Organic chemical raw material reflux device
By designing a reflow device for organic chemical raw materials including a reflow pump, a condenser and a meter, the problems of low reflow efficiency and insufficient control accuracy in the prior art are solved, and efficient and stable reflow process and reaction control are achieved.
Patent Information
- Application Number
- CN202421921260.8
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-08-09
- Publication Date
- 2025-05-30
- Estimated Expiration
- 2034-08-09
AI Technical Summary
The existing reflow device cannot fully condense the steam under high temperature and high pressure conditions, resulting in insufficient condensation liquid, low reflow efficiency, and the flow rate and amount of the reflow liquid cannot be monitored and controlled in real time, affecting the continuity and stability of the reaction.
An organic chemical raw material reflow device is designed, including the first and second reaction tanks, a reflow pump, a condenser and a meter. The steam is introduced into the condenser for condensation through the reflow pump, and the flow rate of the reflow liquid is monitored in real time through the meter.
The effective reflux of the condensate is achieved, the reflux efficiency and control accuracy are improved, the continuity and stability of the reaction are ensured, and the needs of different reaction conditions can be adapted to the needs of different reaction conditions.
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Figure CN222918689U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of chemical raw material processing equipment, in particular to a reflux device for organic chemical raw materials. Background Technique
[0002] In the process of organic chemical reactions, reactants usually need to react under high-temperature conditions, and a large amount of steam will be generated during these reaction processes. If these vapors cannot be effectively recycled, it will lead to problems such as reduced reaction efficiency and waste of resources. Although the reflux devices in the related technologies can improve the reflux efficiency to a certain extent, under high-temperature and high-pressure conditions, the steam cannot be fully condensed in the condensation device, resulting in insufficient condensate volume and low reflux efficiency. The reflux of the condensate depends on gravity and is easily affected by internal pressure changes, so the reflux process is not stable enough, affecting the continuity and stability of the reaction. It is impossible to monitor and control the flow rate and quantity of the reflux liquid in real time, resulting in low control accuracy of the reflux process and difficulty in adapting to the needs of different reaction conditions. In view of this, it is necessary to improve the current reflux device to solve the above problems;
[0003] The above information disclosed in this background technical part is only used to understand the background technology of the inventive concept, and therefore, it may include information that does not constitute prior art. Summary of the Utility Model
[0004] The purpose of the utility model is to provide a reflux device for organic chemical raw materials to solve the problems raised in the above background technology that although the reflux device can improve the reflux efficiency to a certain extent, under high-temperature and high-pressure conditions, the steam cannot be fully condensed in the condensation device, resulting in insufficient condensate volume and low reflux efficiency. The reflux of the condensate depends on gravity and is easily affected by internal pressure changes, so the reflux process is not stable enough, affecting the continuity and stability of the reaction. It is impossible to monitor and control the flow rate and quantity of the reflux liquid in real time, resulting in low control accuracy of the reflux process and difficulty in adapting to the needs of different reaction conditions.
[0005] In order to achieve the above purpose, the utility model adopts the following technical solutions:
[0006] An organic chemical raw material reflux device, comprising a fixing frame, a first reaction tank and a second reaction tank. The upper end of the fixing frame is fixedly installed with a reaction tank fixing frame. Inside the reaction tank fixing frame, the first reaction tank and the second reaction tank are fixedly installed. The upper end of the fixing frame is fixedly installed with a first reflux pump and a second reflux pump. The first reflux pump and the second reflux pump are connected to the inside of the first reaction tank and the second reaction tank through pipelines. The first reflux pump and the second reflux pump are respectively connected to one side of the first reaction tank and the second reaction tank through a first reflux condenser pipe and a second reflux condenser pipe. On one side of the first reflux pump and the second reflux pump, a first meter and a second meter are respectively installed. On one side of the first reflux pump and the second reflux pump, a first discharge port and a second discharge port are respectively provided.
[0007] As a preferred technical solution, a pump body motor and a second pump body motor are fixedly installed at the upper end of the fixing frame. The first pump body motor and the second pump body motor are respectively connected to the first pump body and the second pump body. The first pump body and the second pump body are respectively connected to a first feed port and a second feed port through pipelines. The first feed port and the second feed port are respectively connected to the first reaction tank and the second reaction tank through pipelines.
[0008] As a preferred technical solution, a first servo motor and a second servo motor are respectively installed at the upper ends of the first reaction tank and the second reaction tank. The lower ends of the first servo motor and the second servo motor are respectively fixedly connected to a first stirring blade and a second stirring blade.
[0009] As a preferred technical solution, a first pressure relief valve and a second pressure relief valve are respectively installed at the upper ends of the first reaction tank and the second reaction tank.
[0010] As a preferred technical solution, a controller is fixedly installed at the upper end of the fixing frame. The controller is electrically connected to the first pump body motor, the second pump body motor, the first servo motor, the second servo motor, the first pressure relief valve, the second pressure relief valve, the first reflux pump, the first meter, the second reflux pump, and the second meter.
[0011] The beneficial effects of the present utility model are:
[0012] Through this device, during the reaction process, the organic chemical raw materials in the reaction tank will generate steam. These steam enter the first reflux condenser pipe and the second reflux condenser pipe through the first reflux pump and the second reflux pump, ensuring that the condensate can be effectively transported back to the reaction tank to achieve a continuous reflux process. The first meter and the second meter are respectively installed on one side of the first reflux pump and the second reflux pump to monitor the flow rate of the reflux liquid in real time. Description of the Drawings
[0013] Figure 1 It is a schematic structural diagram of an organic chemical raw material reflux device proposed by the present utility model;
[0014] Figure 2 The structural schematic diagram of a reflux device for organic chemical raw materials proposed by the present utility model;
[0015] Figure 3 The structural schematic diagram of the stirring blade of a reflux device for organic chemical raw materials proposed by the present utility model.
[0016] In the figure: 1 fixing frame, 2 first pump body motor, 201 first pump body, 202 first feed inlet, 3 second pump body motor, 301 second pump body, 302 second feed inlet, 4 reaction tank fixing frame, 5 controller, 6 first reaction tank, 7 second reaction tank, 8 first servo motor, 801 first stirring blade, 9 second servo motor, 901 second stirring blade, 10 first pressure relief valve, 11 second pressure relief valve, 12 first reflux pump, 121 first meter, 122 first discharge port, 13 second reflux pump, 131 second meter, 132 second discharge port, 14 first reflux condenser, 15 second reflux condenser. Specific embodiments
[0017] Next, the technical solutions in the embodiments of the present utility model will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all of the embodiments.
[0018] In the description of the present utility model, it should be understood that the orientation or positional relationship indicated by the terms "center", "longitudinal", "transverse", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", etc. is based on the orientation or positional relationship shown in the drawings, and is only for the convenience of describing the present utility model and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus cannot be understood as a limitation to the present utility model.
[0019] In addition, the terms "first" and "second" are only used for descriptive purposes, and cannot be understood as indicating or implying relative importance or implicitly indicating the quantity of the indicated technical features. Thus, the features defined with "first" and "second" may explicitly or implicitly include one or more of such features. In the description of the present utility model, "a plurality" means two or more, unless otherwise specifically defined.
[0020] Refer to Figures 1-3, An organic chemical raw material reflux device, comprising a fixed frame 1, a first reaction tank 6 and a second reaction tank 7. At the upper end of the fixed frame 1, a first pump body motor 2 and a second pump body motor 3 are fixedly installed. The first pump body motor 2 and the second pump body motor 3 are respectively connected to a first pump body 201 and a second pump body 301. The first pump body 201 and the second pump body 301 are respectively connected to a first feed inlet 202 and a second feed inlet 302 through pipelines. The first feed inlet 202 and the second feed inlet 302 are respectively connected to the first reaction tank 6 and the second reaction tank 7 through pipelines.
[0021] Among them, at the upper end of the fixed frame 1, a reaction tank fixing frame 4 is fixedly installed. Inside the reaction tank fixing frame 4, a first reaction tank 6 and a second reaction tank 7 are fixedly installed. At the upper end of the fixed frame 1, a first reflux pump 12 and a second reflux pump 13 are fixedly installed. The first reflux pump 12 and the second reflux pump 13 are connected to the inside of the first reaction tank 6 and the second reaction tank 7 through pipelines. The first reflux pump 12 and the second reflux pump 13 are respectively connected to one side of the first reaction tank 6 and the second reaction tank 7 through a first reflux condenser pipe 14 and a second reflux condenser pipe 15. On one side of the first reflux pump 12 and the second reflux pump 13, a first meter 121 and a second meter 131 are respectively installed. On one side of the first reflux pump 12 and the second reflux pump 13, a first discharge port 122 and a second discharge port 132 are respectively provided.
[0022] With this design, when the first pump body motor 2 and the second pump body motor 3 are started, they drive the first pump body 201 and the second pump body 301 to work. The first pump body 201 and the second pump body 301 are respectively connected to the first feed inlet 202 and the second feed inlet 302 through pipelines, realizing the transportation of raw materials. The raw materials enter the first reaction tank 6 and the second reaction tank 7 through the first feed inlet 202 and the second feed inlet 302, and the chemical reaction starts. The first pump body motor 2 and the second pump body motor 3 are respectively connected to the first pump body 201 and the second pump body 301, ensuring the continuous and stable supply of raw materials.
[0023] During the reaction process, the organic chemical raw materials in the reaction tank will generate steam. These steams enter the first reflux condenser pipe 14 and the second reflux condenser pipe 15 through the first reflux pump 12 and the second reflux pump 13, ensuring that the condensate can be effectively transported back into the reaction tank, realizing a continuous reflux process. The first meter 121 and the second meter 131 are respectively installed on one side of the first reflux pump 12 and the second reflux pump 13, and are used to monitor the flow rate of the reflux liquid in real time.
[0024] In other embodiments, a first servo motor 8 and a second servo motor 9 are respectively installed at the upper ends of the first reaction tank 6 and the second reaction tank 7. The lower ends of the first servo motor 8 and the second servo motor 9 are respectively fixedly connected to a first stirring blade 801 and a second stirring blade 901.
[0025] Through this design, the first servo motor 8 and the second servo motor 9 can drive the stirring blades 801 and the stirring blades 901 to stir in the reaction tank, ensuring sufficient mixing of the reactants, improving the reaction efficiency and the uniformity of the products. The precise control of the servo motor can adjust the stirring speed according to actual needs, thereby adapting to different reaction conditions and enhancing the applicability and flexibility of the device.
[0026] In other embodiments, a first pressure relief valve 10 and a second pressure relief valve 11 are installed at the upper ends of the first reaction tank 6 and the second reaction tank 7, respectively.
[0027] Through this design, the first pressure relief valve 10 and the second pressure relief valve 11 can monitor the pressure inside the reaction tank, and adjust the pressure inside the reaction tank by releasing during the reaction process to prevent safety problems caused by excessive pressure.
[0028] In other embodiments, a controller 5 is fixedly installed on the upper end of the fixed frame 1, and the controller 5 is electrically connected to the first pump body motor 2, the second pump body motor 3, the first servo motor 8, the second servo motor 9, the first pressure relief valve 10, the second pressure relief valve 11, the first reflux pump 12, the first meter 121, the second reflux pump 13, and the second meter 131.
[0029] In this embodiment, during the reaction process, the organic chemical raw materials in the reaction tank will generate steam, and the steam enters the first reflux condenser 14 and the second reflux condenser 15 through the first reflux pump 12 and the second reflux pump 13, ensuring that the condensate can be effectively transported back to the reaction tank to achieve a continuous reflux process. The first meter 121 and the second meter 131 are respectively installed on one side of the first reflux pump 12 and the second reflux pump 13, for real-time monitoring of the flow rate of the reflux liquid.
[0030] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes within the technical scope disclosed by the present invention according to the technical scheme and the utility model concept of the present invention, which should be covered by the protection scope of the present invention.
Claims
1. An organic chemical raw material reflux device, comprising a fixed frame (1), a first reaction tank (6) and a second reaction tank (7), characterized in that: A reaction tank fixing frame (4) is fixedly mounted on the upper end of the fixing frame (1), a first reaction tank (6) and a second reaction tank (7) are fixedly mounted inside the reaction tank fixing frame (4), a first reflux pump (12) and a second reflux pump (13) are fixedly mounted on the upper end of the fixing frame (1), the first reflux pump (12) and the second reflux pump (13) are connected to the inside of the first reaction tank (6) and the second reaction tank (7) through a pipeline, the first reflux pump (12) and the second reflux pump (13) are connected to one side of the first reaction tank (6) and the second reaction tank (7) through a first reflux condenser (14) and a second reflux condenser (15) respectively, a first metering device (121) and a second metering device (131) are respectively mounted on one side of the first reflux pump (12) and the second reflux pump (13), and a first discharge port (122) and a second discharge port (132) are respectively provided on one side of the first reflux pump (12) and the second reflux pump (13).
2. An organic chemical raw material reflux device according to claim 1, characterized in that: A first pump body motor (2) and a second pump body motor (3) are fixedly mounted on the upper end of the fixing frame (1); the first pump body motor (2) and the second pump body motor (3) are respectively connected to the first pump body (201) and the second pump body (301); the first pump body (201) and the second pump body (301) are respectively connected to the first feed port (202) and the second feed port (302) via a pipeline; the first feed port (202) and the second feed port (302) are respectively connected to the first reaction tank (6) and the second reaction tank (7) via a pipeline.
3. The organic chemical raw material reflux device according to claim 1, characterized in that: A first servo motor (8) and a second servo motor (9) are respectively installed at the upper ends of the first reaction tank (6) and the second reaction tank (7); and a first stirring blade (801) and a second stirring blade (901) are respectively fixedly connected to the lower ends of the first servo motor (8) and the second servo motor (9).
4. The organic chemical raw material reflux device according to claim 1, characterized in that: A first pressure relief valve (10) and a second pressure relief valve (11) are respectively installed at the upper ends of the first reaction tank (6) and the second reaction tank (7).
5. The organic chemical raw material reflux device according to claim 1, characterized in that: A controller (5) is fixedly mounted on the upper end of the fixing frame (1), and the controller (5) is electrically connected to the first pump body motor (2), the second pump body motor (3), the first servo motor (8), the second servo motor (9), the first pressure relief valve (10), the second pressure relief valve (11), the first reflux pump (12), the first metering device (121), the second reflux pump (13), and the second metering device (131).