure: 1. tank body, 2. bracket, 3. shaft tube, 4. bearing seat, 5. jacket, 6. interlayer, 7. unloading butterfly valve, 8. top cover, 9. gas inlet and outlet pipes, 10. hot water reflux pipe, 11. hot water pipe, 12. hydraulic motor, 13. gear, 14. ethanol vaporizer, 15. hot water generator, 16. titanium filter rod, 17. automatic cleaning nozzle, 18. cleaning pipe, 19. tight cover handle, 20. hanging ear, 21. step ladder, 22. platform, 23. fence, 24. water bucket, 25. water distribution plate, 26. outer covering. DETAILED DESCRIPTION
[0026] The following is a further detailed description of the pure ethanol gas sterilizer of the utility model in conjunction with the accompanying drawings.
[0027] Combined with Figures 1 to 4A pure ethanol gas sterilizer comprises a tank body 1 and a bracket 2, wherein the left and right ends of the tank body 1 are in a frustum shape, the shaft tubes 3 at the two ends of the tank body 1 are rotatably connected to the bearing seat 4 of the bracket 2, the tank body 1 is provided with a jacket 5 on the outside, the jacket 5 and the tank body 1 form a closed interlayer 6, the tank body 1 is provided with a discharge butterfly valve 7 at the lower end, and a top cover 8 at the upper end, the shaft tube 3 on one side of the tank body 1 is provided with a fixed gas inlet and outlet pipe 9 and a hot water return pipe 10, and the shaft tube 3 on the other side of the tank body 1 is provided with a hot water pipe 11; the gas inlet and outlet pipe 9 passes through the shaft tube 3, and three pipe openings are provided at the outer end, each of which is provided with a valve; the shaft tube 3 is a double-layer tube, and the hot water return pipe 10 and the hot water pipe 11 are both rotatably connected to the shaft tube 3;
[0028] A hydraulic motor 12 is provided at an upper portion of one side of the bracket 2, and the hydraulic motor 12 is transmission-connected to a gear 13 of the shaft tube 3;
[0029] It also includes an ethanol vaporizer 14 and a hot water generator 15. The ethanol vaporizer 14, the gas inlet and outlet pipes 9, and the titanium filter rod 16 in the tank body 1 are connected in sequence, and the hot water generator 15, the hot water pipe 11, the interlayer 6, and the hot water reflux pipe 10 are connected in sequence in a closed loop.
[0030] The conical surfaces at both ends of the tank body 1 are provided with automatic cleaning nozzles 17, and the automatic cleaning nozzles 17 extend to the inner wall of the tank body 1. The tank body 1 is also provided with a cleaning pipe 18, and the cleaning pipe 18 is located in the shaft tube 3 close to the hot water pipe 11. The cleaning pipe 18 is connected to the two automatic cleaning nozzles 17.
[0031] The top cover 8 is provided with a cover-tightening handle 19 , and a hanging ear 20 is provided on one side of the top cover 8 , and the hanging ear 20 is fixedly connected to the tank body 1 .
[0032] A step ladder 21 is provided at one side of the bracket 2 , a platform 22 is provided at the upper end of the step ladder 21 , the hydraulic motor 12 is provided on the platform 22 , and a fence 23 is provided on the platform 22 .
[0033] The hydraulic motor 12 is on the same side as the hot water pipe 11 .
[0034] A retractable water receiving bucket 24 is provided at the lower part of the unloading butterfly valve 7 .
[0035] A water dividing plate 25 is provided inside the hot water pipe 11 , and the inner end of the water dividing plate 25 enters the interlayer 6 and is fixedly connected to the tank body 1 .
[0036] The jacket 5 is provided with an outer sheath 26 outside.
[0037] During the specific implementation of the utility model, the platform 22 is accessed from the step ladder 21, the top cover 8 is opened, the material is put into the tank body 1, the top cover 8 is closed, the ethanol vaporizer 14 and the hot water generator 15 are started, the hydraulic motor 12 is started to drive the tank body to rotate in one direction at a speed of 8-10 rpm, the vacuum pump is started to evacuate the gas inlet and outlet pipes 9 to the maximum limit and then the vacuum pump is turned off, the nitrogen bottle is connected to the gas inlet and outlet pipes 9, the valve is opened to fill nitrogen until the vacuum degree in the tank body 1 drops to 0 and then the vacuum pump is turned off, and then the vacuum pump is used to evacuate the tank body to the maximum limit from the gas inlet and outlet pipes 9 and then the vacuum pump is turned off. Start the ethanol vaporizer 14, hot water generator 15 and hydraulic motor 12, preheat for several minutes, inject ethanol through the ethanol vaporizer 14 until ethanol no longer enters, close the ethanol vaporizer 14, hot water generator 15 and hydraulic motor 12, let it stand for 1-2 hours, restart the hot water generator 15, vacuum pump and hydraulic motor 12, drive the tank body 1 to rotate in one direction at a speed of 8-10 rpm, and then keep hot water circulating in the interlayer 6. After running for 0.5-1 hour, close the hot water generator 15, vacuum pump and hydraulic motor 12, open the nitrogen valve to fill nitrogen until the pressure inside and outside the tank body 1 is balanced, then close it, open the top cover 8, and finally open the unloading butterfly valve 7 to unload the material. The titanium filter rod 16 is used to intake air into the tank body 1 and prevent the material from being discharged.
[0038] The water receiving bucket 24 is moved to the lower part of the discharge butterfly valve 7, the cleaning equipment connected to the cleaning pipe 18 is started, the automatic cleaning nozzle 17 cleans the inner wall of the tank body 1, and the water receiving bucket 24 discharges the sewage.
[0039] Practical application test results: Taking Huangzhizi as an example, after ethanol gas sterilization, the loss of gardenia glycoside content is less than 5%.
[0040] The above describes the utility model and its implementation methods, which is not restrictive. The drawings show only one implementation method of the utility model, and the actual structure is not limited thereto. In short, if ordinary technicians in this field are inspired by it and design structural methods and embodiments similar to the technical solution without creative design without departing from the purpose of the invention of the utility model, they should all fall within the protection scope of the utility model.
Claims
1. A pure ethanol gas sterilizer, characterized in that: The invention comprises a tank body (1) and a bracket (2), wherein the left and right ends of the tank body (1) are in a frustum shape, the shaft tubes (3) at the two ends of the tank body (1) are rotatably connected to the bearing seat (4) of the bracket (2), the outside of the tank body (1) is provided with a jacket (5), the jacket (5) and the tank body (1) form a closed interlayer (6), the lower end of the tank body (1) is provided with a discharge butterfly valve (7), and the upper end is provided with a top cover (8), the shaft tube (3) on one side of the tank body (1) is provided with a fixed gas inlet and outlet pipe (9) and a hot water return pipe (10), and the shaft tube (3) on the other side of the tank body (1) is provided with a hot water pipe (11); the gas inlet and outlet pipe (9) passes through the inside of the shaft tube (3), and three pipe openings are provided at the outer end, each of which is provided with a valve; the shaft tube (3) is a double-layer tube, and the hot water return pipe (10) and the hot water pipe (11) are both rotatably connected to the shaft tube (3); A hydraulic motor (12) is provided on an upper portion of one side of the bracket (2), and the hydraulic motor (12) is transmission-connected to a gear (13) of the shaft tube (3); It also includes an ethanol vaporizer (14) and a hot water generator (15); the ethanol vaporizer (14), the gas inlet and outlet pipes (9), and the titanium filter rod (16) in the tank body (1) are connected in sequence; and the hot water generator (15), the hot water pipe (11), the interlayer (6), and the hot water return pipe (10) are connected in sequence in a closed loop.
2. A pure ethanol gas sterilizer according to claim 1, characterized in that: The conical surfaces at both ends of the tank body (1) are provided with automatic cleaning nozzles (17), and the automatic cleaning nozzles (17) extend to the inner wall of the tank body (1). The tank body (1) is also provided with a cleaning pipe (18), and the cleaning pipe (18) is located in the shaft pipe (3) close to the hot water pipe (11), and the cleaning pipe (18) is connected to the two automatic cleaning nozzles (17).
3. A pure ethanol gas sterilizer according to claim 1, characterized in that: The top cover (8) is provided with a cover-tightening handle (19), and a hanging ear (20) is provided on one side of the top cover (8), and the hanging ear (20) is fixedly connected to the tank body (1).
4. A pure ethanol gas sterilizer according to claim 1, characterized in that: A step ladder (21) is provided on one side of the bracket (2), a platform (22) is provided at the upper end of the step ladder (21), the hydraulic motor (12) is arranged on the platform (22), and the platform (22) is provided with a fence (23).
5. A pure ethanol gas sterilizer according to claim 1 or 4, characterized in that: The hydraulic motor (12) is located on the same side as the hot water pipe (11).
6. A pure ethanol gas sterilizer according to claim 1 or 2, characterized in that: A retractable water receiving bucket (24) is provided at the lower part of the discharge butterfly valve (7).
7. A pure ethanol gas sterilizer according to claim 1, characterized in that: A water dividing plate (25) is provided at the inner end of the shaft tube (3) of the hot water pipe (11); the water dividing plate (25) enters the interlayer (6) and is fixedly connected to the tank body (1).
8. A pure ethanol gas sterilizer according to claim 1 or 7, characterized in that: The jacket (5) is provided with an outer sheath (26) outside.