Quantitative detection reaction device based on air pressure measurement
By designing the plug and liquid hole structure in the reaction bottle, the problem of reduced detection sensitivity caused by improper injection of hydrogen peroxide in a closed reaction bottle was solved, and rapid and accurate detection of the barometer was achieved.
Patent Information
- Application Number
- CN202422286009.5
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-19
- Publication Date
- 2025-09-30
- Estimated Expiration
- 2034-09-19
AI Technical Summary
In a closed reaction bottle, improper injection of hydrogen peroxide leads to reduced sensitivity of the barometer detection and inaccurate quantitative detection.
A quantitative detection reaction device was designed, which included a reaction bottle, an inner bottle cap, a bottle stopper, an inner bottle plate, and a plug. The liquid hole was blocked by the plug, and the target content was quickly detected using a barometer to ensure the sealing and accuracy of the reaction between hydrogen peroxide and platinum nanoparticles.
The barometer can quickly, sensitively and accurately quantitatively detect the target content, ensuring the sealing of the detection process and the controllability of the reaction.
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Figure CN223393411U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of reaction devices, in particular to a quantitative detection reaction device based on air pressure measurement. Background Art
[0002] If the target content to be detected in the closed reaction bottle is different, it will cause air pressure of different intensities. Then, a linear quantitative detection relationship can be established by accurately measuring the air pressure value in the reaction bottle, thereby accurately detecting the target content. For example, platinum nanoparticles can catalyze hydrogen peroxide to produce oxygen, thereby producing an air pressure value reading. Therefore, when the platinum nanoparticle content increases with the target content, the air pressure value in the detection reaction bottle will also increase linearly, thereby achieving quantitative detection of the target. However, when a needle-type syringe is used to inject hydrogen peroxide in a closed reaction bottle system, as long as hydrogen peroxide is injected into the reaction bottle a little, oxygen will immediately be generated in the bottle to generate air pressure, which will cause the remaining hydrogen peroxide to be unable to be injected into it. However, if the amount of hydrogen peroxide added is not enough, then one is that it cannot guarantee that enough oxygen will be produced to be detected by the barometer, and the second is that the speed of oxygen generation slows down, which will all lead to reduced detection sensitivity and inaccurate quantitative detection. Summary of the Invention
[0003] To this end, the present invention provides a quantitative detection reaction device based on air pressure measurement to solve the above-mentioned problems in the prior art.
[0004] In order to achieve the above purpose, the present invention provides the following technical solutions:
[0005] According to the first aspect of the present invention, a quantitative detection reaction device based on air pressure measurement includes a reaction bottle, an inner bottle cap, a bottle stopper, a bottle inner plate and a stopper column. The inner bottle cap is inserted on the reaction bottle. The bottle inner plate is provided in the reaction bottle. A liquid hole is provided on the bottle inner plate. The stopper column is connected to the inner bottle cap, the bottle stopper is provided in the inner bottle cap, and the stopper column is used to seal the liquid hole.
[0006] Furthermore, it also includes a rubber ring, which is covered on the inner bottle cap and located above the bottle stopper.
[0007] Furthermore, it also includes an outer bottle cap, which is detachably connected to the reaction bottle, and the inner bottle cap, bottle stopper, and bottle inner plate are all located in the structure after the outer bottle cap is connected to the reaction bottle.
[0008] Furthermore, the inner bottle cap includes an inner cap body and a connecting rod. The inner cap body is inserted into the reaction bottle, and the stopper is connected to the inner cap body through the connecting rod.
[0009] Furthermore, the inner bottle cap also includes an inner cap baffle, and the inner cap baffle is connected to a side of the inner cap body facing away from the connecting rod, and the inner cap baffle abuts against the upper end of the reaction bottle.
[0010] Furthermore, the rubber ring includes a rubber pad and a sealing ring. The rubber pad is arranged on the surface of the inner cover baffle, and the sealing ring is arranged on the surface of the rubber ring. The axis of the sealing ring is collinear with the axis of the liquid hole.
[0011] Furthermore, the rubber ring also includes an outer rubber ring, which is arranged on the surface of the rubber pad and located at the outer periphery of the sealing ring, and the rubber pad is connected to the inner bottle cap through the outer rubber ring.
[0012] Furthermore, the reaction bottle includes a bottle body, a transition part and a bottleneck. The bottleneck is connected to the bottle body through the transition part. The inner plate of the bottle is installed in the bottleneck. The inner cover body is inserted on the bottleneck. The connecting rod and the plug are both located in the bottleneck.
[0013] Furthermore, the upper surface of the bottle inner plate is inclined from the periphery toward the liquid through hole.
[0014] Furthermore, the plug is shaped like a truncated cone.
[0015] The utility model has the following advantages: through the coordinated arrangement of the plug column, the liquid hole, the bottle inner plate, the inner bottle cover and the bottle plug, the barometer can quickly, sensitively and accurately realize the quantitative detection of the content of the target substance, and the setting of the bottle plug can ensure the sealing of the entire detection process. BRIEF DESCRIPTION OF THE DRAWINGS
[0016] To more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the following briefly introduces the drawings required for the embodiments or the description of the prior art. Obviously, the drawings described below are merely illustrative, and those skilled in the art can, without inventive effort, derive other implementation drawings based on the provided drawings.
[0017] The structures, proportions, sizes, etc. illustrated in this specification are intended solely to complement the contents disclosed herein and to facilitate understanding and reading by persons familiar with the art. They are not intended to limit the conditions under which the present invention may be implemented and therefore have no substantive technical significance. Any structural modifications, changes in proportions, or adjustments in size, without affecting the efficacy and objectives of the present invention, shall remain within the scope of the technical contents disclosed herein.
[0018] Figure 1 、 one An exploded diagram of a quantitative detection reaction device based on gas pressure measurement;
[0019] Figure 2 、 one A front view of a quantitative detection reaction device based on air pressure measurement;
[0020] Figure 3 、 oneA cross-sectional view of a front view of a quantitative detection reaction device based on gas pressure measurement;
[0021] Figure 4 、 one A cross-sectional view of a reaction bottle of a quantitative detection reaction device based on gas pressure measurement;
[0022] Figure 5 、 one A three-dimensional diagram of the inner bottle cap of a quantitative detection reaction device based on air pressure measurement;
[0023] Figure 6 、 one A three-dimensional diagram of a rubber ring of a quantitative detection reaction device based on air pressure measurement;
[0024] Figure 7 、 one A three-dimensional diagram of an outer bottle cap of a quantitative detection reaction device based on air pressure measurement;
[0025] In the figure: 1. reaction bottle, 11. bottle body, 12. transition part, 14. bottleneck, 2. inner bottle cap, 21. inner cap body, 22. inner cap baffle, 23. connecting rod, 3. rubber ring, 31. rubber pad, 32. outer rubber ring, 33. sealing ring, 4. outer bottle cap, 41. outer cap body, 42. inner ring groove, 43. outer cap connecting part, 5. bottle stopper, 6. stopper column, 7. bottle inner plate, 71. liquid hole. DETAILED DESCRIPTION
[0026] The following describes the implementation of the present invention through specific embodiments. Those skilled in the art can readily understand the other advantages and benefits of the present invention from the contents disclosed in this specification. Obviously, the embodiments described are only a portion of the embodiments of the present invention, not all of them. All other embodiments derived by persons of ordinary skill in the art based on the embodiments of the present invention without inventive effort are also within the scope of protection of the present invention.
[0027] like Figures 1 to 7 As shown, a quantitative detection reaction device based on air pressure measurement in the embodiment of the first aspect of the present invention includes a reaction bottle 1, an inner bottle cap 2, a bottle stopper 5, a bottle inner plate 7 and a plug column 6. The inner bottle cap 2 is inserted on the reaction bottle 1. The reaction bottle 1 is provided with a bottle inner plate 7. The bottle inner plate 7 is provided with a liquid hole 71. The plug column 6 is connected to the inner bottle cap 2. The bottle stopper 5 is provided in the inner bottle cap 2. The plug column 6 is used to seal the liquid hole 71.
[0028] In the above embodiment, it should be noted that the bottle stopper 5 is made of a material that can withstand the reducing properties of hydrogen peroxide, the inner bottle cap 2 is connected to the reaction bottle 1 by a threaded connection, platinum nanoparticles are stored in the reaction bottle 1, and hydrogen peroxide is stored between the bottle inner plate 7 and the inner bottle cap 2. At this time, the inner bottle cap 2 is in a tightened state, and the plug 6 blocks the liquid hole 71 to separate hydrogen peroxide from the platinum catalyst. When the target content needs to be detected, the inner bottle cap 2 is rotated in the opposite direction to drive the plug 6 to disengage from the liquid hole 71, and hydrogen peroxide falls into the reaction bottle 7 due to gravity. At this time, the sensor head of the barometer pierces the bottle stopper 5 to perform pressure detection, ensuring that a sufficient amount of hydrogen peroxide reacts quickly with the platinum nanoparticles, so that the barometer can quickly, sensitively and accurately achieve quantitative detection of the target content.
[0029] The technical effect achieved by the above embodiment is: through the coordinated arrangement of the plug 6, the liquid hole 71, the bottle inner plate 7, the inner bottle cap 2 and the bottle plug 5, the barometer can quickly, sensitively and accurately realize the quantitative detection of the content of the target substance. The arrangement of the bottle plug 5 can ensure the sealing of the entire detection process and at the same time ensure the sealing of the entire device for storing hydrogen peroxide and platinum nanoparticles when no detection is required.
[0030] Optional, such as Figures 1 to 7 As shown, in some embodiments, a rubber ring 3 is further included, which is covered on the inner bottle cap 2 and located above the bottle stopper 5.
[0031] In the above optional embodiment, it should be noted that the upper surface of the bottle stopper 5 abuts against the lower surface of the rubber ring 3 .
[0032] The beneficial effect of the above optional embodiment is that when the content of the target substance needs to be quantitatively detected, the sensor head of the barometer passes through the rubber ring 3 and then pierces the bottle stopper 5, which can further ensure that the entire detection process is carried out in a sealed environment.
[0033] Optional, such as Figures 1 to 7 As shown, in some embodiments, it also includes an outer bottle cap 4, which is detachably connected to the reaction bottle 1, and the inner bottle cap 2, the bottle stopper 5, and the bottle inner plate 7 are all located in the structure after the outer bottle cap 4 is connected to the reaction bottle 1.
[0034] In the above optional embodiment, it should be noted that the outer bottle cap 4 includes an outer cover body 41 and an outer cover connecting portion 43, the connecting portion 42 and the outer cover body 41 are integrally formed, an inner ring groove 42 is provided on the inner side of the connecting portion 42, and the outer cover body 42 is connected to the reaction bottle 1 by a threaded connection.
[0035] The beneficial effect of the above optional embodiment is that the convenience of carrying the device is ensured by the provision of the outer bottle cap 4, and the risk of accidentally puncturing the bottle cork 5 when carrying it is avoided.
[0036] Optional, such as Figures 1 to 7 As shown, in some embodiments, the inner bottle cap 2 includes an inner cap body 21 and a connecting rod 23 . The inner cap body 21 is inserted into the reaction bottle 1 , and the plug 6 is connected to the inner cap body 21 through the connecting rod 23 .
[0037] The inner bottle cap 2 further includes an inner cap baffle 22 . The inner cap baffle 22 is connected to a side of the inner cap body 21 facing away from the connecting rod 23 . The inner cap baffle 22 abuts against the upper end of the reaction bottle 1 .
[0038] In the above optional embodiment, it should be noted that there are multiple connecting rods 23, and the multiple connecting rods 23 are arranged in a circular array between the inner cover body 21 and the plug column 6, and the inner cover body 21 is threadedly connected to the reaction bottle 1.
[0039] The beneficial effects of the above optional embodiments are: the setting of the connecting rod 23 ensures the reliability of the connection between the inner cover body 21 and the plug 6, and the setting of the inner cover baffle 22 can prevent the inner bottle cover 2 from falling into the reaction bottle 1 due to improper force.
[0040] Optional, such as Figures 1 to 7 As shown, in some embodiments, the rubber ring 3 includes a rubber pad 31 and a sealing ring 33. The rubber pad 31 is disposed on the surface of the inner cap baffle 22, and the sealing ring 33 is disposed on the surface of the rubber ring 3. The axis of the sealing ring 33 is collinear with the axis of the liquid passage hole 71. The rubber ring 3 also includes an outer rubber ring 32, which is disposed on the surface of the rubber pad 31 and is located on the outer periphery of the sealing ring 33. The rubber pad is connected to the inner bottle cap 2 via the outer rubber ring 32.
[0041] In the above optional embodiment, it should be noted that the inner diameter of the sealing ring 33 is slightly smaller than the diameter of the barometer's sensing head. During detection, the barometer's sensing head and the sealing ring 33 are in a completely sealed state.
[0042] The outer rubber ring 32 is connected to the inner bottle cap 2 by means of a snap connection or an interference fit connection.
[0043] The beneficial effect of the above optional embodiment is that the sealing performance of the entire device is further ensured by the arrangement of the sealing ring 33 and the outer rubber ring 32 .
[0044] Optional, such as Figures 1 to 7 As shown, in some embodiments, the reaction bottle 1 includes a bottle body 11, a transition portion 12 and a bottleneck 14. The bottleneck 14 is connected to the bottle body 11 through the transition portion 12. The bottle inner plate 7 is installed in the bottleneck 14. The inner cover body 21 is inserted on the bottleneck 14. The connecting rod 23 and the plug 6 are both located in the bottleneck 14.
[0045] In the above optional embodiment, it should be noted that the inner cover body 21 is connected to the bottleneck 14 by means of a threaded connection, and the inner cover baffle 22 abuts against the end of the bottleneck 14 away from the transition portion 12 .
[0046] Specifically, the outer rubber ring 32 is connected to the inner cover body 21 by means of snap connection or interference fit, and the rubber pad 31 is attached to the upper surface of the inner cover baffle 22 .
[0047] The beneficial effect of the above optional embodiment is that the separation of hydrogen peroxide and platinum nanoparticles is more accurately achieved by installing the bottle inner plate 7 in the bottle neck 14.
[0048] Optional, such as Figures 1 to 7 As shown, in some embodiments, the upper surface of the bottle inner plate 7 is inclined from the periphery toward the liquid hole 31.
[0049] In the above optional embodiment, it should be noted that the cross-sectional shape of the bottle inner plate 7 is formed by combining two opposite right-angled trapezoids.
[0050] Optional, such as Figures 1 to 7 As shown, in some embodiments, the plug 6 is truncated cone-shaped.
[0051] In the above optional embodiment, it should be noted that the plug 6 is made of rubber or silicone and the upper surface of the bottle inner plate 7 is inclined from the periphery toward the liquid hole 31, so that when hydrogen peroxide is required to react with platinum nanoparticles, hydrogen peroxide can quickly flow through the liquid hole 31 into the bottle body 11 of the reaction bottle 1.
[0052] The beneficial effect of the above optional embodiment is that the truncated cone shape of the plug 6 can ensure the sealing effect of the plug 6 on the liquid hole 71 while indirectly achieving controllable speed and flow rate of hydrogen peroxide flowing into the bottle body 11.
[0053] Although the present invention has been described in detail above using general descriptions and specific embodiments, it will be apparent to those skilled in the art that modifications or improvements may be made to the present invention. Therefore, such modifications or improvements, without departing from the spirit of the present invention, are within the scope of protection claimed herein.
[0054] The terms "upper", "lower", "left", "right", "middle", etc. used in this specification are only for the convenience of description and are not intended to limit the scope of implementation of the present invention. Changes or adjustments to their relative relationships should be considered as the scope of implementation of the present invention without substantially changing the technical content.
Claims
1. A quantitative detection reaction device based on air pressure measurement, characterized in that: The invention comprises a reaction bottle (1), an inner bottle cap (2), a bottle stopper (5), a bottle inner plate (7) and a stopper column (6), wherein the inner bottle cap (2) is inserted into the reaction bottle (1), the bottle inner plate (7) is arranged in the reaction bottle (1), a liquid passage hole (71) is provided on the bottle inner plate (7), the stopper column (6) is connected to the inner bottle cap (2), the bottle stopper (5) is arranged in the inner bottle cap (2), and the stopper column (6) is used to block the liquid passage hole (71).
2. A quantitative detection reaction device based on air pressure measurement according to claim 1, characterized in that: It also includes a rubber ring (3), which is covered on the inner bottle cap (2), and the rubber ring (3) is located above the bottle stopper (5).
3. The quantitative detection reaction device based on air pressure measurement according to claim 1, characterized in that: The invention also includes an outer bottle cap (4), which is detachably connected to the reaction bottle (1); and the inner bottle cap (2), the bottle stopper (5), and the bottle inner plate (7) are all located in the structure after the outer bottle cap (4) is connected to the reaction bottle (1).
4. The quantitative detection reaction device based on air pressure measurement according to claim 1, characterized in that: The inner bottle cap (2) comprises an inner cap body (21) and a connecting rod (23); the inner cap body (21) is inserted into the reaction bottle (1); and the plug (6) is connected to the inner cap body (21) via the connecting rod (23).
5. The quantitative detection reaction device based on air pressure measurement according to claim 4, characterized in that: The inner bottle cap (2) further comprises an inner cap baffle (22), and a side of the inner cap body (21) facing away from the connecting rod (23) is connected to the inner cap baffle (22), and the inner cap baffle (22) abuts against the upper end of the reaction bottle (1).
6. The quantitative detection reaction device based on air pressure measurement according to claim 2, characterized in that: The rubber ring (3) comprises a rubber pad (31) and a sealing ring (33), wherein the rubber pad (31) is arranged on the surface of the inner cover baffle (22), and the sealing ring (33) is arranged on the surface of the rubber ring (3), and the axis of the sealing ring (33) is collinear with the axis of the liquid hole (71).
7. The quantitative detection reaction device based on air pressure measurement according to claim 6, characterized in that: The rubber ring (3) further comprises an outer rubber ring (32), wherein the outer rubber ring (32) is arranged on the surface of the rubber pad (31) and is located on the outer periphery of the sealing ring (33), and the rubber pad is connected to the inner bottle cap (2) via the outer rubber ring (32).
8. The quantitative detection reaction device based on air pressure measurement according to claim 4, characterized in that: The reaction bottle (1) comprises a bottle body (11), a transition portion (12) and a bottleneck (14); the bottleneck (14) is connected to the bottle body (11) via the transition portion (12); the bottle inner plate (7) is installed in the bottleneck (14); the inner cover (21) is inserted into the bottleneck (14); and the connecting rod (23) and the plug (6) are both located in the bottleneck (14).
9. The quantitative detection reaction device based on air pressure measurement according to claim 1, characterized in that: The upper surface of the bottle inner plate (7) is inclined from the periphery toward the liquid passage hole (71).
10. The quantitative detection reaction device based on air pressure measurement according to claim 1, characterized in that: The plug (6) is shaped like a truncated cone.