Evodia rutaecarpa high-temperature instantaneous sterilization equipment

By designing a high-temperature instantaneous sterilization device for Everrucia using superheated steam, the problem of the existing sterilization method poor performance on Everrucia microbial load processing is solved, and a safe, fast and continuous sterilization effect is achieved, which is suitable for powder and granular materials.

CN223233016UActive Publication Date: 2025-08-19YANGTZE RIVER PHARM CO LTD
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Patent Information

Application Number
CN202422369015.7
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-09-27
Publication Date
2025-08-19
Estimated Expiration
2034-09-27

AI Technical Summary

Technical Problem

The existing sterilization methods are poor in the microbial load processing of Everrucia, which poses safety risks and cannot achieve continuous production, especially the sterilization needs of powder and granular materials are difficult to meet.

Method used

The physically sterilized superheated steam is used as the medium, and through the combined equipment design of vacuum feed, screw feed, sterilization chamber, separation device and superheater, the full contact between the material and the superheated steam is achieved, combined with the stirring paddle and the air filtration system, ensuring uniform sterilization, rapid and safe.

Benefits of technology

The load on Everrucia microbials has been significantly reduced, from 100,000 cfu to less than 100 cfu. The equipment operation is safe and reliable, without agglomeration and coking, and is suitable for continuous sterilization of powder and granular materials.

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Abstract

The utility model discloses high-temperature instantaneous sterilization equipment for fructus evodiae, which comprises a vacuum feeding tank, a feeder is arranged below an outlet of the vacuum feeding tank, an outlet of a screw feeder extends into the feeder, an outlet of the feeder is connected with a first inlet of a sterilization bin, and an outlet of a steam generator is connected with an inlet of a superheater. An outlet of the superheater is connected with a second inlet of the sterilization bin, an outlet of the sterilization bin is connected with a first inlet of the separation device through a first inclined pipe, an inlet of the air filter is connected with a fan, an outlet of the air filter is connected with an inlet of the four-way valve, and a first outlet of the four-way valve is connected with a third inlet of the sterilization bin. A second outlet of the four-way valve is connected with the first inclined pipe, a third outlet of the four-way valve is connected with a condenser, an outlet of the condenser is connected with a steam-water separator, and an outlet of the steam-water separator is connected with a second inlet of the separation device. According to the utility model, physical sterilization'superheated steam 'is used as a medium, and the device has the characteristics of uniform heating, good penetrability and rapid sterilization.
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Description

Technical Field

[0001] The utility model belongs to the technical field of sterilization, and in particular relates to a high-temperature instantaneous sterilization device for Evodia rutaecarpa. Background Art

[0002] Evodia rutaecarpa, also known as Wuyu, tea ladle, lacquer ladle, stinky ladle tree, left-leaf pure yuzi, and rice ladle, is generally divided into several varieties: large-flowered Evodia rutaecarpa, medium-flowered Evodia rutaecarpa, and small-flowered Evodia rutaecarpa. It grows in sparse forests or shrubs from plains to mountainous areas at altitudes up to 1,500 meters, often found on sunny slopes. Small to large-scale cultivation occurs in various regions. The young fruit, after being soaked and dried, becomes the traditional Chinese medicine Evodia rutaecarpa, also known as Wuyu. It is a bitter stomachic and analgesic, also used as an anthelmintic. Its hot, bitter, and pungent properties dispel cold, relieve pain, and calm nausea. It is used to treat headaches or epigastric pain caused by liver and stomach deficiency and yin turbidity. However, the high microbial load on Evodia rutaecarpa seriously affects the quality of subsequent pharmaceutical production, necessitating sterilization.

[0003] Common sterilization methods currently available on the market include ethylene oxide sterilization, ozone sterilization, ultraviolet sterilization, and microwave sterilization. However, each of these sterilization methods has limitations. For example, ethylene oxide sterilization is flammable and explosive, and residues can cause product mutations. Ozone sterilization is harmful to the human body and is not suitable for easily oxidized products. Ultraviolet sterilization has poor penetration and is mainly used for disinfecting air and surfaces. Microwave sterilization is not suitable for materials with low moisture content or heat-sensitive components. Dry heat sterilization can easily cause the material to dissipate volatile components, leading to local overheating, charring, and agglomeration. 60CO-γ irradiation sterilization can leave residues, affecting the safety of the material in the later stages of production. Most existing sterilization methods operate intermittently and cannot meet the continuous sterilization requirements of powdered and granular materials. Summary of the Invention

[0004] The purpose of this utility model is to address the deficiencies of the above-mentioned existing technologies and to provide a high-temperature instantaneous sterilization device for Evodia rutaecarpa, which uses physical sterilization "superheated steam" as the medium, has the characteristics of uniform heating, good penetrability, rapid sterilization, safety and reliability, and no caking and coking.

[0005] The technical solutions adopted in this utility model are as follows:

[0006] A high-temperature instantaneous sterilization device for Evodia rutaecarpa, comprising a vacuum feeding tank, a screw feeder, a sterilization chamber, a separator, an air filter, a four-way valve, a steam generator and a superheater. A feeder is provided below the bottom outlet of the vacuum feeding tank, the outlet of the screw feeder extends into the feeder, the outlet of the feeder is connected to a first inlet of the sterilization chamber through a pipeline, the outlet of the steam generator is connected to the inlet of the superheater through a pipeline, the outlet of the superheater is connected to the second inlet of the sterilization chamber through a pipeline, the outlet of the sterilization chamber is connected to the first inlet of the separator through a first inclined pipe, the outlet of the separator is connected to a storage device through a second inclined pipe, the inlet of the air filter is connected to a fan through a pipeline, the outlet of the air filter is connected to the inlet of the four-way valve through a pipeline, the first outlet of the four-way valve is connected to the third inlet of the sterilization chamber through a pipeline, the second outlet of the four-way valve is connected to the first inclined pipe through a pipeline, the third outlet of the four-way valve is connected to a condenser through a pipeline, the outlet of the condenser is connected to a steam-water separator through a pipeline, and the outlet of the steam-water separator is connected to the second inlet of the separator through a pipeline.

[0007] Preferably, the separation device comprises a plurality of cyclone separators connected in parallel.

[0008] Preferably, the storage device comprises a plurality of storage bins connected in parallel.

[0009] Preferably, a sealing valve is provided on the pipeline between the feeder and the first inlet of the sterilization chamber.

[0010] Preferably, a stirring shaft and stirring paddles are provided in the sterilization chamber, and the stirring paddles are evenly distributed on the stirring shaft.

[0011] The utility model also includes a control cabinet, which is respectively connected with the vacuum feeding tank, the screw feeder, the sterilization chamber, the separation device, the air filter, the feeder, the condenser, the steam-water separator, the fan, the steam generator and the superheater through lines.

[0012] The beneficial effects of this utility model include: using superheated steam as a physical sterilization medium, it offers uniform heating, good penetration, rapid sterilization, safety, and reliability, while preventing agglomeration and coking. During operation, the superheater generates pure steam, which is piped into the sterilization chamber. The material is fed from a feeder through a sealed valve into the sterilization chamber, where it is fully exposed to the superheated steam via a stirring paddle. The high-speed flow of superheated steam suspended within the sterilization chamber reduces the microbial load of the material (Evodia rutaecarpa) from 100,000 CFU before sterilization to less than 100 CFU. The sterilized material passes through a separator for gas-material separation and cooling, and then enters a storage device for use, minimizing the loss of active ingredients. BRIEF DESCRIPTION OF THE DRAWINGS

[0013] Figure 1 It is a structural diagram of the utility model;

[0014] In the figure, 1 is a vacuum feeding tank; 2 is a screw feeder; 3 is a sterilization chamber; 4 is a separation device; 5 is an air filter; 6 is a feeder; 7 is a storage device; 8 is a four-way valve; 9 is a condenser; 10 is a steam-water separator; 11 is a fan; 12 is a steam generator; and 13 is a superheater. DETAILED DESCRIPTION

[0015] The present invention will be further described below with reference to the accompanying drawings:

[0016] like Figure 1 As shown, the utility model is a high-temperature instantaneous sterilization equipment for Evodia rutaecarpa, which includes a vacuum feeding tank 1, a screw feeder 2, a sterilization chamber 3, a separation device 4, an air filter 5, a four-way valve 8, a steam generator 12 and a superheater 13. A feeder 6 is provided below the bottom outlet of the vacuum feeding tank 1, the outlet of the screw feeder 2 extends into the interior of the feeder 6, and the outlet of the feeder 6 is connected to the first inlet of the sterilization chamber 3 through a pipeline; the outlet of the steam generator 12 is connected to the inlet of the superheater 13 through a pipeline, and the outlet of the superheater 13 is connected to the The second inlet is connected, and hot steam is generated in the steam generator 12. The hot steam is further heated by the superheater 13 and then input into the sterilization chamber 3 through the pipeline; a stirring shaft and a stirring paddle are provided in the sterilization chamber 3, and the stirring paddles are evenly distributed on the stirring shaft. A sealing valve is provided on the pipeline between the feeder 6 and the first inlet of the sterilization chamber 3. The material is delivered to the sterilization chamber 3 by the feeder 6 through the sealing valve. At this time, the material is fully in contact with the superheated steam in the sterilization chamber 3 through the stirring paddle, and the bacteria in the material are killed by the thermal effect generated by the superheated steam suspended in the high-speed flow in the chamber.

[0017] The outlet of the sterilization chamber 3 in the present invention is connected to the first inlet of the separation device 4 via a first inclined tube. The sterilized material passes through the separation device 4 for gas-material separation. The separation device 4 includes multiple parallel cyclone separators, specifically two parallel cyclone separators, with a one-way valve provided between the two parallel cyclone separators. When the material is heavy, the operator can close the one-way valve and select one cyclone separator to perform gas-material separation; when the material is light, the operator can open the one-way valve and select two cyclone separators to perform gas-material separation.

[0018] The outlet of the separation device 4 in the present invention is connected to the storage device 7 through a second inclined pipe. The separated materials enter the storage device 7 and wait for use. The storage device 7 includes multiple parallel storage bins, specifically two parallel storage bins. A discharge valve is provided at the bottom of each storage bin. A one-way valve is provided between the two parallel storage bins. The operator can decide whether to open the one-way valve according to the amount of material.

[0019] The inlet of the air filter 5 in the present invention is connected to a fan 11 via a pipeline, which is used to continuously draw external air into the air filter 5 for filtration. The outlet of the air filter 5 is connected to the inlet of the four-way valve 8 via a pipeline. The first outlet of the four-way valve 8 is connected to the third inlet of the sterilization chamber 3 via a pipeline. The second outlet of the four-way valve 8 is connected to the first inclined pipe via a pipeline. The third outlet of the four-way valve 8 is connected to the condenser 9 via a pipeline. The outlet of the condenser 9 is connected to the steam-water separator 10 via a pipeline. The outlet of the steam-water separator 10 is connected to the second inlet of the separation device 4 via a pipeline. The filtered air is divided into three air flows under the suction of the fan 11. The first air flow is blown into the sterilization chamber 3, which sterilizes materials in batches. This part of the air is used to blow all the sterilized materials in this batch in the sterilization chamber 3 into the first inclined tube, so as not to affect the sterilization quality of the next batch of materials; the second air flow is blown into the inside of the first inclined tube to provide the first inclined tube with power to transport materials; the third air flow is blown into the condenser 9 for condensation, and after condensation, it enters the steam-water separator 10 to separate the cold air. The cold air is finally directly input into the separation device 4, so that the materials entering the separation device 4 are separated by gas and material and cooled.

[0020] The utility model also includes a control cabinet, which is connected to the vacuum feeding tank 1, the screw feeder 2, the sterilization chamber 3, the separation device 4, the air filter 5, the condenser 9, the steam-water separator 10, the fan 11, the steam generator 12 and the superheater 13 through lines; the control cabinet is used to provide the power required for the operation of the above-mentioned devices and set the operating time of each device.

[0021] The use process of this utility model is as follows:

[0022] During operation, steam generator 12 generates hot steam, which is further heated by superheater 13 before being piped into sterilization chamber 3. Simultaneously, material is delivered from feeder 6 through a sealed valve to sterilization chamber 3, where it is fully exposed to the superheated steam via agitators. Bacteria in the material are killed by the thermal effect of the high-speed superheated steam suspended in sterilization chamber 3. The sterilized material is then transported through a first inclined pipe to separation device 4 for gas-material separation.

[0023] At the same time, the air filter 5 continuously draws in and filters the outside air through the fan 11. The filtered air is divided into three air flows under the suction of the fan 11. The first air flow is blown into the sterilization chamber 3. The sterilization chamber 3 sterilizes the materials in batches. This part of the air is used to blow all the sterilized materials in this batch in the sterilization chamber 3 into the first inclined tube, and is purged once every 6 seconds so as not to affect the sterilization quality of the next batch of materials; the second air flow is blown into the inside of the first inclined tube to provide the first inclined tube with power to transport materials; the third air flow is blown into the condenser 9 for condensation, and after condensation, it enters the gas-water separator 10 to separate the cold air. The cold air is finally directly input into the separation device 4, so that the material entering the separation device 4 is also cooled while undergoing gas-material separation.

[0024] Finally, the separated and cooled material is transported to the storage device 7 through the second inclined pipe to wait for subsequent use.

[0025] Other undescribed parts of the present invention are the same as those in the prior art.

Claims

1. A high-temperature instantaneous sterilization device for Evodia rutaecarpa, characterized by It comprises a vacuum feeding tank (1), a screw feeder (2), a sterilization chamber (3), a separation device (4), an air filter (5), a four-way valve (8), a steam generator (12) and a superheater (13). A feeder (6) is provided below the bottom outlet of the vacuum feeding tank (1), the outlet of the screw feeder (2) extends into the interior of the feeder (6), the outlet of the feeder (6) is connected to the first inlet of the sterilization chamber (3) through a pipeline, the outlet of the steam generator (12) is connected to the inlet of the superheater (13) through a pipeline, the outlet of the superheater (13) is connected to the second inlet of the sterilization chamber (3) through a pipeline, and the outlet of the sterilization chamber (3) is connected to the separation device (4) through a first inclined pipe. ), the outlet of the separation device (4) is connected to the storage device (7) through a second inclined tube, the inlet of the air filter (5) is connected to the fan (11) through a pipeline, the outlet of the air filter (5) is connected to the inlet of the four-way valve (8) through a pipeline, the first outlet of the four-way valve (8) is connected to the third inlet of the sterilization chamber (3) through a pipeline, the second outlet of the four-way valve (8) is connected to the first inclined tube through a pipeline, the third outlet of the four-way valve (8) is connected to the condenser (9) through a pipeline, the outlet of the condenser (9) is connected to the steam-water separator (10) through a pipeline, and the outlet of the steam-water separator (10) is connected to the second inlet of the separation device (4) through a pipeline.

2. The high-temperature instantaneous sterilization equipment for Evodia rutaecarpa according to claim 1, characterized in that The separation device (4) comprises a plurality of cyclone separators connected in parallel.

3. The high temperature instantaneous sterilization equipment for Evodia rutaecarpa according to claim 1 is characterized in that The storage device (7) comprises a plurality of storage bins connected in parallel.

4. The high-temperature instantaneous sterilization equipment for Evodia rutaecarpa according to claim 1 is characterized in that A sealing valve is provided on the pipeline between the feeder (6) and the first inlet of the sterilization chamber (3).

5. The high temperature instantaneous sterilization equipment for Evodia rutaecarpa according to claim 1 is characterized in that A stirring shaft and stirring paddles are provided in the sterilization chamber (3), and the stirring paddles are evenly distributed on the stirring shaft.

6. The high-temperature instantaneous sterilization equipment for Evodia rutaecarpa according to claim 1 is characterized in that It also includes a control cabinet, which is connected to the vacuum feeding tank (1), the screw feeder (2), the sterilization chamber (3), the separation device (4), the air filter (5), the feeder (6), the condenser (9), the steam-water separator (10), the fan (11), the steam generator (12) and the superheater (13) through lines.