Separating tank for furfuryl alcohol reaction liquid

By designing a furfurol reaction liquid separation tank including a storage tank and a temporary storage tank, the reaction liquid is sprayed out with a spiral bent pipe and hydrogen is separated through the funnel-type lower liquid port, the problem of incomplete hydrogen separation in the prior art is solved, and a more efficient separation effect is achieved and the purpose of reducing furfurol and catalyst consumption is achieved.

CN222677258UActive Publication Date: 2025-03-28ZHUCHENG TAISHENG CHEM CO LTD
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Patent Information

Application Number
CN202421160401.9
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-05-24
Publication Date
2025-03-28
Estimated Expiration
2034-05-24

AI Technical Summary

Technical Problem

When the existing hollow tank separation device separates hydrogen, the hydrogen will contain a small amount of furfuryl alcohol and catalyst, resulting in incomplete separation of hydrogen and causing consumption of furfuryl alcohol and catalyst.

Method used

A separation tank of furfuryl alcohol reaction liquid is designed, including a storage tank and a temporary storage barrel. The reaction liquid is sprayed out through a spiral bent pipe, so that the liquid spiral downstream along the inner side wall of the funnel-type lower liquid port, and the separated hydrogen is discharged through the central air outlet pipe to improve the separation effect.

Benefits of technology

The reaction liquid and hydrogen are further separated, the consumption of furfuryl alcohol and catalyst is reduced, and the efficiency of subsequent processing and use is improved.

✦ Generated by Eureka AI based on patent content.

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Abstract

A separating tank for furfuryl alcohol reaction liquid comprises a tank body and a funnel type liquid discharging port located in the center of the tank body, a feeding pipe penetrates through the top of the tank body, a spiral bent pipe located above the liquid discharging port is arranged at the lower end of the feeding pipe, a liquid outlet of the spiral bent pipe is tightly attached to the upper edge of the liquid discharging port, and the liquid outlet enters along the tangent line of the upper edge of the liquid discharging port. A liquid discharge pipe is arranged at the bottom of the tank body; and an air outlet pipe penetrating through the top of the tank body is arranged above the center of the liquid discharge port. When hydrogen in furfuryl alcohol dehydrogenation reaction liquid is separated, the liquid outlet of the spiral bent pipe is tightly attached to the upper edge of the liquid discharging opening and enters along the tangent line of the upper edge of the liquid discharging opening, so that the liquid outlet spirally moves downwards on the inner side wall of the funnel type liquid discharging opening, and the separation effect of the reaction liquid and the hydrogen is improved; in addition, when cleaning is needed, clean water is introduced into the flushing pipe and is uniformly sprayed out from a plurality of nozzles of the hollow disc, so that the inner side wall of the liquid discharging opening is uniformly flushed, and the cleaning liquid is more thorough.
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Description

Technical Field

[0001] The utility model relates to a separation device, in particular to a separation tank for furfuryl alcohol reaction liquid. Background Art

[0002] The furfuryl alcohol dehydrogenation reaction liquid contains a small amount of hydrogen. After cooling, gas-liquid separation is performed and the separated hydrogen is reused. At present, the separation is mainly carried out through hollow tanks. The liquid enters the bottom of the hollow tank, and the hydrogen rises to the top and is discharged from the tank. During the separation process, a small amount of furfuryl alcohol and catalyst will be carried in the hydrogen, which will adhere to the pipeline, resulting in incomplete hydrogen separation and consumption of a small amount of furfuryl alcohol and catalyst, which is not conducive to subsequent processing and use. Utility Model Content

[0003] In order to solve the above problems, the utility model aims to provide a separation tank for furfuryl alcohol reaction liquid.

[0004] To achieve the above-mentioned purpose, the technical solution of the utility model is: a separation tank for furfuryl alcohol reaction liquid, including a storage tank and a temporary storage barrel body, the storage tank is connected to the top of the temporary storage barrel body through a feeding pump, an overflow pipe connected to the storage tank is arranged on one side of the top of the temporary storage barrel body, a regulating valve is arranged on the side above the bottom of the temporary storage barrel body, the top of the temporary storage barrel body is also connected to the top of the storage tank through a balancing pipe, and a feeding pipe is arranged on the top of the storage tank.

[0005] Furthermore, a liquid level gauge is provided on one side of the storage tank and the temporary storage barrel.

[0006] Furthermore, a drain valve for emptying is provided on one side of the bottom of the storage tank.

[0007] Furthermore, the temporary storage barrel is arranged vertically, the storage tank is arranged horizontally, and the volume of the storage tank is much larger than that of the temporary storage barrel.

[0008] Furthermore, the lower end of the temporary storage barrel is connected to the upper end of the storage tank through a drain pipe.

[0009] When the utility model separates hydrogen from the furfuryl alcohol dehydrogenation reaction liquid, the hydrogen is sprayed out through the feed pipe and the spiral bend pipe. Since the liquid outlet of the spiral bend pipe is closely attached to the upper edge of the lower liquid outlet and enters along the tangent line of the upper edge of the lower liquid outlet, the liquid moves downward in a spiral on the inner side wall of the funnel-shaped lower liquid outlet, thereby facilitating the liquid to flow downward, and the separated hydrogen is discharged through the central gas outlet pipe, thereby improving the separation effect of the reaction liquid and the hydrogen, and the separation is more thorough.

[0010] In addition, when cleaning is required, the flushing pipe is connected to clean water, and the clean water is evenly sprayed from multiple nozzles of the hollow disc, thereby evenly flushing the inner wall of the lower liquid port, and the cleaning liquid is more thorough. BRIEF DESCRIPTION OF THE DRAWINGS

[0011] The utility model is now further described with reference to the accompanying drawings.

[0012] Figure 1 It is a schematic diagram of the main structure of the utility model. DETAILED DESCRIPTION

[0013] like Figure 1 As shown, a separation tank for furfuryl alcohol reaction liquid comprises a tank body 1 and a funnel-shaped lower liquid port 2 located in the center of the tank body 1, a feed pipe 3 is passed through the top of the tank body 1, a spiral bend pipe 4 is arranged at the lower end of the feed pipe 3 and is located above the lower liquid port 2, a liquid outlet of the spiral bend pipe 4 is closely attached to the upper edge of the lower liquid port 2, and enters along the tangent line of the upper edge of the lower liquid port 2, a drain pipe 5 is arranged at the bottom of the tank body 1, and an air outlet pipe 6 passing through the top of the tank body 1 is arranged above the center of the lower liquid port 2.

[0014] To facilitate cleaning, a hollow disc 7 is provided in the tank body 1 above the lower liquid port 2, a plurality of nozzles 8 are provided around the hollow disc 7, a flushing pipe 9 penetrating the top of the tank body 1 is provided at the top center of the hollow disc 7, a liquid level gauge 10 is provided on the side wall of the tank body 1, a safety pressure relief valve 11 is provided on the top of the tank body 1, and a pressure gauge 12 is provided on one side of the top of the tank body 1.

[0015] Working principle of this utility model:

[0016] The furfuryl alcohol dehydrogenation reaction liquid is ejected through the feed pipe 3 and the spiral bend pipe 4. Since the liquid outlet of the spiral bend pipe 4 is close to the upper edge of the lower liquid port 2 and enters along the tangent line of the upper edge of the lower liquid port 2, the liquid moves downward in a spiral on the inner wall of the funnel-shaped lower liquid port 2, thereby facilitating the liquid to flow downward, and the separated hydrogen is discharged through the central outlet pipe 6, thereby improving the separation effect of the reaction liquid and the hydrogen, and the separation is more thorough;

[0017] When cleaning is required, the flushing pipe 9 is connected to clean water, and the clean water is evenly sprayed from the multiple nozzles 8 of the hollow disc 7, so as to evenly flush the inner wall of the lower liquid port 2, and the cleaning liquid is more thorough.

[0018] The above description is only an illustrative embodiment of the present invention and is not intended to limit the scope of the present invention. Any equivalent changes and modifications made by any person skilled in the art without departing from the concept and principle of the present invention shall fall within the scope of protection of the present invention.

Claims

1. A separation tank for furfuryl alcohol reaction liquid, comprising a tank body (1) and a funnel-shaped liquid outlet (2) located in the center of the tank body (1), characterized in that: A feed pipe (3) passes through the top of the tank body (1); a spiral bend pipe (4) is provided at the lower end of the feed pipe (3) and is located above the lower liquid port (2); a liquid outlet of the spiral bend pipe (4) is closely attached to the upper edge of the lower liquid port (2) and enters along a tangent line of the upper edge of the lower liquid port (2); a liquid discharge pipe (5) is provided at the bottom of the tank body (1); and an air outlet pipe (6) passing through the top of the tank body (1) is provided above the center of the lower liquid port (2).

2. The separation tank for the furfuryl alcohol reaction liquid according to claim 1, characterized in that: A hollow disc (7) is arranged in the tank body (1) above the lower liquid port (2), a plurality of nozzles (8) are arranged around the hollow disc (7), and a flushing pipe (9) penetrating the top of the tank body (1) is arranged at the top center of the hollow disc (7).

3. The separation tank for the furfuryl alcohol reaction liquid according to claim 1, characterized in that: A liquid level gauge (10) is provided on the side wall of the tank body (1).

4. The separation tank for the furfuryl alcohol reaction liquid according to claim 1, characterized in that: A safety pressure relief valve (11) is provided on the top of the tank body (1).

5. The separation tank for the furfuryl alcohol reaction liquid according to claim 1, characterized in that: A pressure gauge (12) is provided on one side of the top of the tank body (1).