Stirring reaction device for preparing benzotriazole

Abstract

The utility model discloses a stirring reaction device for preparing benzotriazole, which belongs to the technical field of benzotriazole preparation and comprises a motor, a machine cover is fixedly connected outside the motor, a rotor of the motor is fixedly connected with a rotating sleeve, the rotating sleeve is rotatably mounted in the machine cover, a transmission rod is slidably mounted in the rotating sleeve, and the transmission rod is fixedly connected with the machine cover. A shaft seat is rotatably connected to the lower portion of the machine cover, an auxiliary spring is fixedly connected between the shaft seat and the machine cover, a stirring barrel is fixedly connected to the lower portion of the shaft seat, a rotating frame is fixedly connected to the interior of the stirring barrel, and after materials are poured into the stirring barrel and the machine cover and the stirring barrel are closed, a transmission rod is buckled with the rotating frame, so that the stirring barrel is driven to rotate; the motor is used for driving the rotating sleeve to rotate, the rotating sleeve drives the transmission rod to rotate, the transmission rod drives the rotating frame to rotate, centrifugal force is used for driving the swing plate to stretch outwards, the swing plate stirs materials in the stirring barrel, after the rotating frame is static, the swing plate is retracted into the rotating frame by means of the gravity of the swing plate, and the interior of the stirring barrel is conveniently cleaned.

Description

Technical Field

[0001] This invention belongs to the field of benzotriazole preparation technology, and particularly relates to a stirring reaction apparatus for the preparation of benzotriazole. Background Technology

[0002] The preparation of benzotriazole requires stirring in a stirred reactor. In a broad sense, a reactor is a container where physical or chemical reactions occur. Through the structural design and parameter configuration of the container, the heating, evaporation, cooling and low-to-high-speed mixing functions required by the process can be achieved.

[0003] Because the stirring claw structure of conventional reactors is fixed, when cleaning impurities inside, the stirring claw gets stuck inside, hindering the cleaning process. This makes the cleaning operation after shutting down a conventional reactor for the preparation of benzotriazole quite troublesome.

[0004] To address these issues, we propose a stirred reaction apparatus for the preparation of benzotriazole. Utility Model Content

[0005] The purpose of this invention is to solve the problem of cumbersome cleaning operations after shutting down conventional benzotriazole preparation reactors, and to propose a stirring reaction device for benzotriazole preparation.

[0006] To achieve the above objectives, the present invention adopts the following technical solution:

[0007] A stirring reaction apparatus for the preparation of benzotriazole includes a motor, an externally fixed cover, a rotating sleeve fixedly connected to the motor rotor, the rotating sleeve being rotatably mounted inside the cover, a transmission rod slidably mounted inside the rotating sleeve, a shaft seat rotatably connected to the lower part of the cover, a booster spring fixedly connected between the shaft seat and the cover, a stirring tank fixedly connected to the lower part of the shaft seat, a rotating frame fixedly connected inside the stirring tank, the upper end of the rotating frame engaging with the transmission rod, a swing plate installed inside the rotating frame, and the cover engaging with the stirring tank cover. After pouring material into the stirring tank and closing the cover and stirring tank, the transmission rod engages with the rotating frame. The motor drives the rotating sleeve to rotate, which in turn drives the transmission rod to rotate, causing the rotating frame to rotate. Centrifugal force causes the swing plate to open outwards, stirring the material inside the stirring tank. When the rotating frame comes to rest, the swing plate retracts into the rotating frame under its own weight, facilitating cleaning of the inside of the stirring tank.

[0008] Preferably, the mixing tank includes a tank body, with baffles uniformly and fixedly connected inside the tank body, and a bearing fixedly connected to the bottom of the tank body. The baffles increase eddy current resistance, thereby ensuring the mixing efficiency of the swing plate, and the bearing guides the rotation of the rotating frame, facilitating the mixing of the target material.

[0009] Preferably, the bearing includes a fixed seat, with a fixed shaft fixedly connected to the upper part of the fixed seat and a limiting plate fixedly connected to the upper part of the fixed seat; the lower part of the fixed seat is fixedly connected to the barrel body. The fixed shaft guides the swing of the lid, and the limiting plate restricts the opening range of the lid, facilitating the opening or closing of the lid.

[0010] Preferably, the cover includes a cover body, a handle is fixedly connected to the upper part of the cover body, and a swing arm is fixedly connected to the outside of the cover body; the lower part of the swing arm is rotatably mounted on a fixed shaft, one end of the assist spring is fixedly connected to the swing arm, the other end of the assist spring is fixedly connected to the fixed shaft, and the motor is fixedly connected to the swing arm. The spring force of the assist spring acts on the swing arm, which in turn acts on the cover body, reducing the force required to open the cover. Simultaneously, the spring force of the assist spring maintains the cover in the open state, facilitating manual operation of the cover.

[0011] Preferably, the rotating sleeve includes a sleeve body with a sliding groove; the sleeve body is fixedly connected to the rotor of the motor, and the sleeve body is rotatably installed inside the cover. The sliding groove guides the transmission rod to slide; when the transmission rod and the rotating frame are misaligned, the transmission rod retracts along the sliding groove until they are aligned, at which point the transmission rod returns to its original position and engages with the rotating frame, facilitating the connection between the transmission rod and the rotating frame.

[0012] Preferably, the transmission rod includes a rod body, a slider is fixedly connected to the outside of the rod body, and a buckle is fixedly connected to the end of the rod body facing away from the slider; the rod body is slidably installed in the sleeve body, and the slider is slidably installed in the slide groove. When the sleeve body rotates, the slide groove acts on the slider, which drives the rod body to rotate, causing the rod body to drive the buckle to rotate, thus facilitating the rotation of the transmission rod by the rotating sleeve.

[0013] Preferably, the rotating frame includes a frame body, with a limit block fixedly connected inside the frame body, and a fastener fixedly connected to the upper end of the frame body; the lower part of the frame body is rotatably connected to a bearing, and the fastener is engaged with the fastener block. When the transmission rod drives the fastener to rotate, the fastener drives the frame body to rotate, facilitating the rotating frame to drive the swing plate to revolve.

[0014] Preferably, the swing plate includes a plate body with a notch at its lower end; the upper part of the plate body is rotatably mounted on the upper inner wall of the frame, and the notch is in movable contact with a limiting block. When the frame rotates the plate body, the plate body opens outward; when the rotating frame stops rotating, the fixed seat retracts into the frame body by gravity, facilitating the automatic unfolding and retraction of the swing plate.

[0015] In summary, the technical effects and advantages of this utility model are as follows:

[0016] 1. Pour the material into the mixing tank, close the machine cover and the mixing tank, and then connect the transmission rod to the rotating frame. Use the motor to drive the rotating sleeve to rotate, which in turn drives the transmission rod to rotate, which in turn drives the rotating frame to rotate. Use centrifugal force to drive the swing plate to open outward, so that the swing plate can stir the material in the mixing tank. When the rotating frame stops, let the swing plate return to the rotating frame by its own weight, which makes it easy to clean the inside of the mixing tank.

[0017] 2. The baffles are used to increase the eddy current resistance, thereby ensuring the mixing efficiency of the swing plate. The bearings guide the rotation of the rotating frame to facilitate the mixing of the target material.

[0018] 3. The machine cover is guided to swing using a fixed shaft, and the opening range of the machine cover is limited by a limiting plate, making it convenient to open or close the machine cover.

[0019] 4. The spring force of the assist spring acts on the swing arm, which in turn acts on the cover, reducing the force required to open the cover. At the same time, the spring force of the assist spring keeps the cover open, making it easy to operate the cover manually.

[0020] 5. The transmission rod is guided to slide using a slide groove. When the angle between the transmission rod and the rotating frame is misaligned, the transmission rod retracts along the slide groove until it is aligned. Then, the transmission rod is reset and engaged with the rotating frame, which facilitates the connection between the transmission rod and the rotating frame.

[0021] 6. When the sleeve rotates, the sliding groove acts on the slider, which in turn drives the rod to rotate, causing the rod to drive the buckle to rotate, thus facilitating the rotation of the sleeve and the transmission rod.

[0022] 7. When the transmission rod drives the buckle to rotate, the buckle drives the frame to rotate, which facilitates the rotating frame to drive the swing plate to revolve.

[0023] 8. When the frame drives the board to revolve, the board opens outward. When the frame stops rotating, the fixed seat retracts into the frame with the help of gravity, which facilitates the automatic unfolding and retraction of the board. Attached Figure Description

[0024] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0025] Figure 2 This is a schematic diagram of the mixing tank structure of this utility model;

[0026] Figure 3 This is a schematic diagram of the bearing structure of this utility model;

[0027] Figure 4 This is a schematic diagram of the cover structure of this utility model;

[0028] Figure 5 This is a schematic diagram of the rotating sleeve structure of this utility model;

[0029] Figure 6This is a schematic diagram of the transmission rod structure of this utility model;

[0030] Figure 7 This is a schematic diagram of the rotating frame structure of this utility model;

[0031] Figure 8 This is a schematic diagram of the swing plate structure of this utility model.

[0032] In the diagram: 1. Motor; 2. Mixing tank; 3. Shaft seat; 4. Machine cover; 5. Rotating sleeve; 6. Transmission rod; 7. Rotating frame; 8. Swing plate; 10. Assist spring; 21. Tank body; 22. Stop bar; 23. Bearing; 31. Fixed seat; 32. Fixed shaft; 33. Limiting plate; 41. Cover; 42. Handle; 43. Swing arm; 51. Sleeve body; 52. Slide groove; 61. Rod body; 62. Slider; 63. Buckle block; 71. Limiting block; 72. Buckle seat; 73. Frame body; 81. Plate body; 82. Notch. Detailed Implementation

[0033] The technical solutions of the utility model embodiments will be clearly and completely described below with reference to the accompanying drawings. Obviously, the described embodiments are only some embodiments of the utility model, and not all embodiments.

[0034] Reference Figure 1 A stirring reaction apparatus for the preparation of benzotriazole includes a motor 1, an external cover 4 fixedly connected to the motor 1, a rotating sleeve 5 fixedly connected to the rotor of the motor 1, the rotating sleeve 5 being rotatably installed inside the cover 4, a transmission rod 6 being slidably installed inside the rotating sleeve 5, a bearing 3 being rotatably connected to the lower part of the cover 4, a booster spring 10 being fixedly connected between the bearing 3 and the cover 4, a stirring tank 2 being fixedly connected to the lower part of the bearing 3, a rotating frame 7 being fixedly connected inside the stirring tank 2, the upper end of the rotating frame 7 being engaged with the transmission rod 6, a swing plate 8 being installed inside the rotating frame 7, and the cover 4 being engaged with the stirring tank 2.

[0035] Reference Figure 1 and 2 The mixing tank 2 includes a tank body 21, with baffles 22 evenly and fixedly connected inside the tank body 21, and a bearing 23 fixedly connected to the bottom of the tank body 21. The baffles 22 increase the eddy current resistance, thereby ensuring the mixing efficiency of the swing plate 8, and the bearing 23 guides the rotation of the rotating frame 7.

[0036] Reference Figure 1 , 2 3. The bearing 3 includes a fixed seat 31, with a fixed shaft 32 fixedly connected to the upper part of the fixed seat 31, and a limiting plate 33 fixedly connected to the upper part of the fixed seat 31; the lower part of the fixed seat 31 is fixedly connected to the barrel body 21. The fixed shaft 32 guides the machine cover 4 to swing, and the limiting plate 33 limits the opening range of the machine cover 4.

[0037] Reference Figure 1 , 3 4. The cover 4 includes a cover body 41, with a handle 42 fixedly connected to the upper part of the cover body 41, and a swing arm 43 fixedly connected to the outside of the cover body 41. The lower part of the swing arm 43 is rotatably mounted on a fixed shaft 32. One end of a power assist spring 10 is fixedly connected to the swing arm 43, and the other end of the power assist spring 10 is fixedly connected to the fixed shaft 32. The motor 1 is fixedly connected to the swing arm 43. The elastic force of the power assist spring 10 acts on the swing arm 43, which in turn acts on the cover body 41, reducing the force required to open the cover 4. At the same time, the elastic force of the power assist spring 10 keeps the cover 4 open.

[0038] Reference Figure 1 , 4 The rotating sleeve 5 includes a sleeve body 51, on which a sliding groove 52 is provided; the sleeve body 51 is fixedly connected to the rotor of the motor 1, and the sleeve body 51 is rotatably installed inside the cover body 41. The sliding groove 52 guides the transmission rod 6 to slide. When the angle between the transmission rod 6 and the rotating frame 7 is misaligned, the transmission rod 6 retracts along the sliding groove 52 until it is aligned, at which point the transmission rod 6 returns to its original position and engages with the rotating frame 7.

[0039] Reference Figure 1 , 5 6. The transmission rod 6 includes a rod body 61, with a slider 62 fixedly connected to the outside of the rod body 61. A fastener 63 is fixedly connected to the end of the rod body 61 facing away from the slider 62. The rod body 61 is slidably installed inside the sleeve 51, and the slider 62 is slidably installed inside the slide groove 52. When the sleeve 51 rotates, the slide groove 52 acts on the slider 62, which drives the rod body 61 to rotate, causing the rod body 61 to drive the fastener 63 to rotate.

[0040] Reference Figure 1 , 2 6 and 7, the rotating frame 7 includes a frame body 73, with a limit block 71 fixedly connected inside the frame body 73, and a fastener 72 fixedly connected to the upper end of the frame body 73; the lower part of the frame body 73 is rotatably connected to the bearing 23, and the fastener 72 is engaged with the fastener block 63. When the transmission rod 6 drives the fastener 72 to rotate, the frame body 73 is driven to rotate through the fastener 72.

[0041] Reference Figure 1 , 3 7 and 8, the swing plate 8 includes a plate body 81, with a notch 82 at the lower end of the plate body 81; the upper part of the plate body 81 is rotatably mounted on the upper inner wall of the frame 73, and the notch 82 is in movable contact with the limiting block 71. When the frame 73 drives the plate body 81 to revolve, the plate body 81 opens outward. When the rotating frame 7 stops rotating, the fixed seat 31 retracts into the frame 73 by gravity.

[0042] Working principle: Pour the material into the mixing tank 2, close the machine cover 4 to the mixing tank 2, and then connect the transmission rod 6 to the rotating frame 7. Use the motor 1 to drive the rotating sleeve 5 to rotate, which in turn drives the transmission rod 6 to rotate, which in turn drives the rotating frame 7 to rotate. Centrifugal force drives the swing plate 8 to open outward, so that the swing plate 8 can stir the material in the mixing tank 2. When the rotating frame 7 stops, the swing plate 8 can be returned to the rotating frame 7 by its own weight.

[0043] The above description is only a preferred embodiment of the utility model, but the protection scope of the utility model is not limited thereto. Any equivalent substitutions or changes made by those skilled in the art within the technical scope disclosed by the utility model, based on the technical solution and the utility model concept, should be included within the protection scope of the utility model.

[0044] The description briefly mentions the application direction of the utility model in relation to existing technologies known to those skilled in the art without modification, and combines them with the utility model to form a complete technology; it avoids excessive popularization of technologies known to those skilled in the art, in order to help those skilled in the art quickly understand the main content of the utility model.

Claims

1. A stirring reaction apparatus for the preparation of benzotriazole, comprising a motor (1), characterized in that: The motor (1) is externally fixedly connected to a cover (4), and a rotating sleeve (5) is fixedly connected to the rotor of the motor (1). The rotating sleeve (5) is rotatably installed inside the cover (4). A transmission rod (6) is slidably installed inside the rotating sleeve (5). A shaft seat (3) is rotatably connected to the lower part of the cover (4). A booster spring (10) is fixedly connected between the shaft seat (3) and the cover (4). A mixing tank (2) is fixedly connected to the lower part of the shaft seat (3). A rotating frame (7) is fixedly connected inside the mixing tank (2). The upper end of the rotating frame (7) is engaged with the transmission rod (6). A swing plate (8) is installed inside the rotating frame (7). The cover (4) is engaged with the mixing tank (2).

2. The stirred reaction apparatus for the preparation of benzotriazole according to claim 1, characterized in that: The mixing tank (2) includes a tank body (21), with baffles (22) evenly fixedly connected inside the tank body (21), and a bearing (23) fixedly connected to the bottom of the tank body (21).

3. The stirred reaction apparatus for the preparation of benzotriazole according to claim 2, characterized in that: The bearing seat (3) includes a fixed seat (31), a fixed shaft (32) is fixedly connected to the upper part of the fixed seat (31), and a limit plate (33) is fixedly connected to the upper part of the fixed seat (31); the lower part of the fixed seat (31) is fixedly connected to the barrel body (21).

4. The stirred reaction apparatus for the preparation of benzotriazole according to claim 3, characterized in that: The cover (4) includes a cover body (41), a handle (42) is fixedly connected to the upper part of the cover body (41), and a swing arm (43) is fixedly connected to the outside of the cover body (41); the lower part of the swing arm (43) is rotatably mounted on a fixed shaft (32), one end of the assist spring (10) is fixedly connected to the swing arm (43), the other end of the assist spring (10) is fixedly connected to the fixed shaft (32), and the motor (1) is fixedly connected to the swing arm (43).

5. The stirred reaction apparatus for the preparation of benzotriazole according to claim 4, characterized in that: The rotating sleeve (5) includes a sleeve body (51) with a sliding groove (52) on the sleeve body (51); the sleeve body (51) is fixedly connected to the rotor of the motor (1), and the sleeve body (51) is rotatably installed inside the cover body (41).

6. The stirred reaction apparatus for the preparation of benzotriazole according to claim 5, characterized in that: The transmission rod (6) includes a rod body (61), a slider (62) is fixedly connected to the outside of the rod body (61), and a buckle (63) is fixedly connected to one end of the rod body (61) facing away from the slider (62); the rod body (61) is slidably installed in the sleeve (51), and the slider (62) is slidably installed in the groove (52).

7. The stirred reaction apparatus for the preparation of benzotriazole according to claim 6, characterized in that: The rotating frame (7) includes a frame (73), with a limiting block (71) fixedly connected inside the frame (73), and a fastener (72) fixedly connected to the upper end of the frame (73); the lower part of the frame (73) is rotatably connected to a bearing (23), and the fastener (72) is fastened and matched with the fastener block (63).

8. The stirred reaction apparatus for the preparation of benzotriazole according to claim 7, characterized in that: The swing plate (8) includes a plate body (81), and a notch (82) is provided at the lower end of the plate body (81); the upper part of the plate body (81) is rotatably installed on the upper inner wall of the frame (73), and the notch (82) is in contact with the limiting block (71).

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