Cholic acid purification device

Abstract

The utility model relates to the technical field of cholic acid purification, in particular to a cholic acid purification device which comprises a bottom plate, a centrifugal device fixedly connected to the top of the bottom plate through a second fixing rod, a first filtering box body fixedly connected to the top of the bottom plate through a first fixing rod, and a second filtering box body fixedly connected to the first filtering box body through a fifth fixing rod. The second filtering box body is fixedly connected with a distillation box body through a fourth fixing rod, the distillation box body is fixedly connected with a condensation recovery box body through a condensation pipe, a stirring barrel is fixedly installed at the top of the first filtering box body, a bile feeding port and an ethanol feeding port are formed in the top of the stirring barrel, and a first telescopic rod stretches out and draws back to drive a first long strip to move. Filtering of the bile and ethanol mixed solution is accelerated, the ethanol and cholic acid mixed solution generated by the first filtering box body, the second filtering box body and the condensation recycling box body is centrifugally layered, the centrifugally layered liquid flows into the drying box to dry the ethanol solution, and finally cholic acid is obtained.

Description

Technical Field

[0001] The utility model relates to the technical field of bile acid purification, in particular to a bile acid purification device. Background Art

[0002] Bile acid extraction, bile acid exists in the bile of cattle, sheep, and pigs; bile acid is a monohydrate in the form of white flaky crystals, and bile acid is synthesized by the liver and discharged into the duodenum with bile. As one of the components of digestive juice, it can promote the digestion and absorption of lipid substances. Bile acid is only slightly soluble in water, and direct baking to extract bile acid will contain many impurities, but bile acid is soluble in ethanol solution, so ethanol extraction can improve the extraction rate and purity of bile acid.

[0003] A purification device for bile acid purification, whose official account authorized by China is CN 216093076 U, is used in conjunction with the components of a first cleaning mechanism to clean blood and other body fluids on bile acid; by setting the above-mentioned second cleaning mechanism, the quality of bile acid cleaning is guaranteed to a certain extent, thereby improving the quality and efficiency of bile acid purification.

[0004] However, this patent still has certain shortcomings when used. Although this patent removes surface foreign matter during the extraction process, it still contains impurities inside. Although the extraction process can be achieved, the purity of the extracted bile acid is not high, and bile acid is slightly soluble in water, but not completely insoluble in water. Therefore, the waste liquid generated during the cleaning process will also contain a small amount of bile acid. Moreover, when transferring the cleaned bile to another box, this patent uses the slope of the filter membrane to drive the bile to slide downward. In this process, the bile may adhere to the filter membrane and cannot flow normally, which will affect the extraction rate of bile acid and cause loss. Utility Model Content

[0005] The purpose of the utility model is to provide a bile acid purification device to solve the problems raised in the above background technology.

[0006] In order to achieve the above purpose, the utility model provides the following technical solutions:

[0007] A bile acid purification device comprises a bottom plate, wherein the bottom of the bottom plate is respectively fixedly connected with a support frame and a support box, the top of the bottom plate is respectively fixedly connected with a first fixing rod, a second fixing rod and a third fixing rod, the top of the first fixing rod is fixedly connected with a first filter box, the top of the first filter box is fixedly connected with a stirring barrel, the top of the stirring barrel is respectively provided with a bile inlet and an ethanol inlet, the first filter box is fixedly connected with a second filter box through a fifth fixing rod, a first connecting pipe is fixedly connected between the first filter box and the second filter box, and the top of the second filter box is fixedly connected with an ethanol storage The ethanol storage box is fixedly connected to an automatic sprayer at the bottom, the side of the second filter box is fixedly connected to a fourth fixing rod, the side of the fourth fixing rod is fixedly connected to a distillation box, the top of the bottom plate is fixedly connected to the distillation box through a third fixing rod, a second connecting pipe is fixedly connected between the second filter box and the distillation box, the top of the distillation box is fixedly connected to a condenser, the bottom of the condenser is fixedly connected to a condensation recovery box, the top of the second fixing rod is fixedly connected to a centrifugal box, the bottom of the centrifugal box is fixedly connected to a drying box, and the side of the drying box is movably connected to a box door.

[0008] As a preferred solution of the utility model, both sides of the first filter box are movably connected with a first vibrator, the sides of the first vibrator are fixedly connected with a first filter net, and both sides of the second filter box are movably connected with a second vibrator, and the sides of the second vibrator are fixedly connected with a second filter net.

[0009] As a preferred solution of the utility model, the side of the first filter box is movably connected to a first telescopic rod, the side of the first telescopic rod is fixedly connected to a first long strip, the side of the second filter box is movably connected to a second telescopic rod, and the side of the second telescopic rod is fixedly connected to a second long strip.

[0010] As a preferred solution of the utility model, a first motor is installed on the top of the stirring barrel, a stirring rod is fixedly connected to the output end of the first motor, and a stirring fan blade is fixedly connected to the side of the stirring rod.

[0011] As a preferred solution of the utility model, a distillation heating plate is fixedly connected to the center of the distillation box, and the surface of the distillation heating plate has raised bumps.

[0012] As a preferred solution of the utility model, a support box is fixedly connected to the bottom of the centrifugal box body, a second motor is placed in the support box, an output end of the second motor is fixedly connected to a rotating rod, and a centrifugal bucket is fixedly connected to the top of the rotating rod.

[0013] As a preferred solution of the utility model, the surface of the centrifugal bucket is provided with small holes of equal diameter and evenly distributed, and the centrifugal bucket and the rotating rod are both made of stainless steel.

[0014] As a preferred solution of the utility model, the bottoms of the first filter box, the second filter box and the condensation recovery box are all movably connected with liquid outlet pipes, and the other ends of the liquid outlet pipes extend into the centrifugal box.

[0015] Compared with the prior art, the beneficial effects of the utility model are:

[0016] 1. In the utility model, through the coordinated use of the first telescopic rod, the first strip and the first filter, when the bile and ethanol solution are in the stirring barrel and stirred evenly, they fall onto the first filter, and the mixed liquid on the top of the first filter is filtered by the first vibrators on both sides of the first filter, and the first telescopic rod is extended to drive the first strip to move back and forth, so as to accelerate the filtration of the bile-ethanol mixed liquid and push the screened large particles to the second filter box through the first connecting pipe, and the large particles are mixed with ethanol again through the coordinated use of the ethanol storage box and the automatic sprayer, and the bile acid in the large particles is extracted and filtered again through the coordinated use of the second telescopic rod, the second strip, the second filter and the second vibrator, and the remaining residue is pushed to the distillation box through the second connecting pipe, and heated by the distillation heating plate, and the evaporated gas of ethanol condenses into liquid from the condenser and flows to the condensation recovery box.

[0017] 2. In the utility model, the ethanol bile acid mixture produced by the first filter box, the second filter box and the condensation recovery box flows into the centrifugal box through the liquid outlet pipe, and the ethanol bile acid mixture is centrifugally layered by the coordinated use of the second motor, the rotating rod and the centrifugal barrel. The liquid of the centrifugal layer flows to the drying box to dry the ethanol solution, and finally bile acid is obtained. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] Figure 1 It is an overall schematic diagram of the utility model;

[0019] Figure 2 This is a cross-sectional schematic diagram of the mixing barrel of the utility model;

[0020] Figure 3 It is a cross-sectional schematic diagram of the extraction device of the utility model;

[0021] Figure 4 It is a cross-sectional schematic diagram of the centrifugal barrel of the utility model.

[0022] In the figure: 1, stirring barrel; 2, bile inlet; 3, first motor; 4, first filter box; 5, first vibrator; 6, first fixing rod; 7, bottom plate; 8, support frame; 9, box door; 10, drying box; 11, centrifugal box; 12, second fixing rod; 13, condensation recovery box; 14, distillation box; 15, ethanol storage box; 16, second filter box; 17, first connecting pipe; 18, second connecting pipe; 19, third fixing rod; 20, stirring Stirring rod; 21. Stirring fan blades; 22. Ethanol inlet; 23. First telescopic rod; 24. First long strip; 25. Second vibrator; 26. First filter; 27. Second telescopic rod; 28. Second long strip; 29. ​​Automatic sprayer; 30. Fourth fixed rod; 31. Second filter; 32. Condenser; 33. Centrifugal barrel; 34. Rotating rod; 35. Second motor; 36. Support box; 37. Fifth fixed rod; 38. Liquid outlet pipe; 39. Distillation heating plate. DETAILED DESCRIPTION

[0023] The technical solutions in the embodiments of the utility model will be clearly and completely described below in conjunction with the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, rather than all of the embodiments. Based on the embodiments of the utility model, all other embodiments obtained by ordinary technicians in this field without making creative work are within the scope of protection of the utility model.

[0024] For examples, see Figure 1-4 , the utility model provides a technical solution:

[0025] A bile acid purification device comprises a bottom plate 7, a support frame 8 and a support box 36 are fixedly connected to the bottom of the bottom plate 7, a first fixing rod 6, a second fixing rod 12 and a third fixing rod 19 are fixedly connected to the top of the bottom plate 7, a first filter box 4 is fixedly connected to the top of the first fixing rod 6, a stirring barrel 1 is fixedly connected to the top of the first filter box 4, a bile inlet 2 and an ethanol inlet 22 are respectively opened on the top of the stirring barrel 1, the first filter box 4 is fixedly connected to the second filter box 16 through a fifth fixing rod 37, a first connecting pipe 18 is fixedly connected between the first filter box 4 and the second filter box 16, and an ethanol storage box 15 is fixedly connected to the top of the second filter box 16 The bottom of the ethanol storage box 15 is fixedly connected to an automatic sprayer 29, the side of the second filter box 16 is fixedly connected to a fourth fixing rod 30, the side of the fourth fixing rod 30 is fixedly connected to the distillation box 14, the top of the bottom plate 7 is fixedly connected to the distillation box 14 through a third fixing rod 19, a second connecting pipe 17 is fixedly connected between the second filter box 16 and the distillation box 14, the top of the distillation box 14 is fixedly connected to a condenser 32, the bottom of the condenser 32 is fixedly connected to a condensation recovery box 13, the top of the second fixing rod 12 is fixedly connected to a centrifugal box 11, the bottom of the centrifugal box 11 is fixedly connected to a drying box 10, and the side of the drying box 10 is movably connected to a box door 9.

[0026] In this embodiment, Figure 2 and Figure 3 As shown, both sides of the first filter box 4 are movably connected with the first vibrator 5, and the side of the first vibrator 5 is fixedly connected with the first filter screen 26, both sides of the second filter box 16 are movably connected with the second vibrator 25, and the side of the second vibrator 25 is fixedly connected with the second filter screen 31, the side of the first filter box 4 is movably connected with the first telescopic rod 23, and the side of the first telescopic rod 23 is fixedly connected with the first long strip 24, the side of the second filter box 16 is movably connected with the second telescopic rod 27, and the side of the second telescopic rod 27 is fixedly connected with the second long strip 28.

[0027] Among them, through the coordinated use of the first telescopic rod 23, the first strip 24 and the first filter 26, when the bile and ethanol solution are in the stirring barrel 1 and are evenly stirred, they fall onto the first filter 26, and the mixed liquid on the top of the first filter 26 is filtered by the first vibrators 5 on both sides of the first filter 26. The first telescopic rod 23 is extended and retracted to drive the first strip 24 to move back and forth, thereby accelerating the filtration of the bile-ethanol mixed liquid and pushing the screened large particles through the first connecting pipe 17 to the second filter box 16. Through the coordinated use of the ethanol storage box 15 and the automatic sprayer 29, the large particles are mixed with ethanol again. Through the coordinated use of the second telescopic rod 27, the second strip 28, the second filter 31 and the second vibrator 25, the bile acid in the large particles is extracted and filtered again, and the remaining residue is pushed to the distillation box 14 through the second connecting pipe 18, and heated by the distillation heating plate 39. The evaporated gas of ethanol condenses into liquid from the condenser 32 and flows to the condensation recovery box 13.

[0028] In this embodiment, Figure 1 and Figure 4 As shown, a first motor 3 is installed on the top of the mixing barrel 1, and a stirring rod 20 is fixedly connected to the output end of the first motor 3, and a stirring fan blade 21 is fixedly connected to the side of the stirring rod 20, a distillation heating plate 39 is fixedly connected to the center of the distillation box 14, and the surface of the distillation heating plate 39 has raised bumps, a support box 36 is fixedly connected to the bottom of the centrifugal box 11, a second motor 35 is placed in the support box 36, and a rotating rod 34 is fixedly connected to the output end of the second motor 35, the bottom of the first filter box 4, the second filter box 16 and the condensation recovery box 13 are all movably connected with a liquid outlet pipe 38, and the other end of the liquid outlet pipe 38 extends to the top of the rotating rod 34 in the centrifugal box 11 and is fixedly connected to a centrifugal bucket 33, and the surface of the centrifugal bucket 33 is provided with small holes of equal diameter and evenly distributed, and the materials of the centrifugal bucket 33 and the rotating rod 34 are both stainless steel.

[0029] Among them, the ethanol bile acid mixture produced by the first filter box 4, the second filter box 16 and the condensation recovery box 13 flows into the centrifugal box 11 through the liquid outlet pipe 38, and the ethanol bile acid mixture is centrifugally layered by the coordinated use of the second motor 35, the rotating rod 34 and the centrifugal bucket 33. The centrifugally layered liquid flows to the drying box 10 for drying, and bile acid is obtained after the ethanol solution is dried.

[0030] The working process of the utility model: when the bile acid purification device designed by the present invention is in operation, the switches of the first motor 3 and the second motor 35 are first turned on, and animal bile and ethanol solution in corresponding proportions are put in from the bile inlet 2 and the ethanol inlet 22 on the top of the stirring barrel 1, and the stirring rod 20 is driven by the first motor 3 to rotate, and the animal bile and the ethanol solution are stirred evenly so that they are fully fused and then fall into the first filter box 4, and the mixed liquid is filtered and processed by the first filter screen 26 and the first vibrator 5, and the filtered residue is pushed to the second filter box 16 through the first connecting pipe 17 by the first telescopic rod 23 and the first strip 24, and the ethanol and the residue are mixed again by the ethanol storage box 15 and the automatic sprayer 29 on the top of the second filter box 16. , through the coordinated use of the second vibrator 25, the second filter screen 31, the second telescopic rod 27 and the second strip 28, the ethanol residue mixed liquid is filtered and the residue is pushed into the distillation box 14 through the second connecting pipe 18, and the residue is distilled through the distillation heating plate 39 in the distillation box 14. The ethanol gas produced by the distillation is condensed into liquid through the condenser 32 and flows into the condensation recovery box 13. The ethanol bile acid mixed liquid formed in the first filter box 4, the second filter box 16 and the condensation recovery box 13 flows into the centrifugal bucket 33 inside the centrifugal box 11 through the liquid outlet pipe 38. The second motor 35 drives the rotating rod 34 to rotate the centrifugal bucket 33, and the ethanol bile acid mixed liquid is centrifuged. The ethanol bile acid mixed liquid after centrifugation flows into the drying box 10, and bile acid is obtained after drying in the drying box 10.

[0031] In the description of this specification, the description with reference to the terms "one embodiment", "example", "specific example", etc. means that the specific features, structures, materials or characteristics described in conjunction with the embodiment or example are included in at least one embodiment or example of the utility model. In this specification, the schematic representation of the above terms does not necessarily refer to the same embodiment or example. Moreover, the specific features, structures, materials or characteristics described can be combined in any one or more embodiments or examples in a suitable manner.

[0032] The preferred embodiments of the utility model disclosed above are only used to help explain the utility model. The preferred embodiments do not describe all the details in detail, nor do they limit the utility model to the specific implementation methods described. Obviously, many modifications and changes can be made according to the content of this specification. This specification selects and specifically describes these embodiments in order to better explain the principles and practical applications of the utility model, so that technicians in the relevant technical field can well understand and use the utility model. The utility model is limited only by the claims and their full scope and equivalents.

Claims

1. A bile acid purification device, comprising a bottom plate (7), characterized in that: The bottom of the bottom plate (7) is respectively fixedly connected to a support frame (8) and a support box (36); the top of the bottom plate (7) is respectively fixedly connected to a first fixing rod (6), a second fixing rod (12) and a third fixing rod (19); the top of the first fixing rod (6) is fixedly connected to a first filter box (4); the top of the first filter box (4) is fixedly connected to a stirring barrel (1); the top of the stirring barrel (1) is respectively provided with a bile inlet (2) and an ethanol inlet (22); the first filter box (4) is fixedly connected to a second filter box (16) via a fifth fixing rod (37); a first connecting pipe (18) is fixedly connected between the first filter box (4) and the second filter box (16); the top of the second filter box (16) is fixedly connected to an ethanol storage box (15); the ethanol storage box (15) is 5), the bottom of which is fixedly connected to an automatic sprayer (29), the side of the second filtering box (16) is fixedly connected to a fourth fixing rod (30), the side of the fourth fixing rod (30) is fixedly connected to a distillation box (14), the top of the bottom plate (7) is fixedly connected to the distillation box (14) via a third fixing rod (19), a second connecting pipe (17) is fixedly connected between the second filtering box (16) and the distillation box (14), the top of the distillation box (14) is fixedly connected to a condenser (32), the bottom of the condenser (32) is fixedly connected to a condensation recovery box (13), the top of the second fixing rod (12) is fixedly connected to a centrifugal box (11), the bottom of the centrifugal box (11) is fixedly connected to a drying box (10), and the side of the drying box (10) is movably connected to a box door (9).

2. A bile acid purification device according to claim 1, characterized in that: Both sides of the first filter box (4) are movably connected to a first vibrator (5), and the side of the first vibrator (5) is fixedly connected to a first filter net (26); both sides of the second filter box (16) are movably connected to a second vibrator (25), and the side of the second vibrator (25) is fixedly connected to a second filter net (31).

3. A bile acid purification device according to claim 1, characterized in that: A first telescopic rod (23) is movably connected to the side of the first filter box (4), and a first long strip (24) is fixedly connected to the side of the first telescopic rod (23); a second telescopic rod (27) is movably connected to the side of the second filter box (16), and a second long strip (28) is fixedly connected to the side of the second telescopic rod (27).

4. A bile acid purification device according to claim 1, characterized in that: A first motor (3) is installed on the top of the stirring barrel (1); a stirring rod (20) is fixedly connected to the output end of the first motor (3); and a stirring fan blade (21) is fixedly connected to the side of the stirring rod (20).

5. A bile acid purification device according to claim 1, characterized in that: A distillation heating plate (39) is fixedly connected to the center of the distillation box (14), and the surface of the distillation heating plate (39) has raised bumps.

6. A bile acid purification device according to claim 1, characterized in that: A support box (36) is fixedly connected to the bottom of the centrifugal housing (11), a second motor (35) is placed in the support box (36), an output end of the second motor (35) is fixedly connected to a rotating rod (34), and a centrifugal bucket (33) is fixedly connected to the top of the rotating rod (34).

7. A bile acid purification device according to claim 6, characterized in that: The surface of the centrifugal bucket (33) is provided with small holes of equal diameter and evenly distributed, and the centrifugal bucket (33) and the rotating rod (34) are both made of stainless steel.

8. A bile acid purification device according to claim 1, characterized in that: The bottoms of the first filter housing (4), the second filter housing (16) and the condensation recovery housing (13) are all movably connected with a liquid outlet pipe (38), and the other ends of the liquid outlet pipes (38) extend into the centrifugal housing (11).

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