Germanium ingot placing rack

By designing a germanium ingot placement rack and using a support frame to support the germanium ingots in a tilted and suspended position, the problems of low efficiency and pure water residue in the nitrogen drying operation of germanium ingots were solved, achieving a highly efficient and thorough drying effect.

CN223470472UActive Publication Date: 2025-10-24安徽光智科技有限公司
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Patent Information

Application Number
CN202422560253.6
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-10-22
Publication Date
2025-10-24
Estimated Expiration
2034-10-22

AI Technical Summary

Technical Problem

The existing technology for drying germanium ingots with nitrogen has low efficiency and suffers from problems such as residual pure water and contamination from impurities caused by changes in posture.

Method used

Design a germanium ingot placement rack, including a support frame, a base plate, a high bar assembly, and a low bar assembly. The germanium ingot is supported by a first low support bar, a second low support bar, and a high support bar, achieving tilted and suspended positioning of the germanium ingot, avoiding changes in posture during handheld operation, and using unidirectional nitrogen blowing for drying.

Benefits of technology

This method improves the efficiency of nitrogen drying of germanium ingots, avoids pure water residue and impurity contamination, and achieves thorough drying of germanium ingots.

✦ Generated by Eureka AI based on patent content.

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Abstract

The germanium ingot placing frame comprises a supporting frame, and the supporting frame comprises a bottom plate, a high bar assembly and a low bar assembly; the high bar assembly comprises a high supporting bar, and the high bar assembly is fixed to the bottom plate so that the high supporting bar can be suspended above the bottom plate; the low bar assembly comprises a first low supporting bar and a second low supporting bar, the low bar assembly is fixed to the bottom plate so that the first low supporting bar and the second low supporting bar can be suspended above the bottom plate, the first low supporting bar, the second low supporting bar and the high supporting bar are spaced from one another in the left-right direction and are parallel to one another, and the first low supporting bar is higher than the second low supporting bar; the high support lever is higher than the second low support lever; the first low support lever, the second low support lever and the high support lever are used together for supporting the bottom surface of the germanium ingot by the second low support lever and the high support lever, and the first low support lever is propped against and supports the end surface of the germanium ingot, so that the germanium ingot is obliquely suspended and supported relative to the bottom plate and is positioned on the first low support lever, the second low support lever and the high support lever; and carrying out nitrogen blow-drying operation.
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Description

TECHNICAL FIELD

[0001] The present disclosure relates to the field of germanium materials, and more particularly to a germanium ingot placing rack. BACKGROUND

[0002] Before high-purity germanium polycrystalline zone melting and single crystal pulling, the raw material germanium ingot needs to be subjected to etching treatment. For example, Chinese patent document CN113718257A published on November 30, 2021, wherein the etched germanium ingot is placed in a pure water tank for repeated rinsing and nitrogen blowing.

[0003] The nitrogen blowing process is as follows: the operator wears a hundred-level clean glove on both hands, holds the germanium ingot rinsed with pure water with one hand, and holds a nitrogen gun with the other hand, and blows dry the germanium ingot in a hundred-level clean table.

[0004] This hand-held nitrogen blowing causes the hand-held part of the germanium ingot to be unable to be directly blown dry, and requires the previously hand-held part to be blown dry after the germanium ingot is blown dry except for the hand-held part, which causes inconvenience and reduces efficiency.

[0005] In addition, since the hand-held nitrogen blowing is adopted, the operator needs to change the posture of the hand holding the germanium ingot to blow dry the germanium ingot without dead angles, which reduces the operation efficiency, and the residual pure water on the surface of the germanium ingot may flow back under the impact of nitrogen due to the change of the posture, increasing the probability of residual pure water on the germanium ingot.

[0006] In addition, even if the operator wears a hundred-level clean glove on both hands, impurities from the hundred-level clean glove may be left on the surface of the germanium ingot during contact with the germanium ingot, which is not conducive to improving the product quality of high-purity germanium polycrystalline zone melting and single crystal pulling. CONTENT OF THE UTILITY MODEL

[0007] In view of the problems in the background art, an object of the present disclosure is to provide a germanium ingot placing rack which can improve the operation efficiency of nitrogen blowing of the germanium ingot.

[0008] Another object of the present disclosure is to provide a germanium ingot placing rack which can avoid the phenomenon of residual water flowing back under the impact of nitrogen.

[0009] Still another object of the present disclosure is to provide a germanium ingot placing rack which can realize blowing dry of the entire germanium ingot without dead angles.

[0010] Thus, a germanium ingot placing rack is provided, which includes a support rack, the support rack including a bottom plate, a high bar assembly, and a low bar assembly; the high bar assembly including a high support bar, the high bar assembly being fixed to the bottom plate so that the high support bar is suspended above the bottom plate; the low bar assembly including a first low support bar and a second low support bar, the low bar assembly being fixed to the bottom plate so that the first low support bar and the second low support bar are suspended above the bottom plate, the first low support bar, the second low support bar, and the high support bar being spaced apart from each other and parallel to each other in a left-right direction, the first low support bar being higher than the second low support bar in an up-down direction, and the high support bar being higher than the second low support bar in the up-down direction; the first low support bar, the second low support bar, and the high support bar being used together to: the second low support bar and the high support bar supporting a bottom surface of the germanium ingot, and the first low support bar abutting against an end surface of the germanium ingot, so that the germanium ingot is supported and positioned on the first low support bar, the second low support bar, and the high support bar in an inclined manner relative to the bottom plate, for nitrogen blowing dry operation of the germanium ingot.

[0011] The beneficial effects of the present disclosure are as follows.

[0012] In the germanium ingot placing rack according to the present disclosure, by the provision of the first low support bar, the second low support bar, and the high support bar, the second low support bar and the high support bar support a bottom surface of the germanium ingot, and the first low support bar abuts against an end surface of the germanium ingot, so that the germanium ingot is supported and positioned on the first low support bar, the second low support bar, and the high support bar in an inclined manner relative to the bottom plate, for nitrogen blowing dry operation of the germanium ingot, which avoids the posture change operation of the hand-held operation in the background art, and improves the operation efficiency of the nitrogen blowing dry operation of the germanium ingot.

[0013] In addition, since the germanium ingot is supported and positioned on the first low support bar, the second low support bar, and the high support bar in an inclined manner, there is no posture change of the hand holding the germanium ingot as in the background art, which avoids the phenomenon of backflow of residual water under the impact of nitrogen, and only one-way nitrogen blowing dry from the high support bar side to the second low support bar side is needed, eliminating the residual pure water on the germanium ingot.

[0014] In addition, during nitrogen blowing dry, since only one-way nitrogen blowing dry from the high support bar side to the second low support bar side is needed, the entire germanium ingot can be blown dry without dead angle from the high support bar side to the second low support bar side. BRIEF DESCRIPTION OF DRAWINGS

[0015] Figure 1 is an exploded view of the germanium ingot placing rack according to the present disclosure.

[0016] Figure 2 is an assembly view of the germanium ingot placing rack according to the present disclosure, in which the germanium ingot is shown in dashed lines.

[0017] In which, the reference numeral is explained as follows:

[0018] 100 germanium ingot placing rack 124 high front sliding block

[0019] D1 front-rear direction 125 high rear slide

[0020] D2 left-right direction 13 low bar assembly

[0021] D3 up-down direction 131 first low support bar

[0022] 1 support frame 132 second low support bar

[0023] 11 bottom plate 133 low front support post

[0024] 111 front slide 133a top surface

[0025] 112 rear slide 134 low rear support post

[0026] 113 front passage 134a top surface

[0027] 114 front low slide 135 low rear slide

[0028] 115 front surface 136 low rear slide

[0029] 116 rear surface F spacer flange

[0030] 12 high bar assembly S screw hole

[0031] 121 high support bar 14 screw

[0032] 122 high front support post 2 clip

[0033] 122a top surface 200 germanium ingot

[0034] 123 high rear support post 200a bottom surface

[0035] 123a top surface 200b end surface DETAILED DESCRIPTION

[0036] The accompanying drawings illustrate embodiments of the present disclosure and, it is to be understood that the disclosed embodiments are merely representative of the present disclosure, the present disclosure can be embodied in various forms, therefore, the specific details disclosed herein should not be interpreted as limiting, but merely as a basis for the claims and as a representative basis for teaching one of ordinary skill in the art to variously embody the present disclosure.

[0037] Referring to Figure 1 and Figure 2, The germanium ingot placing rack 100 according to the present disclosure comprises a support frame 1. The support frame 1 comprises a bottom plate 11, a high bar assembly 12, and a low bar assembly 13. The high bar assembly 12 comprises a high support bar 121, and the high bar assembly 12 is fixed on the bottom plate 11 so that the high support bar 121 is suspended above the bottom plate 11. The low bar assembly 13 comprises a first low support bar 131 and a second low support bar 132, and the low bar assembly 13 is fixed on the bottom plate 11 so that the first low support bar 131 and the second low support bar 132 are suspended above the bottom plate 11, the first low support bar 131, the second low support bar 132, and the high support bar 121 are spaced apart from each other and parallel to each other in the left-right direction D2, the first low support bar 131 is higher than the second low support bar 132 in the up-down direction D3, and the high support bar 121 is higher than the second low support bar 132 in the up-down direction D3. The first low support bar 131, the second low support bar 132, and the high support bar 121 together serve to: the second low support bar 132 and the high support bar 121 support the bottom surface 200a of the germanium ingot 200, and the first low support bar 131 abuts against the end surface 200b of the germanium ingot 200, so that the germanium ingot 200 is supported and positioned on the first low support bar 131, the second low support bar 132, and the high support bar 121 in an inclined manner relative to the bottom plate 11, for nitrogen blowing dry operation of the germanium ingot 200.

[0038] In the germanium ingot placing rack 100 according to the present disclosure, by the arrangement of the first low support bar 131, the second low support bar 132, and the high support bar 121, the second low support bar 132 and the high support bar 121 support the bottom surface 200a of the germanium ingot 200, and the first low support bar 131 abuts against the end surface 200b of the germanium ingot 200, so that the germanium ingot 200 is supported and positioned on the first low support bar 131, the second low support bar 132, and the high support bar 121 in an inclined manner relative to the bottom plate 11, for nitrogen blowing dry operation of the germanium ingot 200, which avoids the posture change operation of the hand-held operation in the background art, and improves the operation efficiency of the nitrogen blowing dry of the germanium ingot 200.

[0039] In addition, since the germanium ingot 200 is supported and positioned on the first low support bar 131, the second low support bar 132, and the high support bar 121 in an inclined manner, there is no posture change of the hand holding the germanium ingot in the background art, which avoids the phenomenon of backflow of residual water under the impact of nitrogen, and only one-way nitrogen blowing dry from the high support bar 121 side to the second low support bar 132 side is needed, which eliminates the residual water on the germanium ingot.

[0040] In addition, during nitrogen blowing dry, since only one-way nitrogen blowing dry from the high support bar 121 side to the second low support bar 132 side is needed, the entire germanium ingot can be blown dry without dead angle from the high support bar 121 side to the second low support bar 132 side.

[0041] In order to increase the inclination angle of the germanium ingot 200 positioned on the first low support rod 131, the second low support rod 132 and the high support rod 121, in an example, the first low support rod 131 is lower than the high support rod 121 in the up-down direction D3.

[0042] In an example, the first low support rod 131, the second low support rod 132 and the high support rod 121 are all round rods. In this way, the contact between the first low support rod 131 and the end surface 200b of the germanium ingot 200 is a line contact, and the contact between the second low support rod 132 and the high support rod 121 and the bottom surface 200a of the germanium ingot 200 is also a line contact, so that the drying is simple, effective and fast for the line contact part when the nitrogen gas is blown dry.

[0043] As shown in Figure 1 and Figure 2 , in an example, the first low support rod 131, the second low support rod 132 and the high support rod 121 all extend along the front-rear direction D1.

[0044] In order to improve the work efficiency, as shown in Figure 1 and Figure 2 , in an example, the first low support rod 131, the second low support rod 132 and the high support rod 121 are all provided with a plurality of interval flanges F which are spaced apart along the length and protrude radially outward, and the part between any two adjacent interval flanges F of the first low support rod 131, the second low support rod 132 and the high support rod 121 is used to suspend and support a corresponding germanium ingot 200 on the first low support rod 131, the second low support rod 132 and the high support rod 121 in an inclined manner relative to the bottom plate 11. In this way, a plurality of germanium ingots 200 can be placed on the first low support rod 131, the second low support rod 132 and the high support rod 121 at the same time, and the nitrogen gas drying operation is performed in sequence.

[0045] As shown in Figure 1 and Figure 2 , in an example, the high rod assembly 12 further includes a high front support column 122 and a high rear support column 123. The high front support column 122 and the high rear support column 123 face each other along the front-rear direction D1, and the two ends of the high support rod 121 are fixed to the top of the high front support column 122 and the top of the high rear support column 123 respectively, and the bottom of the high front support column 122 and the bottom of the high rear support column 123 are fixed to the bottom plate 11. The low rod assembly 13 further includes a low front support column 133 and a low rear support column 134. The low front support column 133 and the low rear support column 134 face each other along the front-rear direction D1, and the two ends of the first low support rod 131 and the two ends of the second low support rod 132 are fixed to the top of the low front support column 133 and the top of the low rear support column 134 respectively, and the bottom of the low front support column 133 and the bottom of the low rear support column 134 are fixed to the bottom plate 11.

[0046] Further, the high support bar 121 is fixed at both ends thereof to opposite sides of the high front support column 122 and the high rear support column 123, and is lower than the top surface 122a of the high front support column 122 and the top surface 123a of the high rear support column 123. The first low support bar 131 and the second low support bar 132 are fixed at both ends thereof to opposite sides of the low front support column 133 and the low rear support column 134, and the both ends of the first low support bar 131 are lower than the top surface 133a of the low front support column 133 and the top surface 134a of the low rear support column 134. Thus, the portions of the sides of the high front support column 122 and the high rear support column 123 near the top surfaces 122a and 123a can function as the aforementioned spacing flanges F, and the portions of the sides of the low front support column 133 and the low rear support column 134 near the top surfaces 133a and 134a can function as the aforementioned spacing flanges F.

[0047] For ease of assembly and disassembly, with reference to Figure 1 and Figure 2 In one example, the base plate 11 includes a front slide 111 and a rear slide 112, the front slide 111 being formed through the base plate 11 in the left-right direction D2 and being open upward, and the rear slide 112 being formed through the base plate 11 in the left-right direction D2 and being open upward. The high bar assembly 12 further includes a high front slide block 124 and a high rear slide block 125, the high front slide block 124 being fixed to a bottom end of the high front support column 122, and the high rear slide block 125 being fixed to a bottom end of the high rear support column 123, the high front slide block 124 and the portion of the high front support column 122 near the bottom being in sliding engagement with the front slide 111, and the high rear slide block 125 and the portion of the high rear support column 123 near the bottom being in sliding engagement with the rear slide 112. The low bar assembly 13 further includes a low front slide block 135 and a low rear slide block 136, the low front slide block 135 being fixed to a bottom end of the low front support column 133, and the low rear slide block 136 being fixed to a bottom end of the low rear support column 134, the low front slide block 135 and the portion of the low front support column 133 near the bottom being in sliding engagement with the front slide 111, and the low rear slide block 136 and the portion of the low rear support column 134 near the bottom being in sliding engagement with the rear slide 112.

[0048] Further, in one example, as Figure 1 and Figure 2As shown, the base plate 11 further includes a front channel 113 and a rear channel 114. The front channel 113 extends rearward from the front surface 115 of the base plate 11 to connect to the front slideway 111, and the rear channel 114 extends forward from the rear surface 116 of the base plate 11 to connect to the rear slideway 112. The high front slider 124, the high rear slider 125, the low front slider 135, and the low rear slider 136 are provided with screw holes S on their respective surfaces. The support frame 1 further includes a plurality of screws 14, each screw 14 being configured to screw into a screw hole S in a corresponding one of the high front slider 124, the high rear slider 125, the low front slider 135, and the low rear slider 136 to secure the corresponding one of the high front slider 124, the high rear slider 125, the low front slider 135, and the low rear slider 136 to the base plate 11.

[0049] exist Figure 1 In the example shown in FIG, the high front slider 124 forms an inverted T-shape with the high front support column 122; the high rear slider 125 forms an inverted T-shape with the high rear support column 123; the low front slider 135 forms an inverted T-shape with the low front support column 133; and the low rear slider 136 forms an inverted T-shape with the low rear support column 134. The high front slider 124, the low front slider 135, and the front slide 111 can be formed in a dovetail groove arrangement. Similarly, the high rear slider 125, the low rear slider 136 and the rear slide 112 can be formed in a dovetail groove arrangement.

[0050] like Figure 1 and Figure 2 As shown, in one example, the germanium ingot display rack 100 further includes a clamp 2 for clamping the germanium ingot 200 onto the support rack 1. The clamp 2 is a polypropylene (PP) clamp or a polytetrafluoroethylene (PTFE) clamp. The first low support bar 131, the second low support bar 132, and the upper support bar 121 are all polypropylene rods or polytetrafluoroethylene rods. By using the polypropylene or polytetrafluoroethylene clamp for the clamp 2 and the polypropylene or polytetrafluoroethylene rods for the first low support bar 131, the second low support bar 132, and the upper support bar 121, the components that come into contact with the germanium ingot do not require Class 100 clean gloves, thereby eliminating impurities from Class 100 clean gloves used in prior art during contact with the germanium ingot.

[0051] It is noted that the germanium ingot placement rack 100 according to the present disclosure is not only suitable for nitrogen drying of germanium ingots before high-purity germanium polycrystalline zone melting and single crystal pulling, but also suitable for nitrogen drying of low-purity germanium ingots.

[0052] The above detailed description is used to describe a number of exemplary embodiments, but this document is not intended to be limited to the explicitly disclosed combinations. Therefore, unless otherwise stated, the various features disclosed herein may be combined to form multiple additional combinations that are not shown for the sake of brevity.

Claims

1. A germanium ingot placing rack characterized in that, the germanium ingot placing rack (100) comprises a support frame (1), the support frame (1) comprises a bottom plate (11), a high bar assembly (12), and a low bar assembly (13); the high bar assembly (12) comprises a high support bar (121), and the high bar assembly (12) is fixed to the bottom plate (11) so that the high support bar (121) is suspended above the bottom plate (11); the low bar assembly (13) comprises a first low support bar (131) and a second low support bar (132), and the low bar assembly (13) is fixed to the bottom plate (11) so that the first low support bar (131) and the second low support bar (132) are suspended above the bottom plate (11), the first low support bar (131), the second low support bar (132), and the high support bar (121) are spaced apart from and parallel to each other in a left-right direction (D2), the first low support bar (131) is higher than the second low support bar (132) in an up-down direction (D3), and the high support bar (121) is higher than the second low support bar (132) in the up-down direction (D3); the first low support bar (131), the second low support bar (132), and the high support bar (121) are used together to support a bottom surface (200a) of a germanium ingot (200) by the second low support bar (132) and the high support bar (121), and to abut an end surface (200b) of the germanium ingot (200) by the first low support bar (131), so that the germanium ingot (200) is supported and positioned on the first low support bar (131), the second low support bar (132), and the high support bar (121) in an inclined manner relative to the bottom plate (11) to perform a nitrogen blowing dry operation on the germanium ingot (200). 2.The germanium ingot placing rack according to claim 1, characterized in that, the first low support bar (131), the second low support bar (132), and the high support bar (121) are all round bars. 3.The germanium ingot placing rack according to claim 1, characterized in that, the first low support bar (131), the second low support bar (132), and the high support bar (121) all extend in a front-rear direction (D1). 4.The germanium ingot placing rack according to claim 1, characterized in that, the first low support bar (131), the second low support bar (132), and the high support bar (121) are each provided with a plurality of spacing flanges (F) spaced apart along the length and protruding radially outward, a portion between any two adjacent spacing flanges (F) of the first low support bar (131), the second low support bar (132), and the high support bar (121) is used to support a corresponding germanium ingot (200) in an inclined manner relative to the bottom plate (11) on the first low support bar (131), the second low support bar (132), and the high support bar (121). 5.The germanium ingot placing rack according to claim 1, characterized in that, the high bar assembly (12) further comprises a high front support column (122) and a high rear support column (123). The high front support column (122) and the high rear support column (123) face each other in the front-rear direction (D1), and the two ends of the high support bar (121) are fixed to the top of the high front support column (122) and the top of the high rear support column (123), respectively, and the bottom of the high front support column (122) and the bottom of the high rear support column (123) are fixed to the bottom plate (11); The low bar assembly (13) further includes a low front support column (133) and a low rear support column (134); The low front support column (133) and the low rear support column (134) face each other in the front-rear direction (D1), and the two ends of the first low support bar (131) and the two ends of the second low support bar (132) are fixed to the top of the low front support column (133) and the top of the low rear support column (134), respectively, and the bottom of the low front support column (133) and the bottom of the low rear support column (134) are fixed to the bottom plate (11).

6. The germanium ingot placing rack according to claim 5, wherein The two ends of the high support bar (121) are fixed to the opposite sides of the high front support column (122) and the high rear support column (123) and are lower than the top surface (122a) of the high front support column (122) and the top surface (123a) of the high rear support column (123); The two ends of the first low support bar (131) and the two ends of the second low support bar (132) are fixed to the opposite sides of the low front support column (133) and the low rear support column (134), and the two ends of the first low support bar (131) are lower than the top surface (133a) of the low front support column (133) and the top surface (134a) of the low rear support column (134).

7. The germanium ingot placing rack according to claim 5, wherein The bottom plate (11) includes a front slide (111) and a rear slide (112), the front slide (111) penetrates the bottom plate (11) in the left-right direction (D2) and is open upward, and the rear slide (112) penetrates the bottom plate (11) in the left-right direction (D2) and is open upward; The high bar assembly (12) further includes a high front slide block (124) and a high rear slide block (125), the high front slide block (124) is fixed to the bottom end of the high front support column (122), the high rear slide block (125) is fixed to the bottom end of the high rear support column (123), the high front slide block (124) and the portion of the high front support column (122) close to the bottom are used for sliding combination with the front slide (111), and the high rear slide block (125) and the portion of the high rear support column (123) close to the bottom are used for sliding combination with the rear slide (112); The low bar assembly (13) further includes a low front slide block (135) and a low rear slide block (136), the low front slide block (135) is fixed to the bottom end of the low front support column (133), the low rear slide block (136) is fixed to the bottom end of the low rear support column (134), the low front slide block (135) and the portion of the low front support column (133) close to the bottom are used for sliding combination with the front slide (111), and the low rear slide block (136) and the portion of the low rear support column (134) close to the bottom are used for sliding combination with the rear slide (112).

8. The germanium ingot placing rack according to claim 7, wherein The bottom plate (11) further comprises a front channel (113) and a rear channel (114), the front channel (113) extending from the front surface (115) of the bottom plate (11) rearward to communicate with the front slide (111), and the rear channel (114) extending from the rear surface (116) of the bottom plate (11) forward to communicate with the rear slide (112); The high front slide block (124), the high rear slide block (125), the low front slide block (135) and the low rear slide block (136) are provided with screw holes (S) on the surfaces of the corresponding sides, The support frame (1) further comprises a plurality of screws (14), each screw (14) being used for being screwed with the screw hole (S) of the corresponding one of the high front slide block (124), the high rear slide block (125), the low front slide block (135) and the low rear slide block (136) to fix the corresponding one of the high front slide block (124), the high rear slide block (125), the low front slide block (135) and the low rear slide block (136) to the bottom plate (11).

9. The germanium ingot placing frame according to claim 7, wherein, The high front slide block (124) forms an inverted T shape with the high front support column (122); The high rear slide block (125) forms an inverted T shape with the high rear support column (123); The low front slide block (135) forms an inverted T shape with the low front support column (133); The low rear slide block (136) forms an inverted T shape with the low rear support column (134).

10. The germanium ingot placing frame according to claim 1, wherein, The germanium ingot placing frame (100) further comprises a clip (2) for clamping the germanium ingot (200) to the support frame (1); The clip (2) is a polypropylene clip or a polytetrafluoroethylene clip; The first low support column (131), the second low support column (132) and the high support column (121) are polypropylene columns or polytetrafluoroethylene columns.

Citation Information

Patent Citations

  • Germanium ingot corrosion method

    CN113718257A