Novel ammonium sulfate saturator

Abstract

The utility model relates to the technical field of chemical equipment, in particular to a novel ammonium sulfate saturator which comprises a saturator tank body, a top cover is fixedly installed on the top of the saturator tank body, a liquid inlet pipe is fixedly installed on the top cover, a liquid inlet ring is fixedly installed at the bottom end of the liquid inlet pipe, a notch is formed in one side of the liquid inlet ring, and a liquid outlet is formed in the other side of the liquid inlet ring. A plurality of nozzles are fixedly installed at the bottom of the liquid inlet ring, an air inlet pipe is further fixedly installed on the top cover, an air inlet ring is fixedly installed at the bottom end of the air inlet pipe, a plurality of air outlet holes are formed in the bottom face of the air inlet ring, the liquid inlet ring and the air inlet ring are both located in the saturator tank, the liquid inlet ring is located above the air inlet ring, and the air inlet pipe penetrates out of the notch. A temperature control electric heater is fixedly installed on a barrel body of the saturator tank body, a stirring shaft is fixedly installed at the tail end of an output shaft of the stirring motor, and stirring blades are fixedly installed on the stirring shaft. The reaction kettle is beneficial to full mixing reaction and convenient to produce and prepare.

Description

Technical Field

[0001] This utility model relates to the field of chemical equipment technology, and more specifically, to a novel ammonium sulfate saturator. Background Technology

[0002] In the field of chemical production, ammonium sulfate is an important chemical product that is widely used in agricultural fertilizers, industrial raw materials and many other aspects. As a key piece of equipment for producing ammonium sulfate, the performance of the ammonium sulfate saturator directly affects the quality of ammonium sulfate products and production efficiency.

[0003] Traditional ammonium sulfate saturators typically use one pipe to transport gas and another to transport liquid during operation. The ends of these pipes are straight, which hinders gas-liquid mixing. From a crystallization perspective, insufficient gas-liquid mixing within the equipment results in significant differences in the size of the generated ammonium sulfate crystals. Small crystals tend to agglomerate, increasing operational difficulty in subsequent filtration and drying processes, reducing product purity and appearance quality, and impacting its effectiveness in high-end agricultural fertilizers and industrial applications with stringent quality requirements. Therefore, we propose a novel ammonium sulfate saturator. Utility Model Content

[0004] The purpose of this invention is to provide a novel ammonium sulfate saturator to address the deficiencies mentioned in the background art.

[0005] To achieve the above objectives, this utility model provides the following technical solution:

[0006] A novel ammonium sulfate saturator includes a saturator tank. A top cover is fixedly installed on the top of the saturator tank. An inlet pipe is fixedly installed on the top cover. An inlet ring is fixedly installed at the bottom end of the inlet pipe. A notch is provided on one side of the inlet ring. Multiple nozzles are fixedly installed at the bottom of the inlet ring. An air inlet pipe is also fixedly installed on the top cover. An air inlet ring is fixedly installed at the bottom end of the air inlet pipe. Multiple air outlet holes are provided on the bottom surface of the air inlet ring arranged in a ring at equal intervals. Both the inlet ring and the air inlet ring are located inside the saturator tank. The inlet ring is located above the air inlet ring. The air inlet pipe extends out from the notch.

[0007] Preferably, a conical cylinder is fixedly installed at the bottom of the saturator tank, a discharge pipe is fixedly installed at the bottom end of the conical cylinder, and a discharge valve is fixedly installed on the discharge pipe.

[0008] Preferably, the conical cylinder is funnel-shaped, and the plane containing the inner wall of the conical cylinder is inclined downward at 45° to 60°.

[0009] Preferably, a plurality of support legs are fixedly installed at the bottom of the saturator tank, and a fixed base is fixedly installed at the bottom end of the support legs.

[0010] Preferably, a temperature-controlled electric heater is fixedly installed on the cylinder of the saturator tank, and the fixed base is fixedly installed on the ground.

[0011] Preferably, a stirring motor is fixedly installed at the center of the upper surface of the top cover, and a vertically arranged stirring shaft is fixedly installed at the end of the output shaft of the stirring motor. Stirring blades are fixedly installed on the stirring shaft, and the stirring blades are located inside the saturator tank.

[0012] Preferably, a booster pump is provided on one side of the saturator tank. A suction pipe is fixedly installed at the inlet end of the booster pump, and a delivery pipe is fixedly installed at the outlet end of the booster pump. Multiple distribution pipes are fixedly installed on the end of the delivery pipe, and multiple nozzles are fixedly installed at the bottom of the distribution pipe. The nozzles are located inside the saturator tank.

[0013] Preferably, the nozzle is located between the liquid inlet ring and the air inlet ring, and the suction pipe is connected to an external medicine delivery pipeline.

[0014] Compared with the prior art, the beneficial effects of this utility model are:

[0015] 1. This utility model achieves uniform and efficient entry of sulfuric acid solution and ammonia gas into the saturator tank and full contact by means of an inlet pipe with a notch and multiple nozzles set in the top cover, and an inlet pipe with an air inlet ring with equally spaced air outlet holes, with the inlet ring located above the air inlet ring. This results in improved gas-liquid mass transfer efficiency, accelerated reaction rate, more uniform gas-liquid mixing, and reduced particle size differences of the generated ammonium sulfate crystals.

[0016] 2. This utility model facilitates the discharge of crystallized ammonium sulfate products through the setting of a conical cylinder, discharge pipe, and discharge valve. The specific inclination angle of the conical cylinder can effectively prevent material residue and improve the smoothness of discharge. The support legs and fixed base provide stable support for the equipment.

[0017] 3. This utility model promotes solution mixing and crystal growth through the coordinated use of a stirring motor, stirring shaft, and stirring blades, resulting in more uniform crystallization. The addition of a booster pump, suction pipe, delivery pipe, distribution pipe, and nozzle allows external liquid to be introduced into the tank in the form of spraying. Furthermore, the nozzle is located between the liquid inlet ring and the air inlet ring, optimizing the reaction environment and enhancing the reaction effect, thereby comprehensively improving the quality and efficiency of ammonium sulfate production. Attached Figure Description

[0018] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0019] Figure 2 This is one of the partial structural schematic diagrams of this utility model;

[0020] Figure 3 This is a schematic diagram of the intake ring structure of this utility model;

[0021] Figure 4 This is the second partial structural schematic diagram of the present utility model;

[0022] The meanings of the labels in the diagram are as follows:

[0023] 1. Saturator tank; 10. Conical cylinder; 11. Discharge pipe; 12. Discharge valve; 13. Support leg; 131. Fixed base; 14. Temperature-controlled electric heater; 15. Top cover;

[0024] 2. Inlet pipe; 20. Inlet ring; 21. Notch; 22. Nozzle;

[0025] 3. Intake pipe; 30. Intake ring; 31. Exhaust port;

[0026] 4. Stirring motor; 40. Stirring shaft; 41. Stirring blades;

[0027] 5. Booster pump; 50. Suction pipe; 51. Delivery pipe; 52. Distribution pipe; 53. Nozzle. Detailed Implementation

[0028] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0029] Please see Figures 1-4 This utility model provides a technical solution: a novel ammonium sulfate saturator, including a saturator tank 1, a top cover 15 fixedly installed on the top of the saturator tank 1, an inlet pipe 2 fixedly installed on the top cover 15, an inlet ring 20 fixedly installed at the bottom end of the inlet pipe 2, a notch 21 provided on one side of the inlet ring 20, and multiple nozzles 22 fixedly installed at the bottom of the inlet ring 20. The two ends of the inlet ring 20 near the notch 21 are not connected to the outside, in order to ensure the liquid pressure at the nozzle 22, so that the liquid can be sprayed out from the nozzle 22 more smoothly;

[0030] Specifically, an air inlet pipe 3 is fixedly installed on the top cover 15, and an air inlet ring 30 is fixedly installed at the bottom end of the air inlet pipe 3. Multiple air outlet holes 31 arranged in a ring at equal intervals are provided on the bottom surface of the air inlet ring 30. Both the liquid inlet ring 20 and the air inlet ring 30 are located inside the saturator tank 1. The liquid inlet ring 20 is located above the air inlet ring 30. The air inlet pipe 3 passes through the notch 21, so that the sulfuric acid solution is evenly sprayed downward from the nozzle 22 of the liquid inlet ring 20, and the ammonia gas is discharged from the air outlet holes 31 of the air inlet ring 30. The two are in full contact inside the saturator tank 1, which greatly improves the gas-liquid mass transfer efficiency and accelerates the reaction rate.

[0031] In this embodiment, a conical cylinder 10 is fixedly installed at the bottom of the saturator tank 1, and a discharge pipe 11 is fixedly installed at the bottom end of the conical cylinder 10. A discharge valve 12 is fixedly installed on the discharge pipe 11. The conical cylinder 10 is funnel-shaped, and the plane of the inner wall of the conical cylinder 10 is inclined downward at 45° to 60°, so that the material can flow more smoothly into the discharge pipe 11 under the action of gravity, effectively preventing material residue and improving discharge efficiency.

[0032] Specifically, multiple support legs 13 are fixedly installed at the bottom of the saturator tank 1, and a fixed base 131 is fixedly installed at the bottom of the support legs 13. The fixed base 131 is fixedly installed on the ground, so that the saturator can be placed stably on the ground and ensure the stability of the equipment during operation.

[0033] Furthermore, a temperature-controlled electric heater 14 is fixedly installed on the cylinder of the saturator tank 1, which allows the temperature inside the saturator to be adjusted according to the reaction requirements, providing a suitable temperature environment for the ammonium sulfate production reaction, which is beneficial to improving reaction efficiency and product quality.

[0034] In addition, a stirring motor 4 is fixedly installed at the center of the upper surface of the top cover 15. A stirring shaft 40 is fixedly installed at the end of the output shaft of the stirring motor 4 in a vertical position. A stirring blade 41 is fixedly installed on the stirring shaft 40. The stirring blade 41 is located inside the saturator tank 1 to stir the reaction materials in the tank, promote uniform mixing of the solution, accelerate the reaction process, and make the crystallization process more uniform, thereby improving the quality of the ammonium sulfate product.

[0035] It is worth noting that a booster pump 5 is installed on one side of the saturator tank 1. A suction pipe 50 is fixedly installed at the water inlet end of the booster pump 5, and a delivery pipe 51 is fixedly installed at the water outlet end of the booster pump 5. Multiple uniformly distributed pipes 52 are fixedly installed on the end of the delivery pipe 51, and multiple nozzles 53 are fixedly installed at the bottom of the uniformly distributed pipes 52. The nozzles 53 are located inside the saturator tank 1. The nozzles 53 are located between the liquid inlet ring 20 and the air inlet ring 30. The suction pipe 50 is connected to the external chemical liquid delivery pipeline, which can add auxiliary agents according to production needs, optimize the reaction environment, and further improve the reaction effect and product quality. At the same time, after connecting the suction pipe 50 to the external water source, water can be delivered into the saturator tank 1 for cleaning operations.

[0036] Finally, it should be noted that the temperature-controlled electric heater 14, stirring motor 4, and booster pump 5 involved in this utility model are all general standard parts or parts known to those skilled in the art. Their structures and principles can be learned by those skilled in the art through technical manuals or conventional experimental methods. In the spare parts of this device, all the above-mentioned electrical components, which refer to power elements, electrical components, and the matching controller and power supply, are connected by wires. The specific connection methods should refer to the working principle of this utility model. The electrical connections between each electrical component are completed in the order of operation. The detailed connection methods are all technologies known in the art.

[0037] In use, the novel ammonium sulfate saturator of this invention involves connecting the temperature-controlled electric heater 14 to a power source and adjusting it to a suitable temperature for preheating the reaction. Then, sulfuric acid solution is supplied to the inlet ring 20 via the inlet pipe 2. Since the two ends of the inlet ring 20 near the notch 21 are closed, the liquid pressure at the nozzle 22 is ensured, allowing the solution to be smoothly and evenly sprayed downwards from the nozzle 22. Simultaneously, ammonia gas enters the inlet ring 30 via the inlet pipe 3 and exits from the equally spaced outlet holes 31 at its bottom, fully contacting the sulfuric acid solution sprayed from the nozzle 22 within the saturator tank 1, accelerating the reaction. Additionally, the stirring motor 4 is turned on, driving the stirring shaft 40 and stirring blades 41 to stir the reaction materials, promoting uniform mixing and crystallization.

[0038] If auxiliary agents need to be added, connect the suction pipe 50 to the external liquid delivery pipeline, start the booster pump 5, and the liquid is sprayed out from the nozzle 53 through the delivery pipe 51 and the distribution pipe 52. It participates in the reaction between the liquid inlet ring 20 and the air inlet ring 30 to optimize the environment. After the reaction is completed, open the discharge valve 12, and the ammonium sulfate crystals are smoothly discharged from the discharge pipe 11 under the action of the conical cylinder 10.

[0039] After the equipment has been used for a period of time, the suction pipe 50 can be connected to an external water source, the booster pump 5 can be started, and the water can be sprayed through the nozzle 53 to clean the inside of the saturator tank 1 to maintain the equipment in good operating condition.

[0040] The foregoing has shown and described the basic principles, main features, and advantages of this utility model. Those skilled in the art should understand that this utility model is not limited to the above embodiments. The embodiments and descriptions in the specification are merely preferred examples and are not intended to limit the utility model. Various changes and modifications can be made to this utility model without departing from its spirit and scope, and all such changes and modifications fall within the scope of the claimed utility model. The scope of protection of this utility model is defined by the appended claims and their equivalents.

Claims

1. A novel ammonium sulfate saturator, comprising a saturator tank (1), characterized in that: A top cover (15) is fixedly installed on the top of the saturator tank (1). An inlet pipe (2) is fixedly installed on the top cover (15). An inlet ring (20) is fixedly installed at the bottom end of the inlet pipe (2). A notch (21) is provided on one side of the inlet ring (20). Multiple nozzles (22) are fixedly installed at the bottom of the inlet ring (20). An air inlet pipe (3) is also fixedly installed on the top cover (15). An air inlet ring (30) is fixedly installed at the bottom end of the air inlet pipe (3). Multiple air outlet holes (31) are arranged in a ring shape at equal intervals on the bottom surface of the air inlet ring (30). The inlet ring (20) and the air inlet ring (30) are both located inside the saturator tank (1). The inlet ring (20) is located above the air inlet ring (30). The air inlet pipe (3) passes through the notch (21).

2. The novel ammonium sulfate saturator according to claim 1, characterized in that: A conical cylinder (10) is fixedly installed at the bottom of the saturator tank (1), and a discharge pipe (11) is fixedly installed at the bottom end of the conical cylinder (10). A discharge valve (12) is fixedly installed on the discharge pipe (11).

3. The novel ammonium sulfate saturator according to claim 2, characterized in that: The conical cylinder (10) is funnel-shaped, and the plane of the inner wall of the conical cylinder (10) is inclined downward at 45° to 60°.

4. The novel ammonium sulfate saturator according to claim 1, characterized in that: The bottom of the saturator tank (1) is fixedly equipped with a plurality of support legs (13), and the bottom end of the support legs (13) is fixedly equipped with a fixed base (131).

5. The novel ammonium sulfate saturator according to claim 4, characterized in that: A temperature-controlled electric heater (14) is fixedly installed on the cylinder of the saturator tank (1), and the fixed base (131) is fixedly installed on the ground.

6. The novel ammonium sulfate saturator according to claim 1, characterized in that: A stirring motor (4) is fixedly installed at the center of the upper surface of the top cover (15). A stirring shaft (40) is fixedly installed at the end of the output shaft of the stirring motor (4). A stirring blade (41) is fixedly installed on the stirring shaft (40). The stirring blade (41) is located inside the saturator tank (1).

7. The novel ammonium sulfate saturator according to claim 1, characterized in that: A booster pump (5) is provided on one side of the saturator tank (1). A suction pipe (50) is fixedly installed at the inlet end of the booster pump (5), and a delivery pipe (51) is fixedly installed at the outlet end of the booster pump (5). Multiple uniformly distributed pipes (52) are fixedly installed on the end of the delivery pipe (51), and multiple nozzles (53) are fixedly installed at the bottom of the uniformly distributed pipes (52). The nozzles (53) are located inside the saturator tank (1).

8. The novel ammonium sulfate saturator according to claim 7, characterized in that: The nozzle (53) is located between the liquid inlet ring (20) and the air inlet ring (30), and the suction pipe (50) is connected to the external medicine delivery pipe.

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