Chemical transfer equipment capable of automatically adjusting PH

By arranging an insert PH detection probe at the top of the transfer tank of the chemical transfer equipment and combining with an efficient heat exchange device, the automatic adjustment of the PH value in the transfer tank is achieved, the problem of PH detection error in existing equipment is solved, and the stability of the equipment is improved Sex and safety.

CN222489997UActive Publication Date: 2025-02-18SHENYANG DONGRUI FINE CHEM CO LTD
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Patent Information

Application Number
CN202323617035.3
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2023-12-29
Publication Date
2025-02-18
Estimated Expiration
2033-12-29

AI Technical Summary

Technical Problem

Due to the exothermic effect during the sulfuric acid dilution process, existing chemical transit equipment leads to errors in the detection results of the PH detection equipment, making it difficult to effectively monitor and adjust the PH value in the transit tank, thereby affecting the safety and stability of the equipment.

Method used

A chemical transfer equipment that can automatically adjust PH is designed. By arranging an insert PH detection probe at the top of the transfer tank, combined with a cooling and heat exchange device with efficient heat exchange, the PH value in the transfer tank is monitored in real time and adjusted according to the PH value. The feed amount of concentrated sulfuric acid and the flow rate of diluted water can prevent the PH detection probe from working unstable due to heat exothermic.

Benefits of technology

Accurate monitoring and automatic adjustment of the PH value in the transfer tank of chemical transit equipment is achieved, avoiding equipment damage and safety hazards caused by fluctuations in PH value, and improving the stability and safety of the equipment.

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Abstract

The utility model discloses chemical engineering transfer equipment capable of automatically adjusting PH, which comprises a transfer tank, the transfer tank is a kettle body with a cavity structure, the top end and the bottom end of the transfer tank are respectively provided with a feeding port and a discharging port, the feeding port is connected with a feeding pipe through a connector, the discharging port is connected with an acid discharge pump through a discharging pipe, and the acid discharge pump is connected with an acid storage tank. A concentrated sulfuric acid feeding pipe is arranged on the transfer tank, and a water supply pipe is connected to the transfer tank; the utility model relates to the technical field of chemical transfer equipment, in particular to chemical transfer equipment capable of automatically adjusting PH, which is characterized in that a plug-in PH detection probe is arranged at the top end of a transfer tank, the PH detection probe is used for detecting the PH of a mixed solution in the transfer tank, and the feeding amount of concentrated sulfuric acid and the flow of dilution water are adjusted according to the PH value; meanwhile, the cooling heat exchange device capable of efficiently exchanging heat is wrapped outside the PH probe, so that heat generated by dilution of concentrated sulfuric acid is taken away, and the PH detection probe works in a reasonable temperature interval.
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Description

Technical Field

[0001] The utility model relates to the technical field of chemical transfer equipment, in particular to chemical transfer equipment capable of automatically adjusting pH. Background Art

[0002] In modern chemical equipment, transfer tanks are a type of equipment that is often used to prepare sulfuric acid. The diluted concentrated sulfuric acid needs to be mixed in the transfer tank before being discharged. Due to the small size of the transfer tank, the liquid level in the transfer tank needs to be controlled. If the transfer tank is too full, the acid will overflow and endanger the environment; emptying the transfer tank will cause the acid discharge pump to run idle, causing equipment damage; and since a large amount of heat will be generated during the dilution of concentrated sulfuric acid, the pH value of the transfer equipment needs to be monitored and adjusted in real time to avoid dilution too quickly, causing the dilution liquid to boil and causing equipment damage. Existing transfer equipment usually uses pH detection equipment to detect the internal pH, but due to the exothermic effect during the dilution of sulfuric acid, it is easy to cause errors in the detection results of the pH detection equipment. In view of this, in-depth research was conducted on the above-mentioned issues, resulting in this case. Utility Model Content

[0003] In view of the deficiencies of the prior art, the utility model provides a chemical transfer device capable of automatically adjusting pH, thereby solving the problems of the prior art.

[0004] To achieve the above purpose, the utility model is implemented through the following technical solutions: a chemical transfer equipment capable of automatically adjusting pH, comprising a transfer tank, the transfer tank being a kettle body with a cavity structure, the top and bottom of the transfer tank being respectively provided with a feed port and a feed port, the feed port being connected with a feed pipe through a joint, the feed port being connected with an acid discharge pump through a feed pipe, the transfer tank being provided with a concentrated sulfuric acid feeding pipe, and the transfer tank being connected with a water supply pipe;

[0005] The concentrated sulfuric acid feeding pipe and the water supply pipe are respectively connected with a pair of control valves;

[0006] The top surface of the transfer tank is provided with an insertion slot, a limit seat is inserted in the insertion slot, a detection rod is connected to the bottom of the limit seat, a PH detection probe is provided at the bottom of the detection rod, and the main body of the PH detection probe is wrapped at the bottom of the detection rod with only the head end exposed outside;

[0007] A cooling water inlet pipe and a cooling water outlet pipe are symmetrically arranged on both sides of the detection rod. The ends of the cooling water inlet pipe and the cooling water outlet pipe are connected to a heat exchange cooling sleeve groove with an annular structure. The heat exchange cooling sleeve groove is wrapped around the outside of the main body of the PH detection probe.

[0008] Preferably, a water inlet joint and a water outlet joint are provided at the ends of the cooling water inlet pipe and the cooling water outlet pipe.

[0009] Preferably, the cooling water inlet pipe and the cooling water outlet pipe are both cylindrical through grooves connected to the heat exchange cooling jacket groove.

[0010] Preferably, a plurality of heat exchange fins are arranged in a ring array outside the main body of the PH detection probe, and the heat exchange cooling jacket groove is sleeved on the heat exchange fins.

[0011] Preferably, the limiting seat is a plate with a partially conical structure and a polygonal cross-section, and the insertion groove matches the limiting seat structure.

[0012] Preferably, a transmission wiring seat connected to the detection rod is provided on the limit seat.

[0013] Beneficial Effects

[0014] The utility model provides a chemical transfer equipment capable of automatically adjusting pH. The utility model has the following beneficial effects: the chemical transfer equipment capable of automatically adjusting pH, by arranging an inserted pH detection probe at the top of the transfer tank, uses the pH detection probe to detect the pH of the mixed liquid in the transfer tank, adjusts the feed amount of concentrated sulfuric acid and the flow rate of dilution water according to the pH value, and at the same time, a high-efficiency heat exchange cooling device is wrapped outside the pH probe to take away the heat generated by the dilution of concentrated sulfuric acid, so that the pH detection probe works in a reasonable temperature range. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] Figure 1 This is a schematic diagram of the main structure of a chemical transfer equipment capable of automatically adjusting pH described in the utility model.

[0016] Figure 2 The utility model is a partial cross-sectional structural schematic diagram of a chemical transfer equipment capable of automatically adjusting pH.

[0017] Figure 3 This is a partial axonometric structural diagram of a chemical transfer equipment capable of automatically adjusting pH described in the utility model.

[0018] Figure 4 It is a partial enlarged structural schematic diagram of a chemical transfer equipment capable of automatically adjusting pH described in the utility model.

[0019] In the figure: 1. Transfer tank; 2. Loading port; 3. Discharging port; 4. Acid discharge pump; 5. Concentrated sulfuric acid feeding pipe; 6. Water supply pipe; 7. Control valve; 8. Limit seat; 9. Detection rod; 10. PH detection probe; 11. Cooling water inlet pipe; 12. Cooling water outlet pipe; 13. Heat exchange cooling jacket groove; 14. Heat exchange plate; 15. Transmission terminal block. DETAILED DESCRIPTION

[0020] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0021] See also Figure 1-4 The utility model provides an implementation scheme: in the application process of the transfer tank 1, in order to avoid the boiling of sulfuric acid caused by the excessive dilution rate of sulfuric acid, thereby endangering the safety of equipment and personnel, the transfer tank 1 at this stage needs to monitor the pH in the transfer tank 1 in addition to the liquid level. The present application discloses a chemical transfer equipment that can automatically adjust the pH. The equipment is based on the transfer tank 1. The transfer tank 1 is a kettle body with a cavity structure. The top and bottom of the transfer tank 1 are respectively provided with a feeding port 2 and a feeding port 3. The feed port 2 is connected to a feed pipe through a joint, and additives are added into the transfer tank 1 through the feed pipe. The feed port 3 is connected to an acid discharge pump 4 through a feed pipe for discharging diluted sulfuric acid. The transfer tank 1 is provided with a concentrated sulfuric acid feeding pipe 5, and concentrated sulfuric acid is injected into the transfer tank 1 through the concentrated sulfuric acid feeding pipe 5. Dilution water is injected through a water supply pipe 6 to complete the dilution of the concentrated sulfuric acid. A pair of control valves 7 are respectively connected to the concentrated sulfuric acid feeding pipe 5 and the water supply pipe 6. The control valve 7 is electrically connected to the detection device to control the feed rates of the two.

[0022] According to the instruction manual Figure 1-3 It can be seen that an insertion slot is provided on the top surface of the transfer tank 1, and a limit seat 8 is inserted in the insertion slot. The insertion slot is used to limit the limit seat 8 to fix the posture of the detection rod 9. The detection rod 9 is used to extend the PH detection probe 10 into the mixed liquid. The bottom end of the detection rod 9 is provided with a PH detection probe 10. The main body of the PH detection probe 10 is wrapped at the bottom of the detection rod 9, and only the head end is exposed to the outside. The head end of the PH detection probe 10 contacts the mixed liquid to monitor the PH value of the mixed liquid in real time. At the same time, a heat exchange cooling jacket groove 13 is wrapped on the outside of the PH detection probe 10. Water is supplied to the heat exchange cooling jacket groove 13 through the cooling water inlet pipe 11. The running water is used to absorb the heat released by the PH detection probe 10 due to the dilution of concentrated sulfuric acid, and then discharged from the cooling water outlet pipe 12, so as to keep the PH detection probe 10 working in a reasonable temperature range.

[0023] As a preferred solution, further, water inlet joints and water outlet joints are provided at the ends of the cooling water inlet pipe 11 and the cooling water outlet pipe 12 to facilitate connection with the external water supply pipe 6 .

[0024] As a preferred solution, further, the cooling water inlet pipe 11 and the cooling water outlet pipe 12 are both cylindrical through grooves connected to the heat exchange cooling jacket groove 13, and the cylindrical through groove structure facilitates the circulation of water.

[0025] As a preferred solution, further, a plurality of heat exchange fins 14 are arranged in a circular array outside the main body of the PH detection probe 10 , and the heat exchange cooling sleeve groove 13 is sleeved on the heat exchange fins 14 to improve the heat exchange efficiency of the PH detection probe 10 .

[0026] As a preferred solution, further, the limit seat 8 is a plate with a partially conical structure of a polygonal cross-section, and the insertion slot is structurally matched with the limit seat 8. Through the structural matching of the insertion slot and the limit seat 8, the axial limitation of the limit seat 8 is achieved to prevent the detection rod 9 from rolling.

[0027] As a preferred solution, further, a transmission connection seat 15 is provided on the limit seat 8 and is connected to the detection rod 9 for receiving the detection data of the pH detection probe 10.

[0028] From the above, it can be generally known that the chemical transfer equipment that can automatically adjust the pH value arranges an inserted pH detection probe 10 at the top of the transfer tank 1, uses the pH detection probe 10 to detect the pH of the mixed liquid in the transfer tank 1, and adjusts the feed amount of concentrated sulfuric acid and the flow rate of dilution water according to the pH value. At the same time, a high-efficiency heat exchange cooling device is wrapped outside the pH probe to take away the heat generated by the dilution of concentrated sulfuric acid, so that the pH detection probe 10 works in a reasonable temperature range.

[0029] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A chemical transfer equipment capable of automatically adjusting pH, comprising a transfer tank (1), wherein the transfer tank (1) is a kettle body with a cavity structure, wherein a feeding port (2) and a feeding port (3) are respectively arranged at the top and bottom of the transfer tank (1), wherein the feeding port (2) is connected to a feeding pipe via a joint, and the feeding port (3) is connected to an acid discharge pump (4) via a feeding pipe, wherein: The transfer tank (1) is provided with a concentrated sulfuric acid feeding pipe (5), and the transfer tank (1) is connected with a water supply pipe (6); The concentrated sulfuric acid feeding pipe (5) and the water supply pipe (6) are respectively connected to a pair of control valves (7); The top surface of the transfer tank (1) is provided with an insertion slot, a limit seat (8) is inserted in the insertion slot, a detection rod (9) is connected to the bottom of the limit seat (8), a pH detection probe (10) is provided at the bottom end of the detection rod (9), and the main body of the pH detection probe (10) is wrapped at the bottom of the detection rod (9) with only the head end exposed outside; A cooling water inlet pipe (11) and a cooling water outlet pipe (12) are symmetrically arranged on both sides of the detection rod (9); the ends of the cooling water inlet pipe (11) and the cooling water outlet pipe (12) are connected to a heat exchange cooling sleeve groove (13) with an annular structure; and the heat exchange cooling sleeve groove (13) is wrapped around the outside of the main body of the pH detection probe (10).

2. A chemical transfer equipment capable of automatically adjusting pH according to claim 1, characterized in that: A water inlet joint and a water outlet joint are provided at the ends of the cooling water inlet pipe (11) and the cooling water outlet pipe (12).

3. A chemical transfer equipment capable of automatically adjusting pH according to claim 2, characterized in that: The cooling water inlet pipe (11) and the cooling water outlet pipe (12) are both cylindrical through grooves connected to the heat exchange cooling jacket groove (13).

4. A chemical transfer equipment capable of automatically adjusting pH according to claim 3, characterized in that: A plurality of heat exchange fins (14) are arranged in a ring array outside the main body of the PH detection probe (10), and the heat exchange cooling jacket groove (13) is sleeved on the heat exchange fins (14).

5. A chemical transfer equipment capable of automatically adjusting pH according to claim 4, characterized in that: The limiting seat (8) is a plate with a partially conical structure and a polygonal cross-section, and the insertion groove matches the limiting seat (8) structure.

6. The chemical transfer equipment capable of automatically adjusting pH according to claim 5, characterized in that: The limit seat (8) is provided with a transmission connection seat (15) connected to the detection rod (9).