Distillation device for producing high-softening-point resin
By designing a distillation device including stirring and scraper, the problem of difficulty in vacuuming and cleaning of raw materials during distillation is solved, efficient distillation and condensation are achieved, and the softening point of the resin is improved and Overall efficiency.
Patent Information
- Application Number
- CN202420000872.7
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-01-02
- Publication Date
- 2025-02-25
- Estimated Expiration
- 2034-01-02
AI Technical Summary
The existing distillation device used for the production of high softening point resin cannot effectively vacuum during the distillation process, which affects the distillation effect. The raw materials are prone to adhere to the inner wall of the kettle during stirring, making it difficult to clean.
A distillation device including a steam generating unit, a distillation stirring unit, a condensing unit and a collection unit is designed. The stirring is carried out through a stirring shaft and a stirring rod, and the distillation is accelerated, and the raw materials adhered to the inner wall of the distillation tank are scraped through a scraper. At the same time, the condenser and the circulation tube are combined for double cooling to increase the condensation speed.
It improves the distillation effect, can more effectively remove low-molecular materials, improves the softening point of the resin, and at the same time, the condensation speed is accelerated through double-layer cooling, improves the overall distillation efficiency, and simplifies the post-cleaning process.
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Figure CN222517748U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of high softening point resin production, in particular to a distillation device for high softening point resin production. Background Art
[0002] Terpene resin is a general term for polymers obtained by cationic polymerization using terpene compounds as raw materials. It is a type of yellow to light yellow, transparent or translucent solid. Generally, the terpene resin includes terpene resin, α-pinene resin, β-pinene resin, dipentene resin, etc.
[0003] It is very difficult to obtain high softening point resin at present. This is because only by increasing the vacuum degree can low molecules on the surface of the material be extracted, and low molecules at the bottom of the material are difficult to distill out.
[0004] As disclosed in Chinese patent CN213285708U, a distillation device for producing high softening point resin includes a distillation kettle, a steam generator, a condenser, a receiving cylinder and a vacuum unit. The distillation kettle includes a kettle body and a top cover arranged on the kettle body. The bottom of the kettle body is provided with an annular steam pipeline, and a plurality of through holes are provided on the annular steam pipeline. The steam generator is connected with the annular steam pipeline through a longitudinal steam pipeline. A low molecular weight material discharge port is provided on the top cover, and the low molecular weight material discharge port is connected with the receiving cylinder through the condenser. The receiving cylinder is also connected with a vacuum unit. The utility model introduces high temperature and high pressure steam into the annular steam pipeline, and the high temperature and high pressure steam evaporates rapidly in the distillation kettle and is discharged upward from the through hole of the annular steam pipeline. On the one hand, it replaces the stirring paddle in the traditional distillation kettle; on the other hand, it enables the low molecular weight material below the kettle to be distilled out with the high pressure steam to obtain a resin product with a high softening point.
[0005] However, the distillation device for producing high softening point resin does not directly evacuate the distillation kettle, which affects the distillation effect. In addition, when stirring in the distillation kettle, raw materials will adhere to the inner wall of the kettle, which will be troublesome to clean if not removed in time.
[0006] Therefore, we proposed a distillation device for high softening point resin production to solve the above problems. Utility Model Content
[0007] The purpose of the utility model is to provide a distillation device for producing high softening point resins to solve the problems raised in the above background technology.
[0008] To achieve the above object, the utility model provides the following technical solution: a distillation device for high softening point resin production, comprising an operating table and a support column, wherein the support column is fixedly installed at the four corners of the bottom surface of the operating table, a support base is fixedly installed on the bottom surface of the support column, and a distillation device is arranged on the upper surface of the operating table;
[0009] The distillation device includes a steam generating unit, a distillation stirring unit, a condensing unit and a collecting unit. The steam generating unit includes a steam generator and a steam conveying pipe. The steam generator is fixedly installed on one side of the upper surface of the operating table, and the steam conveying pipe is fixedly installed on the upper surface of the steam generator.
[0010] Preferably, the distillation stirring unit includes a stirring module and a heating module, the stirring module includes a cover plate, a fixed rod, a driving motor, a stirring shaft, a bearing, a stirring rod, a connecting rod and a scraper, the cover plate is arranged above the operating table, the fixed rod is fixedly installed on the upper surface of the cover plate, the driving motor is fixedly installed on the upper surface of the fixed rod, the stirring shaft is fixedly installed on the output end of the driving motor, the bearing is fixedly installed on the outer surface of the stirring shaft, the stirring rod is fixedly installed on the outer surface of the stirring shaft, the connecting rod is fixedly installed on the outer surface of the stirring shaft, and the scraper is fixedly installed on the side of one end of the connecting rod.
[0011] Preferably, the heating module includes a distillation tank, a heating layer, a protective layer, a power box, a vacuum pump and an exhaust pipe. The distillation tank is fixedly installed on the upper surface of the operating table, the bottom surface of the cover plate is fixedly connected to the upper surface of the distillation tank, the heating layer is fixedly installed on the outer surface of the distillation tank, the protective layer is fixedly installed on the outer surface of the heating layer, the power box is fixedly installed on the bottom surface of the operating table, the power box and the heating layer are electrically connected, the vacuum pump is fixedly installed on the upper surface of the operating table, and the exhaust pipe is fixedly installed on the upper surface of the vacuum pump.
[0012] Preferably, the condensing unit includes a connecting pipe, a condenser, a water tank, a water inlet pipe and a circulating pipe. The connecting pipe is fixedly installed on the upper surface of the cover plate, the condenser is fixedly installed on the surface of one end of the connecting pipe, the water tank is fixedly installed on the upper surface of the operating table, the water inlet pipe is fixedly installed on the upper surface of the water tank, the circulating pipe is fixedly installed on the outer surface of the condenser, and both ends of the circulating pipe are fixedly connected to the water tank.
[0013] Preferably, the collecting unit comprises a collecting tube and a collecting box, the collecting tube is fixedly mounted on the bottom surface of the condenser, the collecting box is fixedly mounted on the upper surface of the operating table, and the side surface of one end of the collecting tube is fixedly connected to the side surface of the collecting box.
[0014] Preferably, a discharge pipe is fixedly installed on the bottom surface of the operating table, a connecting flange is fixedly installed on the outer surface of the discharge pipe, a valve body is fixedly installed on the bottom surface of the connecting flange, a valve stem is fixedly installed on the inner wall of the valve body, a valve lever is fixedly installed on the outer surface of the valve stem, and a handle is fixedly installed on the side of one end of the valve stem.
[0015] Preferably, three holes are passed through the upper surface of the cover plate, and the three holes are fixedly connected to the steam delivery pipe, the exhaust pipe and the connecting pipe respectively, and the side surface of one end of the scraper is in contact with the inner wall of the distillation tank.
[0016] Compared with the prior art, the beneficial effects of the utility model are:
[0017] 1. The distillation device for the production of high softening point resin can rotate and stir the raw materials during distillation by arranging a stirring shaft and a stirring rod to accelerate distillation and improve the distillation effect. At the same time, the connecting rod drives the scraper to rotate and scrape the raw materials attached to the inner wall of the distillation tank to facilitate better participation in distillation.
[0018] 2. The distillation device for the production of high softening point resin is provided with a condenser, and a circulation pipe is fixedly installed on the outer surface of the condenser. Both ends of the circulation pipe are connected to a water tank. Water can be supplied through the water tank so that the circulation pipe can cool the condenser, and the cooling function of the condenser itself can be used for double-layer cooling, so that the condensation speed is improved. BRIEF DESCRIPTION OF THE DRAWINGS
[0019] Figure 1 This is a schematic diagram of the main structure of the utility model;
[0020] Figure 2 for Figure 1 A schematic diagram of the local enlarged structure at point A in the middle;
[0021] Figure 3 This is a schematic diagram of the stirring mechanism structure of the utility model;
[0022] Figure 4 It is a schematic diagram of the bottom structure of the utility model.
[0023] In the figure: 1. operating table; 2. supporting column; 201. supporting base; 3. distillation tank; 301. heating layer; 302. protective layer; 303. power box; 304. cover plate; 305. fixing rod; 306. driving motor; 307. stirring shaft; 308. bearing; 309. stirring rod; 310. connecting rod; 311. scraper; 312. steam generator; 313. steam delivery pipe; 314. vacuum pump; 315. exhaust pipe; 316. connecting pipe; 317. condenser; 318. collecting pipe; 319. collecting box; 320. water tank; 321. water inlet pipe; 322. circulation pipe; 323. discharge pipe; 324. connecting flange; 325. valve body; 326. valve stem; 327. valve lever; 328. handle. DETAILED DESCRIPTION
[0024] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.
[0025] See also Figure 1-Figure 4 , the utility model provides a technical solution:
[0026] Embodiment 1: A distillation device for producing high softening point resin, comprising an operating table 1 and a support column 2, wherein the support column 2 is fixedly mounted at the four corners of the bottom surface of the operating table 1, a support base 201 is fixedly mounted on the bottom surface of the support column 2, and a distillation device is arranged on the upper surface of the operating table 1;
[0027] The distillation device includes a steam generating unit, a distillation stirring unit, a condensing unit and a collecting unit. The steam generating unit includes a steam generator 312 and a steam delivery pipe 313. The steam generator 312 is fixedly installed on one side of the upper surface of the operating table 1, and the steam delivery pipe 313 is fixedly installed on the upper surface of the steam generator 312.
[0028] The distillation stirring unit includes a stirring module and a heating module. The stirring module includes a cover plate 304, a fixed rod 305, a driving motor 306, a stirring shaft 307, a bearing 308, a stirring rod 309, a connecting rod 310 and a scraper 311. The cover plate 304 is arranged above the operating table 1, the fixed rod 305 is fixedly installed on the upper surface of the cover plate 304, the driving motor 306 is fixedly installed on the upper surface of the fixed rod 305, the stirring shaft 307 is fixedly installed on the output end of the driving motor 306, the bearing 308 is fixedly installed on the outer surface of the stirring shaft 307, the stirring rod 309 is fixedly installed on the outer surface of the stirring shaft 307, the connecting rod 310 is fixedly installed on the outer surface of the stirring shaft 307, and the scraper 311 is fixedly installed on the side of one end of the connecting rod 310. By arranging the stirring shaft 307 and the stirring rod 309, the raw materials can be rotated to stir during distillation to accelerate distillation and improve the distillation effect. At the same time, the connecting rod 310 drives the scraper 311 to rotate to scrape the raw materials attached to the inner wall of the distillation tank 3 for better participation in distillation.
[0029] The heating module includes a distillation tank 3, a heating layer 301, a protective layer 302, a power box 303, a vacuum pump 314 and an exhaust pipe 315. The distillation tank 3 is fixedly installed on the upper surface of the operating table 1, the bottom surface of the cover plate 304 is fixedly connected to the upper surface of the distillation tank 3, the heating layer 301 is fixedly installed on the outer surface of the distillation tank 3, the protective layer 302 is fixedly installed on the outer surface of the heating layer 301, the power box 303 is fixedly installed on the bottom surface of the operating table 1, the power box 303 and the heating layer 301 are electrically connected, the vacuum pump 314 is fixedly installed on the upper surface of the operating table 1, and the exhaust pipe 315 is fixedly installed on the upper surface of the vacuum pump 314.
[0030] The power box 303 supplies power to the heating layer 301 to heat the distillation tank 3. At the same time, the vacuum pump 314 is started to evacuate the inside of the distillation tank 3 through the exhaust pipe 315. The steam generator 312 inputs steam into the distillation tank 3 through the steam delivery pipe 313. The stirring shaft 307 drives the stirring rod 309 to rotate to stir the raw materials for better reaction. At the same time, the connecting rod 310 drives the scraper 311 to rotate to scrape off the raw materials adhering to the inner wall of the distillation tank 3.
[0031] Embodiment 2: Based on embodiment 1, the condensing unit includes a connecting pipe 316, a condenser 317, a water tank 320, a water inlet pipe 321 and a circulation pipe 322. The connecting pipe 316 is fixedly mounted on the upper surface of the cover plate 304, the condenser 317 is fixedly mounted on one end surface of the connecting pipe 316, the water tank 320 is fixedly mounted on the upper surface of the operating table 1, the water inlet pipe 321 is fixedly mounted on the upper surface of the water tank 320, the circulation pipe 322 is fixedly mounted on the outer surface of the condenser 317, and both ends of the circulation pipe 322 are fixedly connected to the water tank 320. By setting the condenser 317, A circulation pipe 322 is fixedly installed on the outer surface of the condenser 317. Both ends of the circulation pipe 322 are connected to the water tank 320. The water tank 320 can supply water so that the circulation pipe 322 can cool the condenser 317. The cooling function of the condenser 317 itself is used to perform double-layer cooling so that the condensation speed is improved. The collection unit includes a collection pipe 318 and a collection box 319. The collection pipe 318 is fixedly installed on the bottom surface of the condenser 317, and the collection box 319 is fixedly installed on the upper surface of the operating table 1. The side surface of one end of the collection pipe 318 is fixedly connected to the side surface of the collection box 319.
[0032] A discharge pipe 323 is fixedly installed on the bottom surface of the operating table 1, a connecting flange 324 is fixedly installed on the outer surface of the discharge pipe 323, a valve body 325 is fixedly installed on the bottom surface of the connecting flange 324, a valve stem 326 is fixedly installed on the inner wall of the valve body 325, a valve lever 327 is fixedly installed on the outer surface of the valve stem 326, a handle 328 is fixedly installed on the side of one end of the valve stem 326, three holes are passed through the upper surface of the cover plate 304, and the three holes are respectively fixedly connected to the steam delivery pipe 313, the exhaust pipe 315 and the connecting pipe 316, and one end of the scraper 311 is in contact with the inner wall of the distillation tank 3.
[0033] The steam after distillation is poured into the condenser 317 through the connecting pipe 316. The condenser 317 condenses the steam through its own upper and lower ports. At the same time, the water tank 320 is filled with water through the water inlet pipe 321 and then sent to the circulation pipe 322. The circulation pipe 322 is wrapped around the outer surface of the condenser 317 to accelerate the condensation of the steam.
[0034] It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variants thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device. In the absence of further restrictions, the elements defined by the statement "comprise a ..." do not exclude the presence of other identical elements in the process, method, article or device including the elements.
Claims
1. A distillation device for producing a high softening point resin, comprising an operating table (1) and a support column (2), wherein the support column (2) is fixedly mounted at the four corners of the bottom surface of the operating table (1), and a support base (201) is fixedly mounted on the bottom surface of the support column (2), characterized in that: The upper surface of the operating table (1) is provided with a distillation device; The distillation device comprises a steam generating unit, a distillation stirring unit, a condensing unit and a collecting unit; the steam generating unit comprises a steam generator (312) and a steam conveying pipe (313); the steam generator (312) is fixedly mounted on one side of the upper surface of the operating table (1); and the steam conveying pipe (313) is fixedly mounted on the upper surface of the steam generator (312).
2. A distillation apparatus for producing high softening point resin according to claim 1, characterized in that: The distillation stirring unit comprises a stirring module and a heating module, wherein the stirring module comprises a cover plate (304), a fixed rod (305), a driving motor (306), a stirring shaft (307), a bearing (308), a stirring rod (309), a connecting rod (310) and a scraper (311), wherein the cover plate (304) is arranged above the operating table (1), the fixed rod (305) is fixedly mounted on the upper surface of the cover plate (304), the driving motor (306) is fixedly mounted on the upper surface of the fixed rod (305), the stirring shaft (307) is fixedly mounted on the output end of the driving motor (306), the bearing (308) is fixedly mounted on the outer surface of the stirring shaft (307), the stirring rod (309) is fixedly mounted on the outer surface of the stirring shaft (307), the connecting rod (310) is fixedly mounted on the outer surface of the stirring shaft (307), and the scraper (311) is fixedly mounted on the side surface of one end of the connecting rod (310).
3. A distillation apparatus for producing high softening point resin according to claim 2, characterized in that: The heating module comprises a distillation tank (3), a heating layer (301), a protective layer (302), a power supply box (303), a vacuum extractor (314) and an exhaust pipe (315); the distillation tank (3) is fixedly mounted on the upper surface of the operating table (1); the bottom surface of the cover plate (304) is fixedly connected to the upper surface of the distillation tank (3); the heating layer (301) is fixedly mounted on the outer surface of the distillation tank (3); the protective layer (302) is fixedly mounted on the outer surface of the heating layer (301); the power supply box (303) is fixedly mounted on the bottom surface of the operating table (1); the power supply box (303) and the heating layer (301) are electrically connected; the vacuum extractor (314) is fixedly mounted on the upper surface of the operating table (1); and the exhaust pipe (315) is fixedly mounted on the upper surface of the vacuum extractor (314).
4. A distillation apparatus for producing high softening point resin according to claim 1, characterized in that: The condensing unit comprises a connecting pipe (316), a condenser (317), a water tank (320), a water inlet pipe (321) and a circulation pipe (322); the connecting pipe (316) is fixedly mounted on the upper surface of the cover plate (304); the condenser (317) is fixedly mounted on the surface of one end of the connecting pipe (316); the water tank (320) is fixedly mounted on the upper surface of the operating table (1); the water inlet pipe (321) is fixedly mounted on the upper surface of the water tank (320); the circulation pipe (322) is fixedly mounted on the outer surface of the condenser (317); and both ends of the circulation pipe (322) are fixedly connected to the water tank (320).
5. The distillation device for producing high softening point resin according to claim 1, characterized in that: The collection unit comprises a collection tube (318) and a collection box (319); the collection tube (318) is fixedly mounted on the bottom surface of the condenser (317); the collection box (319) is fixedly mounted on the upper surface of the operating table (1); and a side surface of one end of the collection tube (318) is fixedly connected to a side surface of the collection box (319).
6. A distillation apparatus for producing high softening point resin according to claim 1, characterized in that: A discharge pipe (323) is fixedly mounted on the bottom surface of the operating table (1); a connecting flange (324) is fixedly mounted on the outer surface of the discharge pipe (323); a valve body (325) is fixedly mounted on the bottom surface of the connecting flange (324); a valve stem (326) is fixedly mounted on the inner wall of the valve body (325); a valve lever (327) is fixedly mounted on the outer surface of the valve stem (326); and a handle (328) is fixedly mounted on the side surface of one end of the valve stem (326).
7. A distillation apparatus for producing high softening point resin according to claim 2, characterized in that: The upper surface of the cover plate (304) is penetrated by three holes, and the three holes are respectively fixedly connected to the steam delivery pipe (313), the exhaust pipe (315) and the connecting pipe (316), and the side surface of one end of the scraper (311) is in contact with the inner wall of the distillation tank (3).
Citation Information
Patent Citations
Distillation device for producing high-softening-point resin
CN213285708U