Electrode high-pressure reaction kettle with double windows

By setting a crushing box and a crushing motor in the electrode high-pressure reactor, the problem of difficult crushing of metal materials is solved, the contact area between the metal materials and the solution is increased, the dissolution speed is accelerated, and the dissolution efficiency is improved.

CN223312031UActive Publication Date: 2025-09-09ANHUI KEMI INSTR CO LTD
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Patent Information

Application Number
CN202422770419.7
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-11-14
Publication Date
2025-09-09
Estimated Expiration
2034-11-14

AI Technical Summary

Technical Problem

Existing electrode high-pressure reactors have difficulty in breaking metal materials into a size that is convenient for dissolution, resulting in a less than ideal dissolution rate.

Method used

A crushing box and a crushing motor are set in the reactor. The metal material is pre-processed by a crushing knife and cut into a certain size to increase the contact area with the solution. A sealing structure is used to improve the sealing and stability of the reactor.

Benefits of technology

By pre-treating the metal material, the contact area between the metal material and the solution is increased, which significantly accelerates the dissolution rate and improves the dissolution efficiency.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to a double-window electrode high-pressure reaction kettle in the technical field of electrode high-pressure reaction kettles, which comprises a reaction kettle body, and the upper end of the reaction kettle body is fixedly connected with a pair of transparent plates; when the reaction kettle is used, a metal material is put into the crushing box, then the base is pushed to drive the crushing box to enter the reaction kettle body together, then the crushing motor is started, the metal material is cut up through the crushing cutter, the cut-up material penetrates through the filter plate and the conveying hole and falls on the inner bottom wall of the reaction kettle body, and after crushing is completed, the metal material is discharged out of the reaction kettle body. When the reaction kettle is used, the crushing box is moved out of the reaction kettle body, a solution is added into the reaction kettle body, the crushed material is dissolved under the action of the electrode and the solution, and personnel can observe the dissolving process through the transparent plate, so that when the reaction kettle is used, the metal material can be pretreated and cut into a certain size; the contact area with a solution is increased, and the dissolving speed is accelerated.
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Description

Technical Field

[0001] The utility model relates to an electrode high-pressure reactor with double windows, and in particular to an electrode high-pressure reactor with double windows used in the field of electrode high-pressure reactors. Background Art

[0002] Electrode high-pressure reactor is a kind of mechanical equipment. When in use, the electrode high-pressure reactor promotes chemical reactions by providing a high-temperature and high-pressure environment. It shows its superiority especially when dealing with flammable, explosive and toxic media.

[0003] The specification of Chinese patent CN208574597U discloses an electrochemical high-pressure reactor, which includes a reactor body, a reactor cover, and a stirring device. The reactor body is also provided with a cathode and an anode for the electrochemical reaction. To increase the electrochemical reaction rate, there are more than one cathode and anode, which are arranged in an alternating pattern and powered by a pulsed power supply to reduce electrode reactivity. The electrochemical high-pressure reactor can be used for both anode metal dissolution reactions and cathode deposition reactions.

[0004] The above reactor mainly relies on the action of electrodes and solution to dissolve metal materials when processing them. Since there is no mechanism for crushing the metal materials, it is difficult to crush the metal materials into a size that is easy to dissolve, which makes its dissolution rate less than ideal. Utility Model Content

[0005] In view of the above-mentioned prior art, the technical problem to be solved by the present invention is that the existing electrode high-pressure reactor is difficult to crush the metal material into a size that is convenient for dissolution, thereby making its dissolution rate less than ideal.

[0006] The top end of the support frame is provided with a threaded groove, and the inner thread of the threaded groove is connected to the threaded ring. The upper end of the threaded ring is fixedly connected to the crushing box, and the inner thread of the crushing box is connected to the sealing cover. The inner end of the upper end of the sealing cover is fixedly connected to the crushing motor, and the output end of the crushing motor is fixedly connected to the vertical pipe. The outer end of the vertical pipe is fixedly connected to a plurality of crushing knives. A feeding hole is provided on the sealing cover, a filter plate is fixedly connected to the inner wall of the crushing box, and a conveying hole is provided on the base. One end of the crushing box close to the reactor body is fixedly connected to a rectangular plate, and the side end of the reactor body is provided with a rectangular groove movably inserted with the rectangular plate. One end of the base away from the rectangular plate is fixedly connected to a limiting tube, and the inner thread of the limiting tube is connected to a moving tube. The upper end of the support plate is provided with a pair of limiting grooves movably inserted with the moving tube.

[0007] In the above-mentioned double-window electrode high-pressure reactor, the contact area between the metal material and the solution can be increased, thereby improving the dissolution efficiency.

[0008] As a further improvement of the present application, the outer end of the rectangular plate is fixedly connected to a sealing frame, and the outer end of the sealing frame is tightly fitted with the inner wall of the rectangular groove.

[0009] As a further improvement of the present application, the conveying hole is connected to the outer end of the crushing box, a pair of sliders are fixedly connected to the lower end of the base and the sealing frame respectively, and a pair of sliding grooves are opened at the upper end of the support plate.

[0010] As a further improvement of the present application, a pair of fixed grooves are provided at the upper end of the sealing cover, and fixed blocks are fixedly connected to the inner bottom surfaces of the fixed grooves.

[0011] As another improvement of the present application, a sponge board is placed on the upper end of the transparent plate, the upper end of the sponge board is fixedly connected to a movable frame, the lower end of the movable frame is fixedly connected to a plug-in tube, and a pair of plug-in slots rotatably connected to the plug-in tube are opened at the upper end of the reactor body.

[0012] In summary, when the reactor is in use, it can pre-treat the metal material, cut it into a certain size, increase its contact area with the solution, accelerate the dissolution speed, and improve the dissolution efficiency. BRIEF DESCRIPTION OF THE DRAWINGS

[0013] Figure 1 Schematic diagram of the overall structure of the first and second embodiments of the present application;

[0014] Figure 2 Schematic diagram of the rectangular plate and the rectangular plate structure of the first embodiment and the second embodiment of the present application;

[0015] Figure 3 For this application Figure 2 A partial enlarged schematic diagram in the middle;

[0016] Figure 4 For this application Figure 2 A partial enlarged schematic diagram of point B in the middle;

[0017] Figure 5 For this application Figure 2 A partial enlarged schematic diagram of point C in the middle;

[0018] Figure 6 This is a schematic diagram of the crushing box movement according to the first embodiment of the present application;

[0019] Figure 7 This is a schematic diagram of the cross-sectional structure of the crushing box of the first embodiment of this application.

[0020] Description of the numbers in the figure:

[0021] 1. Reactor body; 2. Transparent plate; 3. Support plate; 4. Base; 5. Threaded ring; 6. Conveying hole; 7. Crushing box; 8. Sealing cover; 9. Crushing motor; 10. Vertical pipe; 11. Crushing knife; 12. Feeding hole; 13. Filter plate; 14. Rectangular plate; 15. Rectangular groove; 16. Limiting tube; 17. Moving tube; 18. Limiting groove; 19. Sealing frame; 20. Slider; 21. Slide; 22. Fixed block; 23. Sponge plate; 24. Moving frame; 25. Plug-in tube. DETAILED DESCRIPTION

[0022] Two implementation modes of the present application are described in detail below with reference to the accompanying drawings.

[0023] The first implementation method:

[0024] Figure 1-7 The invention discloses a double-window electrode high-pressure reactor, comprising a reactor body 1, wherein a pair of transparent plates 2 are fixedly connected to the upper end of the reactor body 1. When in use, since there is no light source in the reactor body 1 and the sight is dark, one of the transparent plates 2 can be used to provide illumination, and the other transparent plate 2 can be used to facilitate personnel to view the interior of the reactor body 1. A support plate 3 is fixedly connected to the side end of the reactor body 1, and a base 4 is placed on the upper end of the support plate 3. A threaded groove is provided on the upper end of the base 4, and a threaded ring 5 is connected to the inner thread of the threaded groove. A crushing box 7 is fixedly connected to the upper end of the threaded ring 5. The threaded ring 5 is used to facilitate personnel to remove the crushing box 7 from the base 4 for cleaning. A sealing cover 8 is connected to the inner thread of the crushing box 7, and the inner end of the sealing cover 8 is fixedly connected to the inner thread of the sealing cover 8. Crushing motor 9. Those skilled in the art can make the best choice of the model of crushing motor 9, such as model Y80M1-2. A vertical pipe 10 is fixedly connected to the output end of the crushing motor 9, and a plurality of crushing knives 11 are fixedly connected to the outer end of the vertical pipe 10. A feeding hole 12 is provided on the sealing cover 8. A filter plate 13 is fixedly connected to the inner wall of the crushing box 7. A conveying hole 6 is provided on the base 4. The end of the crushing box 7 close to the reactor body 1 is fixedly connected to a rectangular plate 14. A rectangular groove 15 movably inserted with the rectangular plate 14 is provided at the side end of the reactor body 1. A limiting tube 16 is fixedly connected to the end of the base 4 away from the rectangular plate 14. The internal thread of the limiting tube 16 is connected to a moving tube 17. The upper end of the support plate 3 is provided with a pair of limiting grooves 18 movably inserted with the moving tube 17.

[0025] The outer end of the rectangular plate 14 is fixedly connected to a sealing frame 19. The sealing frame 19 can be used to improve the sealing of the rectangular plate 14 in the rectangular groove 15. The outer end of the sealing frame 19 fits tightly against the inner wall of the rectangular groove 15. The conveying hole 6 is connected to the outer end of the crushing box 7. The upper end of the support plate 3 is provided with a pair of slide grooves 21. The lower ends of the base 4 and the sealing frame 19 are fixedly connected with a pair of sliders 20 that are slidably connected to the slide grooves 21. The sliders 20 can improve the stability of the base 4 and the sealing frame 19, making it difficult to move up. A pair of fixed grooves are provided at the upper end of the sealing cover 8. A fixed block 22 is fixedly connected to the inner bottom surface of the fixed groove. The upper end of the fixed block 22 is flush with the upper end of the fixed groove. When in use, the fixed block 22 is held by hand to facilitate personnel to manually remove the sealing cover 8 from the crushing box 7.

[0026] When processing metal materials and dissolving them, the sealing cover 8 needs to be taken out from the crushing box 7. After taking it out, the metal materials are put into the crushing box 7 and fall on the filter plate 13. Then the sealing cover 8 is reset to seal the materials in the crushing box 7. Then the movable tube 17 is manually rotated to remove the lower end of the movable tube 17 from the limiting groove 18. Then, force is applied to the base 4, the crushing box 7 and the rectangular plate 14 so that the above three pass through the rectangular groove 15 and enter the reactor body 1 (combined with the above). Figure 6 As shown), then manually rotate the movable tube 17 so that its lower end is inserted into the corresponding limiting groove 18 to fix the limiting tube 16, thereby fixing the crushing box 7 in the reactor body 1;

[0027] After the crushing box 7 is pushed into the reactor body 1, the crushing motor 9 needs to be started so that its output end drives the vertical pipe 10 and the crushing knife 11 to rotate in the crushing box 7 to crush the metal material. After the metal material is cut into a certain size, the material will pass through the filter plate 13 and the conveying hole 6 and fall onto the inner bottom surface of the reactor body 1;

[0028] After pre-treating the metal material, the lower end of the movable tube 17 needs to be manually removed from the limiting groove 18, and then the limiting tube 16 is pulled to drive the base 4 to move out of the reactor body 1. The rectangular groove 15 is sealed with the sealing frame 19 and the rectangular plate 14 to improve the sealing of the reactor body 1. Finally, the solution is poured into the reactor body 1 from the upper end thereof, and the metal material is dissolved under the action of the electrodes and the solution.

[0029] In summary, when the reactor is in use, it can pre-treat the metal material, cut it into a certain size, increase its contact area with the solution, accelerate the dissolution speed, and improve the dissolution efficiency.

[0030] Second implementation method:

[0031] This embodiment adds the following structure based on the first embodiment, and the rest of the structure remains the same as the first embodiment, as follows:

[0032] Figure 2 It is shown that a sponge plate 23 is placed on the upper end of the transparent plate 2, a movable frame 24 is fixedly connected to the upper end of the sponge plate 23, and a plug-in tube 25 is fixedly connected to the lower end of the movable frame 24. A pair of plug-in slots rotatably connected to the plug-in tube 25 are opened at the upper end of the reactor body 1.

[0033] When the reactor body 1 is not in use, the sponge plate 23 needs to be covered on the transparent plate 2 to prevent dust and foreign matter from adhering to the transparent plate 2. When the reactor body 1 is in use and the interior of the reactor body 1 needs to be observed through the transparent plate 2, the plug-in tube 25 needs to be rotated to drive the sponge plate 23 and the movable frame 24 to move away from the transparent plate 2 (combined with Figure 2 As shown), personnel can view the interior of the reactor body 1 through the transparent plate 2. After use, the sponge plate 23 can be moved and repeatedly moved on the transparent plate 2 to wipe off foreign matter adhering to the transparent plate 2. Finally, the sponge plate 23 is covered on the transparent plate 2 again to protect it.

[0034] In view of current actual needs, the protection scope of the above-mentioned implementation mode adopted in this application is not limited to this. Various changes made within the knowledge scope of technical personnel in this field without departing from the concept of this application still fall within the protection scope of this utility model.

Claims

1. A double-window electrode high-pressure reactor, comprising a reactor body (1), characterized in that: A pair of transparent plates (2) are fixedly connected to the upper end of the reactor body (1), a support plate (3) is fixedly connected to the side end of the reactor body (1), a base (4) is placed on the upper end of the support plate (3), a thread groove is provided on the upper end of the base (4), a threaded ring (5) is connected to the inner thread of the thread groove, a crushing box (7) is fixedly connected to the upper end of the threaded ring (5), a sealing cover (8) is fixedly connected to the inner thread of the crushing box (7), and a crushing motor (9) is fixedly connected to the inner part of the upper end of the sealing cover (8). A vertical pipe (10) is fixedly connected to the output end of the crushing motor (9), a plurality of crushing knives (11) are fixedly connected to the outer end of the vertical pipe (10), a feed hole (12) is provided on the sealing cover (8), a filter plate (13) is fixedly connected to the inner wall of the crushing box (7), a conveying hole (6) is provided on the base (4), a rectangular plate (14) is fixedly connected to one end of the crushing box (7) close to the reactor body (1), and a rectangular groove (15) is provided on the side end of the reactor body (1) for movably inserting with the rectangular plate (14); One end of the base (4) away from the rectangular plate (14) is fixedly connected to a limiting tube (16), the internal thread of the limiting tube (16) is connected to a movable tube (17), and the upper end of the support plate (3) is provided with a pair of limiting grooves (18) movably inserted into the movable tube (17).

2. The double-window electrode high-pressure reactor according to claim 1, characterized in that: The outer end of the rectangular plate (14) is fixedly connected to a sealing frame (19), and the outer end of the sealing frame (19) is tightly fitted with the inner wall of the rectangular groove (15).

3. The double-window electrode high-pressure reactor according to claim 2, characterized in that: The conveying hole (6) is connected to the outer end of the crushing box (7), a pair of slide grooves (21) are provided at the upper end of the support plate (3), and a pair of sliders (20) slidably connected to the slide grooves (21) are fixedly connected to the lower ends of the base (4) and the sealing frame (19).

4. The double-window electrode high-pressure reactor according to claim 3, characterized in that: A pair of fixed grooves are formed at the upper end of the sealing cover (8), and a fixed block (22) is fixedly connected to the inner bottom surface of the fixed groove.

5. The double-window electrode high-pressure reactor according to claim 4, characterized in that: A sponge plate (23) is placed on the upper end of the transparent plate (2), the upper end of the sponge plate (23) is fixedly connected to a movable frame (24), the lower end of the movable frame (24) is fixedly connected to a plug-in tube (25), and the upper end of the reactor body (1) is provided with a pair of plug-in slots rotatably connected to the plug-in tube (25).

Citation Information

Patent Citations

  • Electrochemistry high -pressure batch autoclave

    CN208574597U